CN105929246A - Closed coaxial transmission line test system and method for representing dielectric property of sample to be tested - Google Patents
Closed coaxial transmission line test system and method for representing dielectric property of sample to be tested Download PDFInfo
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Abstract
本发明公开了一种测试液体及固体材料介电特性的闭合同轴传输线测试系统,该闭合同轴传输线测试系统包括测试夹具、矢量网络分析仪、计算机和测试连接线;测试夹具包括双向SMA接头、螺钉、防水橡胶垫圈、两端开口连通结构的转接头、具有电磁屏蔽效应的样品室、样品室内导体和待测样品;测试夹具由四孔法兰、柱状筒形聚四氟乙烯和双向SMA接头双母头同轴内导体构成。本发明基于传输反射法与去嵌入技术的有机结合,在不依赖专属定制校准件或对夹具进行复杂数学建模的情况下去除夹具接口的测试寄生效应,实现对液体与固体材料介电特性的精确测量;对测试样品处理要求低,夹具安装简洁,测试工作频率范围扩展灵活,适用范围广。
The invention discloses a closed coaxial transmission line test system for testing the dielectric properties of liquid and solid materials. The closed coaxial transmission line test system includes a test fixture, a vector network analyzer, a computer and a test connection line; the test fixture includes a bidirectional SMA connector , screws, waterproof rubber gaskets, adapters with openings at both ends, sample chambers with electromagnetic shielding effects, conductors in the sample chambers and samples to be tested; the test fixture consists of four-hole flanges, cylindrical PTFE and two-way SMA connectors. The female coaxial inner conductor is formed. Based on the organic combination of transmission reflection method and de-embedding technology, the present invention removes the test parasitic effect of the fixture interface without relying on exclusive customized calibration parts or complex mathematical modeling of the fixture, and realizes the dielectric properties of liquid and solid materials. Accurate measurement; low requirements for test sample processing, simple fixture installation, flexible expansion of test working frequency range, and wide application range.
Description
技术领域technical field
本发明属于微波测试领域,涉及对于液体材料、固体或固体粉末材料的介电特性的表征,特别涉及一种表征液体及固体材料介电特性的闭合同轴传输线测试系统。The invention belongs to the field of microwave testing, and relates to the characterization of the dielectric properties of liquid materials, solid or solid powder materials, in particular to a closed coaxial transmission line testing system for characterizing the dielectric properties of liquid and solid materials.
背景技术Background technique
材料的介电特性是每种材料独有的电气特征,对于材料介电特性的准确测量与表征对于材料的恰当使用至关重要。通过对材料介电特性的掌握,可以为许多电子应用提供关键的设计参数信息,通过对材料介电特性的深入了解,在食品安全检测、医疗设备设计与使用、航空航天设计等领域的应用带来帮助,快速准确的掌握材料的介电特性对提高行业产品设计、流程质量检验的效率助益良多。The dielectric properties of a material are the unique electrical characteristics of each material, and accurate measurement and characterization of the dielectric properties of a material is critical to its proper use. Through the mastery of the dielectric properties of materials, key design parameter information can be provided for many electronic applications. Through an in-depth understanding of the dielectric properties of materials, it can be used in food safety testing, medical equipment design and use, aerospace design and other fields. Come to help, quickly and accurately grasp the dielectric properties of materials is of great help to improve the efficiency of product design and process quality inspection in the industry.
对于材料介电特性的测量,主要有同轴探头法、同轴/波导传输线法、自由空间法、平行板法和谐振腔法。同轴传输线法因其具有宽频带测量(50MHz-60GHz),对测试样品加工要求较低,适用测试样品种类多样,测试快速且结果准确而倍加受到关注,但是由于闭合同轴传输线夹具需要连接仪器,其转接头在其中必不可少,从而在最终测试结果中因接头的寄生效应对测试结果的准确性造成不容忽视的影响。已有的校正方法在于根据夹具的特定尺寸定制相应的校准件,或是通过复杂的数学建模模拟接头的S参数来消除接头在S参数中的寄生效应。定制的校准件适用范围有限,成本高,建模费时同时不能完全的去除接头影响。已有的去嵌入技术可以实现在获得夹具接头S参数的前提下实现对测试去寄生效应的效果,但鲜有具体简单可供实现的方法。For the measurement of dielectric properties of materials, there are mainly coaxial probe method, coaxial/waveguide transmission line method, free space method, parallel plate method and resonant cavity method. The coaxial transmission line method has attracted more attention because of its wide-band measurement (50MHz-60GHz), low processing requirements for test samples, various types of test samples, fast test and accurate results, but because the closed coaxial transmission line fixture needs to be connected to the instrument , the adapter is essential in it, so the parasitic effect of the connector in the final test result should have a non-negligible impact on the accuracy of the test result. The existing calibration method is to customize the corresponding calibration parts according to the specific size of the fixture, or to eliminate the parasitic effect of the joint in the S parameter by simulating the S parameter of the joint through complex mathematical modeling. Customized calibration parts have limited scope of application, high cost, time-consuming modeling and cannot completely remove the influence of joints. The existing de-embedding technology can achieve the effect of de-parasitic effect on the test under the premise of obtaining the S-parameters of the fixture joint, but there are few specific and simple methods that can be realized.
