CN105973648A - Soil pore water sampling method - Google Patents

Soil pore water sampling method Download PDF

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Publication number
CN105973648A
CN105973648A CN201610259802.3A CN201610259802A CN105973648A CN 105973648 A CN105973648 A CN 105973648A CN 201610259802 A CN201610259802 A CN 201610259802A CN 105973648 A CN105973648 A CN 105973648A
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CN
China
Prior art keywords
sampling
steel pipe
pipe
soil
pvb
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Pending
Application number
CN201610259802.3A
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Chinese (zh)
Inventor
李明
吕晨
刘滨硕
刘宝林
李忠和
吴磊
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Jilin Jianzhu University
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Jilin Jianzhu University
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Priority to CN201610259802.3A priority Critical patent/CN105973648A/en
Publication of CN105973648A publication Critical patent/CN105973648A/en
Pending legal-status Critical Current

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    • GPHYSICS
    • G01MEASURING; TESTING
    • G01NINVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
    • G01N1/00Sampling; Preparing specimens for investigation
    • G01N1/02Devices for withdrawing samples
    • G01N1/10Devices for withdrawing samples in the liquid or fluent state
    • G01N1/16Devices for withdrawing samples in the liquid or fluent state with provision for intake at several levels
    • GPHYSICS
    • G01MEASURING; TESTING
    • G01NINVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
    • G01N1/00Sampling; Preparing specimens for investigation
    • G01N1/02Devices for withdrawing samples
    • G01N1/10Devices for withdrawing samples in the liquid or fluent state
    • G01N2001/1031Sampling from special places
    • GPHYSICS
    • G01MEASURING; TESTING
    • G01NINVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
    • G01N1/00Sampling; Preparing specimens for investigation
    • G01N1/02Devices for withdrawing samples
    • G01N1/10Devices for withdrawing samples in the liquid or fluent state
    • G01N1/14Suction devices, e.g. pumps; Ejector devices
    • G01N2001/1418Depression, aspiration

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  • Life Sciences & Earth Sciences (AREA)
  • Hydrology & Water Resources (AREA)
  • Physics & Mathematics (AREA)
  • Health & Medical Sciences (AREA)
  • Chemical & Material Sciences (AREA)
  • Analytical Chemistry (AREA)
  • Biochemistry (AREA)
  • General Health & Medical Sciences (AREA)
  • General Physics & Mathematics (AREA)
  • Immunology (AREA)
  • Pathology (AREA)
  • Sampling And Sample Adjustment (AREA)

Abstract

The invention discloses a soil pore water sampling method and sampling device; each steel pipe is internally sheathed with a layer of rubber pipe, and one end of each steel pipe is mounted on a fixed disc through a fixing riveting joint, the bottom end of each steel pipe is fixedly provided with a sampling probe, and the top of each steel pipe is connected with one PVB pipe; the PVB pipes are connected on a sampling box, the sampling box at least comprises six mutually-independent storage spaces, and each PVB pipe is separately connected on one storage space; each storage space is provided with a suction port; each PVB pipe is provided with a valve. The sampling probes with different depths are arranged, and soil pore water at different depths is sampled; through a way of firstly sampling upper-layer water and then sampling lower-layer soil water, the impact of different orders is solved; the sampling box with a plurality of different mutually-independent spaces is arranged, and collection and detection of the sampling water at different depths are achieved.

