CN105907221A - High-temperature-resistant coating material and preparation method thereof - Google Patents

High-temperature-resistant coating material and preparation method thereof Download PDF

Info

Publication number
CN105907221A
CN105907221A CN201610304294.6A CN201610304294A CN105907221A CN 105907221 A CN105907221 A CN 105907221A CN 201610304294 A CN201610304294 A CN 201610304294A CN 105907221 A CN105907221 A CN 105907221A
Authority
CN
China
Prior art keywords
water
agent
parts
ammonium
coating material
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Pending
Application number
CN201610304294.6A
Other languages
Chinese (zh)
Inventor
费邦忠
周正华
郭庆
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
ANHUI HUAHUI PLASTIC TECHNOLOGY Co Ltd
Original Assignee
ANHUI HUAHUI PLASTIC TECHNOLOGY Co Ltd
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by ANHUI HUAHUI PLASTIC TECHNOLOGY Co Ltd filed Critical ANHUI HUAHUI PLASTIC TECHNOLOGY Co Ltd
Priority to CN201610304294.6A priority Critical patent/CN105907221A/en
Publication of CN105907221A publication Critical patent/CN105907221A/en
Pending legal-status Critical Current

Links

Classifications

    • C—CHEMISTRY; METALLURGY
    • C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
    • C09D—COATING COMPOSITIONS, e.g. PAINTS, VARNISHES OR LACQUERS; FILLING PASTES; CHEMICAL PAINT OR INK REMOVERS; INKS; CORRECTING FLUIDS; WOODSTAINS; PASTES OR SOLIDS FOR COLOURING OR PRINTING; USE OF MATERIALS THEREFOR
    • C09D151/00—Coating compositions based on graft polymers in which the grafted component is obtained by reactions only involving carbon-to-carbon unsaturated bonds; Coating compositions based on derivatives of such polymers
    • C09D151/003—Coating compositions based on graft polymers in which the grafted component is obtained by reactions only involving carbon-to-carbon unsaturated bonds; Coating compositions based on derivatives of such polymers grafted on to macromolecular compounds obtained by reactions only involving unsaturated carbon-to-carbon bonds
    • C—CHEMISTRY; METALLURGY
    • C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08F—MACROMOLECULAR COMPOUNDS OBTAINED BY REACTIONS ONLY INVOLVING CARBON-TO-CARBON UNSATURATED BONDS
    • C08F259/00—Macromolecular compounds obtained by polymerising monomers on to polymers of halogen containing monomers as defined in group C08F14/00
    • C08F259/02—Macromolecular compounds obtained by polymerising monomers on to polymers of halogen containing monomers as defined in group C08F14/00 on to polymers containing chlorine
    • C08F259/04—Macromolecular compounds obtained by polymerising monomers on to polymers of halogen containing monomers as defined in group C08F14/00 on to polymers containing chlorine on to polymers of vinyl chloride
    • C—CHEMISTRY; METALLURGY
    • C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
    • C09D—COATING COMPOSITIONS, e.g. PAINTS, VARNISHES OR LACQUERS; FILLING PASTES; CHEMICAL PAINT OR INK REMOVERS; INKS; CORRECTING FLUIDS; WOODSTAINS; PASTES OR SOLIDS FOR COLOURING OR PRINTING; USE OF MATERIALS THEREFOR
    • C09D5/00—Coating compositions, e.g. paints, varnishes or lacquers, characterised by their physical nature or the effects produced; Filling pastes
    • C09D5/18—Fireproof paints including high temperature resistant paints
    • C—CHEMISTRY; METALLURGY
    • C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
    • C09D—COATING COMPOSITIONS, e.g. PAINTS, VARNISHES OR LACQUERS; FILLING PASTES; CHEMICAL PAINT OR INK REMOVERS; INKS; CORRECTING FLUIDS; WOODSTAINS; PASTES OR SOLIDS FOR COLOURING OR PRINTING; USE OF MATERIALS THEREFOR
    • C09D7/00—Features of coating compositions, not provided for in group C09D5/00; Processes for incorporating ingredients in coating compositions
    • C09D7/40—Additives
    • C09D7/60—Additives non-macromolecular
    • C09D7/61—Additives non-macromolecular inorganic
    • C—CHEMISTRY; METALLURGY
    • C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
    • C09D—COATING COMPOSITIONS, e.g. PAINTS, VARNISHES OR LACQUERS; FILLING PASTES; CHEMICAL PAINT OR INK REMOVERS; INKS; CORRECTING FLUIDS; WOODSTAINS; PASTES OR SOLIDS FOR COLOURING OR PRINTING; USE OF MATERIALS THEREFOR