现有技术“一种测试材料电磁特性的同轴夹具”(申请号201420584461.3),进行测试的探头组装程序复杂,复杂结构不利于保证测试结果准确性,同时会使样品测试的流程加长,不利于样品的快速测试,固定的转接头类型不利于测试频率的扩展。现有技术“固体及粉末材料的宽频带变温介电常数测试”(申请号201510305197.4),其对于测试夹具的测试中的耦合效应的去除是通过传统的TRL校准方式实现的,需要定制特定尺寸校准件,而校准件的制作要求极高,大大提高了生产成本,同时校准的结果不能很好的保证,同时该测试系统不能对液体样品介电特性进行测试。In the existing technology "a coaxial fixture for testing the electromagnetic properties of materials" (application number 201420584461.3), the assembly procedure of the probe for testing is complicated, and the complex structure is not conducive to ensuring the accuracy of test results. At the same time, it will lengthen the process of sample testing, which is not conducive to The fast test of the sample, the fixed adapter type is not conducive to the expansion of the test frequency. Existing technology "Broadband Variable Temperature Permittivity Test of Solid and Powder Materials" (Application No. 201510305197.4), the removal of the coupling effect in the test of the test fixture is achieved through the traditional TRL calibration method, which requires customized calibration of specific dimensions However, the production requirements of the calibration parts are extremely high, which greatly increases the production cost. At the same time, the results of the calibration cannot be well guaranteed. At the same time, the test system cannot test the dielectric properties of the liquid sample.
发明内容Contents of the invention
针对现有技术中同轴传输线测试方法测试夹具中接头在测试过程中产生的寄生效应难以去除,特定测试材料对应用频率范围要求较高,特定的同轴传输线夹具工作范围有限,测试频率范围扩展困难的问题。本发明提供一种表征液体及固体材料介电特性的闭合同轴传输线测试系统,具体是一种闭合同轴传输线探头,该闭合同轴传输线测试系统校正结果准确,测试频率范围可供扩展的测试体系,实现对测试样品材料的介电特性的测量。For the coaxial transmission line test method in the prior art, it is difficult to remove the parasitic effect generated by the connector in the test fixture during the test process. Specific test materials have higher requirements on the application frequency range. The specific coaxial transmission line fixture has a limited working range and the test frequency range is expanded. difficult question. The invention provides a closed coaxial transmission line test system for characterizing the dielectric properties of liquid and solid materials, specifically a closed coaxial transmission line probe, the correction result of the closed coaxial transmission line test system is accurate, and the test frequency range can be extended for testing system to realize the measurement of the dielectric properties of the test sample material.
为了实现目的,本发明的技术方案为:In order to realize the purpose, technical scheme of the present invention is:
一种表征液体及固体材料介电特性的闭合同轴传输线测试系统,该闭合同轴传输线测试系统包括测试夹具、矢量网络分析仪9、计算机10和测试连接线11;测试夹具包括双向SMA接头、螺钉4、防水橡胶垫圈5、两端开口连通结构的转接头6、具有电磁屏蔽效应的样品室7、样品室内导体8和待测样品。A closed coaxial transmission line test system for characterizing the dielectric properties of liquid and solid materials, the closed coaxial transmission line test system includes a test fixture, a vector network analyzer 9, a computer 10 and a test connection line 11; the test fixture includes a bidirectional SMA connector, Screws 4, waterproof rubber gaskets 5, adapters 6 with openings at both ends connected to each other, sample chambers 7 with electromagnetic shielding effects, conductors 8 in the sample chambers, and samples to be tested.
