CN105943456A - Tea saponin shampoo and preparation method thereof - Google Patents

Tea saponin shampoo and preparation method thereof Download PDF

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Publication number
CN105943456A
CN105943456A CN201610454137.3A CN201610454137A CN105943456A CN 105943456 A CN105943456 A CN 105943456A CN 201610454137 A CN201610454137 A CN 201610454137A CN 105943456 A CN105943456 A CN 105943456A
Authority
CN
China
Prior art keywords
tea saponin
shampoo
thoroughly decomposed
fermentation liquid
stalk
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Pending
Application number
CN201610454137.3A
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Chinese (zh)
Inventor
万家林
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Hefei Fengruilong Biological Technology Co Ltd
Original Assignee
Hefei Fengruilong Biological Technology Co Ltd
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Hefei Fengruilong Biological Technology Co Ltd filed Critical Hefei Fengruilong Biological Technology Co Ltd
Priority to CN201610454137.3A priority Critical patent/CN105943456A/en
Publication of CN105943456A publication Critical patent/CN105943456A/en
Pending legal-status Critical Current

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Classifications

    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00Cosmetics or similar toiletry preparations
    • A61K8/18Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/96Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution
    • A61K8/97Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution from algae, fungi, lichens or plants; from derivatives thereof
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00Cosmetics or similar toiletry preparations
    • A61K8/18Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/30Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
    • A61K8/60Sugars; Derivatives thereof
    • A61K8/602Glycosides, e.g. rutin
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00Cosmetics or similar toiletry preparations
    • A61K8/18Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/92Oils, fats or waxes; Derivatives thereof, e.g. hydrogenation products thereof
    • A61K8/922Oils, fats or waxes; Derivatives thereof, e.g. hydrogenation products thereof of vegetable origin
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61QSPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
    • A61Q17/00Barrier preparations; Preparations brought into direct contact with the skin for affording protection against external influences, e.g. sunlight, X-rays or other harmful rays, corrosive materials, bacteria or insect stings
    • A61Q17/005Antimicrobial preparations
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61QSPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
    • A61Q5/00Preparations for care of the hair
    • A61Q5/006Antidandruff preparations
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61QSPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
    • A61Q5/00Preparations for care of the hair
    • A61Q5/02Preparations for cleaning the hair
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61QSPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
    • A61Q5/00Preparations for care of the hair
    • A61Q5/12Preparations containing hair conditioners
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K2800/00Properties of cosmetic compositions or active ingredients thereof or formulation aids used therein and process related aspects
    • A61K2800/80Process related aspects concerning the preparation of the cosmetic composition or the storage or application thereof
    • A61K2800/85Products or compounds obtained by fermentation, e.g. yoghurt, beer, wine

Abstract

The invention provides tea saponin shampoo and a preparation method thereof. The shampoo is prepared from the following raw materials in percentage by weight: 40-60 percent of a straw fermentation broth, 20-30 percent of tea saponin, 10-20 percent of a conditioner, 1-5 percent of a thickening agent, and 0.2-0.8 percent of herbal essential oil, wherein the straw fermentation broth is prepared by fermenting wheat straws and rice straws by decomposed mixed bacteria. The preparation method comprises the following steps: (1) weighing the straw fermentation broth according to weight percentage, adding into an emulsification tank, heating to 70-80 DEG C, dissolving the tea saponin into the straw fermentation broth, and cooling to 35-45 DEG C; and (2) adding the conditioner, the thickening agent and the herbal essential oil into the stirring tank in the step (1), uniformly stirring, cooling to room temperature, and standing for 10-12 hours. The tea saponin shampoo is prepared from the raw materials without toxic or side effect on human bodies, and has the characteristics of simple production process and low cost and energy consumption, is easy to control, and is easy for batch production.