    • C09D7/00—Features of coating compositions, not provided for in group C09D5/00; Processes for incorporating ingredients in coating compositions
    • C09D7/40—Additives
    • C09D7/60—Additives non-macromolecular
    • C09D7/63—Additives non-macromolecular organic
    • C—CHEMISTRY; METALLURGY
    • C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
    • C09D—COATING COMPOSITIONS, e.g. PAINTS, VARNISHES OR LACQUERS; FILLING PASTES; CHEMICAL PAINT OR INK REMOVERS; INKS; CORRECTING FLUIDS; WOODSTAINS; PASTES OR SOLIDS FOR COLOURING OR PRINTING; USE OF MATERIALS THEREFOR
    • C09D7/00—Features of coating compositions, not provided for in group C09D5/00; Processes for incorporating ingredients in coating compositions
    • C09D7/40—Additives
    • C09D7/65—Additives macromolecular
    • C—CHEMISTRY; METALLURGY
    • C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
    • C09D—COATING COMPOSITIONS, e.g. PAINTS, VARNISHES OR LACQUERS; FILLING PASTES; CHEMICAL PAINT OR INK REMOVERS; INKS; CORRECTING FLUIDS; WOODSTAINS; PASTES OR SOLIDS FOR COLOURING OR PRINTING; USE OF MATERIALS THEREFOR
    • C09D7/00—Features of coating compositions, not provided for in group C09D5/00; Processes for incorporating ingredients in coating compositions
    • C09D7/40—Additives
    • C09D7/70—Additives characterised by shape, e.g. fibres, flakes or microspheres
    • C—CHEMISTRY; METALLURGY
    • C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08K—Use of inorganic or non-macromolecular organic substances as compounding ingredients
    • C08K2201/00—Specific properties of additives
    • C08K2201/011—Nanostructured additives
    • C—CHEMISTRY; METALLURGY
    • C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08K—Use of inorganic or non-macromolecular organic substances as compounding ingredients
    • C08K2201/00—Specific properties of additives
    • C08K2201/014—Additives containing two or more different additives of the same subgroup in C08K
    • C—CHEMISTRY; METALLURGY
    • C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08L—COMPOSITIONS OF MACROMOLECULAR COMPOUNDS
    • C08L2201/00—Properties
    • C08L2201/02—Flame or fire retardant/resistant
    • C—CHEMISTRY; METALLURGY
    • C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08L—COMPOSITIONS OF MACROMOLECULAR COMPOUNDS
    • C08L2205/00—Polymer mixtures characterised by other features
    • C08L2205/03—Polymer mixtures characterised by other features containing three or more polymers in a blend
    • C08L2205/035—Polymer mixtures characterised by other features containing three or more polymers in a blend containing four or more polymers in a blend

Abstract

The invention relates to a high-temperature-resistant coating material and a preparation method thereof. The coating material is mainly prepared from the following ingredients: hydroxyl-terminated dimethyl silicone rubber, a TGIC curing agent, diacyloxy heptane dibutyl tin, borax, an ammonium polyphosphate heat-resistant assistant, an acidic oxidant, a sand ripple agent, fume silica, transparent zinc oxide, asbestos powder, nano-silica, chlorinated rubber, titania, talcum powder, barium sulfate, an anti-settling agent, an antifoamer, pigments, leucoxene powder, bamboo fungi, water, black plums, radix astragali, poria cocos, fritillary bulbs, fructus aurantii, Chinese angelica, PVA, starch, ammonia water, a mixture of AA and AAm, ammonium persulfate, ammonium bisulfite, polyvinyl alcohol, a cross-linking agent, active magnesia, casein, sodium hydroxide, hydroquinone, alkali lignin and a silane coupling agent. The coating material prepared by the preparation method provided by the invention is free of off flavors, the formaldehyde content is far lower than that in national standards, and meanwhile, a particular fragrance is released, so that the coating material is applicable to household electrical appliances and furniture; the high-temperature resistance and cold resistance are high, and the defects of the existing coating materials are effectively overcome.