双向SMA接头一侧通过双向SMA接头双母头同轴内导体3与样品室内导体8插接相连,并通过螺纹与转接头6相接旋紧,并通过螺钉4经由双向SMA接头外导体双头SMA螺纹带四孔法兰1将整个双向SMA接头固定在转接头6上,另一侧通过测试连接线11与矢量网络分析仪9对应端口连接;转接头6的另一端通过内孔螺纹与样品室7接合,内孔螺纹末尾处为环形凹槽,用以安装环形防水橡胶垫圈5。双向SMA接头双母头同轴内导体3的两端母头尺寸参考SMA接头母头内导体尺寸制作,即双向SMA接头双母头同轴内导体3的两端母头尺寸与SMA接头母头内导体相同,均含有对称开缝内陷的圆柱形孔,孔终端为同轴锥形孔。矢量网络分析仪9通过测试连接线11与闭合同轴传输线夹具连接,对待测样品进行测试;计算机10与矢量网络分析仪9连接,进行数据采集与计算分析。所述的双端开口筒形样品室7的两端口处通过螺纹连接转接头6,内部环形腔放置待测样品。One side of the two-way SMA connector is plugged and connected to the conductor 8 in the sample chamber through the double-female coaxial inner conductor 3 of the two-way SMA connector, and is connected with the adapter 6 through the screw thread and tightened, and the outer conductor of the two-way SMA connector is double-ended through the screw 4 SMA threaded four-hole flange 1 fixes the entire two-way SMA connector on the adapter 6, and the other side is connected to the corresponding port of the vector network analyzer 9 through the test connection line 11; the other end of the adapter 6 is connected to the sample chamber 7 through the inner hole thread Engagement, the end of the inner hole thread is an annular groove, which is used to install the annular waterproof rubber gasket 5. Two-way SMA connector double-female coaxial inner conductor 3. The size of the female head at both ends of the coaxial inner conductor 3 refers to the size of the inner conductor of the SMA connector female head. The inner conductors are the same, and both contain cylindrical holes with symmetrical slits and insets, and the hole terminals are coaxial tapered holes. The vector network analyzer 9 is connected to the closed coaxial transmission line fixture through the test connection line 11 to test the sample to be tested; the computer 10 is connected to the vector network analyzer 9 for data collection and calculation analysis. The two ports of the double-ended open cylindrical sample chamber 7 are threadedly connected to the adapter 6, and the inner annular cavity places the sample to be tested.
所述的双向SMA接头由四孔法兰1、柱状筒形聚四氟乙烯2和双向SMA接头双母头同轴内导体3构成;双向SMA接头均为母头,母头两端均为外螺纹。所述的柱状筒形聚四氟乙烯2填充在四孔法兰1与双向SMA接头双母头同轴内导体3之间,柱状筒形聚四氟乙烯2的内直径等于双向SMA接头双母头同轴内导体3的直径,外直径等于双向SMA接头外导体的内直径,长度等于双向SMA接头双母头同轴内导体3的长度。将双向SMA接头双母头同轴内导体3插入已加工好的柱状筒形聚四氟乙烯2,然后将组装好的整体插入双向SMA接头外导体双头SMA螺纹带四孔法兰1,构成双向SMA接头。The bidirectional SMA joint is composed of a four-hole flange 1, a cylindrical cylindrical polytetrafluoroethylene 2 and a bidirectional SMA joint with double female heads and coaxial inner conductors 3; The cylindrical cylindrical polytetrafluoroethylene 2 is filled between the four-hole flange 1 and the coaxial inner conductor 3 of the double female head of the bidirectional SMA joint, and the inner diameter of the cylindrical cylindrical polytetrafluoroethylene 2 is equal to The diameter of the inner conductor 3 in the shaft, the outer diameter is equal to the inner diameter of the outer conductor of the bidirectional SMA joint, and the length is equal to the length of the coaxial inner conductor 3 of the double-female head of the bidirectional SMA joint. Insert the double-female coaxial inner conductor 3 of the bidirectional SMA connector into the processed cylindrical PTFE 2, and then insert the assembled whole into the bidirectional SMA connector outer conductor double-headed SMA threaded four-hole flange 1 to form a bidirectional SMA connector.
所述的样品室内导体8两端为插针,其尺寸与双向SMA接头双母头同轴内导体3两端的母头尺寸相配合,样品室内导体8除去插针的主体长度与样品室7相等,主体部分直径与双向SMA接头双母头同轴内导体3直径相等,样品室内导体8插入双向SMA接头双母头同轴内导体3的同轴锥形孔中;样品室内导体8,双向SMA接头内导体3与环形样品室7处于同一中轴线上,待测样品置于与双向SMA接头相接的两个转接头6之间。所述的样品室为双端开口环形样品室,内部环形腔用以盛放待测样品。The two ends of the conductor 8 in the sample chamber are pins, the size of which matches the size of the female head at both ends of the double-female coaxial inner conductor 3 of the bidirectional SMA connector. The main body length of the conductor 8 in the sample chamber is equal to that of the sample chamber 7 except for the pins. , the diameter of the main body is equal to the diameter of the double-female coaxial inner conductor 3 of the bidirectional SMA connector, and the conductor 8 in the sample chamber is inserted into the coaxial tapered hole of the double-female coaxial inner conductor 3 of the bidirectional SMA connector; the conductor 8 in the sample chamber is bidirectional SMA The inner conductor 3 of the connector is on the same central axis as the annular sample chamber 7, and the sample to be tested is placed between two adapters 6 connected to the bidirectional SMA connector. The sample chamber is an annular sample chamber with double-ended openings, and the inner annular chamber is used to hold samples to be tested.
