CN105921452A - Cleaning of rhinestone gluing powder and recycling process of cleaning liquid - Google Patents
Cleaning of rhinestone gluing powder and recycling process of cleaning liquid Download PDFInfo
- Publication number
- CN105921452A CN105921452A CN201610290554.9A CN201610290554A CN105921452A CN 105921452 A CN105921452 A CN 105921452A CN 201610290554 A CN201610290554 A CN 201610290554A CN 105921452 A CN105921452 A CN 105921452A
- Authority
- CN
- China
- Prior art keywords
- cleaning
- water drilling
- cleanout fluid
- viscose glue
- glue powder
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Granted
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Classifications
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B08—CLEANING
- B08B—CLEANING IN GENERAL; PREVENTION OF FOULING IN GENERAL
- B08B3/00—Cleaning by methods involving the use or presence of liquid or steam
- B08B3/04—Cleaning involving contact with liquid
- B08B3/08—Cleaning involving contact with liquid the liquid having chemical or dissolving effect
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B08—CLEANING
- B08B—CLEANING IN GENERAL; PREVENTION OF FOULING IN GENERAL
- B08B3/00—Cleaning by methods involving the use or presence of liquid or steam
- B08B3/04—Cleaning involving contact with liquid
- B08B3/10—Cleaning involving contact with liquid with additional treatment of the liquid or of the object being cleaned, e.g. by heat, by electricity or by vibration
-
- C—CHEMISTRY; METALLURGY
- C02—TREATMENT OF WATER, WASTE WATER, SEWAGE, OR SLUDGE
- C02F—TREATMENT OF WATER, WASTE WATER, SEWAGE, OR SLUDGE
- C02F1/00—Treatment of water, waste water, or sewage
- C02F1/52—Treatment of water, waste water, or sewage by flocculation or precipitation of suspended impurities
-
- C—CHEMISTRY; METALLURGY
- C02—TREATMENT OF WATER, WASTE WATER, SEWAGE, OR SLUDGE
- C02F—TREATMENT OF WATER, WASTE WATER, SEWAGE, OR SLUDGE
- C02F1/00—Treatment of water, waste water, or sewage
- C02F1/66—Treatment of water, waste water, or sewage by neutralisation; pH adjustment
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- Chemical & Material Sciences (AREA)
- Life Sciences & Earth Sciences (AREA)
- Hydrology & Water Resources (AREA)
- Engineering & Computer Science (AREA)
- Environmental & Geological Engineering (AREA)
- Water Supply & Treatment (AREA)
- Organic Chemistry (AREA)
- Chemical Kinetics & Catalysis (AREA)
- General Chemical & Material Sciences (AREA)
- Detergent Compositions (AREA)
- Processing Of Solid Wastes (AREA)
Abstract
The invention discloses cleaning of rhinestone gluing powder and a recycling process of cleaning liquid. The process comprises the following steps: (S1) rhinestones bonded with gluing powder are dipped by using alkaline cleaning liquid; (S2) the rhinestones and the gluing powder are stirred and washed by using a stirrer; (S3) the rhinestones and the cleaning liquid are separated; (S4) the cleaning liquid is precipitated by using metal salt; and (S5) precipitates and the cleaning liquid are separated; and the cleaning liquid is diluted to realize recycling. The cleaning of the rhinestone gluing powder and the recycling process of the cleaning liquid are simple in operation, short in time consumption and low in energy consumption, and can effectively remove the gluing powder without damaging rhinestone samples. In addition, the cleaning liquid produced by the method can realize recycling and reduce the production cost and the environmental pollution, and is higher in application prospect.
Description
Technical field
The invention belongs to field of inorganic nonmetallic material, relate to crystal glass processing technique field, particularly relate to a kind of water drilling and glue
The cleaning of rubber powder and cleanout fluid circulation re-use technique.
Background technology
In traditional water drilling processing technique, the grinding of water drilling base pearl is it is critical that a ring.Water drilling base bead mill cuts glue used
Powder i.e. viscose glue powder, would generally stick to above water drilling after ground completes, and needs viscose glue powder from water drilling sur-face peeling, stripping
Substantial amounts of cleaning emulsion can be produced after from.General way is to be directly discharged in environment, and this not only can produce substantial amounts of pollution,
And production cost can be increased.In order to reduce producing cost, enterprise wishes by improving the work cleaning removal water drilling surface viscose glue powder
Skill, processes and cleans emulsion, to reach to reuse the purpose of these cleanout fluid.
