CN105961794A - Preparation method of sugar products rich in laver protein and laver polysaccharide - Google Patents
Preparation method of sugar products rich in laver protein and laver polysaccharide Download PDFInfo
- Publication number
- CN105961794A CN105961794A CN201610283391.1A CN201610283391A CN105961794A CN 105961794 A CN105961794 A CN 105961794A CN 201610283391 A CN201610283391 A CN 201610283391A CN 105961794 A CN105961794 A CN 105961794A
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- Prior art keywords
- thallus porphyrae
- container
- solution
- laver
- rich
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- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
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Classifications
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- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23G—COCOA; COCOA PRODUCTS, e.g. CHOCOLATE; SUBSTITUTES FOR COCOA OR COCOA PRODUCTS; CONFECTIONERY; CHEWING GUM; ICE-CREAM; PREPARATION THEREOF
- A23G3/00—Sweetmeats; Confectionery; Marzipan; Coated or filled products
- A23G3/34—Sweetmeats, confectionery or marzipan; Processes for the preparation thereof
- A23G3/36—Sweetmeats, confectionery or marzipan; Processes for the preparation thereof characterised by the composition containing organic or inorganic compounds
- A23G3/48—Sweetmeats, confectionery or marzipan; Processes for the preparation thereof characterised by the composition containing organic or inorganic compounds containing plants or parts thereof, e.g. fruits, seeds, extracts
-
- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23G—COCOA; COCOA PRODUCTS, e.g. CHOCOLATE; SUBSTITUTES FOR COCOA OR COCOA PRODUCTS; CONFECTIONERY; CHEWING GUM; ICE-CREAM; PREPARATION THEREOF
- A23G3/00—Sweetmeats; Confectionery; Marzipan; Coated or filled products
- A23G3/34—Sweetmeats, confectionery or marzipan; Processes for the preparation thereof
- A23G3/36—Sweetmeats, confectionery or marzipan; Processes for the preparation thereof characterised by the composition containing organic or inorganic compounds
- A23G3/42—Sweetmeats, confectionery or marzipan; Processes for the preparation thereof characterised by the composition containing organic or inorganic compounds characterised by the carbohydrates used, e.g. polysaccharides
-
- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23G—COCOA; COCOA PRODUCTS, e.g. CHOCOLATE; SUBSTITUTES FOR COCOA OR COCOA PRODUCTS; CONFECTIONERY; CHEWING GUM; ICE-CREAM; PREPARATION THEREOF
- A23G3/00—Sweetmeats; Confectionery; Marzipan; Coated or filled products
- A23G3/34—Sweetmeats, confectionery or marzipan; Processes for the preparation thereof
- A23G3/36—Sweetmeats, confectionery or marzipan; Processes for the preparation thereof characterised by the composition containing organic or inorganic compounds
- A23G3/44—Sweetmeats, confectionery or marzipan; Processes for the preparation thereof characterised by the composition containing organic or inorganic compounds containing peptides or proteins
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- Life Sciences & Earth Sciences (AREA)
- Chemical & Material Sciences (AREA)
- Inorganic Chemistry (AREA)
- Engineering & Computer Science (AREA)
- Food Science & Technology (AREA)
- Polymers & Plastics (AREA)
- Proteomics, Peptides & Aminoacids (AREA)
- Botany (AREA)
- Health & Medical Sciences (AREA)
- Molecular Biology (AREA)
- Edible Seaweed (AREA)
Abstract
The invention relates to a preparation method of sugar products rich in laver protein and laver polysaccharide. The preparation method comprises the following steps of step I, soaking laver so as to prepare a laver solution, and bombarding the laver solution with ultrasonic waves; step II, transferring the laver solution to a second container, heating the laver solution by using the second container, and maintaining the temperature to be 75-90 DEG C; step III, adding chitosan to the second container, adjusting the pH value of the laver solution to be 2.5-3.5, and after a reaction of 3-5 hours, generating floccule using the chitosan as a flocculant in the second container; and step IV, performing floccule separation on the reacted laver solution, and adding the separated floccule to syrup for sugar making treatment. Laver sweets prepared by the preparation method of sugar products rich in laver protein and laver polysaccharide, provided by the invention, are rich in nutrient components of laver the polysaccharide and the like, and besides, have the advantages of being convenient to eat, sweet and delicious in taste, suitable for all kinds of crowds and the like.
Description
Technical field
Invention relates to laver product production technical field, more specifically, particularly to one rich in there being purple
The sugar prod preparation method of dish albumen and Porphyra Polysaccharide.