Description

Tea saponin shampoo and preparation method thereof
Technical field
The invention belongs to shampoo technical field, be specifically related to a kind of tea saponin shampoo and preparation method thereof.
Background technology
Shampoo, also known as shampoo, shampoo or shampoo, is the hair being most widely used and scalp base Plinth nursing cosmetic product, is one of requisite the articles for daily use in people's daily life.Typically use sulphuric acid The triethanolamine of fatty alcohol and the salt-mixture of oxyammonia, lauric acid/dodecanoic acid isopropanol amide, formaldehyde, polyoxyethylene, Lanoline, spice, colorant and water are as raw material.Currently mainly kind, by transparency can be divided into transparent type, Pearly-lustre type and milkiness type;Conditioner shampoo, neutral shampoo, oiliness shampoo, dryness shampoo can be divided into by function, Anti-dandruff shampoo, dyeing shampoo etc..Shampoo on market adds certain additive and change mostly Learning synthesis detergent, improper use can make the undue defat of scalp, causes root of hair pruritus, inflammation, makes hair quality be subject to Damage.
Tea saponin is by the class candy glycoside compound extracted in Camellia sinensis seed, is a kind of sky of good performance So surfactant, has good emulsifying, disperses, foams, the function such as moistens, and have antiinflammatory, Analgesia, the pharmacological action such as impermeabilisation.The most just there is the custom utilizing tea seed cake to wash hair in China.In tea seed cake Containing tea saponin, protein, natural Oleum Camelliae etc., life-time service have only bits, antipruritic, deoil, sterilize, repair Effect of multiple damaged hair, the most obvious blackening and generating hair effect.It was verified that tea saponin wash my hair is not only Have send out loose, smooth, anti-dandruff, the advantage such as antipruritic, have effect of clean hair care, and stingless to skin Sharp, allergy effect, uses safety.Along with the raising of people's living standard with to environmental protection, Green Lifestyle Pursuit, some natural plant raw materials are gradually introduced in hair shampoo article.Through retrieval, Chinese patent CN101129310A, CN102836097A, CN101390816A etc. all disclose containing tea saponin shampoo Or tea saponin shampoo formula and processing technology etc., and document [tea saponin and the application in cosmetics thereof, Beijing Technology and Business University's journal, 2009,27 (3)] disclose high-grade shampoo and natural herb shampoo formula. Although all containing tea saponin in these technical products, also contain contained by routine shampoo (dew) is each simultaneously Kind of synthetic chemical, although having certain hair care, hair caring effect, but there is also pollution environment, production The problems such as complex process.
Summary of the invention
Deficiency and people's needs to green ecological environment-friendly products for prior art products, it is provided that a kind of Tea saponin shampoo, the raw material that product of the present invention uses is without any side effects to human body, has production technology Simple and easily controllable, cost and energy consumption is low, be prone to the feature of batch production.
The technical scheme is that and be achieved in that:
A kind of tea saponin shampoo, calculates according to percetage by weight, makes including following raw material:
Stalk fermentation liquid 40-60%, tea saponin 20-30%, conditioner 10-20%, thickening agent 1-5%, plant Thing quintessence oil 0.2-0.8%;
Wherein, described stalk fermentation liquid be wheat stalk and rice straw prepared by the mixed fermentation that becomes thoroughly decomposed and ?.
Further, in wheat stalk and rice straw, inoculation is become thoroughly decomposed bacterium, watering regulation water content to 55-60%, Under heat-retaining condition, 40-50 DEG C of compost fermentation 7-10 days, must become thoroughly decomposed material, on centrifugal for the described material that becomes thoroughly decomposed Clear liquid, is stalk fermentation liquid.
Further, described conditioner selected from hydroxypropyl guar gum, polysiloxane quaternary ammonium, D-panthenol with sun from One or more mixing in subbundle element.
Further, described thickening agent one or more mixing in sodium chloride, ammonium chloride and sodium sulfate.
Further, described plants essential oil is Herba Lysimachiae foenum-graeci quintessence oil, Fructus Citri Limoniae oil, Oleum Caryophylli or Oleum menthae.
It is a further object to provide the preparation method of a kind of tea saponin shampoo, comprise the following steps:
1) weigh stalk fermentation liquid according to percentage by weight, add emulsifying and fill interior, be heated to 70-80 DEG C, so After tea saponin added in stalk fermentation liquid dissolve, be then cooled to 35-45 DEG C;
2) conditioner, thickening agent and plants essential oil are all added step 1) agitator tank in, after stirring, It is cooled to room temperature, then stands 10-12h;
Wherein, described stalk fermentation liquid be wheat stalk and rice straw prepared by the mixed fermentation that becomes thoroughly decomposed and ?.
