CN105942530A - Squid protein powder - Google Patents

Squid protein powder Download PDF

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Publication number
CN105942530A
CN105942530A CN201610298711.0A CN201610298711A CN105942530A CN 105942530 A CN105942530 A CN 105942530A CN 201610298711 A CN201610298711 A CN 201610298711A CN 105942530 A CN105942530 A CN 105942530A
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China
Prior art keywords
squid
powder
parts
egg albumen
enzymolysis
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CN201610298711.0A
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Chinese (zh)
Inventor
谢超
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Zhejiang Ocean University ZJOU
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Zhejiang Ocean University ZJOU
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Priority to CN201610298711.0A priority Critical patent/CN105942530A/en
Publication of CN105942530A publication Critical patent/CN105942530A/en
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    • AHUMAN NECESSITIES
    • A23FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
    • A23JPROTEIN COMPOSITIONS FOR FOODSTUFFS; WORKING-UP PROTEINS FOR FOODSTUFFS; PHOSPHATIDE COMPOSITIONS FOR FOODSTUFFS
    • A23J1/00Obtaining protein compositions for foodstuffs; Bulk opening of eggs and separation of yolks from whites
    • A23J1/04Obtaining protein compositions for foodstuffs; Bulk opening of eggs and separation of yolks from whites from fish or other sea animals
    • AHUMAN NECESSITIES
    • A23FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
    • A23JPROTEIN COMPOSITIONS FOR FOODSTUFFS; WORKING-UP PROTEINS FOR FOODSTUFFS; PHOSPHATIDE COMPOSITIONS FOR FOODSTUFFS
    • A23J1/00Obtaining protein compositions for foodstuffs; Bulk opening of eggs and separation of yolks from whites
    • A23J1/10Obtaining protein compositions for foodstuffs; Bulk opening of eggs and separation of yolks from whites from hair, feathers, horn, skins, leather, bones, or the like
    • AHUMAN NECESSITIES
    • A23FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
    • A23VINDEXING SCHEME RELATING TO FOODS, FOODSTUFFS OR NON-ALCOHOLIC BEVERAGES AND LACTIC OR PROPIONIC ACID BACTERIA USED IN FOODSTUFFS OR FOOD PREPARATION
    • A23V2002/00Food compositions, function of food ingredients or processes for food or foodstuffs

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  • Life Sciences & Earth Sciences (AREA)
  • Chemical & Material Sciences (AREA)
  • Zoology (AREA)
  • Biochemistry (AREA)
  • Engineering & Computer Science (AREA)
  • Food Science & Technology (AREA)
  • Polymers & Plastics (AREA)
  • Marine Sciences & Fisheries (AREA)
  • Meat, Egg Or Seafood Products (AREA)

Abstract

The present invention relates to squid protein powder. The squid protein powder comprises the following raw materials in parts by weight: 150-220 parts of squid extracts, 80-100 parts of vegetable powder, 80-100 parts of corn syrups, 20-30 parts of fruit powder, 10-20 parts of an aid agent and 40-60 parts of bone meal. The squid protein powder is prepared from wastes of squid skin and viscera, which can turn the squid wastes into treasures, reduce environmental pollution, also greatly save the production cost of biological enzymolyzed proteins and achieve the effects of getting two results from one effort. The product is rich in micromolecular proteins, active peptides, amino acids, nucleotides, vitamins and trace elements, and can be made into nutritional and health-care products, snack foods and body regulating products. The quality of the products is improved and the residual values of the squid skin and squid viscera are developed. The product is simple in preparation process, low in cost, short in production time and high in efficiency.