Background technology
Thallus Porphyrae is the general designation in marine alternate algae, belongs to Rhodophyceae, Bangia fuscopurpurea section.Thallus Porphyrae is grown on shallow sea
On the rock of Intertidal zone, the element such as its rich in proteins and iodine, phosphorus, calcium, it can be edible, simultaneously
Thallus Porphyrae can also be used as medicine, and makes Chinese medicine, has resolving phlegm and softening hard masses, effect that clearing away heat and promoting diuresis, the kidney invigorating are nourished heart.
In the prior art, Thallus Porphyrae is all to be made into as dry Thallus Porphyrae, owing to dry Thallus Porphyrae is more crisp, daily edible
Time, the salted Brassicae siccus slag that can drop more, the most very inconvenient edible.It addition, Thallus Porphyrae directly eats its mouth
The micro-raw meat of taste, is not suitable as snacks and eats.
Summary of the invention
In sum, how to provide a kind of laver to be easy to the coated snack product eaten, become this area skill
Art personnel's problem demanding prompt solution.
The invention provides a kind of rich in there being the sugar prod preparation method of Thallus Porphyrae albumen and Porphyra Polysaccharide, should
Method specifically includes:
Step one, in the first container, Thallus Porphyrae is carried out soak preparation become Thallus Porphyrae solution, pass through afterwards
Thallus Porphyrae solution is bombarded by ultrasound wave；
Step 2, being transferred in second container by Thallus Porphyrae solution, second container has heating function, utilizes
Thallus Porphyrae solution is heated and makes its temperature maintain 75-90 DEG C by second container；
Step 3, in second container, add chitosan, and regulate the acid-base value of Thallus Porphyrae solution to 2.5-3.5,
Through the reaction of 3-5 hour, in described second container, generate the floccule with chitosan as flocculant；
Step 4, reacted Thallus Porphyrae solution is carried out floccule separation, and isolated floccule is added
Enter in syrup and carry out sugaring process.
Preferably, in step one, use distilled water or deionized water that Thallus Porphyrae is soaked, its material
Liquor ratio is 1:18-1:23.
Preferably, described second container is can the reacting furnace of pressure-bearing；In step 2, described second holds
The device pressure when reaction is 1.5-2.0 atmospheric pressure.
Preferably, in described step 3, floccule lock out operation is concretely comprised the following steps: utilize centrifugal
Machine is centrifuged 3-4.5 minute under the rotating speed of 5000rpm, then obtains flocky precipitate.
Preferably, in described step 3, floccule lock out operation is concretely comprised the following steps: utilize film to divide
Cotton-shaped separator is obtained from method.
Preferably, in described step 2, use eddy heating for heating mode to the Thallus Porphyrae in described second container
Solution heats.
Preferably, the concrete operations of described step one are: first crushed by Thallus Porphyrae, are then added to described
In first container, it is proportionally added into distilled water or deionized water, is warming up to 75-85 DEG C and maintains 2-5 hour, it
After utilize ultrasound wave that Thallus Porphyrae solution is bombarded.
Preferably, a kind of in described step, Thallus Porphyrae is carried out carefully by the ultrasound wave utilizing frequency to be more than 25000hz
Born of the same parents' fragmentation procedure, its concrete action is: utilize ultrasonic transducer towards Thallus Porphyrae and to keep 1.0-1.5cm with it
Spacing distance, application time 2.5s-3.5s, dwell time 10.0s-15.0s, repeat above-mentioned action 3-10 time.
The present invention provide rich in there being the sugar prod preparation method of Thallus Porphyrae albumen and Porphyra Polysaccharide, pass through the method
The Thallus Porphyrae sugar of preparation is i.e. rich in there being the nutritional labeling such as Porphyra Polysaccharide, Porphyra Polysaccharide, and meanwhile, it also has food
By advantages such as convenience, sweet, the suitable various people of taste.
Detailed description of the invention
Below in conjunction with embodiment, embodiments of the present invention are described in further detail.Following example are used
In the explanation present invention, but can not be used for limiting the scope of the present invention.
In describing the invention, except as otherwise noted, " multiple " are meant that two or more, its
It is for only for ease of and describes the present invention and simplify description rather than instruction or the device of hint indication or element
Must have specific orientation, with specific azimuth configuration and operation, therefore it is not intended that to the present invention
Restriction.Additionally, term " first ", " second ", " the 3rd " etc. are only used for describing purpose, and it is not understood that
For instruction or hint relative importance.
In describing the invention, it should be noted that unless otherwise clearly defined and limited, term " phase
Even ", " connection " should be interpreted broadly, for example, it may be fixing connection, it is also possible to be to removably connect,
Or be integrally connected；Can be to be mechanically connected, it is also possible to be electrical connection；Can be to be joined directly together, it is possible to
To be indirectly connected to by intermediary.For the ordinary skill in the art, can be with concrete condition
Understand above-mentioned term concrete meaning in the present invention.