所述的双向SMA接头、样品室7、转接头6、双向SMA接头双母头同轴内导体3和样品室内导体8均为奥氏体304不锈钢,可以有效减少测试样品对测试系统的腐蚀损坏,同时由于材料为非磁性,也能够有效避免测试系统自身材料对样品介电特性测试带来的影响。双向SMA接头1和样品室7的内表面,SMA接头内导体3和样品室内导体8的表面均要求抛光,以保证测试微波信号传输的稳定。The two-way SMA connector, the sample chamber 7, the adapter 6, the double-female coaxial inner conductor 3 of the two-way SMA connector and the conductor 8 in the sample chamber are all austenitic 304 stainless steel, which can effectively reduce the corrosion damage of the test sample to the test system , and because the material is non-magnetic, it can also effectively avoid the influence of the test system's own material on the dielectric property test of the sample. The inner surfaces of the two-way SMA connector 1 and the sample chamber 7, the surfaces of the inner conductor 3 of the SMA connector and the conductor 8 in the sample chamber are all required to be polished to ensure the stability of the test microwave signal transmission.
所述的待测样品为液体或固体材料,待测样品置于与双向SMA接头相接的两个转接头之间。待测样品在样品室中完全填充,待测样品为内径与样品室内导体直径相等,外径与样品室内直径相等,长度与样品室长度相等的柱形筒状,以便于样品介电特性的准确测量,对于固体粉末或液体样品则直接在安装好一侧转接头的夹具中进行填充。The sample to be tested is a liquid or solid material, and the sample to be tested is placed between two adapters connected with the two-way SMA connector. The sample to be tested is completely filled in the sample chamber, and the sample to be tested is a cylindrical tube with the inner diameter equal to the diameter of the conductor in the sample chamber, the outer diameter equal to the diameter of the sample chamber, and the length equal to the length of the sample chamber, so as to facilitate the accurate measurement of the dielectric properties of the sample. Measurement, for solid powder or liquid samples, it is directly filled in the fixture with one side adapter installed.
采用上述闭合同轴传输线测试系统表征待测样品介电特性的方法,具体包括以下步骤:The method for characterizing the dielectric properties of a sample to be tested by using the above-mentioned closed coaxial transmission line test system specifically includes the following steps:
第一步,准备测试仪器,采集数据The first step is to prepare the test equipment and collect data
将计算机与矢量网络分析仪相连,获取来自测试仪器的数据;将测试连接线与矢量网络分析仪对应端口相接,用标准校准件对矢量网络分析仪进行全双端口校正,校正完毕后保存校正数据到矢量网络分析仪中。Connect the computer to the vector network analyzer to obtain the data from the test instrument; connect the test connection line to the corresponding port of the vector network analyzer, use the standard calibration parts to perform full dual-port calibration on the vector network analyzer, and save the calibration after calibration data into a vector network analyzer.
第二步,测试双向SMA接头的S参数The second step is to test the S parameters of the bidirectional SMA connector
将双向SMA接头与矢量网络分析仪双端口的测试连接线连接,通过对双向SMA接头进行扫频测试获取双向SMA接头的全S参数Sa 11、Sa 21、Sa 12、Sa 22,并将矢量网络分析仪测得的数据保存到计算机,通过实际测试获得双向SMA接头的S参数。Connect the bidirectional SMA connector to the test cable of the dual port of the vector network analyzer, and obtain the full S parameters S a 11 , S a 21 , S a 12 , and S a 22 of the bidirectional SMA connector by performing a frequency sweep test on the bidirectional SMA connector, And save the data measured by the vector network analyzer to the computer, and obtain the S-parameters of the two-way SMA joint through actual testing.
第三步,组装测试夹具,将待测样品放入样品室内The third step is to assemble the test fixture and put the sample to be tested into the sample chamber
从测试夹具的一侧开始组装,将双向SMA接头与转接头一侧相连并旋紧,用螺钉将SMA接头与转接头固定,在转接头另一侧与样品室接合的内孔螺纹末尾环形凹槽内放入防水橡胶垫圈。Assemble from one side of the test fixture, connect the two-way SMA connector to one side of the adapter and tighten it, fix the SMA connector and the adapter with screws, and make a ring-shaped recess at the end of the inner hole thread that connects with the sample chamber on the other side of the adapter Put the waterproof rubber gasket in the slot.
测试夹具的另一侧将样品室内导体与双向SMA接头相连,然后将双向SMA接头旋入转接头对应连接SMA接头的一侧螺纹内,旋紧后用螺钉将SMA接头与转接头固定,保证后期夹具连接测试线时SMA接头不会发生额外转动;转接头与品室相接并旋紧,并放入防水橡胶垫圈。On the other side of the test fixture, connect the conductor in the sample chamber to the two-way SMA connector, then screw the two-way SMA connector into the thread on the side of the adapter corresponding to the SMA connector, and fix the SMA connector and the adapter with screws after tightening to ensure When the fixture is connected to the test line, the SMA connector will not rotate additionally; the adapter is connected to the sample chamber and screwed tightly, and a waterproof rubber gasket is placed.