Description

A kind of squid egg albumen powder
Technical field
The present invention relates to technical field of health care food, particularly relate to one and there is antioxidation and remove free radical, improve immunity Squid egg albumen powder.
Background technology
Along with culture fishery and the development of Marine Fishing Industry, the yield of China's aquatic products is just continuously increased, and annual production reaches 1000 More than ten thousand tons, squid is the marine products edible animal that a kind of economic worth is higher, belongs to Mollusca Cephalopoda.The nutriture value of squid Being worth the highest, meat softness is trickle, delicious flavour.In China market, mainly new Fresh squid and the dried squids of supply, also have Manufactured squid snack food.
Fresh squid's long-distance transport inconvenience, cost of transportation is higher, and storage period is short, needs for this it is carried out deep processing, current city On field, squid is machined with shredded squid, dried squids and minced fish.In general, in remaining after squid processed acquirement edible part The processing byproduct of the composition such as dirty, skin accounts for the 30% of toatl proportion, and the one-tenth of processing byproduct is grouped into: moisture 63%, thick fat Fat 22.5%, crude protein 13.5% remaining 1%, these garbages domestic some be processed into the molten slurry of squid, some is worked as Do rubbish emergency burial, this most still huge waste to fishery resources, but also there is the hidden danger of environmental pollution.Along with existing For ocean processing industry and the development of aquaculture, the comprehensive utilization of squid garbage increasingly comes into one's own.
Egg albumen powder is the nutrient that a class is important, and its existence is closely connected with the various activities of life, such as participates in body Constitute and the metabolism of body, participate in hereditary information and constitute and metabolism, the most also provide heat for body.
Summary of the invention
It is an object of the invention to solve existing squid waste utilization few, waste serious defect and provide one to have Antioxidation and removing free radical, the squid egg albumen powder of raising immunity.
To achieve these goals, the present invention is by the following technical solutions:
A kind of squid egg albumen powder, described squid egg albumen powder is made up of the raw material of following weight portion: squid extract 150-220 part, vegetable Powder 80-100 part, corn syrup 80-100 part, fruit powder 20-30 part, auxiliary agent 10-20 part and bone meal 40-60 part.In this technology In scheme, use squid skin and the leftover bits and pieces of internal organs, the waste material of squid can not only be turned waste into wealth, reduce environmental pollution, and Also it is greatly saved the protelytic production cost of enzyme, reaches the effect killed two birds with one stone;In product rich in small protein, Bioactive peptide, aminoacid, nucleotide, electrolytes and minerals;Product can make nutrient and healthcare products, leisure food, conditioning Product, improve product quality, have developed the surplus value of squid skin and squid viscera.
As preferably, the preparation method of described squid extract comprises the following steps: select fresh or through the flowing water of 0-4 DEG C The squid thawed processes remaining squid skin and internal organs, obtains fish slurry after homogenate, is soaked by fish slurry at 75-100 DEG C in soak Bubble 30-60min, and carry out ultrasonic Treatment, with the Mel ice water solution rinsing that mass concentration is 1.7-2.2% after pulling out simultaneously 30-80min, clear water adds the lipase adding 30-40U/g in fish slurry, under the conditions of 30-35 DEG C, enzymolysis processing after cleaning 60-75min, obtains defat homogenate;In defat homogenate, add proteolytic enzyme, after enzymolysis terminates, temperature is risen to 90-100 DEG C keeps 20-30min, makes enzyme-deactivating, obtain enzymolysis solution;Enzymolysis solution is cooled to 15 DEG C of 8000-10000rpm be centrifuged, Take supernatant to carry out being concentrated in vacuo to 10-15% and obtain squid extract.
As preferably, each component of soak is respectively as follows: edible salt 1.5-2.5%, Folium Camelliae sinensis 5-10%, carbon by weight percentage Acid hydrogen sodium 1.0-2.0%, vitamin c 0.2-0.4%, glutathion 0.5-0.7%, surplus is water, the frequency of ultrasound wave during immersion treatment Rate is 35-55KHz.
As preferably, the addition of proteolytic enzyme is every milliliter of defat homogenate 3000-3500U, described proteolytic enzyme For protein incision enzyme and albumen excision enzyme, it is 7-8 at pH value, under conditions of temperature is 45-50 DEG C, enzymolysis 5-6h.
As preferably, Vegetable powder be mass ratio be the Semen Maydis powder of 1:3:1:2:3:5, Semen sojae atricolor powder, Mai Mendong, Fructus Rubi, lotus Leaf powder and Radix Dauci Sativae powder.