Description

A kind of high-temperature resistant coating and preparation method thereof
Technical field:
The present invention designs a kind of chemistry painting industry and preparation method thereof, be specifically related to a kind of high-temperature resistant coating and Preparation method.
Background technology:
On market, dragons and fishes jumbled together for existing coating, protects the coating of household electrical appliances to occur especially on household electrical appliances furniture Time length is long afterwards, it is impossible to reach antiseptic property, cold-proof, in order to meet the market demand, is badly in need of research and development one Plant preferable coating.
Summary of the invention:
The technical problem to be solved is to overcome the defect of prior art, it is provided that a kind of field is big Beans plantation herbicide and preparation method thereof in early days.
The technical problem to be solved realizes by the following technical solutions.
A kind of high-temperature resistant coating, it is characterised in that: mainly it is composed of the following components in parts by weight:
Terminal hydroxy group dimethyl silicone rubber: 10-15 part, TGIC curing agent: 2-3 part, two acyl-oxygen heptane two fourths Ji Xi: 1-2 part, borax: 3-5 part, APP heatproof auxiliary agent: 1-2 part, acidic oxidation agent: 5-6 Part, sand streak agent: 7-9 part, fume colloidal silica: 1-2 part, transparent zinc oxide: 3-5 part, flake asbestos: 3-5 part, nano silicon: 10-12 part, chlorinated rubber: 16-18 part, titanium dioxide: 2-5 part, Talcum powder: 6-9 part, barium sulfate: 3-6 part, anti-settling agent: 1-2 part, defoamer: 1-2 part, pigment: 10-12 part, titanium stone white powder: 30-35 part, dictyophora phalloidea: 60-70 part, water: 1000-1100 part, dark plum: 10-15 part, the Radix Astragali: 10-15 part, Poria cocos: 10-15 part, the bulb of fritillary: 10-15 part, Fructus Aurantii: 10-15 part, Radix Angelicae Sinensis: 10-15 part, PVA:50-60 part, starch: 12-15 part, ammoniacal liquor: 5-15 part, AA, AAm are mixed Compound: 0.3-0.4 part, ammonium persulfate: 0.2-0.3 part, ammonium bisulfite: 0.2-0.3 part, polyethylene Alcohol: 10-15 part, crosslinking agent: 0.1-0.2 part, activated magnesia 0.5-1 part, casein: 2-5 part, NaOH: 0.1-0.2 part, hydroquinones: 0.2-0.5 part, alkali lignin: 1-2 part, silane coupler: 0.1-0.2 part.
Mainly comprise the steps that
1) cut into slices after dictyophora phalloidea being cleaned, be immersed in evaporated milk, treat that evaporated milk is absorbed totally by dictyophora phalloidea, take peanut, Grinds, is sprinkled upon on dictyophora phalloidea；
2) being ground by nano silicon, milling time is 60min, and grinding rate is 600 turns/min, Put in reactor；
3) take chlorinated rubber, titanium dioxide, talcum powder, barium sulfate, anti-settling agent, defoamer, pigment, Titanium stone white powder, dictyophora phalloidea, mixing adds in reactor；
4) take in dark plum, the Radix Astragali, Poria cocos, the bulb of fritillary, Fructus Aurantii, Radix Angelicae Sinensis grinds addition cucurbit, add The water of 50%, distillation, collect distilled water；
5) distilled water is added in reactor, filter with the detailed catalogue filter screen of 300 mesh, filter out thicker Particle, pulverize；
6) PVA and 13% water are mixed in addition reactor, within 4 hours, make PVA be completely dissolved with 90 DEG C of stirrings, It is cooled to 75 DEG C, ammonium persulfate, ammonium bisulfite and 2% water are mixed, dropping AA, AAm mixture and mistake Ammonium sulfate, ammonium bisulfite and water mixed solution, drip off for about 1-2 hour, insulation reaction 1 hour, then Add starch, continue to add thermal agitation 1 hour, add silane coupler stirring, drop to less than 50 DEG C to temperature, With discharging after ammoniacal liquor regulation pH value；