Description

A kind of soil pore water method of sampling
Technical field
The invention belongs to soil sampling technical field, especially relate to one and be applied to study different depth soil The soil pore water method of sampling of water characteristic.
Background technology
In environmental science, the field such as ecological and agriculture, need soil pore water is carried out sampling analysis, The environmental behaviours such as the migration of research pollutant and the conversion of nutrient substance.In order to fully soil characteristic be entered Row experimental study, scientific research institution establishes the most large-scale test percolating filter, by gathering the soil of percolating filter Earth percolating water detects soil regime all-sidedly and accurately.The soil water carries out sample collection, and scientific analysis is studied, Can be that environmental monitoring provides a large amount of visual data and ecological, environmental protection suggestion.Therefore, to soil pore water Sampling analysis is of crucial importance, and the sampling of soil pore water is it is generally required to complete by special sampling tool. The quality of sampling tool is related to sampling efficiency and the sampling precision of soil pore water, for sampling analysis Have a very big impact.
Although starting that various sampling apparatus and the method for sampling occur at present, but, current sampling apparatus or Person's method of sampling is when sampling, if being acquired the water sample of diverse location different depth analyzing, then by In having two variablees, having bigger diversity, impact analysis precision, and if at same position pair Different depth is sampled, if then the method for sampling and device are improper, and shadow of once sampling before also easily causing Ring the extraction accuracy of a rear sample water, also affect the analysis precision of data, therefore, in order to study difference The situation of level soil pore water, needs to design a kind of novel soil pore water method of sampling, in order to carry The precision of high data analysis.
Summary of the invention
The present invention is directed to existing technical problem, it is provided that a kind of soil pore water method of sampling, it is by setting Put the sampling probe of different depth, it is achieved that the sampling of different depth soil pore water, meanwhile, utilize weight Power sinking principle, by first upper water being sampled, after mode that lower soil water is sampled, Solving the impact that order is different, the present invention is provided with the sampling with multiple different separate spaces Case, it is achieved that the collection of different depth sample water and detection, the inventive method is simple, easy to use, adopts Sample precision is high.
For achieving the above object, the present invention provides following technical scheme: a kind of soil pore water method of sampling, It is characterized in that, it comprises the following steps:
(1) sampling apparatus prepares and connects and install:
I () chooses the steel pipe that six length the most uniformly increase, sheathed one layer of rubber tube in steel pipe, so After, one end of every steel pipe is arranged on fixed disk by fixing riveted joint, and ensures six roots of sensation length not Same steel pipe stretches out the length of fixed disk lower surface and becomes gradient uniformity to increase successively;
(ii) sampling probe is fixed in the bottom at every steel pipe, it is desirable to each sampling probe and steel pipe Interior rubber tube is connected firm, is embedded in by every steel pipe afterwards in the soil of required test, then It is all connected with a PVB pipe on the top of every steel pipe, and PVB pipe is connected on sampling box, wherein, Sampling box at least includes six separate memory spaces, and each PVB pipe is all connected with a storage sky Between;
(iii) on every PVB pipe, a valve it is respectively provided with;
(2) sampling of soil pore water:
A () is first turned on the valve on the PVB pipe that is connected with the shortest steel pipe, then, and will be with this PVB The air pressure that pipe is connected in the memory space of corresponding sampling box is set to negative pressure, to the soil being in the superiors Earth pore water is sampled, and sample 10-15ml, closes this valve;
Open the valve on the PVB pipe being connected with secondary short steel pipe after (b), then, will be with this PVB The air pressure that pipe is connected in the memory space of corresponding sampling box is set to negative pressure, to the soil being in time upper strata Earth pore water is sampled, and sample 10-15ml, closes this valve afterwards;
C () repeats step (a) or (b), in order to carry out the soil water of the probe being in bottom successively Sampling, in order to first upper layer of soil water is sampled, after lower soil water is sampled;
D (), sampling Multifunctional water instrument are the most successively to the difference stored respectively in sampling box The soil water of level carries out detecting and record.
Further, as preferably, in step (a)-(c) in described step (2), by connecting It is negative pressure that the mode of vacuum pump realizes each memory space.
Further, as preferably, in the step (ii) in described step (1), stretch in soil the shortest The a length of 15-20cm of steel pipe, and the length difference of two steel pipes of adjacent lengths is 12cm.
Further, as preferably, in described step (1), described fixed disk is steel design.
Further, the invention provides a kind of soil pore water sampling apparatus, it is characterised in that: it includes Steel pipe, fixed disk, valve and the sampling box that six length the most uniformly increases, wherein, in every steel pipe The most sheathed one layer of rubber tube, and one end of every steel pipe is all arranged on fixed disk by fixing riveted joint, The steel pipe that six roots of sensation length is different stretches out the length of fixed disk lower surface and becomes gradient uniformity to increase successively, every steel A sampling probe is fixed in the bottom of pipe, and each sampling probe is connected firm with the rubber tube in steel pipe, The top of every steel pipe is all connected with a PVB pipe, and PVB pipe is connected on sampling box, and sampling box at least wraps Include six separate memory spaces, and each PVB pipe be all individually connected on a memory space, It is provided with pump orifice on each memory space, and on every PVB pipe, is respectively provided with a valve.