As preferably, fruit powder be mass ratio be the cherry powder of 1:2:3, Hawaii fruit powder and Herba Saussureae Involueratae fruit powder.
As preferably, described auxiliary agent is the mixture of vitamin E, Mel, Radix Codonopsis and Herba Menthae powder, vitamin E, Mel, Radix Codonopsis is 1:5:1:2 with the mass ratio of the mixture of Herba Menthae powder.
As preferably, bone meal used be broken into 1-10 μm by fishbone, Os Bovis seu Bubali, Os Caprae seu Ovis, Os Sus domestica powder after little through 85-95 DEG C Fire infusion 10-12h makes soup, and being then concentrated into moisture is 1% to be crushed to 30-100 μm and make.
The invention has the beneficial effects as follows:
1) use squid skin and the leftover bits and pieces of internal organs, the waste material of squid can not only be turned waste into wealth, minimizing environmental pollution, but also significantly Save the protelytic production cost of enzyme, reach the effect killed two birds with one stone;
2) rich in small protein, bioactive peptide, aminoacid, nucleotide, electrolytes and minerals in product;
3) product can make nutrient and healthcare products, leisure food, conditioning product, improves product quality, have developed squid skin and squid The surplus value of internal organs;
4) product preparation process of the present invention is simple, low cost, and Production Time is short, and efficiency is high.
Detailed description of the invention
Technical scheme in the embodiment of the present invention will be carried out clear, complete description below, it is clear that described embodiment It is only a part of embodiment of the present invention rather than whole embodiments.Based on the embodiment in the present invention, the common skill in this area All other embodiments that art personnel are obtained under not making creative work premise, broadly fall into the scope of protection of the invention.
Vegetable powder be mass ratio be the Semen Maydis powder of 1:3:1:2:3:5, Semen sojae atricolor powder, Mai Mendong, Fructus Rubi, Folium Nelumbinis powder and recklessly trailing plants Bu Fen.
Fruit powder be mass ratio be the cherry powder of 1:2:3, Hawaii fruit powder and Herba Saussureae Involueratae fruit powder.
Described auxiliary agent is the mixture of vitamin E, Mel, Radix Codonopsis and Herba Menthae powder, vitamin E, Mel, Radix Codonopsis and Herba Menthae The mass ratio of the mixture of powder is 1:5:1:2.Vitamin E, Radix Codonopsis and Herba Menthae powder is added in Mel, ultrasonic in 50 DEG C of water-baths 30min, supersonic frequency is that 50hz obtains.
Embodiment 1
A kind of squid egg albumen powder, described squid egg albumen powder is made up of the raw material of following weight portion: squid extract 150 parts, Vegetable powder 80 Part, corn syrup 80 parts, fruit powder 20 parts, auxiliary agent 10 parts and bone meal 40 parts.
The preparation method of described squid extract comprises the following steps: select fresh or through 0-4 DEG C flowing water thaw squid Process remaining squid skin and internal organs, after homogenate, obtain fish slurry, fish slurry is soaked at 75 DEG C in soak 30min, and same Shi Jinhang ultrasonic Treatment, with the Mel ice water solution rinsing 30min that mass concentration is 1.7% after pulling out, clear water adds after cleaning Fish slurry adds the lipase of 30U/g, under the conditions of 30 DEG C, enzymolysis processing 60min, obtains defat homogenate;Even to defat Serosity adds proteolytic enzyme, after enzymolysis terminates, temperature is risen to 90 DEG C and keeps 20min, make enzyme-deactivating, obtain enzymolysis solution; Enzymolysis solution is cooled to 15 DEG C of 8000rpm be centrifuged, takes supernatant and carry out being concentrated in vacuo to 10% and obtain squid extract;Wherein, Each component of soak is respectively as follows: edible salt 1.5% by weight percentage, Folium Camelliae sinensis 5%, sodium bicarbonate 1.0%, vitamin c 0.2%, Glutathion 0.5%, surplus is water, and during immersion treatment, the frequency of ultrasound wave is 35KHz;The addition of proteolytic enzyme is every milli Rising defat homogenate 3000U, described proteolytic enzyme is protein incision enzyme and albumen excision enzyme, is 7 at pH value, and temperature is Under conditions of 45 DEG C, enzymolysis 5h.
Bone meal used is made through 85 DEG C little fire infusion 10h after being broken into 1-10 μm by fishbone, Os Bovis seu Bubali, Os Caprae seu Ovis, Os Sus domestica powder Soup, being then concentrated into moisture is 1% to be crushed to 30-100 μm and make.
Weigh squid extract by weight to be dissolved in ethanol, be subsequently adding Vegetable powder, corn syrup, fruit powder, auxiliary agent and bone Powder, uses 220 DEG C of spray drying of spray-dried tower to obtain squid egg albumen powder, and then the cabinet-type purple low-light temperature 90 DEG C kills Sterilize in bacterium machine 2min, quantitative package, normal temperature storage.