7) water taking polyvinyl alcohol, activated magnesia and 10% carries out mix and blend, and temperature controls 90-92 DEG C, treat that polyvinyl alcohol, activated magnesia are dissolved completely in water, be cooled to 65-70 DEG C, add The water insulation reaction of casein, alkali lignin, hydroquinones and 5% 2 hours, is subsequently adding crosslinking agent and 5% Water, continues insulation reaction 1 hour, and dropping NaOH and the water mixed liquid of 5% stir 5-10 minute；
8) by step 6) and step 7) gained mixture is in step 5) granular powder mixing；
9) take terminal hydroxy group dimethyl silicone rubber, TGIC curing agent, two acyl-oxygen heptane dibutyl tins, boron simultaneously Sand, APP heatproof auxiliary agent, acidic oxidation agent, sand streak agent, fume colloidal silica, transparent zinc oxide, Flake asbestos, grinds, and the water adding 10% adds hot mixing；
10) finally by step 9) gained mixture addition step 8) in, stirring obtains coating.
The invention has the beneficial effects as follows: coating prepared by this law, free from extraneous odour, content of formaldehyde is far below country Standard, discharges a kind of exclusive fragrance simultaneously, it is adaptable to use on family's household electrical appliances and furniture, high temperature resistant, Cold tolerance is high, effectively solves the deficiency of existing coating.
Detailed description of the invention:
For the technological means making the present invention realize, creation characteristic, reach purpose and effect and be readily apparent from Solve, below in conjunction with specific embodiment, the present invention is expanded on further.
Specific embodiment 1: a kind of high-temperature resistant coating, is mainly composed of the following components in parts by weight:
Terminal hydroxy group dimethyl silicone rubber: 10 parts, TGIC curing agent: 2 parts, two acyl-oxygen heptane dibutyl tins: 1 part, borax: 3 parts, APP heatproof auxiliary agent: 1 part, acidic oxidation agent: 5 parts, sand streak agent: 7 parts, Fume colloidal silica: 1 part, transparent zinc oxide: 3 parts, flake asbestos: 3 parts, nano silicon: 10 parts, Chlorinated rubber: 16 parts, titanium dioxide: 2 parts, talcum powder: 6 parts, barium sulfate: 3 parts, anti-settling agent: 1 Part, defoamer: 1 part, pigment: 10 parts, titanium stone white powder: 30 parts, dictyophora phalloidea: 60 parts, water: 1000 parts, Dark plum: 10 parts, the Radix Astragali: 10 parts, Poria cocos: 10 parts, the bulb of fritillary: 10 parts, Fructus Aurantii: 10 parts, Radix Angelicae Sinensis: 10 parts, PVA:50 part, starch: 12 parts, ammoniacal liquor: 5 parts, AA, AAm mixture: 0.3 part, over cure Acid ammonium: 0.2 part, ammonium bisulfite: 0.2 part, polyvinyl alcohol: 10 parts, crosslinking agent: 0.1 part, live Property 0.5 part of magnesia, casein: 2 parts, NaOH: 0.1 part, hydroquinones: 0.2 part, alkali wood Element: 1 part, silane coupler: 0.1 part.
Specific embodiment 2: a kind of high-temperature resistant coating, is mainly composed of the following components in parts by weight:
Terminal hydroxy group dimethyl silicone rubber: 15 parts, TGIC curing agent: 3 parts, two acyl-oxygen heptane dibutyl tins: 2 parts, borax: 5 parts, APP heatproof auxiliary agent: 2 parts, acidic oxidation agent: 6 parts, sand streak agent: 9 parts, Fume colloidal silica: 2 parts, transparent zinc oxide: 5 parts, flake asbestos: 5 parts, nano silicon: 12 parts, Chlorinated rubber: 18 parts, titanium dioxide: 5 parts, talcum powder: 9 parts, barium sulfate: 6 parts, anti-settling agent: 2 Part, defoamer: 2 parts, pigment: 12 parts, titanium stone white powder: 35 parts, dictyophora phalloidea: 70 parts, water: 1100 parts, Dark plum: 15 parts, the Radix Astragali: 15 parts, Poria cocos: 15 parts, the bulb of fritillary: 15 parts, Fructus Aurantii: 15 parts, Radix Angelicae Sinensis: 15 parts, PVA:60 part, starch: 15 parts, ammoniacal liquor: 15 parts, AA, AAm mixture: 0.4 part, over cure Acid ammonium: 0.3 part, ammonium bisulfite: 0.3 part, polyvinyl alcohol: 15 parts, crosslinking agent: 0.2 part, activity 1 part of magnesia, casein: 5 parts, NaOH: 0.2 part, hydroquinones: 0.5 part, alkali lignin: 2 Part, silane coupler: 0.2 part.
Mainly comprise the steps that
1) cut into slices after dictyophora phalloidea being cleaned, be immersed in evaporated milk, treat that evaporated milk is absorbed totally by dictyophora phalloidea, take peanut, Grinds, is sprinkled upon on dictyophora phalloidea；
2) being ground by nano silicon, milling time is 60min, and grinding rate is 600 turns/min, Put in reactor；
3) take chlorinated rubber, titanium dioxide, talcum powder, barium sulfate, anti-settling agent, defoamer, pigment, Titanium stone white powder, dictyophora phalloidea, mixing adds in reactor；
4) take in dark plum, the Radix Astragali, Poria cocos, the bulb of fritillary, Fructus Aurantii, Radix Angelicae Sinensis grinds addition cucurbit, add The water of 50%, distillation, collect distilled water；
5) distilled water is added in reactor, filter with the detailed catalogue filter screen of 300 mesh, filter out thicker Particle, pulverize；
6) PVA and 13% water are mixed in addition reactor, within 4 hours, make PVA be completely dissolved with 90 DEG C of stirrings, It is cooled to 75 DEG C, ammonium persulfate, ammonium bisulfite and 2% water are mixed, dropping AA, AAm mixture and mistake Ammonium sulfate, ammonium bisulfite and water mixed solution, drip off for about 1-2 hour, insulation reaction 1 hour, then Add starch, continue to add thermal agitation 1 hour, add silane coupler stirring, drop to less than 50 DEG C to temperature, With discharging after ammoniacal liquor regulation pH value；
7) water taking polyvinyl alcohol, activated magnesia and 10% carries out mix and blend, and temperature controls 90-92 DEG C, treat that polyvinyl alcohol, activated magnesia are dissolved completely in water, be cooled to 65-70 DEG C, add The water insulation reaction of casein, alkali lignin, hydroquinones and 5% 2 hours, is subsequently adding crosslinking agent and 5% Water, continues insulation reaction 1 hour, and dropping NaOH and the water mixed liquid of 5% stir 5-10 minute；
8) by step 6) and step 7) gained mixture is in step 5) granular powder mixing；
9) take terminal hydroxy group dimethyl silicone rubber, TGIC curing agent, two acyl-oxygen heptane dibutyl tins, boron simultaneously Sand, APP heatproof auxiliary agent, acidic oxidation agent, sand streak agent, fume colloidal silica, transparent zinc oxide, Flake asbestos, grinds, and the water adding 10% adds hot mixing；
10) finally by step 9) gained mixture addition step 8) in, stirring obtains coating.
The general principle of the present invention, principal character and advantages of the present invention have more than been shown and described.One's own profession Skilled person will appreciate that of industry, the present invention is not restricted to the described embodiments, above-described embodiment and explanation The principle that the present invention is simply described described in book, without departing from the spirit and scope of the present invention, The present invention also has various changes and modifications, and these changes and improvements both fall within claimed invention model In enclosing.Claimed scope is defined by appending claims and equivalent thereof.