第四步,测试待测样品The fourth step is to test the sample to be tested
将测试夹具两端与连接矢量网络分析仪两端口的测试连接线相连并旋紧,对待测样品进行扫频测试,并将测得的测试夹具的双端口全参数Sm 11、Sm 21、Sm 12、Sm 22导入计算机保存。Connect the two ends of the test fixture to the test connection wires connected to the two ports of the vector network analyzer and tighten them, perform a frequency sweep test on the sample to be tested, and measure the two-port full parameters of the test fixture S m 11 , S m 21 , S m 12 and S m 22 are imported into the computer and saved.
第五步,去除测试寄生效应,计算介电特性参数The fifth step is to remove the test parasitic effect and calculate the dielectric characteristic parameters
通过将第二步测得的全S参数Sa 11、Sa 21、Sa 12、Sa 22以及第四步测得的全S参数Sm 11、Sm 21、Sm 12、Sm 22进行传输散射参数变换得到相应的T参数Ta 11、Ta 12、Ta 21、Ta 22和对应的Tm 11、Tm 21、Tm 12、Tm 22;通过链式传输矩阵计算去除双向SMA接头带来的测试寄生效应,得到纯粹待测样品的T参数Td 11、Td 21、Td 12、Td 22,进而通过矩阵变换得到测试样品对应的全S参数Sd 11、Sd 21、Sd 12、Sd 22;利用得到的待测样品全S参数通过传输反射法反演即可得到样品的的介电特性,所述的介电特性包括复介电常数、复磁导率、样品损耗正切或品质因数。By combining the full S parameters S a 11 , S a 21 , S a 12 , S a 22 measured in the second step and the full S parameters S m 11 , S m 21 , S m 12 , S m measured in the fourth step 22 Transform transmission and scattering parameters to obtain corresponding T parameters T a 11 , T a 12 , T a 21 , T a 22 and corresponding T m 11 , T m 21 , T m 12 , T m 22 ; Calculate and remove the test parasitic effect caused by the bidirectional SMA connector, and obtain the T parameters T d 11 , T d 21 , T d 12 , T d 22 of the pure sample to be tested, and then obtain the corresponding full S parameter S d of the test sample through matrix transformation 11 , S d 21 , S d 12 , S d 22 ; the dielectric properties of the sample can be obtained by using the obtained full S parameters of the sample to be measured through transmission reflection method inversion, and the dielectric properties include complex permittivity , complex permeability, sample loss tangent or quality factor.
基于传输反射法与去嵌入技术的有机结合,在不依赖专属定制校准件或对夹具进行复杂数学建模的情况下去除夹具接口的测试寄生效应,实现对液体与固体材料介电特性的精确测量。Based on the organic combination of transmission reflection method and de-embedding technology, the test parasitic effect of the fixture interface can be removed without relying on exclusive custom calibration parts or complex mathematical modeling of the fixture, and the accurate measurement of the dielectric properties of liquid and solid materials can be realized .
本发明的有益效果:Beneficial effects of the present invention:
1)由于夹具接头部分被设计为与矢量网络分析仪测试用接线接头尺寸、螺纹和内导体相对应的双向接头,可以通过直接测试获得接头的散射参数,通过对应测试结果的矩阵变换与运算即可去除同轴传输线法夹具中接头测试寄生效应,对于传输反射法测试样品介电特性的过程中接头寄生效应的去除不需要依据夹具的尺寸定制特定的校准件,应对不同的接头类型,不依赖建立复杂的数学模型来去除接头的附加测试影响,去除方法可行性好,去除结果准确可靠。1) Since the joint part of the fixture is designed as a two-way joint corresponding to the size, thread and inner conductor of the wiring joint used in the test of the vector network analyzer, the scattering parameters of the joint can be obtained through direct testing, and the matrix transformation and operation corresponding to the test results are It can remove the parasitic effect of the joint test in the fixture of the coaxial transmission line method. For the removal of the joint parasitic effect in the process of testing the dielectric properties of the sample by the transmission reflection method, it is not necessary to customize specific calibration parts according to the size of the fixture, and it can handle different joint types without relying on A complex mathematical model is established to remove the additional test effects of joints, the removal method is feasible, and the removal results are accurate and reliable.
2)测试材料可以为液体、固体或固体粉末;可供测试的种类丰富,适用范围广,对测试样品处理要求低。2) The test material can be liquid, solid or solid powder; there are many types of test available, wide application range, and low requirements for test sample processing.