Embodiment 2
A kind of squid egg albumen powder, described squid egg albumen powder is made up of the raw material of following weight portion: squid extract 180 parts, Vegetable powder 90 Part, corn syrup 90 parts, fruit powder 26 parts, auxiliary agent 15 parts and bone meal 50 parts.
The preparation method of described squid extract comprises the following steps: select fresh or through 0-4 DEG C flowing water thaw squid Process remaining squid skin and internal organs, after homogenate, obtain fish slurry, fish slurry is soaked at 80 DEG C in soak 50min, and same Shi Jinhang ultrasonic Treatment, with the Mel ice water solution rinsing 60min that mass concentration is 2% after pulling out, clear water adds fish after cleaning Slurry adds the lipase of 35U/g, under the conditions of 32 DEG C, enzymolysis processing 65min, obtain defat homogenate;It is homogenized to defat Liquid adds proteolytic enzyme, after enzymolysis terminates, temperature is risen to 95 DEG C and keeps 25min, make enzyme-deactivating, obtain enzymolysis solution; Enzymolysis solution is cooled to 15 DEG C of 9000rpm be centrifuged, takes supernatant and carry out being concentrated in vacuo to 12% and obtain squid extract;Wherein, Each component of soak is respectively as follows: edible salt 2% by weight percentage, Folium Camelliae sinensis 6%, sodium bicarbonate 1.5%, vitamin c 0.3%, Glutathion 0.6%, surplus is water, and during immersion treatment, the frequency of ultrasound wave is 45KHz;The addition of proteolytic enzyme is every milli Rising defat homogenate 3200U, described proteolytic enzyme is protein incision enzyme and albumen excision enzyme, is 7.5 at pH value, temperature Under conditions of being 48 DEG C, enzymolysis 5.5h.
Bone meal used is made through 90 DEG C little fire infusion 11h after being broken into 1-10 μm by fishbone, Os Bovis seu Bubali, Os Caprae seu Ovis, Os Sus domestica powder Soup, being then concentrated into moisture is 1% to be crushed to 30-100 μm and make.
Weigh squid extract by weight to be dissolved in ethanol, be subsequently adding Vegetable powder, corn syrup, fruit powder, auxiliary agent and bone Powder, uses 220 DEG C of spray drying of spray-dried tower to obtain squid egg albumen powder, and then the cabinet-type purple low-light temperature 90 DEG C kills Sterilize in bacterium machine 2min, quantitative package, normal temperature storage.
Embodiment 3
A kind of squid egg albumen powder, described squid egg albumen powder is made up of the raw material of following weight portion: squid extract 220 parts, Vegetable powder 100 Part, corn syrup 100 parts, fruit powder 30 parts, auxiliary agent 20 parts and bone meal 60 parts.
The preparation method of described squid extract comprises the following steps: select fresh or through 0-4 DEG C flowing water thaw squid Process remaining squid skin and internal organs, after homogenate, obtain fish slurry, fish slurry is soaked at 100 DEG C in soak 60min, and same Shi Jinhang ultrasonic Treatment, with the Mel ice water solution rinsing 80min that mass concentration is 2.2% after pulling out, clear water adds after cleaning Fish slurry adds the lipase of 40U/g, under the conditions of 35 DEG C, enzymolysis processing 75min, obtains defat homogenate;Even to defat Serosity adds proteolytic enzyme, after enzymolysis terminates, temperature is risen to 100 DEG C and keeps 30min, make enzyme-deactivating, obtain enzymolysis solution; Enzymolysis solution is cooled to 15 DEG C of 10000rpm be centrifuged, takes supernatant and carry out being concentrated in vacuo to 15% and obtain squid extract;Wherein, Each component of soak is respectively as follows: edible salt 2.5% by weight percentage, Folium Camelliae sinensis 10%, sodium bicarbonate 2.0%, vitamin c 0.4%, Glutathion 0.7%, surplus is water, and during immersion treatment, the frequency of ultrasound wave is 55KHz;The addition of proteolytic enzyme is every milli Rising defat homogenate 3500U, described proteolytic enzyme is protein incision enzyme and albumen excision enzyme, is 8 at pH value, and temperature is Under conditions of 50 DEG C, enzymolysis 6h.
Bone meal used is made through 95 DEG C little fire infusion 12h after being broken into 1-10 μm by fishbone, Os Bovis seu Bubali, Os Caprae seu Ovis, Os Sus domestica powder Soup, being then concentrated into moisture is 1% to be crushed to 30-100 μm and make.
Weigh squid extract by weight to be dissolved in ethanol, be subsequently adding Vegetable powder, corn syrup, fruit powder, auxiliary agent and bone Powder, uses 220 DEG C of spray drying of spray-dried tower to obtain squid egg albumen powder, and then the cabinet-type purple low-light temperature 90 DEG C kills Sterilize in bacterium machine 2min, quantitative package, normal temperature storage.
It should be appreciated that to those skilled in the art, can be improved according to the above description or be converted, And all these modifications and variations all should belong to the protection domain of claims of the present invention.

