CN105928367A - Dry distillation device with furnace lid automatic lifting system and dry distillation method for dry distillation device - Google Patents
Dry distillation device with furnace lid automatic lifting system and dry distillation method for dry distillation device Download PDFInfo
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- CN105928367A CN105928367A CN201610410726.1A CN201610410726A CN105928367A CN 105928367 A CN105928367 A CN 105928367A CN 201610410726 A CN201610410726 A CN 201610410726A CN 105928367 A CN105928367 A CN 105928367A
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- heat
- insulation
- burner hearth
- dry distillation
- heater
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- 238000000197 pyrolysis Methods 0.000 title claims abstract description 45
- 238000000034 method Methods 0.000 title claims abstract description 22
- 239000000463 material Substances 0.000 claims abstract description 113
- 238000009413 insulation Methods 0.000 claims abstract description 96
- 238000010438 heat treatment Methods 0.000 claims abstract description 31
- 238000012544 monitoring process Methods 0.000 claims abstract description 13
- 239000011261 inert gas Substances 0.000 claims abstract description 7
- 238000004321 preservation Methods 0.000 claims description 48
- 239000007789 gas Substances 0.000 claims description 43
- IJGRMHOSHXDMSA-UHFFFAOYSA-N Atomic nitrogen Chemical compound N#N IJGRMHOSHXDMSA-UHFFFAOYSA-N 0.000 claims description 38
- 229910052757 nitrogen Inorganic materials 0.000 claims description 16
- 238000010079 rubber tapping Methods 0.000 claims description 13
- 238000012806 monitoring device Methods 0.000 claims description 7
- 230000005855 radiation Effects 0.000 claims description 6
- 206010020843 Hyperthermia Diseases 0.000 claims description 4
- 239000012298 atmosphere Substances 0.000 claims description 4
- 239000002361 compost Substances 0.000 claims description 4
- 230000000694 effects Effects 0.000 claims description 4
- 230000036031 hyperthermia Effects 0.000 claims description 4
- 238000002955 isolation Methods 0.000 claims description 4
- 230000005619 thermoelectricity Effects 0.000 claims description 4
- 229910006295 Si—Mo Inorganic materials 0.000 claims description 3
- 229910052756 noble gas Inorganic materials 0.000 claims description 3
- 230000005611 electricity Effects 0.000 claims description 2
- 238000000926 separation method Methods 0.000 claims description 2
- QVGXLLKOCUKJST-UHFFFAOYSA-N atomic oxygen Chemical compound [O] QVGXLLKOCUKJST-UHFFFAOYSA-N 0.000 description 7
- 229910052760 oxygen Inorganic materials 0.000 description 7
- 239000001301 oxygen Substances 0.000 description 7
- 210000000038 chest Anatomy 0.000 description 6
- 229910001873 dinitrogen Inorganic materials 0.000 description 6
- 238000003763 carbonization Methods 0.000 description 3
- 238000004140 cleaning Methods 0.000 description 3
- 239000003245 coal Substances 0.000 description 3
- 238000002485 combustion reaction Methods 0.000 description 3
- 238000001816 cooling Methods 0.000 description 3
- 230000008021 deposition Effects 0.000 description 3
- 238000005516 engineering process Methods 0.000 description 3
- 238000004088 simulation Methods 0.000 description 3
- 238000012360 testing method Methods 0.000 description 3
- 230000007812 deficiency Effects 0.000 description 2
- 238000004821 distillation Methods 0.000 description 2
- 235000003642 hunger Nutrition 0.000 description 2
- 210000003141 lower extremity Anatomy 0.000 description 2
- 230000037351 starvation Effects 0.000 description 2
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 description 2
- HMDDXIMCDZRSNE-UHFFFAOYSA-N [C].[Si] Chemical compound [C].[Si] HMDDXIMCDZRSNE-UHFFFAOYSA-N 0.000 description 1
- 230000009286 beneficial effect Effects 0.000 description 1
- 238000006243 chemical reaction Methods 0.000 description 1
- 239000000571 coke Substances 0.000 description 1
- 238000004891 communication Methods 0.000 description 1
- 230000008878 coupling Effects 0.000 description 1
- 238000010168 coupling process Methods 0.000 description 1
- 238000005859 coupling reaction Methods 0.000 description 1
- 238000013461 design Methods 0.000 description 1
- 238000007599 discharging Methods 0.000 description 1
- 208000037265 diseases, disorders, signs and symptoms Diseases 0.000 description 1
- 208000035475 disorder Diseases 0.000 description 1
- 238000002474 experimental method Methods 0.000 description 1
- 238000010304 firing Methods 0.000 description 1
- 239000012299 nitrogen atmosphere Substances 0.000 description 1
- 239000002994 raw material Substances 0.000 description 1
- 238000007789 sealing Methods 0.000 description 1
- 239000000126 substance Substances 0.000 description 1
- 238000006467 substitution reaction Methods 0.000 description 1
- 238000007669 thermal treatment Methods 0.000 description 1
- 239000005439 thermosphere Substances 0.000 description 1
Classifications
-
- F—MECHANICAL ENGINEERING; LIGHTING; HEATING; WEAPONS; BLASTING
- F27—FURNACES; KILNS; OVENS; RETORTS
- F27B—FURNACES, KILNS, OVENS, OR RETORTS IN GENERAL; OPEN SINTERING OR LIKE APPARATUS
- F27B17/00—Furnaces of a kind not covered by any preceding group