3)测试频率范围的扩展可通过夹具双向接头类型与对应样品室同轴内导体的方式实现。SMA接头连接的测试夹具可实现1MHz-18GHz范围的测试,将双向接头类型从SMA换为SSMA可将测试频率上限扩展到38GHz,换为GPO,OSMP,SMP的一种可将测试频率范围扩展到40GHz。测试工作频率范围扩展灵活,适用范围广的特点。3) The expansion of the test frequency range can be realized by means of the bidirectional connector type of the fixture and the coaxial inner conductor of the corresponding sample chamber. The test fixture connected by SMA connector can realize the test in the range of 1MHz-18GHz. Changing the type of bidirectional connector from SMA to SSMA can extend the upper limit of the test frequency to 38GHz, and changing it to one of GPO, OSMP, and SMP can extend the test frequency range to 40GHz. It has the characteristics of flexible expansion of the test working frequency range and wide application range.
4)整体测试操作流程短,夹具安装简洁,操作简单,测试可重复性好。4) The overall test operation process is short, the fixture installation is simple, the operation is simple, and the test repeatability is good.
附图说明Description of drawings
图1是测试夹具得横截面结构示意图;Fig. 1 is a cross-sectional structural schematic diagram of a test fixture;
图2是本发明的测试装置体系示意图;Fig. 2 is a schematic diagram of the testing device system of the present invention;
图3是双向SMA接头结构剖视图;Fig. 3 is a structural cross-sectional view of a bidirectional SMA connector;
图4是双向SMA接头结构左视图;Figure 4 is a left view of the bidirectional SMA joint structure;
图5是转接头结构剖视图;Fig. 5 is a cross-sectional view of the adapter structure;
图6是转接头结构左视图;Figure 6 is a left view of the adapter structure;
图7是转接头结构右视图;Figure 7 is a right view of the adapter structure;
图8是样品室同轴内导体结构示意图;Fig. 8 is a schematic diagram of the structure of the coaxial inner conductor in the sample chamber;
图9是样品室结构示意图;Fig. 9 is a schematic diagram of the structure of the sample chamber;
图中:1四孔法兰;2柱状筒形聚四氟乙烯;3双向SMA接头双母头同轴内导体;4螺钉;5防水橡胶垫圈;6转接头;7样品室;8样品室内导体;9矢量网络分析仪;10计算机;11测试连接线。In the figure: 1 four-hole flange; 2 cylindrical cylindrical PTFE; 3 two-way SMA connector double female coaxial inner conductor; 4 screws; 5 waterproof rubber gasket; 6 adapter; 7 sample room; 8 sample indoor conductor; 9 Vector network analyzer; 10 computer; 11 test connection line.
具体实施方式detailed description
为实现以上效果,下面结合附图与实施例对发明作进一步描述:In order to achieve the above effects, the invention will be further described below in conjunction with the accompanying drawings and embodiments:
一种表征液体及固体材料介电特性的闭合同轴传输线测试系统,如图2所示,包括测试夹具、矢量网络分析仪9、计算机10和测试连接线11;测试夹具的横截面结构示意图如图1所示,测试夹具包括双向SMA接头(图3,4)、螺钉4、防水橡胶垫圈5、两端开口连通结构的转接头6(如图5,6,7)、具有电磁屏蔽效应的样品室7(如图9)、样品室内导体8(如图8)和待测样品。A closed coaxial transmission line test system for characterizing the dielectric properties of liquid and solid materials, as shown in Figure 2, includes a test fixture, a vector network analyzer 9, a computer 10 and a test connection line 11; the cross-sectional structural schematic diagram of the test fixture is as follows As shown in Figure 1, the test fixture includes a two-way SMA connector (Figure 3, 4), a screw 4, a waterproof rubber gasket 5, an adapter 6 with an open connection structure at both ends (Figure 5, 6, 7), an electromagnetic shielding effect The sample chamber 7 (as shown in FIG. 9 ), the conductor 8 in the sample chamber (as shown in FIG. 8 ) and the sample to be tested.
