CN105950073A - High-temperature-resistant binder and preparation method thereof - Google Patents
High-temperature-resistant binder and preparation method thereof Download PDFInfo
- Publication number
- CN105950073A CN105950073A CN201610335692.4A CN201610335692A CN105950073A CN 105950073 A CN105950073 A CN 105950073A CN 201610335692 A CN201610335692 A CN 201610335692A CN 105950073 A CN105950073 A CN 105950073A
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- China
- Prior art keywords
- parts
- resistant binder
- high temperature
- temperature
- water
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Classifications
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- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09J—ADHESIVES; NON-MECHANICAL ASPECTS OF ADHESIVE PROCESSES IN GENERAL; ADHESIVE PROCESSES NOT PROVIDED FOR ELSEWHERE; USE OF MATERIALS AS ADHESIVES
- C09J133/00—Adhesives based on homopolymers or copolymers of compounds having one or more unsaturated aliphatic radicals, each having only one carbon-to-carbon double bond, and at least one being terminated by only one carboxyl radical, or of salts, anhydrides, esters, amides, imides, or nitriles thereof; Adhesives based on derivatives of such polymers
- C09J133/04—Homopolymers or copolymers of esters
-
- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09J—ADHESIVES; NON-MECHANICAL ASPECTS OF ADHESIVE PROCESSES IN GENERAL; ADHESIVE PROCESSES NOT PROVIDED FOR ELSEWHERE; USE OF MATERIALS AS ADHESIVES
- C09J11/00—Features of adhesives not provided for in group C09J9/00, e.g. additives
- C09J11/02—Non-macromolecular additives
- C09J11/04—Non-macromolecular additives inorganic
-
- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09J—ADHESIVES; NON-MECHANICAL ASPECTS OF ADHESIVE PROCESSES IN GENERAL; ADHESIVE PROCESSES NOT PROVIDED FOR ELSEWHERE; USE OF MATERIALS AS ADHESIVES
- C09J11/00—Features of adhesives not provided for in group C09J9/00, e.g. additives
- C09J11/02—Non-macromolecular additives
- C09J11/06—Non-macromolecular additives organic
-
- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09J—ADHESIVES; NON-MECHANICAL ASPECTS OF ADHESIVE PROCESSES IN GENERAL; ADHESIVE PROCESSES NOT PROVIDED FOR ELSEWHERE; USE OF MATERIALS AS ADHESIVES
- C09J11/00—Features of adhesives not provided for in group C09J9/00, e.g. additives
- C09J11/08—Macromolecular additives
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08L—COMPOSITIONS OF MACROMOLECULAR COMPOUNDS
- C08L2201/00—Properties
- C08L2201/08—Stabilised against heat, light or radiation or oxydation
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08L—COMPOSITIONS OF MACROMOLECULAR COMPOUNDS
- C08L2205/00—Polymer mixtures characterised by other features
- C08L2205/03—Polymer mixtures characterised by other features containing three or more polymers in a blend
- C08L2205/035—Polymer mixtures characterised by other features containing three or more polymers in a blend containing four or more polymers in a blend
Abstract
The invention discloses a high-temperature-resistant binder and a preparation method thereof. The high-temperature-resistant binder is prepared from, by weight, 60-70 parts of a pure acrylic emulsion, 45-55 parts of thermosetting epoxy resin, 3-4 parts of ethylene glycol monobutyl ether, 5-8 parts of polysiloxane, 10-12 parts of alumina powder, 25-30 parts of talcum powder, 4-5 parts of nu-butyl methacrylate, 2-4 parts of ammonium dihydrogen phosphate, 10-12 parts of plant oil, 2-4 parts of chitosan, 3-4 parts of polyvinyl alcohol and 500-600 parts of water. Compared with the prior art, the high-temperature-resistant binder is scientific in composition and is prepared from nontoxic and harmless raw materials. The binder has the advantages of high binding strength and thermal resistance and can maintain its physiochemical performance unchanged at high temperature. The preparation method is simple and low in cost.
Description
Technical field
The present invention relates to a kind of high temperature resistant binder and preparation method thereof, belong to chemical material technical field.