Summary of the invention
It is an object of the invention to provide a kind of cleaning of water drilling viscose glue powder and the circulation of cleanout fluid re-uses technique.Above-mentioned for solving
Technical problem, the cleaning of water drilling viscose glue powder of the present invention and the circulation of cleanout fluid re-use technique, comprise the steps: S1, use
The water drilling of attachment viscose glue powder is soaked by alkaline cleaning fluid；S2, uses agitator to be stirred water drilling and viscose glue powder at cleaning
Reason；S3, carries out separating treatment to water drilling and cleanout fluid；S4, uses slaine to cleanout fluid to carrying out precipitation process；S5 is right
Precipitation and cleanout fluid carry out separating treatment, and are diluted processing to cleanout fluid and again recycle.
In described step S1, alkaline cleaning fluid is NaOH solution, and NaOH solution concentration is 0.5mol/L, and soak time is 5 minutes.
In described step S2, mixing time is 10-20 minute, and mixing speed is 100 revs/min.
Described step S3 also includes step S3.1, and described step S3.1 separates water drilling and cleanout fluid for using sub-sieve to filter.
Described step S3 farther includes step S3.2, and described step S3.2 is for using ultra-pure water to carry out overflow cleaning, so water drilling
After sample is placed drying in oven.
In described step S3.1, the time being carried out water drilling with ultra-pure water is 1 minute.
In described step S3.2, it is that water drilling sample is placed in dustless drying baker, after toasting 30 minutes in the environment of 60 DEG C, is down to room temperature,
Take out sample.
Described step S4 includes that step S4.1 and step S4.2, described step S4.1 are addition slaine, described step in cleanout fluid
S4.2 is the pH of regulation cleanout fluid.
In described step S4.1, slaine is ferric nitrate, and ferric nitrate and the additional proportion cleaning emulsion are 20g/L.
In described step S4.2, use the NaOH solution regulation of 1mol/L to clean the pH of emulsion, emulsion pH regulator will be cleaned to 14
After start sedimentation of clocking, the sedimentation time is 40 minutes.
In described step S5, precipitation and cleanout fluid being carried out separating treatment, is transferred in beaker by supernatant, precipitum is dried standby
With.Ultra-pure water is added, by the pH regulator of cleanout fluid to 13.7, such that it is able to realize the recycling of cleanout fluid in supernatant.
The cleaning method that the present invention removes water drilling viscose glue powder is simple to operate, the shortest, and energy consumption is low, it is possible to effectively remove on water drilling viscous
Attached viscose glue powder, and can realize cleanout fluid is recycled.
Accompanying drawing explanation
Fig. 1 is the cleaning of water drilling viscose glue powder of the present invention and the circulation of cleanout fluid re-uses process chart；
Fig. 2 is undressed cleaning emulsion；
Fig. 3 does not regulates cleanout fluid pH settle 30 minutes design sketchs for adding ferric nitrate；
Fig. 4 is for adding ferric nitrate and regulating cleanout fluid pH to 14 10 minutes design sketchs of sedimentation.
Detailed description of the invention
The cleaning of water drilling viscose glue powder a kind of to the present invention and the circulation of cleanout fluid re-use technique work the most below in conjunction with the accompanying drawings
Explanation.
As it is shown in figure 1, the circulation of the cleaning of the present invention a kind of water drilling viscose glue powder and cleanout fluid re-uses technique, first by NaOH
Sample is soaked by solution, is aoxidized by the viscose glue powder of sample surfaces by the Oxidation of NaOH, then will be viscous by stirring action
Rubber powder is removed, then uses sub-sieve separating treatment, obtains clean water and bores sample and clean emulsion.Add to cleaning in emulsion
Enter a certain amount of ferric nitrate and add NaOH solution adjustment cleaning emulsion pH, by complexing and the ferric hydroxide precipitate of ferrum
Adsorption will to clean emulsion settlement separate, finally adjust the pH of cleanout fluid thus realize recycling of cleanout fluid.
Step one, by adhere to viscose glue powder water drilling sample cooling after put in cleaning box, in box, add the NaOH solution of 0.5mol/L,
Now NaOH solution needs to be totally submerged water drilling sample, and the water surface should be kept during this to exceed sample 40mm.NaOH solution
The purpose soaked is to soften viscose glue powder, and is aoxidized by the viscose glue powder of sample surfaces by the Oxidation of NaOH, thus necessary
Controlling soak time, the time of immersion is 5 minutes.