- F27B17/02—Furnaces of a kind not covered by any preceding group specially designed for laboratory use
-
- F—MECHANICAL ENGINEERING; LIGHTING; HEATING; WEAPONS; BLASTING
- F27—FURNACES; KILNS; OVENS; RETORTS
- F27D—DETAILS OR ACCESSORIES OF FURNACES, KILNS, OVENS, OR RETORTS, IN SO FAR AS THEY ARE OF KINDS OCCURRING IN MORE THAN ONE KIND OF FURNACE
- F27D1/00—Casings; Linings; Walls; Roofs
-
- F—MECHANICAL ENGINEERING; LIGHTING; HEATING; WEAPONS; BLASTING
- F27—FURNACES; KILNS; OVENS; RETORTS
- F27D—DETAILS OR ACCESSORIES OF FURNACES, KILNS, OVENS, OR RETORTS, IN SO FAR AS THEY ARE OF KINDS OCCURRING IN MORE THAN ONE KIND OF FURNACE
- F27D1/00—Casings; Linings; Walls; Roofs
- F27D1/18—Door frames; Doors, lids, removable covers
- F27D1/1808—Removable covers
-
- F—MECHANICAL ENGINEERING; LIGHTING; HEATING; WEAPONS; BLASTING
- F27—FURNACES; KILNS; OVENS; RETORTS
- F27D—DETAILS OR ACCESSORIES OF FURNACES, KILNS, OVENS, OR RETORTS, IN SO FAR AS THEY ARE OF KINDS OCCURRING IN MORE THAN ONE KIND OF FURNACE
- F27D11/00—Arrangement of elements for electric heating in or on furnaces
- F27D11/02—Ohmic resistance heating
-
- F—MECHANICAL ENGINEERING; LIGHTING; HEATING; WEAPONS; BLASTING
- F27—FURNACES; KILNS; OVENS; RETORTS
- F27D—DETAILS OR ACCESSORIES OF FURNACES, KILNS, OVENS, OR RETORTS, IN SO FAR AS THEY ARE OF KINDS OCCURRING IN MORE THAN ONE KIND OF FURNACE
- F27D19/00—Arrangements of controlling devices
-
- F—MECHANICAL ENGINEERING; LIGHTING; HEATING; WEAPONS; BLASTING
- F27—FURNACES; KILNS; OVENS; RETORTS
- F27D—DETAILS OR ACCESSORIES OF FURNACES, KILNS, OVENS, OR RETORTS, IN SO FAR AS THEY ARE OF KINDS OCCURRING IN MORE THAN ONE KIND OF FURNACE
- F27D21/00—Arrangements of monitoring devices; Arrangements of safety devices
- F27D21/0014—Devices for monitoring temperature
-
- F—MECHANICAL ENGINEERING; LIGHTING; HEATING; WEAPONS; BLASTING
- F27—FURNACES; KILNS; OVENS; RETORTS
- F27D—DETAILS OR ACCESSORIES OF FURNACES, KILNS, OVENS, OR RETORTS, IN SO FAR AS THEY ARE OF KINDS OCCURRING IN MORE THAN ONE KIND OF FURNACE
- F27D3/00—Charging; Discharging; Manipulation of charge
- F27D3/0084—Charging; Manipulation of SC or SC wafers
-
- F—MECHANICAL ENGINEERING; LIGHTING; HEATING; WEAPONS; BLASTING
- F27—FURNACES; KILNS; OVENS; RETORTS
- F27D—DETAILS OR ACCESSORIES OF FURNACES, KILNS, OVENS, OR RETORTS, IN SO FAR AS THEY ARE OF KINDS OCCURRING IN MORE THAN ONE KIND OF FURNACE
- F27D1/00—Casings; Linings; Walls; Roofs
- F27D1/18—Door frames; Doors, lids, removable covers
- F27D1/1808—Removable covers
- F27D2001/1825—Means for moving the cover
-
- F—MECHANICAL ENGINEERING; LIGHTING; HEATING; WEAPONS; BLASTING
- F27—FURNACES; KILNS; OVENS; RETORTS
- F27D—DETAILS OR ACCESSORIES OF FURNACES, KILNS, OVENS, OR RETORTS, IN SO FAR AS THEY ARE OF KINDS OCCURRING IN MORE THAN ONE KIND OF FURNACE
- F27D19/00—Arrangements of controlling devices
- F27D2019/0003—Monitoring the temperature or a characteristic of the charge and using it as a controlling value
-
- F—MECHANICAL ENGINEERING; LIGHTING; HEATING; WEAPONS; BLASTING
- F27—FURNACES; KILNS; OVENS; RETORTS
- F27M—INDEXING SCHEME RELATING TO ASPECTS OF THE CHARGES OR FURNACES, KILNS, OVENS OR RETORTS
- F27M2003/00—Type of treatment of the charge
- F27M2003/14—Pyrolising
Landscapes
- Engineering & Computer Science (AREA)
- Mechanical Engineering (AREA)
- General Engineering & Computer Science (AREA)
- Health & Medical Sciences (AREA)
- Clinical Laboratory Science (AREA)
- Waste-Gas Treatment And Other Accessory Devices For Furnaces (AREA)
- Processing Of Solid Wastes (AREA)
Abstract
The invention discloses a dry distillation device with a furnace lid automatic lifting system. The dry distillation device comprises a first furnace body, a second furnace body and a heat insulating device, wherein the first furnace body comprises the furnace lid lifting system. The invention further discloses a dry distillation method which comprises the following steps: putting dry distillation materials into a loading material, and separately mounting thermocouples for measuring a material temperature on corresponding contact points of a feed bin; replacing air in the whole box body with inert gas; closing the heat insulating plate; after completing a temperature raising program of a heat-insulating thermal-insulation furnace chamber, feeding the dry distillation materials into a heating area of the loading system to carry out dry distillation; in a dry distillation process, monitoring temperatures of the dry distillation materials at different material-layer heights at any time; after dry distillation, transferring the dry distillation materials into a second furnace chamber, and closing the heat insulating device; and after the temperature of the dry distillation materials is reduced to a needed value, getting out the dry distillation materials to analyze. According to the dry distillation device and the dry distillation method, by virtue of the independently designed furnace lid lifting system, deposits in a furnace are conveniently cleared, and a heating rod is conveniently replaced; and precise temperature control on materials can be realized, so that influences, on dry distillation results, of a temperature, time and the like can be inspected.