Background technology
Traditional waterproof material mainly has the flexible waterproof materials such as waterproof roll, water-repellent paint, sealing cement, and with water
Mud base material is main, adds liquid medicine agent and the rigidity water-proofing material of other auxiliary agent, and China's major part waterproofing work all uses tradition anti-
Water material, for roof waterproof, easily cause aging, dry and cracked, deform, fracture, the phenomenon such as layering, for indoor waterproof, for
Complex-shaped place, constructional difficulties, and to Seepage, quality is more difficult to ensure, in order to meet every profession and trade to water-proof binding
The requirement of agent, produces high-performance, and widely used water-proof adhesive is necessary.
Summary of the invention
It is an object of the invention to provide a kind of high temperature resistant binder and preparation method thereof.
To achieve these goals, the present invention adopts the following technical scheme that
High temperature resistant binder, the weight portion of its constitutive material is: pure-acrylic emulsion 60-70, thermosetting epoxy resin 45-55, different two
Alcohol monobutyl ether 3-4, polysiloxane 5-8, alumina powder 10-12, Pulvis Talci 25-30, n-BMA 4-5, phosphorus
Acid dihydride ammonium 2-4, vegetable oil 10-12, chitosan 2-4, polyvinyl alcohol 3-4 and water 500-600.
High temperature resistant binder, the weight portion of its constitutive material is: pure-acrylic emulsion 65, thermosetting epoxy resin 50, different glycol
Monobutyl ether 3.5, polysiloxane 6, alumina powder 11, Pulvis Talci 28, n-BMA 4.5, ammonium dihydrogen phosphate 3,
Vegetable oil 11, chitosan 3, polyvinyl alcohol 3.5 and water 550.
The manufacture method of high temperature resistant binder, including herein below:
(1) weigh each raw material by the weight portion of constitutive material, first pure-acrylic emulsion, thermosetting epoxy resin and water are added blender
In, it is thoroughly mixed, is subsequently adding different glycol monobutyl ether, polysiloxane, continue for stirring mixing；
(2) weigh alumina powder, Pulvis Talci by weight, calcine 2-3 hour under 400-500 DEG C of high temperature, take out, grind after cooling
Pulverizing is broken, is subsequently adding vegetable oil, chitosan, polyvinyl alcohol, is thoroughly mixed uniformly, standby；
(3) compound of step (2) is added in the blender of step (1), after being thoroughly mixed uniformly, then be added thereto to
Other residue constitutive materials such as n-BMA, ammonium dihydrogen phosphate, mix homogeneously, divides in 40-50 DEG C of insulation 10-30
Clock, is cooled to room temperature, to obtain final product.
Beneficial effects of the present invention:
Compared with prior art, the binding agent scientific formula of the present invention, all use nontoxic raw material, and the present invention has height
Adhesion strength, thermostability specially good effect, have the performance keeping physicochemical property to be basically unchanged, preparation technology of the present invention in high temperature environments
Simply, the beneficial effect such as with low cost.
Detailed description of the invention
Embodiment 1: high temperature resistant binder, the weight (jin) of its constitutive material is: pure-acrylic emulsion 65, thermosetting epoxy resin
50, different glycol monobutyl ether 3.5, polysiloxane 6, alumina powder 11, Pulvis Talci 28, n-BMA 4.5, phosphoric acid
Ammonium dihydrogen 3, vegetable oil 11, chitosan 3, polyvinyl alcohol 3.5 and water 550.
The manufacture method of high temperature resistant binder, including herein below:
(1) weigh each raw material by the weight portion of constitutive material, first pure-acrylic emulsion, thermosetting epoxy resin and water are added blender
In, it is thoroughly mixed, is subsequently adding different glycol monobutyl ether, polysiloxane, continue for stirring mixing；
(2) weigh alumina powder, Pulvis Talci by weight, calcine 2-3 hour under 400-500 DEG C of high temperature, take out, grind after cooling
Pulverizing is broken, is subsequently adding vegetable oil, chitosan, polyvinyl alcohol, is thoroughly mixed uniformly, standby；
(3) compound of step (2) is added in the blender of step (1), after being thoroughly mixed uniformly, then be added thereto to
Other residue constitutive materials such as n-BMA, ammonium dihydrogen phosphate, mix homogeneously, divides in 40-50 DEG C of insulation 10-30
Clock, is cooled to room temperature, to obtain final product.