Claims (2)

1. a high-temperature resistant coating, it is characterised in that: mainly it is composed of the following components in parts by weight:
Terminal hydroxy group dimethyl silicone rubber: 10-15 part, TGIC curing agent: 2-3 part, two acyl-oxygen heptane two fourths Ji Xi: 1-2 part, borax: 3-5 part, APP heatproof auxiliary agent: 1-2 part, acidic oxidation agent: 5-6 Part, sand streak agent: 7-9 part, fume colloidal silica: 1-2 part, transparent zinc oxide: 3-5 part, flake asbestos: 3-5 part, nano silicon: 10-12 part, chlorinated rubber: 16-18 part, titanium dioxide: 2-5 part, Talcum powder: 6-9 part, barium sulfate: 3-6 part, anti-settling agent: 1-2 part, defoamer: 1-2 part, pigment: 10-12 part, titanium stone white powder: 30-35 part, dictyophora phalloidea: 60-70 part, water: 1000-1100 part, dark plum: 10-15 part, the Radix Astragali: 10-15 part, Poria cocos: 10-15 part, the bulb of fritillary: 10-15 part, Fructus Aurantii: 10-15 part, Radix Angelicae Sinensis: 10-15 part, PVA:50-60 part, starch: 12-15 part, ammoniacal liquor: 5-15 part, AA, AAm are mixed Compound: 0.3-0.4 part, ammonium persulfate: 0.2-0.3 part, ammonium bisulfite: 0.2-0.3 part, polyethylene Alcohol: 10-15 part, crosslinking agent: 0.1-0.2 part, activated magnesia 0.5-1 part, casein: 2-5 part, NaOH: 0.1-0.2 part, hydroquinones: 0.2-0.5 part, alkali lignin: 1-2 part, silane coupler: 0.1-0.2 part.
2. according to a kind of high-temperature resistant coating described in claim 1, it is characterised in that: mainly include with Lower step:
1) cut into slices after dictyophora phalloidea being cleaned, be immersed in evaporated milk, treat that evaporated milk is absorbed totally by dictyophora phalloidea, take peanut, Grinds, is sprinkled upon on dictyophora phalloidea；
2) being ground by nano silicon, milling time is 60min, and grinding rate is 600 turns/min, Put in reactor；
3) take chlorinated rubber, titanium dioxide, talcum powder, barium sulfate, anti-settling agent, defoamer, pigment, Titanium stone white powder, dictyophora phalloidea, mixing adds in reactor；
4) take in dark plum, the Radix Astragali, Poria cocos, the bulb of fritillary, Fructus Aurantii, Radix Angelicae Sinensis grinds addition cucurbit, add The water of 50%, distillation, collect distilled water；
5) distilled water is added in reactor, filter with the detailed catalogue filter screen of 300 mesh, filter out thicker Particle, pulverize；
6) PVA and 13% water are mixed in addition reactor, within 4 hours, make PVA be completely dissolved with 90 DEG C of stirrings, It is cooled to 75 DEG C, ammonium persulfate, ammonium bisulfite and 2% water are mixed, dropping AA, AAm mixture and mistake Ammonium sulfate, ammonium bisulfite and water mixed solution, drip off for about 1-2 hour, insulation reaction 1 hour, then Add starch, continue to add thermal agitation 1 hour, add silane coupler stirring, drop to less than 50 DEG C to temperature, With discharging after ammoniacal liquor regulation pH value；
7) water taking polyvinyl alcohol, activated magnesia and 10% carries out mix and blend, and temperature controls 90-92 DEG C, treat that polyvinyl alcohol, activated magnesia are dissolved completely in water, be cooled to 65-70 DEG C, add The water insulation reaction of casein, alkali lignin, hydroquinones and 5% 2 hours, is subsequently adding crosslinking agent and 5% Water, continues insulation reaction 1 hour, and dropping NaOH and the water mixed liquid of 5% stir 5-10 minute；
8) by step 6) and step 7) gained mixture is in step 5) granular powder mixing；
9) take terminal hydroxy group dimethyl silicone rubber, TGIC curing agent, two acyl-oxygen heptane dibutyl tins, boron simultaneously Sand, APP heatproof auxiliary agent, acidic oxidation agent, sand streak agent, fume colloidal silica, transparent zinc oxide, Flake asbestos, grinds, and the water adding 10% adds hot mixing；
10) finally by step 9) gained mixture addition step 8) in, stirring obtains coating.
CN201610304294.6A 2016-05-06 2016-05-06 High-temperature-resistant coating material and preparation method thereof Pending CN105907221A (en)

Priority Applications (1)

Application Number Priority Date Filing Date Title
CN201610304294.6A CN105907221A (en) 2016-05-06 2016-05-06 High-temperature-resistant coating material and preparation method thereof

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
CN201610304294.6A CN105907221A (en) 2016-05-06 2016-05-06 High-temperature-resistant coating material and preparation method thereof

Publications (1)

Publication Number Publication Date
CN105907221A true CN105907221A (en) 2016-08-31

Family

ID=56747954

Family Applications (1)

Application Number Title Priority Date Filing Date
CN201610304294.6A Pending CN105907221A (en) 2016-05-06 2016-05-06 High-temperature-resistant coating material and preparation method thereof

Country Status (1)

Country Link
CN (1) CN105907221A (en)