Step 2, water drilling sample is transferred in beaker together with NaOH solution, uses agitator that water drilling and viscose glue powder are stirred
Cleaning treatment, mixing time is 10-20 minute, and mixing speed is 100 revs/min, realizes water drilling and viscose glue by physical agitation effect
Being kept completely separate of powder.Effect is as shown in table 1:
Table 1
| Scavenging period (min) | Viscose glue powder removal effect | The rate of cleaning |
| 5 | A small amount of removal | 40% |
| 10 | Major part is removed | 82% |
| 20 | The overwhelming majority is removed | 95% |
| 30 | The overwhelming majority is removed | 96% |
Step 3, employing sub-sieve filter and separate water drilling sample and clean emulsion, pour water drilling sample and cleaning emulsion into sub-sieve,
By filtration, water drilling is separated with cleaning emulsion.Then use ultra-pure water that water drilling sample carries out overflow to clean 1 minute, mesh
Be the alkali liquor remained by sample surfaces and a small amount of residual viscose glue powder cleans up, finally sample is placed the ring at 60 DEG C in baking oven
It is down to room temperature after toasting 30 minutes under border, takes out sample.
Step 4, adding ferric nitrate in emulsion to cleaning, ferric nitrate and the ratio cleaning emulsion are 20g/L, and use 1mol/L's
NaOH solution will start sedimentation after cleaning emulsion pH regulator to 14, the sedimentation time is 40 minutes.Purpose is the complexation by ferrum
It is settlement separate that the adsorption of effect and ferric hydroxide precipitate will clean emulsion.Effect of settling contrasts as shown in Figure 2, Figure 3, Figure 4.
Step 5, precipitation and cleanout fluid being carried out separating treatment, be transferred to by supernatant in other containers, precipitum is unified after being dried
Collection processes.Ultra-pure water is added, by the pH regulator of cleanout fluid to 13.7 in supernatant.Now can add in solution new not
Process water drilling sample and soak the washing and cleaning operation carrying out next round, thus realize the recycling of cleanout fluid.
The cleaning of water drilling viscose glue powder of the present invention and the circulation of cleanout fluid re-use technique, simple to operate, and the shortest, energy consumption is low, energy
Enough effectively remove viscose glue powder, and water drilling sample will not be caused damage.Additionally, the cleanout fluid that adopting said method produces can be real
Existing cycling and reutilization, reduces production cost and the pollution to environment thereof.
Below preferred embodiment to the invention is illustrated, but the invention is not limited to described embodiment,
Those of ordinary skill in the art it may also be made that the modification of all equivalents on the premise of the invention spirit or replacing
Changing, modification or the replacement of these equivalents are all contained in the application claim limited range.
Claims (7)
1. the cleaning of a water drilling viscose glue powder and the circulation of cleanout fluid re-use technique, it is characterised in that comprise the steps:
S1, uses alkaline cleaning fluid to soak the water drilling of attachment viscose glue powder；
S2, uses agitator that water drilling and viscose glue powder are stirred cleaning treatment；
S3, carries out separating treatment to water drilling and cleanout fluid；
S4, uses slaine and NaOH solution to cleanout fluid to carrying out precipitation process；
S5, carries out separating treatment to precipitation and cleanout fluid, and is diluted processing to cleanout fluid and again recycles.
The cleaning of water drilling viscose glue powder the most according to claim 1 and the circulation of cleanout fluid re-use technique, it is characterised in that described
In step S1, alkaline cleaning fluid is NaOH solution, and NaOH solution concentration is 0.5mol/L, and soak time is 5 minutes.
The cleaning of water drilling viscose glue powder the most according to claim 1 and the circulation of cleanout fluid re-use technique, it is characterised in that described
In step S2, mixing time is 10-20 minute, and mixing speed is 100 revs/min.
The cleaning of water drilling viscose glue powder the most according to claim 1 and the circulation of cleanout fluid re-use technique, it is characterised in that described
In step S3, using ultra-pure water that water drilling is carried out overflow cleaning, scavenging period is 1 minute, then water drilling sample is placed in nothing
In dirt drying baker, after toasting 30 minutes in the environment of 60 DEG C, it is down to room temperature, takes out sample.
The cleaning of water drilling viscose glue powder the most according to claim 1 and the circulation of cleanout fluid re-use technique, it is characterised in that described
In step S4, added slaine is ferric nitrate, and ferric nitrate and the ratio cleaning emulsion are 20g/L.
The cleaning of water drilling viscose glue powder the most according to claim 1 and the circulation of cleanout fluid re-use technique, it is characterised in that described
In step S4, using the NaOH solution of 1mol/L will to start sedimentation after cleaning emulsion pH regulator to 14, the sedimentation time is 40
Minute.