Claims (3)
1. a high temperature resistant binder, it is characterised in that the weight portion of its constitutive material is: pure-acrylic emulsion 60-70, thermosetting ring
Epoxy resins 45-55, different glycol monobutyl ether 3-4, polysiloxane 5-8, alumina powder 10-12, Pulvis Talci 25-30, methyl-prop
Olefin(e) acid N-butyl 4-5, ammonium dihydrogen phosphate 2-4, vegetable oil 10-12, chitosan 2-4, polyvinyl alcohol 3-4 and water 500-600.
High temperature resistant binder the most according to claim 1, it is characterised in that the weight portion of its constitutive material is: pure third breast
Liquid 65, thermosetting epoxy resin 50, different glycol monobutyl ether 3.5, polysiloxane 6, alumina powder 11, Pulvis Talci 28, methyl
N-butyl acrylate 4.5, ammonium dihydrogen phosphate 3, vegetable oil 11, chitosan 3, polyvinyl alcohol 3.5 and water 550.
3. the manufacture method of a high temperature resistant binder as claimed in claim 1, it is characterised in that include herein below:
(1) weigh each raw material by the weight portion of constitutive material, first pure-acrylic emulsion, thermosetting epoxy resin and water are added blender
In, it is thoroughly mixed, is subsequently adding different glycol monobutyl ether, polysiloxane, continue for stirring mixing；
(2) weigh alumina powder, Pulvis Talci by weight, calcine 2-3 hour under 400-500 DEG C of high temperature, take out, grind after cooling
Pulverizing is broken, is subsequently adding vegetable oil, chitosan, polyvinyl alcohol, is thoroughly mixed uniformly, standby；
(3) compound of step (2) is added in the blender of step (1), after being thoroughly mixed uniformly, then be added thereto to
Other residue constitutive materials such as n-BMA, ammonium dihydrogen phosphate, mix homogeneously, divides in 40-50 DEG C of insulation 10-30
Clock, is cooled to room temperature, to obtain final product.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201610335692.4A CN105950073A (en) | 2016-05-19 | 2016-05-19 | High-temperature-resistant binder and preparation method thereof |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201610335692.4A CN105950073A (en) | 2016-05-19 | 2016-05-19 | High-temperature-resistant binder and preparation method thereof |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| CN105950073A true CN105950073A (en) | 2016-09-21 |
Family
ID=56913265
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN201610335692.4A Pending CN105950073A (en) | 2016-05-19 | 2016-05-19 | High-temperature-resistant binder and preparation method thereof |
Country Status (1)
| Country | Link |
|---|---|
| CN (1) | CN105950073A (en) |
Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN115259676A (en) * | 2022-09-26 | 2022-11-01 | 大城县洪海保温材料有限公司 | Formaldehyde-free high-durability rock wool material and preparation method thereof |
Citations (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN104046307A (en) * | 2014-05-30 | 2014-09-17 | 青岛辰青信息技术有限公司 | High-temperature-resistant sealant |
| CN105462532A (en) * | 2015-12-18 | 2016-04-06 | 天津盛同科技有限公司 | Multifunctional high binding force sealing adhesive |
| CN105505238A (en) * | 2015-12-30 | 2016-04-20 | 王丽萍 | Durable fire-resistant sealant for building |
-
2016
- 2016-05-19 CN CN201610335692.4A patent/CN105950073A/en active Pending
Patent Citations (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN104046307A (en) * | 2014-05-30 | 2014-09-17 | 青岛辰青信息技术有限公司 | High-temperature-resistant sealant |
| CN105462532A (en) * | 2015-12-18 | 2016-04-06 | 天津盛同科技有限公司 | Multifunctional high binding force sealing adhesive |
| CN105505238A (en) * | 2015-12-30 | 2016-04-20 | 王丽萍 | Durable fire-resistant sealant for building |
Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN115259676A (en) * | 2022-09-26 | 2022-11-01 | 大城县洪海保温材料有限公司 | Formaldehyde-free high-durability rock wool material and preparation method thereof |
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| PB01 | Publication | ||
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| WD01 | Invention patent application deemed withdrawn after publication | ||
| WD01 | Invention patent application deemed withdrawn after publication |
Application publication date: 20160921 |