Compared with prior art, the invention has the beneficial effects as follows:
The present invention is by arranging the sampling probe of different depth, it is achieved that adopting of different depth soil pore water Sample, meanwhile, utilizes gravity sinking principle, by first upper water being sampled, after to lower soil water Carrying out the mode sampled, solve the impact that order is different, the present invention is provided with has multiple different phase The sampling box of separate space mutually, it is achieved that the collection of different depth sample water and detection, the inventive method letter Single, easy to use, sampling precision is high.
Accompanying drawing explanation
Fig. 1 is the structural representation of the present invention a kind of soil pore water sampling apparatus;
1-sampling probe one, 2-sampling probe two, 3-sampling probe three, 4-sampling probe four, 5-samples Probe five, 6-sampling probe six, 7-fixes riveted joint, 8-fixed disk, 9-valve, 10-vasculum, 11- Memory space, 12-aspirating hole.
Detailed description of the invention
Below in conjunction with the accompanying drawing in the embodiment of the present invention, the technical scheme in the embodiment of the present invention is carried out Clearly and completely describe, it is clear that described embodiment is only a part of embodiment of the present invention, and It is not all, of embodiment.Based on the embodiment in the present invention, those of ordinary skill in the art are not doing Go out the every other embodiment obtained under creative work premise, broadly fall into the scope of protection of the invention.
Referring to Fig. 1, the present invention provides a kind of technical scheme: a kind of soil pore water method of sampling, it is special Levy and be, it is characterised in that it comprises the following steps:
(1) sampling apparatus prepares and connects and install:
I () chooses the steel pipe that six length the most uniformly increase, sheathed one layer of rubber tube in steel pipe, so After, one end of every steel pipe is arranged on fixed disk 8 by fixing riveted joint 7, and ensures that the six roots of sensation is long Spend different steel pipes to stretch out the length of fixed disk lower surface and become gradient uniformity to increase successively;
(ii) sampling probe, sampling probe 1, sampling probe two are fixed in the bottom at every steel pipe 2, sampling probe 33, sampling probe 44, sampling probe 55, sampling probe 66, it is desirable to each adopt Sample probe is connected firm with the rubber tube in steel pipe, and every steel pipe is embedded in required test afterwards In soil, then the top at every steel pipe is all connected with a PVB pipe, and PVB pipe is connected to sampling On case, wherein, sampling box 10 at least includes six separate memory spaces 11, and each PVB pipe It is all connected with a memory space;
(iii) on every PVB pipe, a valve 9 it is respectively provided with;
(2) sampling of soil pore water:
A () is first turned on the valve 9 on the PVB pipe that is connected with the shortest steel pipe, then, and will be with this PVB The air pressure that pipe is connected in the memory space of corresponding sampling box 10 is set to negative pressure, to being in the superiors Soil pore water is sampled, and sample 10-15ml, closes this valve;
Open the valve 9 on the PVB pipe being connected with secondary short steel pipe after (b), then, will be with this PVB The air pressure that pipe is connected in the memory space of corresponding sampling box is set to negative pressure, to the soil being in time upper strata Earth pore water is sampled, and sample 10-15ml, closes this valve 9 afterwards;
C () repeats step (a) or (b), in order to adopt the soil water of the probe being in bottom successively Sample, in order to first upper layer of soil water is sampled, after lower soil water is sampled;
D (), sampling Multifunctional water instrument are the most successively to the different layers stored respectively in sampling box The secondary soil water carries out detecting and record.
In the present embodiment, in step (a)-(c) in described step (2), by connecting vacuum pump Mode to realize each memory space be negative pressure.In step (ii) in described step (1), stretch into soil The a length of 15-20cm of steel pipe the shortest in earth, and the length difference of two steel pipes of adjacent lengths is 12cm. In described step (1), described fixed disk is steel design.
Additionally, the invention provides a kind of soil pore water sampling apparatus, it is characterised in that: it includes six Steel pipe, fixed disk 8, valve 9 and the sampling box 10 that length the most uniformly increases, wherein, every steel pipe The most sheathed one layer of rubber tube, and one end of every steel pipe is all arranged on fixed disk by fixing riveted joint, The steel pipe that six roots of sensation length is different stretches out the length of fixed disk lower surface and becomes gradient uniformity to increase successively, every steel A sampling probe is fixed in the bottom of pipe, and each sampling probe is connected firm with the rubber tube in steel pipe, The top of every steel pipe is all connected with a PVB pipe, and PVB pipe is connected on sampling box, and sampling box at least wraps Include six separate memory spaces 11, and each PVB pipe is all individually connected to a memory space 11 On, each memory space is provided with pump orifice 12, and on every PVB pipe, is respectively provided with a valve 9。
The present invention is by arranging the sampling probe of different depth, it is achieved that adopting of different depth soil pore water Sample, meanwhile, utilizes gravity sinking principle, by first upper water being sampled, after to lower soil water Carrying out the mode sampled, solve the impact that order is different, the present invention is provided with has multiple different phase The sampling box of separate space mutually, it is achieved that the collection of different depth sample water and detection, the inventive method letter Single, easy to use, sampling precision is high.
Although an embodiment of the present invention has been shown and described, for those of ordinary skill in the art Speech, it is possible to understand that these embodiments can be carried out without departing from the principles and spirit of the present invention Multiple change, revising, replace and modification, the scope of the present invention is limited by claims and equivalent thereof Fixed.