Cited By (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN110903756A (en) * 2019-11-22 2020-03-24 国网江西省电力有限公司电力科学研究院 Intelligent temperature-sensing color-changing RTV coating and preparation method thereof

Citations (4)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN103965752A (en) * 2014-05-06 2014-08-06 张家港江南粉末涂料有限公司 High-temperature-resistant powder coating with good gloss-retention performance and production method thereof
CN104099054A (en) * 2014-06-30 2014-10-15 安徽神舟飞船胶业有限公司 Formula for acrylic acid-polyurethane copolymerized and modified starch adhesive and preparation technology thereof
CN104387877A (en) * 2014-11-06 2015-03-04 浙江兄弟路标涂料有限公司 Color steel tile paint
CN105385165A (en) * 2015-11-30 2016-03-09 安徽省界首市云龙粮机配套工程有限公司 Preparation method of toxin-free environment-friendly composite conveyor belt

Patent Citations (4)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN103965752A (en) * 2014-05-06 2014-08-06 张家港江南粉末涂料有限公司 High-temperature-resistant powder coating with good gloss-retention performance and production method thereof
CN104099054A (en) * 2014-06-30 2014-10-15 安徽神舟飞船胶业有限公司 Formula for acrylic acid-polyurethane copolymerized and modified starch adhesive and preparation technology thereof
CN104387877A (en) * 2014-11-06 2015-03-04 浙江兄弟路标涂料有限公司 Color steel tile paint
CN105385165A (en) * 2015-11-30 2016-03-09 安徽省界首市云龙粮机配套工程有限公司 Preparation method of toxin-free environment-friendly composite conveyor belt

Cited By (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN110903756A (en) * 2019-11-22 2020-03-24 国网江西省电力有限公司电力科学研究院 Intelligent temperature-sensing color-changing RTV coating and preparation method thereof
CN110903756B (en) * 2019-11-22 2022-03-11 国网江西省电力有限公司电力科学研究院 Intelligent temperature-sensing color-changing RTV coating and preparation method thereof

Similar Documents

Publication Publication Date Title
CN105271918A (en) Cement grinding aid and preparation method thereof
CN106588108A (en) Building heat preservation material
CN107283588B (en) A kind of preparation method of anti-aging sleeper composite material
CN105505093B (en) A kind of environment-friendly type glass baking varnish and preparation method thereof
CN105038325A (en) Deodorant iron oxide black pigment and preparation method thereof
CN105831399B (en) A kind of probiotic feed additive and its production method and application
CN105907222A (en) High-temperature-resistant heat-insulating exterior wall coating material and preparation method thereof
CN105907221A (en) High-temperature-resistant coating material and preparation method thereof
CN104312535A (en) Lignin weatherproof fiberboard adhesive and production method thereof
CN105936778A (en) Delicate-fragrance and environmental-protection aqueous coating and preparation method thereof
CN105086519A (en) Antibacterial and bacteriostatic ferric oxide black pigment and preparation method thereof
CN103588419B (en) Method for preparing quartz plate with changeable colors
CN105820672A (en) Household appliance anticorrosive coating and preparation method thereof
CN105038323A (en) Parasite-dispelling iron oxide black pigment and preparation method thereof
CN105369595A (en) Production process of velcro cloth
CN105885498A (en) Antiseptic paint for inner wall of automotive water tank and preparation method of antiseptic paint
CN104388044A (en) High-adhesive-strength lignin fiberboard adhesive and production method thereof
CN105176452A (en) Preparation method for adhesive
CN105820671A (en) Paint with anti-corrosion, safe and reliable base material and preparation method thereof
CN105925076A (en) Coldproof paint for furniture and preparing method thereof
CN102337013B (en) Modified epoxy resin plate
CN106880795A (en) One kind relaxes bowel snakegourd fruit tea and preparation method thereof
CN106221475A (en) A kind of novel environment friendly water-repellent paint
CN105820696A (en) Coating for household appliance finishing degree and gloss retention and preparation method thereof
CN104293288A (en) Lignin thermostable fiberboard adhesive and producing method thereof

Legal Events

Date Code Title Description
C06 Publication
PB01 Publication
C10 Entry into substantive examination
SE01 Entry into force of request for substantive examination
RJ01 Rejection of invention patent application after publication

Application publication date: 20160831

RJ01 Rejection of invention patent application after publication