所述的双向SMA接头由四孔法兰1、柱状筒形聚四氟乙烯2和双向SMA接头双母头同轴内导体3构成;双向SMA接头均为母头,母头两端均为外螺纹。将双向SMA接头双母头同轴内导体3插入已加工好的柱状筒形聚四氟乙烯2,然后将组装好的整体插入双向SMA接头外导体双头SMA螺纹带四孔法兰1,构成双向SMA接头;The bidirectional SMA joint is composed of a four-hole flange 1, a cylindrical cylindrical polytetrafluoroethylene 2 and a bidirectional SMA joint with double female heads and coaxial inner conductors 3; Insert the double-female coaxial inner conductor 3 of the bidirectional SMA connector into the processed cylindrical PTFE 2, and then insert the assembled whole into the bidirectional SMA connector outer conductor double-headed SMA threaded four-hole flange 1 to form a bidirectional SMA connector;
双向SMA接头一侧通过双向SMA接头双母头同轴内导体与样品室内导体8插接相连,并通过螺纹与转接头6相接旋紧,并通过螺钉4经由双向SMA接头外导体双头SMA螺纹带四孔法兰1将整个双向SMA接头固定在转接头6上,另一侧通过测试连接线11与矢量网络分析仪9对应端口连接;转接头6的另一端通过内孔螺纹与样品室7接合,内孔螺纹末尾处为环形凹槽,用以安装环形防水橡胶垫圈5。双向SMA接头双母头同轴内导体3的两端母头尺寸参考SMA接头母头内导体尺寸制作,均含有对称开缝内陷的圆柱形孔,孔终端为同轴锥形孔。矢量网络分析仪9通过测试连接线11与闭合同轴传输线夹具连接,对待测样品进行测试;计算机10与矢量网络分析仪9连接,进行数据采集与计算分析。One side of the two-way SMA connector is plugged and connected to the conductor 8 in the sample chamber through the double-female coaxial inner conductor of the two-way SMA connector, and is connected with the adapter 6 through the thread and screwed tightly, and the outer conductor of the two-way SMA connector is double-ended SMA through the screw 4 The threaded four-hole flange 1 fixes the entire two-way SMA joint on the adapter 6, and the other side is connected to the corresponding port of the vector network analyzer 9 through the test connection line 11; the other end of the adapter 6 is connected to the sample chamber 7 through the internal thread , the end of the inner hole thread is an annular groove for installing the annular waterproof rubber gasket 5. The two-way SMA connector double-female coaxial inner conductor 3 is manufactured with reference to the size of the female inner conductor of the SMA connector. Both contain cylindrical holes with symmetrical slits and indented holes, and the hole terminals are coaxial tapered holes. The vector network analyzer 9 is connected to the closed coaxial transmission line fixture through the test connection line 11 to test the sample to be tested; the computer 10 is connected to the vector network analyzer 9 for data collection and calculation analysis.
采用上述闭合同轴传输线测试系统表征待测样品介电特性的方法,具体包括以下步骤:The method for characterizing the dielectric properties of a sample to be tested by using the above-mentioned closed coaxial transmission line test system specifically includes the following steps:
第一步,准备测试仪器,采集数据The first step is to prepare the test equipment and collect data
将计算机10与矢量网络分析仪9相连,获取来自测试仪器的数据;将测试连接线11与矢量网络分析仪9对应端口相接,用标准校准件对矢量网络分析仪9进行全双端口校正,校正完毕后保存校正数据到矢量网络分析仪9中。The computer 10 is connected with the vector network analyzer 9 to obtain data from the test instrument; the test connection line 11 is connected with the corresponding port of the vector network analyzer 9, and the full two-port correction is carried out to the vector network analyzer 9 with a standard calibration part. Save the calibration data to the vector network analyzer 9 after the calibration is completed.
第二步,测试双向SMA接头的S参数The second step is to test the S parameters of the bidirectional SMA connector
将双向SMA接头与矢量网络分析仪9双端口的测试线11连接,通过对双向SMA接头的扫频测试获取双向SMA接头的全S参数Sa 11、Sa 21、Sa 12、Sa 22,并将矢量网络分析仪9测得的数据保存到计算机10,通过实际测试获得双向SMA接头的S参数。Connect the bidirectional SMA connector to the dual-port test line 11 of the vector network analyzer 9, and obtain the full S parameters S a 11 , S a 21 , S a 12 , and S a 22 of the bidirectional SMA connector through a frequency sweep test on the bidirectional SMA connector , and save the data measured by the vector network analyzer 9 to the computer 10, and obtain the S parameters of the bidirectional SMA joint through actual testing.
第三步,组装测试夹具The third step is to assemble the test fixture
从测试夹具的一侧开始组装,将双向SMA接头与转接头6一侧相连并旋紧,用螺钉4将SMA接头与转接头6固定,在转接头6另一侧与样品室7接合的内孔螺纹末尾环形凹槽内放入防水橡胶垫圈5。Assemble from one side of the test fixture, connect the two-way SMA connector to one side of the adapter 6 and tighten it, use the screw 4 to fix the SMA connector and the adapter 6, and connect the other side of the adapter 6 to the sample chamber 7 Put waterproof rubber washer 5 in the annular groove at the end of the hole thread.
测试夹具的另一侧将样品室内导体8与双向SMA接头相连,然后将双向SMA接头旋入转接头6对应连接SMA接头的一侧螺纹内,旋紧后用螺钉4将SMA接头与转接头6固定,保证后期夹具连接测试线时SMA接头不会发生额外转动;转接头6与品室7相接并旋紧,并放入防水橡胶垫圈5。On the other side of the test fixture, connect the conductor 8 in the sample chamber to the two-way SMA connector, then screw the two-way SMA connector into the thread on the side of the adapter 6 corresponding to the SMA connector, and use the screw 4 to connect the SMA connector to the adapter 6 after tightening. Fix it to ensure that the SMA connector will not rotate additionally when the fixture is connected to the test line in the later stage; the adapter 6 is connected to the product chamber 7 and tightened, and the waterproof rubber gasket 5 is placed.