Description
Technical field
The invention belongs to chemical technology field, particularly relate to the dry of a kind of band bell automatic lifting system
Distillation unit and method for destructive distillation thereof.
Background technology
Retorting technique is that material is heated under isolation air conditions, decomposed, generation coke (or semicoke),
The process of the product such as tar, carbonization gas, has been widely used at the conventional utilization of resources and exploitation, rubbish
Reason and the exploitation of bioenergy.Wherein, dry distilling condition (pyrolysis temperature, retorting time, heating side
Formula, thickness of feed layer etc.) relatively big on the impact of dry distilling product and retort process, need substantial amounts of basis real
Test and investigate checking, think that the industrialization of dry distillation of coal technology provides sufficient data support.
But, the destructive distillation device that current laboratory uses mostly is tubular type gas retort and box dry furnace.Pipe
The mode of heating of formula gas retort is surrounding heating, and the inventory that can investigate is less, with current industrialization
The difference of device is bigger, it is impossible to investigate mode of heating and the impact of thickness of feed layer；And box dry furnace is many
Add airtight destructive distillation device in the cold state for intermittent operation, i.e. material to heat up with stove, after reaction terminates,
Because coal at high temperature contacts oxygen easy firing, can only continue to be placed on furnace cooling in airtight gas retort
Rear discharging.Because during heating up and lowering the temperature, coal all can occur dry distilling, therefore cannot investigate temperature
Degree and the time impact on dry distilling result.The more important thing is, current box dry furnace the most only sets
Furnace temperature, examination is the furnace temperature impact on material dry distilling, if but the space, dry distillation area of batch-type furnace is relatively big,
Then furnace temperature is relatively big with the gap of material temperature, and existing dry distilling experimental provision cannot monitor furnace temperature and difference at any time
Material temperature layer temperature.
There is many deficiencies in the destructive distillation device used due to current laboratory, the most how to improve laboratory
The destructive distillation device used, enable to realize material under setting furnace temperature input and output material, avoid semicoke contour
Contact oxygen combustion under temperature, and furnace temperature and different material temperature layer temperature etc., Cheng Weiren can be monitored at any time
Problem demanding prompt solution.
Summary of the invention
In order to solve the deficiencies in the prior art, it is possible to examination dry distilling condition in detail is to material dry distilling state
Impact, simulates the dry distilling condition of industrialized unit as far as possible, needs to be designed to meet the dry of requirement
Distillation unit.The present invention proposes destructive distillation device and the method for destructive distillation thereof of a kind of band bell automatic lifting system,
With the deposition in easy cleaning stove and be conveniently replaceable heating rod, and can simulate heat accumulating type rotating bed work
Industry device dry distilling condition, can investigate the impact on dry distilling result of the dry distilling conditions such as temperature and time.
The present invention proposes the destructive distillation device of a kind of band bell automatic lifting system, including the first body of heater,
Two bodies of heater, heat ray filter；
Described first body of heater includes body of heater shell, heat-insulation and heat-preservation burner hearth, charging system, furnace cover lifting system
System, heater, material temperature monitoring device, the first gas inlet-outlet；
Described furnace cover lifting system includes bell, bell support bar and furnace cover lifting machine；
The top of described bell support bar is connected with described bell, the bottom of described bell support bar and institute
State furnace cover lifting machine to connect；
Described second body of heater includes body of heater shell, the second burner hearth, fire door, the second gas inlet-outlet, shifting
Dynamic device；
Described first body of heater is disposed adjacent with described second body of heater, described first body of heater heat-insulation and heat-preservation burner hearth
Side arranges opening, and described heat-insulation and heat-preservation burner hearth is connected with described second burner hearth by described opening；
Described charging system is connected with described mobile device, and described mobile device drives described charging system
Move between the described heat-insulation and heat-preservation burner hearth and the burner hearth of described second body of heater of the first body of heater；
Described material temperature monitoring device is for measuring during dry distilling the temperature of diverse location material in described feed bin；
Described heat ray filter is arranged between the first body of heater and the second body of heater, and described heat ray filter is used for hindering
Only the hyperthermia radiation in described heat-insulation and heat-preservation burner hearth is to described second body of heater.