Inoculating bacterium of becoming thoroughly decomposed in wheat stalk and rice straw, watering regulation water content is to 55-60%, in insulation Under the conditions of, 40-50 DEG C of compost fermentation 7-10 days, must become thoroughly decomposed material, to obtain supernatant by centrifugal for the described material that becomes thoroughly decomposed, It is stalk fermentation liquid.Pseudomonas of becoming thoroughly decomposed used in the present invention, in prior art, can be bought in face from the market Obtain.
Beneficial effects of the present invention:
1, in China, annual straw total output is about 8-10 hundred million tons, occupies first place in the world, and especially the north is little Wheat, Semen Maydis and reed sediment substrate are abundant, widely distributed, and growth is concentrated;The generation amount of its straw is with Per Unit Area Grain Yield With total raising produced and increase year by year, but corresponding treatment technology is delayed, thus brings a series of environment With social problem's straw.Straw is generally used to make Crop fertilizer or feedstuff.If tea saponin purity Low, sterilization dandruff is had an impact by the impurity such as its implication protein, organic acid.The present inventor is by big Amount experiment have been surprisingly found that straw after bacterium fermentation of becoming thoroughly decomposed, it has extraordinary with tea saponin coordinated Treatment of dandruff curative effect, 100 squarrose patients of long-term trouble are through experiment in 30 days, patient's head of 98% Scurf is removed completely, and 3 months tracking tests find, the most do not recur.
2, the present invention solves the problem of straw pollution environment, improves the economic benefit of enterprise.Institute of the present invention The raw material used is without any side effects to human body, and have hair care, have one's hair wash, sterilize, antipruritic etc. multiple Effect.Avoid chemistry shampoo to the damage of hair and the stimulation of skin and the pollution to environment.
Detailed description of the invention
Embodiment 1
Prepared by stalk fermentation liquid:
Inoculating bacterium of becoming thoroughly decomposed in wheat stalk and rice straw, watering regulation water content is to 60%, at heat preservation strip Under part, 40 DEG C of compost fermentations 10 days, must become thoroughly decomposed material, to obtain supernatant by centrifugal for the described material that becomes thoroughly decomposed, to be straw Stalk fermentation liquid.
Embodiment 2
Prepared by stalk fermentation liquid:
Inoculating bacterium of becoming thoroughly decomposed in wheat stalk and rice straw, watering regulation water content is to 55%, at heat preservation strip Under part, 50 DEG C of compost fermentations 7 days, must become thoroughly decomposed material, to obtain supernatant by centrifugal for the described material that becomes thoroughly decomposed, to be straw Fermentation liquid.
Embodiment 3
A kind of tea saponin shampoo, makes including following raw material:
Stalk fermentation liquid 60kg that embodiment 1 prepares, tea saponin 20kg, hydroxypropyl guar gum 15kg, Sodium chloride 4.2kg, Herba Lysimachiae foenum-graeci quintessence oil 0.8kg.
The preparation method of tea saponin shampoo, comprises the following steps:
1) weigh stalk fermentation liquid 60kg, add emulsifying and fill interior, be heated to 70 DEG C, then by 20kg tea soap Element addition stalk fermentation liquid dissolves, is then cooled to 35 DEG C;
2) hydroxypropyl guar gum 15kg, sodium chloride 4.2kg and Herba Lysimachiae foenum-graeci quintessence oil 0.8kg are all added step 1) Agitator tank in, after stirring, be cooled to room temperature, then stand 12h, regulate pH by pH adjusting agent To 6.5-7.0.
Embodiment 4
A kind of tea saponin shampoo, calculates according to percetage by weight, makes including following raw material:
Stalk fermentation liquid 50kg that embodiment 2 prepares, tea saponin 25kg, D-panthenol 20kg, sulphuric acid Sodium 4.8kg, Fructus Citri Limoniae oil 0.2kg.
The preparation method of tea saponin shampoo, comprises the following steps:
1) weigh stalk fermentation liquid 57kg, add emulsifying and fill interior, be heated to 80 DEG C, then tea saponin added Enter in stalk fermentation liquid and dissolve, be then cooled to 45 DEG C;
2) D-panthenol 20kg, sodium sulfate 4.8kg and Fructus Citri Limoniae oil 0.2kg are all added step 1) agitator tank In, after stirring, it is cooled to room temperature, then stands 10h.
Embodiment 5
A kind of tea saponin shampoo, calculates according to percetage by weight, makes including following raw material:
Stalk fermentation liquid 48kg that embodiment 1 prepares, D-panthenol 15kg, cationic cellulose 15kg, Conditioner 18kg, sodium chloride 1.8kg, sodium sulfate 1.8kg and Oleum menthae 0.8kg.
The preparation method of tea saponin shampoo, comprises the following steps:
1) weigh stalk fermentation liquid 48kg, add emulsifying and fill interior, be heated to 75 DEG C, then tea saponin added Enter in stalk fermentation liquid and dissolve, be then cooled to 40 DEG C;
2) by D-panthenol 15kg, cationic cellulose 15kg, conditioner 18kg, sodium chloride 1.8kg, sulfur Acid sodium 1.8kg and Oleum menthae 0.8kg all add step 1) agitator tank in, after stirring, be cooled to room Temperature, then stands 10.
The foregoing is only presently preferred embodiments of the present invention, not in order to limit the present invention, all at this Within bright spirit and principle, any modification, equivalent substitution and improvement etc. made, should be included in this Within bright protection domain.