Claims (8)

1. a squid egg albumen powder, it is characterised in that described squid egg albumen powder is made up of the raw material of following weight portion: squid extract 150-220 part, Vegetable powder 80-100 part, corn syrup 80-100 part, fruit powder 20-30 part, auxiliary agent 10-20 part and bone meal 40-60 Part.
A kind of squid egg albumen powder the most according to claim 1, it is characterised in that the preparation method of described squid extract include with Lower step: select squid that is fresh or that thaw through the flowing water of 0-4 DEG C to process remaining squid skin and internal organs, obtain fish slurry after homogenate, Fish slurry is soaked at 75-100 DEG C in soak 30-60min, and carries out ultrasonic Treatment simultaneously, after pulling out, use mass concentration Mel ice water solution for 1.7-2.2% rinses 30-80min, and clear water adds the lipase adding 30-40U/g in fish slurry after cleaning, Under the conditions of 30-35 DEG C, enzymolysis processing 60-75min, obtain defat homogenate;Proteolytic enzyme is added in defat homogenate, After enzymolysis terminates, temperature is risen to 90-100 DEG C and keeps 20-30min, make enzyme-deactivating, obtain enzymolysis solution;Enzymolysis solution is cooled to 15 DEG C of 8000-10000rpm are centrifuged, and take supernatant and carry out being concentrated in vacuo to 10-15% and obtain squid extract.
A kind of squid egg albumen powder the most according to claim 2, it is characterised in that each component of soak is distinguished by weight percentage For: edible salt 1.5-2.5%, Folium Camelliae sinensis 5-10%, sodium bicarbonate 1.0-2.0%, vitamin c 0.2-0.4%, glutathion 0.5-0.7%, Surplus is water, and during immersion treatment, the frequency of ultrasound wave is 35-55KHz.
A kind of squid egg albumen powder the most according to claim 2, it is characterised in that the addition of proteolytic enzyme is every milliliter of defat Homogenate 3000-3500U, described proteolytic enzyme is protein incision enzyme and albumen excision enzyme, is 7-8 at pH value, and temperature is Under conditions of 45-50 DEG C, enzymolysis 5-6h.
A kind of squid egg albumen powder the most according to claim 1, it is characterised in that Vegetable powder be mass ratio be 1:3:1:2:3:5's Semen Maydis powder, Semen sojae atricolor powder, Mai Mendong, Fructus Rubi, Folium Nelumbinis powder and Radix Dauci Sativae powder.
A kind of squid egg albumen powder the most according to claim 1, it is characterised in that fruit powder be mass ratio be 1:2:3 cherry powder, Hawaii fruit powder and Herba Saussureae Involueratae fruit powder.
A kind of squid egg albumen powder the most according to claim 1, it is characterised in that described auxiliary agent is vitamin E, Mel, Radix Codonopsis With the mixture of Herba Menthae powder, vitamin E, Mel, Radix Codonopsis are 1:5:1:2 with the mass ratio of the mixture of Herba Menthae powder.
A kind of squid egg albumen powder the most according to claim 1, it is characterised in that bone meal used be by fishbone, Os Bovis seu Bubali, Os Caprae seu Ovis, Os Sus domestica powder makes soup through 85-95 DEG C little fire infusion 10-12h after being broken into 1-10 μm, and being then concentrated into moisture is 1% pulverizing Make to 30-100 μm.
CN201610298711.0A 2016-05-06 2016-05-06 Squid protein powder Pending CN105942530A (en)