The cleaning of water drilling viscose glue powder the most according to claim 1 and the circulation of cleanout fluid re-use technique, it is characterised in that described
In step S5, after separating treatment, being transferred to by supernatant in other container, precipitum is standby, then to cleaning after being dried
In liquid, addition ultra-pure water is by its pH regulator to 13.7, thus realizes the recycling of cleanout fluid.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201610290554.9A CN105921452B (en) | 2016-04-28 | 2016-04-28 | A kind of cleaning of water drilling viscose glue powder and the circulation of cleaning solution reuse technique |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201610290554.9A CN105921452B (en) | 2016-04-28 | 2016-04-28 | A kind of cleaning of water drilling viscose glue powder and the circulation of cleaning solution reuse technique |
Publications (2)
| Publication Number | Publication Date |
|---|---|
| CN105921452A true CN105921452A (en) | 2016-09-07 |
| CN105921452B CN105921452B (en) | 2019-06-11 |
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| CN201610290554.9A Active CN105921452B (en) | 2016-04-28 | 2016-04-28 | A kind of cleaning of water drilling viscose glue powder and the circulation of cleaning solution reuse technique |
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Citations (7)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| KR20030091871A (en) * | 2003-11-04 | 2003-12-03 | 주식회사 하나로물산 | Polyurethane binder composite for polishing rheinstone(hot-fix) and separating method of rheinstone |
| CN101176977A (en) * | 2006-11-08 | 2008-05-14 | 陈伟翔 | Processing technique of artificial crystal diamond semi-finished products |
| CN101474767A (en) * | 2009-01-15 | 2009-07-08 | 杭州迈控科技有限公司 | Mechanism for scraping rubber powder of charging/discharging machine of water drill grinding machine |
| CN201544092U (en) * | 2009-11-26 | 2010-08-11 | 杭州迈控科技有限公司 | Bearing reciprocating glue spreader |
| CN201792265U (en) * | 2010-06-30 | 2011-04-13 | 平湖思杰腾汽车设备制造有限公司 | Gluing mechanism for numerical control diamond grinding machine |
| CN102960913A (en) * | 2012-12-18 | 2013-03-13 | 金华冠华水晶有限公司 | Making process of artificial crystal diamond adhesive powder |
| CN104551915A (en) * | 2014-06-10 | 2015-04-29 | 金华冠华水晶有限公司 | Full-automatic water drill grinding-polishing machine and processing technique thereof |
-
2016
- 2016-04-28 CN CN201610290554.9A patent/CN105921452B/en active Active
Patent Citations (7)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| KR20030091871A (en) * | 2003-11-04 | 2003-12-03 | 주식회사 하나로물산 | Polyurethane binder composite for polishing rheinstone(hot-fix) and separating method of rheinstone |
| CN101176977A (en) * | 2006-11-08 | 2008-05-14 | 陈伟翔 | Processing technique of artificial crystal diamond semi-finished products |
| CN101474767A (en) * | 2009-01-15 | 2009-07-08 | 杭州迈控科技有限公司 | Mechanism for scraping rubber powder of charging/discharging machine of water drill grinding machine |
| CN201544092U (en) * | 2009-11-26 | 2010-08-11 | 杭州迈控科技有限公司 | Bearing reciprocating glue spreader |
| CN201792265U (en) * | 2010-06-30 | 2011-04-13 | 平湖思杰腾汽车设备制造有限公司 | Gluing mechanism for numerical control diamond grinding machine |
| CN102960913A (en) * | 2012-12-18 | 2013-03-13 | 金华冠华水晶有限公司 | Making process of artificial crystal diamond adhesive powder |
| CN104551915A (en) * | 2014-06-10 | 2015-04-29 | 金华冠华水晶有限公司 | Full-automatic water drill grinding-polishing machine and processing technique thereof |
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| CN105921452B (en) | 2019-06-11 |
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Effective date of registration: 20220720 Address after: 201800 358 Kefu Road, Jiading District, Shanghai_ Room j2644, Zone E, floor 1, building 4, No. 368 Patentee after: Shanghai Yiyou Information Technology Co.,Ltd. Address before: No.759, 2nd Ring East Road, Longquan street, Wuxing District, Huzhou City, Zhejiang Province Patentee before: HUZHOU TEACHERS College |
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Effective date of registration: 20220725 Address after: 435500 Dashengguanshan Industrial Park, Huangmei County, Huanggang City, Hubei Province Patentee after: HUBEI YUXING CRYSTAL JEWELRY CO.,LTD. Address before: 201800 358 Kefu Road, Jiading District, Shanghai_ Room j2644, Zone E, floor 1, building 4, No. 368 Patentee before: Shanghai Yiyou Information Technology Co.,Ltd. |
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Denomination of invention: A process for cleaning water drill adhesive powder and recycling cleaning fluid Effective date of registration: 20230208 Granted publication date: 20190611 Pledgee: Bank of China Limited Huanggang branch Pledgor: HUBEI YUXING CRYSTAL JEWELRY CO.,LTD. Registration number: Y2023420000032 |