CN105886122A - Lucid ganoderma essential oil and preparation method thereof - Google Patents
Lucid ganoderma essential oil and preparation method thereof Download PDFInfo
- Publication number
- CN105886122A CN105886122A CN201410735282.XA CN201410735282A CN105886122A CN 105886122 A CN105886122 A CN 105886122A CN 201410735282 A CN201410735282 A CN 201410735282A CN 105886122 A CN105886122 A CN 105886122A
- Authority
- CN
- China
- Prior art keywords
- essential oil
- ganoderma
- glossy ganoderma
- ganoderma lucidum
- extraction
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Pending
Links
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- Medicines Containing Plant Substances (AREA)
- Coloring Foods And Improving Nutritive Qualities (AREA)
Abstract
The invention discloses lucid ganoderma essential oil and a preparation method thereof, belonging to the technical field of essential oil and preparation thereof. The essential oil is refined from lucid ganoderma; the preparation process specifically comprises the following steps of: raw material screening, raw material purifying, raw material breaking, extraction of lucid ganoderma essential oil, purification of lucid ganoderma essential oil and blending of lucid ganoderma essential oil, wherein the small-molecular volatile lucid ganoderma essential oil and macromolecular non-volatile lucid ganoderma essential oil are proportionally mixed after the extraction of lucid ganoderma essential oil to obtain a product of pure lucid ganoderma essential oil, and the mixing ratio is 1:(0.25-5.5); finally, the pure lucid ganoderma essential oil is extracted. In the invention, the defects of existing lucid ganoderma application method are perfectly solved, and the active ingredients in the lucid ganoderma are fully extracted by scientific method and flow; the composition of the lucid ganoderma essential oil can be detected and matched and is more scientific; and moreover, the development idea and way of the lucid ganoderma industry are opened up, and a great effect is realized on promoting the industrial value of the lucid ganoderma industry.
Description
Technical field
The invention belongs to essential oil and preparing technical field thereof, particularly relate to glossy ganoderma essential oil and preparation method thereof.
Background technology
Glossy ganoderma is the distinctive a kind of fungi plant of China, has higher medical value, over the past thousands of years, one
Directly be commonly used by people for curing the disease, health, be also widely used in tcm prescription, obtain the generally happiness of people
Like.After glossy ganoderma grows into the stage of ripeness, a large amount of Reishi sporule can be sprayed on fructification canopy, thus clever
Sesame had both contained fructification and also contains Reishi sporule.Draw from current scientific research is analyzed, glossy ganoderma
In principle active component have: ganoderma lucidum triterpene, GL-B, glossy ganoderma nucleosides, glossy ganoderma sterol, glossy ganoderma
Amino acid, trace element etc., wherein: ganoderma lucidum triterpene compounds has isolated up to kind more than 130,
Including: ganoderic acid A, B, C, D, E, G, I, L, Ma, Mb, Mc, Md, Mg etc.；Red
Sesame acid A, B, C, D, E, F, O；Ganoderic acid Dm etc.；GL-B, comprises: D-grape
The group such as sugar, D-galactolipin, D-MANNOSE, D-wood sugar, L-fucose, L-rhamnose, Arabinose
Becoming, concrete composition repeats the most one by one；Glossy ganoderma nucleosides, comprises: glossy ganoderma glycosides, adenosine, urine are fast
The compounds etc. such as purine nucleosides, ganoderpurine, ganoine Ⅰ, ganoine Ⅱ, choline, glycine betaine, nicotinic acid；
Glossy ganoderma sterol (alkene), has kind more than 20, comprise ergosterol and cholesterine, ergosterol palmitate,
5a-stigmastane-3, ergot steroid-7,22-diene-3-ketone, 6a-triol, 22-triolefin, 22-tetraene-3-alcohol etc.；
Amino Acid of Glossy ganoderma and polypeptide, comprise: asparatate, glutamic acid, arginine, lysine, ornithine,
Proline, alanine, glycine, serine, threonine, etc. kind more than 20；Trace element, bag
Contain: organic germanium and Organic Selenium, molybdenum, zinc, cadmium, cobalt, nickel, manganese, iron, phosphorus, boron, magnesium, calcium, copper
Deng, it is all to be present in glossy ganoderma with organic compound form.Due to current people to the use of glossy ganoderma,
Processing mode is the most single, it is common that directly steep in wine the most treated for fructification, or glossy ganoderma is real
Body section, chopping, dice, beat powder for steeping in wine, making tea, stew water, it is the most first that these make usage also be in
Level, simple, coarse stage, the utilizing status simultaneously for effective component of glossy ganoderma is the most very poor.