Further, described charging system includes feed bin, silo support, insulation feed bin supporting plate；
Described feed bin is used for putting dry distilling material；
Described silo support is arranged on described insulation feed bin supporting plate, and described silo support supports institute
State feed bin；
Described insulation feed bin supporting plate is plate object；
Described insulation feed bin supporting plate is arranged and than heat insulation guarantor with described heat-insulation and heat-preservation burner hearth opening parallel
The opening width of temperature burner hearth；When described charging system moves into described heat-insulation and heat-preservation burner hearth, described thermal insulation separation
Hot aggregate bin supporting plate is stuck in outside the aperture position of described heat-insulation and heat-preservation burner hearth.
Further, described first body of heater is positioned at the surface of described second body of heater, described mobile device
It it is turbine screw elevator.
Further, described heater includes that heating rod, thermocouple binding post, hearth thermocouple enter
Mouth, external temperature control system；
Described heating rod uses siliconit or Si-Mo rod；
Described heating rod is arranged on described heat-insulation and heat-preservation burner hearth furnace roof, is perpendicular to the arrangement of described furnace roof；
Described thermocouple binding post is arranged on the furnace roof of described first body of heater；
It is electrically connected with between described external temperature control system and described thermocouple binding post；
Described heating rod is electrically connected with described external temperature control system.
Further, described material temperature monitoring device includes that material temperature monitors binding post, surveys on material temperature thermocouple
Contact point, surveys contact point in material temperature thermocouple, surveys contact point under material temperature thermocouple, surveys material temperature binding post
External tapping, external temperature control system；
On described survey material temperature thermocouple, contact point is arranged on described feed bin top, described survey material temperature thermoelectricity
In idol, contact point is arranged on the middle part of described feed bin, and under described survey material temperature thermocouple, contact point is arranged on institute
State the bottom of feed bin；
Described material temperature monitoring binding post is arranged on described insulation feed bin supporting plate；
Contact point on described survey material temperature thermocouple, survey contact point in material temperature thermocouple, survey material temperature thermocouple
Lower contact point is electrically connected with described material temperature monitoring binding post；
Described material temperature monitoring binding post is electrically connected with described survey material temperature binding post external tapping；
Described survey material temperature binding post external tapping is electrical connected with described external temperature control system；
Described survey material temperature binding post external tapping is sealed interface.
Further, described heat ray filter is intermediate thermal insulating layer；
Described intermediate thermal insulating layer includes heat insulation fireguard, fireguard pusher, screw mandrel slideway；
Described heat insulation fireguard is placed on described screw mandrel slideway, in the traction of described fireguard pusher
Lower movement；
Described heat insulation fireguard, the mainly heat of isolation heat-insulation and heat-preservation burner hearth pass to the second burner hearth；Institute
The effect stating fireguard pusher is the mobile offer power for described heat insulation fireguard；Described screw mandrel is sliding
Road provides moving track for described heat insulation fireguard.
Further, described first gas inlet-outlet include at least one first gas access, at least one
Individual first gas outlet, at least one dry distilling oil gas vent；Described dry distilling oil gas vent connects oil gas and divides
From system；
Described second gas inlet-outlet includes at least one second gas access, at least one second gas
Outlet.
The present invention also proposes a kind of destructive distillation device applying described band bell automatic lifting system and does
The method evaporated, comprises the following steps:
Described charging system is placed in described second burner hearth；
Described dry distilling material is inserted described charging system；Described survey material temperature thermocouple is filled respectively simultaneously
On the corresponding contact point of described feed bin；
By the air inert gas replacement in described heat-insulation and heat-preservation burner hearth and described second burner hearth；
Close described heat ray filter, start described heat-insulation and heat-preservation burner hearth heating schedule；
After the temperature of described heat-insulation and heat-preservation burner hearth is raised to assigned temperature, open described heat ray filter, will
Charging system sends into described heat-insulation and heat-preservation burner hearth dry distilling, and is collected empyreumatic oil by described oil and gas separating system
Gas；
In retort process, by the electricity of measure setup survey material temperature thermocouple output on corresponding contact point
Signal, the at any time temperature of the described dry distilling material of monitoring Different layer of the compost height；
After dry distilling terminates, described second burner hearth is set as inert gas atmosphere；By described charging system
It is delivered to described second burner hearth by described heat-insulation and heat-preservation burner hearth, closes described heat ray filter；
After described dry distilling material reduces the temperature to desirable value in described second burner hearth, take out described dry
Evaporate material to be analyzed.
Further, described noble gas is nitrogen.
Further, heating-up temperature during described heating rod dry distilling is 400 DEG C-1600 DEG C.
The application present invention, can realize following beneficial effect:
(1) mode of radiation heating in employing, successfully the mode of heating of simulation industry preheating furnace, permissible
Simulation industrial condition as much as possible, obtains test parameters for industrialized unit.