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Cited By (6)

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Publication number Priority date Publication date Assignee Title
CN106901380A (en) * 2016-12-30 2017-06-30 浙江海洋大学 A kind of function and service protein peptides low energy electuary preparation method
CN106954730A (en) * 2017-02-13 2017-07-18 浙江海洋大学 A kind of high-nutrition food for strengthening immunologic function and preparation method thereof
CN107095310A (en) * 2017-03-20 2017-08-29 舟山昌国食品有限公司 A kind of processing method of anchovy protein powder
CN107751857A (en) * 2017-11-17 2018-03-06 浙江海洋大学 A kind of preparation method of microbial fermentation squid processing byproduct biological products
CN107912602A (en) * 2017-11-17 2018-04-17 浙江海洋大学 A kind of method that amino-acid nutrition liquid is prepared using squid processing byproduct as raw material
CN108546591A (en) * 2018-04-20 2018-09-18 管天球 A kind of preparation method of selenium-rich tea oil

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Cited By (6)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN106901380A (en) * 2016-12-30 2017-06-30 浙江海洋大学 A kind of function and service protein peptides low energy electuary preparation method
CN106954730A (en) * 2017-02-13 2017-07-18 浙江海洋大学 A kind of high-nutrition food for strengthening immunologic function and preparation method thereof
CN107095310A (en) * 2017-03-20 2017-08-29 舟山昌国食品有限公司 A kind of processing method of anchovy protein powder
CN107751857A (en) * 2017-11-17 2018-03-06 浙江海洋大学 A kind of preparation method of microbial fermentation squid processing byproduct biological products
CN107912602A (en) * 2017-11-17 2018-04-17 浙江海洋大学 A kind of method that amino-acid nutrition liquid is prepared using squid processing byproduct as raw material
CN108546591A (en) * 2018-04-20 2018-09-18 管天球 A kind of preparation method of selenium-rich tea oil

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