The invention provides a kind of rich in there being the sugar prod preparation method of Thallus Porphyrae albumen and Porphyra Polysaccharide,
In the method, the concrete operation step of the present invention includes:
S1, prepare Thallus Porphyrae solution and to its bombard.First one is prepared for the container containing Thallus Porphyrae solution
As the first container, it is the first container with canister or pottery, glass drying oven.By dry Thallus Porphyrae or
The new fresh laver of person, as raw material, is contained in the first container.In an optimal way of the present invention,
If using dry Thallus Porphyrae as raw material, then can be pulverized by craft or machine, then will
Raw material after pulverizing is encased in the first container；If using new fresh laver as raw material, then can pass through
Compaction technology is made into laver soy sauce, then reinstalls in the first container.Thallus Porphyrae raw material is encased in
After one container, the first container content enter pure water or distilled water preparation become Thallus Porphyrae solution.Wherein,
Solid-liquid ratio between Thallus Porphyrae raw material and pure water or distilled water is 1:18-1:23.Thallus Porphyrae solution prepare with
After, at the first Container transfering to ultrasonic generator, then adjust the position of ultrasonic transducer,
Make ultrasonic transducer towards the liquid level of Thallus Porphyrae solution the spacing distance that keeps 1.0-1.5cm with it, beat
Open ultrasonic generator to carry out cell and smash operation.
S2, Thallus Porphyrae solution heat.Preparing second container, the parameter request of second container is: can be to appearance
Solution in device heats, and its heating temperature range is: 0-130 DEG C.Meanwhile, the capacity of second container
More than the capacity of the first container, so the whole Thallus Porphyrae solution in the first container can be contained to second
In container.After Thallus Porphyrae solution is transferred to second container, utilize second container that Thallus Porphyrae solution is added
Heat also makes its temperature maintain 75-90 DEG C.
S3, utilize chitosan extract floccule.Utilize second container that Thallus Porphyrae solution temperature is maintained at
Between 75-90 DEG C.Then, in second container, chitosan is added.After chitosan adds, at purple
Add acid in dish solution, and regulate the acid-base value of Thallus Porphyrae solution to 2.5-3.5, through the reaction of 3-5 hour,
The floccule with chitosan as flocculant is generated in second container.In this step, add in Thallus Porphyrae solution
The acid entered can be hydrochloric acid, lactic acid, food grade phosphoric acid or citric acid.
S4, floccule separate.When second container is after reaction after a while, can be in second container
Generate flocculent deposit.Then, stop heating of second container, and make second container slow cooling to often
Temperature.Then, the solution in second container is derived, is finally separating floccule standby.
S5, floccule is placed into filter filtration on paper 10-25 minute, then floccule is carried out as adjuvant
Sugaring.
Specifically, in step sl, the present invention uses distilled water or deionized water to soak Thallus Porphyrae,
Its solid-liquid ratio is 1:18-1:23.
In order to improve the percentage of damage of laver cell further, thus farthest will laver cell contain
Thallus Porphyrae albumen and Porphyra Polysaccharide be dissolved in aqueous solution, the present invention is being provided with ultrasonic generator
On the basis of, again second container is carried out structure optimization: second container is can the reacting furnace of pressure-bearing；
In step 2, the second container pressure when reaction is 1.5-2.0 atmospheric pressure.Pressurization is used to heat up
Mode, make aqueous solution be rapidly introduced into the intracellular thus Thallus Porphyrae that rises brokenly by increasing container internal pressure
Cell.
In an embodiment of the invention, floccule lock out operation is concretely comprised the following steps: utilize from
Scheming is centrifuged 3-4.5 minute under the rotating speed of 5000rpm, then obtains flocky precipitate.
In yet another embodiment of the present invention, floccule lock out operation is concretely comprised the following steps: utilize
Membrane separation process obtains cotton-shaped separator.
The mode of heating of second container is limited: 1, use eddy heating for heating mode to the purple in second container at this
Dish solution heats.2, employing adds heat pipes heat.In above-mentioned first kind of way, vortex-like fashion heats
Advantage be: enable to Thallus Porphyrae solution and be rapidly heated, and Solutions Center position and solution edge
The firing rate of position is consistent.In the above-mentioned second way, the advantage adding heat pipes heat is: structure
Simply, add heat pipe and be easily installed, change, keep in repair, meanwhile, use and add heat pipes heat for second container
Shape not requirement.