Claims (8)

1. a tea saponin shampoo, it is characterised in that calculate according to percetage by weight, including following raw material Make:
Stalk fermentation liquid 40-60%, tea saponin 20-30%, conditioner 10-20%, thickening agent 1-5%, plant Thing quintessence oil 0.2-0.8%;
Wherein, described stalk fermentation liquid be wheat stalk and rice straw prepared by the mixed fermentation that becomes thoroughly decomposed and ?.
Tea saponin shampoo the most according to claim 1, it is characterised in that in wheat stalk and Oryza sativa L. Straw is inoculated bacterium of becoming thoroughly decomposed, watering regulation water content to 55-60%, under heat-retaining condition, 40-50 DEG C of compost Fermenting 7-10 days, must become thoroughly decomposed material, the described material that becomes thoroughly decomposed is centrifuged to obtain supernatant, is stalk fermentation liquid.
Tea saponin shampoo the most according to claim 1 and 2, it is characterised in that described conditioner selects One or more in hydroxypropyl guar gum, polysiloxane quaternary ammonium, D-panthenol and cationic cellulose Mixing.
Tea saponin shampoo the most according to claim 1 and 2, it is characterised in that described thickening agent selects One or more mixing in sodium chloride, ammonium chloride and sodium sulfate.
Tea saponin shampoo the most according to claim 1 and 2, it is characterised in that described plants essential oil For Herba Lysimachiae foenum-graeci quintessence oil, Fructus Citri Limoniae oil, Oleum Caryophylli or Oleum menthae.
6. the preparation method of a tea saponin shampoo as claimed in claim 1, it is characterised in that include Following steps:
1) weigh stalk fermentation liquid according to percentage by weight, add emulsifying and fill interior, be heated to 70-80 DEG C, so After tea saponin added in stalk fermentation liquid dissolve, be then cooled to 35-45 DEG C;
2) conditioner, thickening agent and plants essential oil are all added step 1) agitator tank in, after stirring, It is cooled to room temperature, then stands 10-12h;
Wherein, described stalk fermentation liquid be wheat stalk and rice straw prepared by the mixed fermentation that becomes thoroughly decomposed and ?.
The preparation method of tea saponin shampoo the most according to claim 6, it is characterised in that at Semen Tritici aestivi Inoculating bacterium of becoming thoroughly decomposed in straw and rice straw, watering regulation water content is to 55-60%, under heat-retaining condition, 40-50 DEG C of compost fermentation 7-10 days, must become thoroughly decomposed material, to obtain supernatant by centrifugal for the described material that becomes thoroughly decomposed, to be straw and send out Ferment liquid.
The preparation method of tea saponin shampoo the most according to claim 6, it is characterised in that described tune Reason agent one in hydroxypropyl guar gum, polysiloxane quaternary ammonium, D-panthenol and cationic cellulose or The multiple mixing of person;One or more mixing in sodium chloride, ammonium chloride and sodium sulfate of described thickening agent.
CN201610454137.3A 2016-06-20 2016-06-20 Tea saponin shampoo and preparation method thereof Pending CN105943456A (en)

Priority Applications (1)

Application Number Priority Date Filing Date Title
CN201610454137.3A CN105943456A (en) 2016-06-20 2016-06-20 Tea saponin shampoo and preparation method thereof

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Application Number Priority Date Filing Date Title
CN201610454137.3A CN105943456A (en) 2016-06-20 2016-06-20 Tea saponin shampoo and preparation method thereof

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Citations (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN101390816A (en) * 2008-11-06 2009-03-25 郴州邦尔泰苏仙油脂有限公司 Formulation of tea saponin shampoo and production technique thereof
CN102210644A (en) * 2011-06-11 2011-10-12 董家华 APG (alkyl polyglucoside) plant environmentally-friendly shampoo
CN105294284A (en) * 2015-11-20 2016-02-03 河北中仓化肥有限公司 Preparation method of straw fermented biological fertilizer

Patent Citations (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN101390816A (en) * 2008-11-06 2009-03-25 郴州邦尔泰苏仙油脂有限公司 Formulation of tea saponin shampoo and production technique thereof
CN102210644A (en) * 2011-06-11 2011-10-12 董家华 APG (alkyl polyglucoside) plant environmentally-friendly shampoo
CN105294284A (en) * 2015-11-20 2016-02-03 河北中仓化肥有限公司 Preparation method of straw fermented biological fertilizer

Non-Patent Citations (1)

* Cited by examiner, † Cited by third party
Title
唐清池: "《生物技术在农业废弃物上的应用与实践》", 31 December 2015 *

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Application publication date: 20160921