(2) it is capable of material to feed under setting furnace temperature, set furnace temperature bottom discharge, can be strict
Investigate the retorting time impact on dry distilling.
(3) temperature of the material of Different layer of the compost height can be monitored at any time, can strictly investigate dry distilling temperature
Degree is on dry distilling product and the impact of retort process.
(4) keep inert gas shielding or system airtight during input and output material, it is to avoid dry distilling product is at height
Oxygen combustion is contacted under temperature.
(5) the furnace cover lifting structure of independent design so that the materials such as the tar in easy cleaning carbonization gas
Deposition in stove, and change the mechanical disorder caused because of reasons such as heating rod damages.
Accompanying drawing explanation
Fig. 1 is that the structure of the destructive distillation device of a kind of band bell automatic lifting system of the embodiment of the present invention is shown
It is intended to.
Reference in accompanying drawing is as follows:
1, upper furnace body
101, body of heater shell；102, heat-insulation and heat-preservation burner hearth；103, feed bin；104, silo support；
105, insulation feed bin supporting plate；106, heating rod；107, hearth thermocouple entrance；
108, material temperature monitoring binding post；109, contact point on material temperature thermocouple is surveyed；
110, contact point in material temperature thermocouple is surveyed；111, contact point under material temperature thermocouple is surveyed；
112, nitrogen inflation inlet；113, nitrogen gas outlet；114, dry distilling oil gas vent；
115, bell support bar；116, furnace cover lifting machine；
2, intermediate thermal insulating layer
201, heat insulation fireguard；202, fireguard pusher；203, screw mandrel slideway；
3, lower furnace body
301, body of heater shell；302, lower hearth；303, fire door；304, nitrogen inflation inlet；
305, nitrogen gas outlet；306, material temperature binding post external tapping is surveyed；
307, converter body support lower limb；308, turbine screw elevator.
Detailed description of the invention
Illustrate embodiments of the present invention below in conjunction with the accompanying drawings.
As it is shown in figure 1, be the destructive distillation device of a kind of band bell automatic lifting system of the embodiment of the present invention
Structural representation, figure includes upper furnace body 1, intermediate thermal insulating layer 2, lower furnace body 3, and upper furnace body 1 is main
If high-temperature retorting district, lower furnace body 3 mainly starvation cooling zone.
See that Fig. 1, upper furnace body 1 include body of heater shell 101, heat-insulation and heat-preservation burner hearth 102, charging system,
Furnace cover lifting system, heater and upper furnace body gas inlet-outlet.
It can be seen from figure 1 that furnace cover lifting system includes bell, bell support bar 115 and furnace cover lifting
Machine 116；The top of bell support bar 115 is connected with bell, the bottom of bell support bar 115 and bell
Elevator 116 connects.When furnace cover lifting machine 116 starts, the top of bell support bar 115 can drive stove
Lid rises, in vertical state.After bell is opened, conveniently replaced heating rod and cleaning heating rod are placed
The deposition in district.
Seeing Fig. 1, upper furnace body 1 is setting up and down with lower furnace body 3, and upper furnace body 1 is positioned at just going up of lower furnace body 3
Side.Opening it is provided with, the heat-insulation and heat-preservation stove of upper furnace body 1 on the downside of the heat-insulation and heat-preservation burner hearth 102 of upper furnace body 1
Thorax 102 passes through open communication with the burner hearth of lower furnace body 3.
As it is shown in figure 1, charging system is connected with turbine screw elevator 308, turbine screw elevator
308 drive charging systems between the heat-insulation and heat-preservation burner hearth 102 and the burner hearth of lower furnace body 3 of upper furnace body 1 on
Lower movement.
It can be seen from figure 1 that intermediate thermal insulating layer 2 is arranged between upper furnace body 1 and lower furnace body 3, middle interval
Thermosphere 2, for stoping the hyperthermia radiation in heat-insulation and heat-preservation burner hearth 102 to lower furnace body 3, avoids lower stove simultaneously
There is oxygen to enter heat-insulation and heat-preservation burner hearth 102 during body 3 burner hearth blow-on door 203, carbonization gas composition is caused shadow
Ring.
See that Fig. 1, intermediate thermal insulating layer 2 include heat insulation fireguard 201, fireguard pusher 202, screw mandrel
Slideway 203.Heat insulation fireguard 201 is placed on screw mandrel slideway 203, at fireguard pusher 202
Traction is lower mobile.Heat insulation fireguard 201 uses heat-insulating heat-preserving material, mainly isolation heat-insulation and heat-preservation stove
Hyperthermia radiation in thorax 102 is to lower furnace body 3；The effect of fireguard pusher 202 is for heat insulation fireguard
The mobile offer power of 201.Fireguard pusher 202 can be electric and pneumatic, its effect be for
The mobile offer power of heat insulation fireguard 201.Screw mandrel slideway 203 provides for heat insulation fireguard 201 and moves
Dynamic track.
It can be seen from figure 1 that charging system includes feed bin 103, silo support 104, insulation feed bin torr
Plate 105.Feed bin 103 is used for putting dry distilling material；Silo support 104 is arranged on insulation feed bin torr
On plate 105.Silo support 104 is from lower support feed bin 103.