In step S1 of the present invention, its concrete operations are: first crushed by Thallus Porphyrae, be then added to first
In container, it is proportionally added into distilled water or deionized water, is warming up to 75-85 DEG C of maintenance 2-5 hour, afterwards
Utilize ultrasound wave that Thallus Porphyrae solution is bombarded.
In step S1 of the present invention, the present invention is that Thallus Porphyrae is entered by the ultrasound wave utilizing frequency to be more than 25000hz
Row cell breakage operates, and its concrete action is: utilize ultrasonic transducer to keep towards Thallus Porphyrae and with it
The spacing distance of 1.0-1.5cm, application time 2.5s-3.5s, dwell time 10.0s-15.0s, repeats above-mentioned
Action 3-10 time.
Owing to the present invention is to utilize ultrasound wave that Thallus Porphyrae solution is carried out cell to smash, simultaneously as ultrasound wave
Propagation of Energy is successively decreased in the solution, therefore, and the feelings cannot being crashed to pieces in order to avoid Thallus Porphyrae solution bottom cell
Condition occurs, the present invention proposes the following two kinds scheme and solves this problem: 1, reduce the first container arranges height
Degree, will the first container be designed to diameter range 15-30cm, height at the tubular structure of 5-8cm；
2, the first container is vibrated so that the solution Vibrotumbling in the first container.The first solution party
In case, by changing the structure of the first container, it is possible to make Thallus Porphyrae solution under static state carry out ultrasonic
Ripple processes；In the second solution, the structure for the first container does not limit, by vibration side
Formula makes the Thallus Porphyrae agitation in the first container, and so enabling to whole Thallus Porphyrae solution can be surpassed
Sonicated.
One of the present invention is embodied as flow process:
In the first container, Thallus Porphyrae is soaked, by ultrasound wave, Thallus Porphyrae solution is bombarded afterwards；
Being transferred in second container by Thallus Porphyrae solution, second container has heating function, utilizes second container
Thallus Porphyrae solution heated and make its temperature maintain 75-90 DEG C, in second container, adding chitosan,
And regulate the acid-base value of Thallus Porphyrae solution to 2.5-3.5, through the reaction of 3-5 hour, raw in second container
Become the floccule with chitosan as flocculant；
Reacted Thallus Porphyrae solution is carried out floccule separation, and isolated floccule is joined syrup
In carry out sugaring process.
In step one, using distilled water or deionized water to soak Thallus Porphyrae, its solid-liquid ratio is
1:18-1:23。
Second container be can the reacting furnace of pressure-bearing, in step 2, the second container pressure when reaction
For 1.5-2.0 atmospheric pressure.
In step 3, floccule lock out operation is concretely comprised the following steps: utilize centrifuge at 5000rpm
Rotating speed under centrifugal 3-4.5 minute, then obtain flocky precipitate.
In step 3, floccule lock out operation is concretely comprised the following steps: utilize membrane separation process to obtain cotton-shaped
Separator.
In step 2, use eddy heating for heating mode that the Thallus Porphyrae solution in second container is heated.
The concrete operations of step one are: first crushed by Thallus Porphyrae, are then added in the first container, by than
Example adds distilled water or deionized water, is warming up to 75-85 DEG C and maintains 2-5 hour, utilizes ultrasound wave pair afterwards
Thallus Porphyrae solution bombards.
A kind of in step, the ultrasound wave utilizing frequency to be more than 25000hz carries out cell breakage operation to Thallus Porphyrae,
Its concrete action is: utilize ultrasonic transducer towards the spacing distance of Thallus Porphyrae liquid level of solution 1.0-1.5cm,
Application time 2.5s-3.5s, dwell time 10.0s-15.0s, repeats above-mentioned action 3-10 time.
Embodiments of the invention in order to example and describe for the sake of and be given, and be not exhaustively or
Person limit the invention to disclosed form.Many modifications and variations are for those of ordinary skill in the art
For be apparent from.Selecting and describing embodiment is in order to the principle of the present invention and reality are more preferably described
Application, and make those of ordinary skill in the art it will be appreciated that the present invention thus design be suitable to special-purpose
The various embodiments with various amendments.
Claims (8)
1. one kind rich in the sugar prod preparation method having Thallus Porphyrae albumen and Porphyra Polysaccharide, it is characterised in that
Step one, in the first container, Thallus Porphyrae is carried out soak preparation become Thallus Porphyrae solution, pass through afterwards
Thallus Porphyrae solution is bombarded by ultrasound wave；
Step 2, being transferred in second container by Thallus Porphyrae solution, second container has heating function, utilizes
Thallus Porphyrae solution is heated and makes its temperature maintain 75-90 DEG C by second container；
Step 3, in second container, add chitosan, and regulate the acid-base value of Thallus Porphyrae solution to 2.5-3.5,
Through the reaction of 3-5 hour, in described second container, generate the floccule with chitosan as flocculant；
Step 4, reacted Thallus Porphyrae solution is carried out floccule separation, and isolated floccule is added
Enter in syrup and carry out sugaring process.