Claims (5)

1. a soil pore water method of sampling, it is characterised in that it comprises the following steps:
(1) sampling apparatus prepares and connects and install:
I () chooses the steel pipe that six length the most uniformly increase, sheathed one layer of rubber tube in steel pipe, so After, one end of every steel pipe is arranged on fixed disk by fixing riveted joint, and ensures six roots of sensation length not Same steel pipe stretches out the length of fixed disk lower surface and becomes gradient uniformity to increase successively;
(ii) sampling probe is fixed in the bottom at every steel pipe, it is desirable in each sampling probe and steel pipe Rubber tube be connected firm, afterwards every steel pipe is embedded in the soil of required test, then exists The top of every steel pipe is all connected with a PVB pipe, and is connected on sampling box by PVB pipe, wherein, adopts Sample case at least includes six separate memory spaces, and each PVB pipe is all connected with a memory space;
(iii) on every PVB pipe, a valve it is respectively provided with;
(2) sampling of soil pore water:
A () is first turned on the valve on the PVB pipe that is connected with the shortest steel pipe, then, and will be with this PVB The air pressure that pipe is connected in the memory space of corresponding sampling box is set to negative pressure, to the soil being in the superiors Earth pore water is sampled, and sample 10-15ml, closes this valve;
Open the valve on the PVB pipe being connected with secondary short steel pipe after (b), then, will be with this PVB The air pressure that pipe is connected in the memory space of corresponding sampling box is set to negative pressure, to the soil being in time upper strata Earth pore water is sampled, and sample 10-15ml, closes this valve afterwards;
C () repeats step (a) or (b), in order to adopt the soil water of the probe being in bottom successively Sample, in order to first upper layer of soil water is sampled, after lower soil water is sampled;
D (), sampling Multifunctional water instrument are the most successively to the different layers stored respectively in sampling box The secondary soil water carries out detecting and record.
A kind of soil pore water method of sampling the most according to claim 1, it is characterised in that: described In step (a)-(c) in step (2), by the way of connecting vacuum pump, realize each storage sky Between be negative pressure.
A kind of soil pore water method of sampling the most according to claim 1, it is characterised in that: described In step (ii) in step (1), stretch into a length of 15-20cm of steel pipe the shortest in soil, and The length difference of two steel pipes of adjacent lengths is 12cm.
A kind of soil pore water method of sampling the most according to claim 1, it is characterised in that: described In step (1), described fixed disk is steel design.
5. according to use in a kind of soil pore water method of sampling described in claim 1-4 any one Sampling apparatus, it is characterised in that: it includes steel pipe that six length the most uniformly increase, fixed disk, valve Door and sampling box, wherein, the most sheathed one layer of rubber tube in every steel pipe, and one end of every steel pipe is the most logical Crossing fixing riveted joint to be arranged on fixed disk, the steel pipe that six roots of sensation length is different stretches out the length of fixed disk lower surface Degree becomes gradient uniformity to increase successively, and a sampling probe, each sampling probe are fixed in the bottom of every steel pipe Being connected firm with the rubber tube in steel pipe, the top of every steel pipe is all connected with a PVB pipe, and PVB manages It is connected on sampling box, and sampling box at least includes six separate memory spaces, and each PVB Guan Jun is individually connected on a memory space, and each memory space is provided with pump orifice, and often A valve it is respectively provided with on root PVB pipe.
CN201610259802.3A 2016-04-21 2016-04-21 Soil pore water sampling method Pending CN105973648A (en)