As it is shown in figure 1, insulation feed bin supporting plate 105 is plate object.Insulation feed bin supporting plate 105
Arrange with heat-insulation and heat-preservation burner hearth 102 opening parallel of upper furnace body 1, and open than heat-insulation and heat-preservation burner hearth 102
Mouth is wide.When charging system moves into heat-insulation and heat-preservation burner hearth 102, heat insulation feed bin supporting plate 105 is stuck in heat insulation
Outside the aperture position of insulation burner hearth 102, play sealing heat-blocking action, thus beneficially upper furnace body 1
The insulation of heat-insulation and heat-preservation burner hearth 102.May be implemented in and feed under setting furnace temperature, set furnace temperature bottom discharge,
Can be strict investigate the retorting time impact on dry distilling.
See that Fig. 1, heater include heating rod 106, thermocouple binding post (not shown), stove
Thorax thermocouple entrance 107 and external temperature control system (not shown).Heating rod 106 can use silicon-carbon
Rod or Si-Mo rod.Heating rod 106 can use mode arranged vertically at heat-insulation and heat-preservation burner hearth 102 furnace roof.
In employing, the mode of radiation heating, can successfully simulate the mode of heating of industry preheating furnace, can use up maximum
Possible simulation industrial condition, obtains test parameters for industrialized unit.Survey thorax warm galvanic couple and pass through stove
Thorax thermocouple entrance 107 extend in heat-insulation and heat-preservation burner hearth stove 102.Thermocouple binding post is at upper furnace body 1
Furnace roof；Survey and be electrically connected with between thorax warm galvanic couple and thermocouple binding post, and for being flexible coupling.
As it is shown in figure 1, material temperature monitoring device includes that material temperature monitors binding post 108, survey on material temperature thermocouple
Contact point 109, surveys contact point 110 in material temperature thermocouple, surveys contact point 111 under material temperature thermocouple, surveys
Material temperature binding post external tapping 306.
Such as Fig. 1, survey contact point 109 on material temperature thermocouple and be arranged on feed bin 103 top, survey material temperature thermoelectricity
In idol, contact point 110 is arranged on the middle part of feed bin 103, surveys contact point 111 under material temperature thermocouple and is arranged on
The bottom of feed bin 103.Survey material temperature thermocouple be separately mounted on above-mentioned contact point, and respectively with material temperature
Monitoring binding post 108 is electrically connected with.Material temperature monitoring binding post 108 is arranged on insulation feed bin supporting plate
On 105；Surveying material temperature binding post external tapping 306 is sealed interface, in order to ensure the airtight of lower hearth 302
Property；Material temperature monitoring binding post 108 is electrically connected with surveying material temperature binding post external tapping 306, and is soft company
Connect.Survey material temperature binding post external tapping 306 to be electrical connected with external temperature control system.
As it is shown in figure 1, upper furnace body gas inlet-outlet includes nitrogen inflation inlet 112, nitrogen gas outlet 113,
Dry distilling oil gas vent 114.The outlet 114 of dry distilling oil gas connects oil and gas separating system (not shown),
Directly condense including a condensed water and collect dry distilling oil gas after twice condensed water indirect condensing.Upper furnace body 1
The reason of heat-insulation and heat-preservation burner hearth 102 inflated with nitrogen is to replace the atmosphere in burner hearth before intensification, it is to avoid material
Oxygen burning is met in retort process；Inert gas shielding is kept, it is to avoid dry distilling product during input and output material
At high temperature contact oxygen combustion.
See that Fig. 1, lower furnace body 3 include that body of heater shell 301, lower hearth 302, fire door 303, nitrogen fill
QI KOU 304, nitrogen gas outlet 305 and converter body support lower limb 307.The purpose of lower hearth 302 inflated with nitrogen
It is to add material rear substitution oven cavity atmosphere, removes oxygen in raw material, be on the other hand to lower the temperature at material
During can be with fast cooling while starvation；Nitrogen can also be substituted with other noble gas.
It can be seen from figure 1 that upper furnace body 1 and lower furnace body 3 transfixion, feed bin supporting plate 105, silo support
104 and feed bin 103 move up and down with material retort process, use turbine screw elevator about 308 defeated
Send.
As it is shown in figure 1, in the present embodiment, apply the destructive distillation device of above-mentioned band bell automatic lifting system
The method of dry distilling is:
To include that feed bin 103, silo support 104, the charging system of insulation feed bin supporting plate 105 are put
In lower hearth 302.
According to experiment condition, material is tested in dry distilling and insert above-mentioned charging system；Material temperature thermoelectricity will be surveyed simultaneously
Occasionally it is attached separately to the upper, middle and lower contact point of feed bin.
Closing fire door, the nitrogen opening lower furnace body 3 nitrogen inflation inlet valve 304 and upper furnace body 1 is given vent to anger
Mouth 113 valves, simultaneously close off lower furnace body 3 nitrogen gas outlet valve 305 and the inflation of upper furnace body 1 nitrogen
Mouth 112 valves, replace the air nitrogen in whole burner hearth.
Close lower furnace body 3 nitrogen inflation inlet valve 304 and nitrogen gas outlet 113 valve of upper furnace body 1.
Close heat insulation fireguard 201, and open heater switch simultaneously, heat-insulation and heat-preservation burner hearth 102 is set and heats up journey
Sequence.