The most according to claim 1 rich in the sugar prod preparation side having Thallus Porphyrae albumen and Porphyra Polysaccharide
Method, it is characterised in that
In step one, using distilled water or deionized water to soak Thallus Porphyrae, its solid-liquid ratio is
1:18-1:23。
The most according to claim 2 rich in the sugar prod preparation side having Thallus Porphyrae albumen and Porphyra Polysaccharide
Method, it is characterised in that
Described second container is can the reacting furnace of pressure-bearing；
In step 2, the described second container pressure when reaction is 1.5-2.0 atmospheric pressure.
The most according to claim 3 rich in the sugar prod preparation side having Thallus Porphyrae albumen and Porphyra Polysaccharide
Method, it is characterised in that
In described step 3, floccule lock out operation is concretely comprised the following steps: utilize centrifuge to exist
It is centrifuged 3-4.5 minute under the rotating speed of 5000rpm, then obtains flocky precipitate.
The most according to claim 4 rich in the sugar prod preparation side having Thallus Porphyrae albumen and Porphyra Polysaccharide
Method, it is characterised in that
In described step 3, floccule lock out operation is concretely comprised the following steps: utilize membrane separation process to obtain
Cotton-shaped separator.
The most according to claim 5 rich in the sugar prod preparation side having Thallus Porphyrae albumen and Porphyra Polysaccharide
Method, it is characterised in that
In described step 2, use eddy heating for heating mode that the Thallus Porphyrae solution in described second container is carried out
Heating.
The most according to claim 6 rich in the sugar prod preparation side having Thallus Porphyrae albumen and Porphyra Polysaccharide
Method, it is characterised in that
The concrete operations of described step one are: first crushed by Thallus Porphyrae, are then added to described first container
In, it is proportionally added into distilled water or deionized water, is warming up to 75-85 DEG C and maintains 2-5 hour, utilize super afterwards
Thallus Porphyrae solution is bombarded by sound wave.
The most according to claim 7 rich in the sugar prod preparation side having Thallus Porphyrae albumen and Porphyra Polysaccharide
Method, it is characterised in that
A kind of in described step, the ultrasound wave utilizing frequency to be more than 25000hz carries out cell breakage behaviour to Thallus Porphyrae
Making, its concrete action is: utilize ultrasonic transducer towards Thallus Porphyrae the interval that keeps 1.0-1.5cm with it
Distance, application time 2.5s-3.5s, dwell time 10.0s-15.0s, repeats above-mentioned action 3-10 time.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201610283391.1A CN105961794A (en) | 2016-04-30 | 2016-04-30 | Preparation method of sugar products rich in laver protein and laver polysaccharide |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201610283391.1A CN105961794A (en) | 2016-04-30 | 2016-04-30 | Preparation method of sugar products rich in laver protein and laver polysaccharide |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| CN105961794A true CN105961794A (en) | 2016-09-28 |
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Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN201610283391.1A Pending CN105961794A (en) | 2016-04-30 | 2016-04-30 | Preparation method of sugar products rich in laver protein and laver polysaccharide |
Country Status (1)
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Citations (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN1687122A (en) * | 2005-03-23 | 2005-10-26 | 江苏大学 | Purple laver protein and polysaccharide product, and method of ultrasonic assistant extraction |
| CN101057625A (en) * | 2007-05-23 | 2007-10-24 | 刘金涛 | Sea treasure candy and its preparation method |
| CN103445229A (en) * | 2013-09-09 | 2013-12-18 | 南京农业大学 | Method for simultaneously and effectively removing laver protein and laver polysaccharide from laver extracting solution |
-
2016
- 2016-04-30 CN CN201610283391.1A patent/CN105961794A/en active Pending
Patent Citations (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN1687122A (en) * | 2005-03-23 | 2005-10-26 | 江苏大学 | Purple laver protein and polysaccharide product, and method of ultrasonic assistant extraction |
| CN101057625A (en) * | 2007-05-23 | 2007-10-24 | 刘金涛 | Sea treasure candy and its preparation method |
| CN103445229A (en) * | 2013-09-09 | 2013-12-18 | 南京农业大学 | Method for simultaneously and effectively removing laver protein and laver polysaccharide from laver extracting solution |
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Application publication date: 20160928 |