将待测样品放入样品室7内,将已组装好的转接头6与样品室7相接并旋紧。Put the sample to be tested into the sample chamber 7, connect the assembled adapter 6 with the sample chamber 7 and tighten it.
第四步,测试待测样品The fourth step is to test the sample to be tested
将测试夹具两端与连接矢量网络分析仪9两端口的测试线11相连并旋紧,对待测样品进行扫频测试,并将测得的夹具双端口全参数Sm 11、Sm 21、Sm 12、Sm 22导入计算机10保存。Connect the two ends of the test fixture with the test line 11 connected to the two ports of the vector network analyzer 9 and tighten them, perform a frequency sweep test on the sample to be tested, and take the measured double-port full parameters of the fixture S m 11 , S m 21 , S m 12 and S m 22 are imported into the computer 10 and saved.
第五步,去除测试寄生效应与计算介电特性参数The fifth step is to remove the test parasitic effect and calculate the dielectric characteristic parameters
通过将第二步测得的全S参数Sa 11、Sa 21、Sa 12、Sa 22以及第四步测得的全S参数Sm 11、Sm 21、Sm 12、Sm 22进行传输散射参数变换得到相应的T参数Ta 11、Ta 12、Ta 21、Ta 22和对应的Tm 11、Tm 21、Tm 12、Tm 22;通过链式传输矩阵计算去除双向SMA接头带来的测试寄生效应,得到纯粹测试样品的T参数Td 11、Td 21、Td 12、Td 22,进而通过矩阵变换得到测试样品对应的全S参数Sd 11、Sd 21、Sd 12、Sd 22;利用得到的测试样品S参数通过传输反射法反演即可得到样品的复介电常数、复磁导率、样品损耗正切或品质因数。By combining the full S parameters S a 11 , S a 21 , S a 12 , S a 22 measured in the second step and the full S parameters S m 11 , S m 21 , S m 12 , S m measured in the fourth step 22 Transform transmission and scattering parameters to obtain corresponding T parameters T a 11 , T a 12 , T a 21 , T a 22 and corresponding T m 11 , T m 21 , T m 12 , T m 22 ; Calculate and remove the test parasitic effect brought by the two-way SMA connector, obtain the T parameters T d 11 , T d 21 , T d 12 , T d 22 of the pure test sample, and then obtain the corresponding full S parameter S d 11 of the test sample through matrix transformation , S d 21 , S d 12 , S d 22 ; the complex permittivity, complex permeability, sample loss tangent or quality factor of the sample can be obtained by inversion of the obtained S parameters of the test sample by the transmission reflection method.
对于对材料工作范围在射频到低于18GHz频段的测试,使用SMA接头即可满足测试的要求。对要求测试材料在更高频段(K频段、Ka频段、Q频段)的介电特性测试与表征则可以通过更换对应工作频段的接头种类(双向SSMA接头,双向GPO、OSMP或SMP接头)与对应的转接头以及相应的样品室同轴内导体来实现。以双向SSMA接头为例,当测试频率上限为38GHz时,可更换双向SSMA接头机及其对应的转接头和样品室同轴内导体,按实施例中的连接方式进行连接测试,可以实现测试系统可供测试频率范围的扩展。For the test of the material working range from radio frequency to below 18GHz frequency band, the use of SMA connectors can meet the test requirements. For testing and characterization of the dielectric properties of the required test materials in higher frequency bands (K-band, Ka-band, Q-band), you can change the type of connectors corresponding to the working frequency band (two-way SSMA connectors, two-way GPO, OSMP or SMP connectors) and corresponding The adapter and the corresponding coaxial inner conductor of the sample chamber are realized. Taking the two-way SSMA joint as an example, when the upper limit of the test frequency is 38GHz, the two-way SSMA joint machine and its corresponding adapter and the coaxial inner conductor of the sample chamber can be replaced, and the connection test can be carried out according to the connection method in the embodiment, and the test system can be realized An extension of the test frequency range is available.
本发明在设计上对于接头在测试中不可避免的测试耦合效应的去除更加方便,将夹具中不可去除的测试部分很好的耦合进夹具中的同时可以实现对于接头S参数的独立测试,通过使用已有的较准件校准后的仪器进行测试可以保证测试结果的准确性,同时设计上的密封性与夹具样品尺寸的要求保证了对于液体样品介电特性的表征。The design of the present invention is more convenient for removing the unavoidable test coupling effect of the joint in the test, and can realize the independent test of the S parameter of the joint while coupling the non-removable test part in the fixture into the fixture. Testing the instrument after calibration with the existing calibrator can ensure the accuracy of the test results. At the same time, the tightness of the design and the requirements of the sample size of the fixture ensure the characterization of the dielectric properties of the liquid sample.
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CN115494308B (en) * | 2022-09-20 | 2024-11-08 | 闽都创新实验室 | Material electromagnetic parameter measuring device and measuring method |
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