Until heat-insulation and heat-preservation burner hearth 102 temperature of upper furnace body 1 to after assigned temperature, open heat insulation fireguard
201, start turbine screw elevator 308, by feed bin 103, silo support 104 and insulation
The thermal treatment zone of upper furnace body 1 sent into by feed bin supporting plate 105, starts dry distilling, and pyrolysis temperature can be 400 DEG C-
1600℃.Dry distilling oil gas is collected from the oil and gas separating system end being connected with dry distilling oil gas vent 114.
In retort process, surveying contact point 109 on material temperature thermocouple by measure setup, surveying in material temperature thermocouple
Contact point 110, surveys the signal of telecommunication of the thermocouple output of contact point 111 under material temperature thermocouple, monitors at any time
The temperature of the material of Different layer of the compost height, can strictly investigate pyrolysis temperature to dry distilling product and retort process
Impact.
After dry distilling terminates, first open nitrogen inflation inlet 304 valve and lower furnace body 3 nitrogen of lower furnace body 3
Gas outlet 305 valve, it is ensured that lower hearth 202 is nitrogen atmosphere, then starts turbine screw elevator
308, by feed bin 103, silo support 104 and insulation feed bin supporting plate 105 by upper furnace body 1
Heat-insulation and heat-preservation burner hearth 102 is transported to lower hearth 302, closes heat insulation fireguard 201, completely cuts off heat.
After temperature of charge drops to desirable value, open lower furnace body 3 fire door 303, take out material and be analyzed.
It should be noted that each embodiment above by reference to described by accompanying drawing is only in order to illustrate the present invention
And unrestricted the scope of the present invention, it will be understood by those within the art that, without departing from this
The amendment on the premise of bright spirit and scope carried out the present invention or equivalent, all should contain
Within the scope of the present invention.
Claims (10)
1. a destructive distillation device for band bell automatic lifting system, including the first body of heater, the second body of heater,
Heat ray filter；
Described first body of heater includes body of heater shell, heat-insulation and heat-preservation burner hearth, charging system, furnace cover lifting system
System, heater, material temperature monitoring device, the first gas inlet-outlet；
Described furnace cover lifting system includes bell, bell support bar and furnace cover lifting machine；
The top of described bell support bar is connected with described bell, the bottom of described bell support bar and institute
State furnace cover lifting machine to connect；
Described second body of heater includes body of heater shell, the second burner hearth, fire door, the second gas inlet-outlet, shifting
Dynamic device；
Described first body of heater is disposed adjacent with described second body of heater, described first body of heater heat-insulation and heat-preservation burner hearth
Side arranges opening, and described heat-insulation and heat-preservation burner hearth is connected with described second burner hearth by described opening；
Described charging system is connected with described mobile device, and described mobile device drives described charging system
Move between the described heat-insulation and heat-preservation burner hearth and the burner hearth of described second body of heater of the first body of heater；
Described material temperature monitoring device is for measuring during dry distilling the temperature of diverse location material in described feed bin；
Described heat ray filter is arranged between the first body of heater and the second body of heater, and described heat ray filter is used for hindering
Only the hyperthermia radiation in described heat-insulation and heat-preservation burner hearth is to described second body of heater.
2. the destructive distillation device of band bell automatic lifting system as claimed in claim 1, it is characterised in that
Described charging system includes feed bin, silo support, insulation feed bin supporting plate；
Described feed bin is used for putting dry distilling material；
Described silo support is arranged on described insulation feed bin supporting plate, and described silo support supports institute
State feed bin；
Described insulation feed bin supporting plate is plate object；
Described insulation feed bin supporting plate is arranged and than heat insulation guarantor with described heat-insulation and heat-preservation burner hearth opening parallel
The opening width of temperature burner hearth；When described charging system moves into described heat-insulation and heat-preservation burner hearth, described thermal insulation separation
Hot aggregate bin supporting plate is stuck in outside the aperture position of described heat-insulation and heat-preservation burner hearth.
3. the destructive distillation device of band bell automatic lifting system as claimed in claim 1, it is characterised in that
Described first body of heater is positioned at the surface of described second body of heater, and described mobile device is the lifting of turbine screw rod
Machine.
4. the destructive distillation device of band bell automatic lifting system as claimed in claim 1, it is characterised in that
Described heater includes heating rod, thermocouple binding post, hearth thermocouple entrance, external temperature control system
System；
Described heating rod uses siliconit or Si-Mo rod；
Described heating rod is arranged on described heat-insulation and heat-preservation burner hearth furnace roof, is perpendicular to the arrangement of described furnace roof；
Described thermocouple binding post is arranged on the furnace roof of described first body of heater；
It is electrically connected with between described external temperature control system and described thermocouple binding post；
Described heating rod is electrically connected with described external temperature control system.