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Cited By (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN108645668A (en) * 2018-07-09 2018-10-12 广州海洋地质调查局 The long-term in-situ sampling of pore water and analytical equipment and its method
CN109724842A (en) * 2019-02-13 2019-05-07 江苏双双高新科技有限公司 A kind of quick Qu Ye mechanism, robot
CN111397969A (en) * 2020-04-22 2020-07-10 南京信息工程大学 Passive in-situ high-resolution pore water sampling device and sampling method

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* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN2478104Y (en) * 2001-05-15 2002-02-20 中国科学院南京土壤研究所 Soil gap water analyzer
JP2010048029A (en) * 2008-08-25 2010-03-04 Machine Service:Kk Improved ground testing method and unsolidified sample collector
CN201555741U (en) * 2009-12-18 2010-08-18 宁夏农林科学院 Soil leakage solution extraction device
US20110242530A1 (en) * 2007-11-09 2011-10-06 The Regents Of The University Of California In-situ soil nitrate ion concentration sensor
CN202533269U (en) * 2012-03-05 2012-11-14 华中农业大学 Potting soil column device suitable for researching soil and soil solution
JP2013104194A (en) * 2011-11-11 2013-05-30 Shimizu Corp Original position testing method and original position testing device
CN203705207U (en) * 2013-12-31 2014-07-09 常州千帆环保科技有限公司 Soil solution sampling device
CN104458339A (en) * 2014-11-07 2015-03-25 中国科学院东北地理与农业生态研究所 Fixed depth pore water monitoring sampler and sampling method

Patent Citations (8)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN2478104Y (en) * 2001-05-15 2002-02-20 中国科学院南京土壤研究所 Soil gap water analyzer
US20110242530A1 (en) * 2007-11-09 2011-10-06 The Regents Of The University Of California In-situ soil nitrate ion concentration sensor
JP2010048029A (en) * 2008-08-25 2010-03-04 Machine Service:Kk Improved ground testing method and unsolidified sample collector
CN201555741U (en) * 2009-12-18 2010-08-18 宁夏农林科学院 Soil leakage solution extraction device
JP2013104194A (en) * 2011-11-11 2013-05-30 Shimizu Corp Original position testing method and original position testing device
CN202533269U (en) * 2012-03-05 2012-11-14 华中农业大学 Potting soil column device suitable for researching soil and soil solution
CN203705207U (en) * 2013-12-31 2014-07-09 常州千帆环保科技有限公司 Soil solution sampling device
CN104458339A (en) * 2014-11-07 2015-03-25 中国科学院东北地理与农业生态研究所 Fixed depth pore water monitoring sampler and sampling method

Cited By (5)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN108645668A (en) * 2018-07-09 2018-10-12 广州海洋地质调查局 The long-term in-situ sampling of pore water and analytical equipment and its method
CN109724842A (en) * 2019-02-13 2019-05-07 江苏双双高新科技有限公司 A kind of quick Qu Ye mechanism, robot
CN109724842B (en) * 2019-02-13 2021-06-01 江苏双双高新科技有限公司 Robot gets liquid mechanism fast
CN111397969A (en) * 2020-04-22 2020-07-10 南京信息工程大学 Passive in-situ high-resolution pore water sampling device and sampling method
CN111397969B (en) * 2020-04-22 2022-03-08 南京信息工程大学 Passive in-situ high-resolution pore water sampling device and sampling method

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