5. the destructive distillation device of band bell automatic lifting system as claimed in claim 1, it is characterised in that
Described material temperature monitoring device includes that material temperature monitors binding post, surveys contact point on material temperature thermocouple, surveys material temperature
Contact point in thermocouple, surveys contact point under material temperature thermocouple, surveys material temperature binding post external tapping, external temperature
Ore-controlling Role；
On described survey material temperature thermocouple, contact point is arranged on described feed bin top, described survey material temperature thermoelectricity
In idol, contact point is arranged on the middle part of described feed bin, and under described survey material temperature thermocouple, contact point is arranged on institute
State the bottom of feed bin；
Described material temperature monitoring binding post is arranged on described insulation feed bin supporting plate；
Contact point on described survey material temperature thermocouple, survey contact point in material temperature thermocouple, survey material temperature thermocouple
Lower contact point is electrically connected with described material temperature monitoring binding post；
Described material temperature monitoring binding post is electrically connected with described survey material temperature binding post external tapping；
Described survey material temperature binding post external tapping is electrical connected with described external temperature control system；
Described survey material temperature binding post external tapping is sealed interface.
6. the destructive distillation device of band bell automatic lifting system as claimed in claim 1, it is characterised in that
Described heat ray filter is intermediate thermal insulating layer；
Described intermediate thermal insulating layer includes heat insulation fireguard, fireguard pusher, screw mandrel slideway；
Described heat insulation fireguard is placed on described screw mandrel slideway, in the traction of described fireguard pusher
Lower movement；
Described heat insulation fireguard, the mainly heat of isolation heat-insulation and heat-preservation burner hearth pass to the second burner hearth；Institute
The effect stating fireguard pusher is the mobile offer power for described heat insulation fireguard；Described screw mandrel is sliding
Road provides moving track for described heat insulation fireguard.
7. the destructive distillation device of band bell automatic lifting system as claimed in claim 1, it is characterised in that
Described first gas inlet-outlet include at least one first gas access, at least one first gas outlet,
At least one dry distilling oil gas vent；Described dry distilling oil gas vent connects oil and gas separating system；
Described second gas inlet-outlet includes at least one second gas access, at least one second gas
Outlet.
8. the destructive distillation device with the band bell automatic lifting system as described in one of claim 1-7
The method carrying out dry distilling, comprises the following steps:
Described charging system is placed in described second burner hearth；
Described dry distilling material is inserted described charging system；Described survey material temperature thermocouple is filled respectively simultaneously
On the corresponding contact point of described feed bin；
By the air inert gas replacement in described heat-insulation and heat-preservation burner hearth and described second burner hearth；
Close described heat ray filter, start described heat-insulation and heat-preservation burner hearth heating schedule；
After the temperature of described heat-insulation and heat-preservation burner hearth is raised to assigned temperature, open described heat ray filter, will
Charging system sends into described heat-insulation and heat-preservation burner hearth dry distilling, and is collected empyreumatic oil by described oil and gas separating system
Gas；
In retort process, by the electricity of measure setup survey material temperature thermocouple output on corresponding contact point
Signal, the at any time temperature of the described dry distilling material of monitoring Different layer of the compost height；
After dry distilling terminates, described second burner hearth is set as inert gas atmosphere；By described charging system
It is delivered to described second burner hearth by described heat-insulation and heat-preservation burner hearth, closes described heat ray filter；
After described dry distilling material reduces the temperature to desirable value in described second burner hearth, take out described dry
Evaporate material to be analyzed.
9. the method for dry distilling as claimed in claim 8, it is characterised in that described noble gas is nitrogen.
10. the method for dry distilling as claimed in claim 8, it is characterised in that during described heating rod dry distilling
Heating-up temperature be 400 DEG C-1600 DEG C.
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| CN201610410726.1A CN105928367B (en) | 2016-06-13 | 2016-06-13 | A kind of destructive distillation device and its method for destructive distillation with bell automatic lifting system |
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Citations (5)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| JPH1036851A (en) * | 1996-07-25 | 1998-02-10 | Daiichi:Kk | Electric resistance carbonization volume reduction oven |
| CN200961100Y (en) * | 2006-09-21 | 2007-10-17 | 朱新发 | Active carbon continuous activation furnace with two temperature section |
| CN102649550A (en) * | 2011-02-25 | 2012-08-29 | 王全祥 | Carbonization-activation integrated activated carbon production apparatus |
| CN104178186A (en) * | 2014-09-09 | 2014-12-03 | 北京神雾环境能源科技集团股份有限公司 | Coal low-temperature carbonization system and method |
| CN205980776U (en) * | 2016-06-13 | 2017-02-22 | 北京神雾环境能源科技集团股份有限公司 | Take automatic operating system's of bell dry distillation device |
-
2016
- 2016-06-13 CN CN201610410726.1A patent/CN105928367B/en active Active
Patent Citations (5)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| JPH1036851A (en) * | 1996-07-25 | 1998-02-10 | Daiichi:Kk | Electric resistance carbonization volume reduction oven |
| CN200961100Y (en) * | 2006-09-21 | 2007-10-17 | 朱新发 | Active carbon continuous activation furnace with two temperature section |
| CN102649550A (en) * | 2011-02-25 | 2012-08-29 | 王全祥 | Carbonization-activation integrated activated carbon production apparatus |
| CN104178186A (en) * | 2014-09-09 | 2014-12-03 | 北京神雾环境能源科技集团股份有限公司 | Coal low-temperature carbonization system and method |
| CN205980776U (en) * | 2016-06-13 | 2017-02-22 | 北京神雾环境能源科技集团股份有限公司 | Take automatic operating system's of bell dry distillation device |
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| CN105928367B (en) | 2018-04-20 |
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