What is essential oil？Very to make detailed inquiries, also may not be certain someone can demonstrate.People hear essential oil and make
Also, after being reform and opening-up with essential oil, present essential oil is the most less popularized.What a lot of people also do not know about
It is essential oil, daily life is understood the channel of essential oil, most of still from SPA beauty parlour,
Or the service of cosmetics company and product introduction learn one or two, due to for self commercial interest
Consideration, these information are grossly inaccurate often, for example, SPA beauty parlour presses for health
The oils rubbed, they also would generally be said to be essential oil, be the most many times artificial oil and essence, no
Being essential oil truly, essential oil is the difficult extraction of comparison, and the essential oil content of plant own is also little,
Can not as SPA beauty parlour one barrel one barrel bring use；Essence in the cosmetics of cosmetics company
Oil content is typically all little, and the dispensing usually used as cosmetics uses；It is exactly also to against on the market
The essential oil of the small bottle packing of various plates, essential oil quality the most on the market is very different, and some is artificial oil
Add essence, some is the less essential oil of content, is to dilute through substrate oil, in general international top-brand
Essential oil is also possible from content to quality, but expensive.Essential oil the most truly is on earth
What？The definition the most generally assert is: essential oil can also be referred to as volatile oil, and English is
essentialoils；Be not common oils common oils English be oil；Essential oil is present in plant
One class have aromatic odor, can out and the volatility oily the most miscible with water becomes with steam distillation
The general name divided；Volatile oil is mixture, and its component is complex；How with terpene, alkene in volatile oil component
Class, alcohols, phenols is common, typically possibly together with little molecule aliphatic compounds and little molecule aromatic compound；
Various volatile oil all have certain optical activity and index of refraction, and index of refraction is that the important of volatile oil Quality Identification depends on
According to, the index of refraction of general volatile oil is all between 1.450～1.560.Abroad for the exploitation of plants essential oil
Being the most deep, especially US and European, the essential oil developed now has kind more than 100, example
If any: clove oil, cardamom essential oil, Chinese ilex essential oil, white birch essential oil, cdear essential oil, ginger essential oil etc.
Deng, the most under development.Wherein ginger is that China originates in plant, and before 2500, Confucius said:
" do not remove ginger food, seldom food ".I other words on each dining table, it is necessary to ginger to be had is eaten, but regular meal
All can not eat ginger, this is the long-lived secret recipe that Confucius oneself says, the regrettably patent of ginger essential oil more
Rest in American-European company hand；Cloves original producton location in Indonesia Ma Luji archipelago, clove oil special
Profit is also in the hand of American-European company；Such example is too numerous to enumerate.Glossy ganoderma essential oil is not only that I passes through
Long-term study and research institute to glossy ganoderma obtain, and are the most more intended to a kind of resource that centering state endemic species is taked
Protected mode, is got ahead of others by American-European company the most again.
Summary of the invention
In view of above-mentioned the deficiencies in the prior art, it is an object of the invention to provide glossy ganoderma essential oil and preparation side thereof
Method, by the way of distillation and the pure glossy ganoderma essential oil of solvent extraction combined extraction, without flux oil, substrate oil
With other Prof. Du Yucang composition.
The technical solution used in the present invention is to achieve these goals: a kind of glossy ganoderma essential oil and preparation side thereof
Method, uses glossy ganoderma to refine essential oil, and detailed preparation process is:
The first step, raw material screening: lucidum variety selects red sesame and purple sesame, selection maturation woodization
Ganoderma lucidum fruitbody, and go, unless plant of ganoderma lucidum impurity, to remove the rotten individual and individuality of form alienation；Choosing
Shape-selective state is complete, and the glossy ganoderma of full color is individual；
Second step, purification of raw materials: by raw material ganoderma lucidum fruitbody, through the screening of impurity screening machine and vibrations
Separate, the grains of sand and large granular impurity are removed；By raw material ganoderma lucidum fruitbody, clean through cleaning machine,
Again by little granule foreign and dust, and other impurity cleans up；By the ganoderma lucidum fruitbody through over cleaning,
It is dried process through air-dry machine, low temperature drying room；By through over cleaning, the dry ganoderma lucidum fruitbody processed, protect
Hold dry, low temperature storage, mildew-resistant anti-metamorphic；
3rd step, raw material are broken: use closed disintegrating machine, glossy ganoderma that will process through purge drying
Entity carries out break process, and this crumbling method is cryogenic pulverization, and breaking temperature controls at subzero 5 degrees Celsius
Between 5 degrees Celsius above freezing；The purpose of cryogenic pulverization is to produce higher temperature, from without making
Become effective component of glossy ganoderma volatilization；Broken standard controls, the ganoderma lucidum fruitbody particle diameter control after broken
System is between 0.1 millimeter to 1.5 millimeter；
4th step, extracting ganoderma essential oil: through above-mentioned 3 steps, the ganoderma lucidum fruitbody particle handled well
Raw material, uses steam distillation and extraction method, solvent extraction and resin extraction method to carry out extraction of essential oil；
5th step, purification glossy ganoderma essential oil: in order to obtain purer glossy ganoderma essential oil, use vacuum distillation extraction
Follow the example of, purify glossy ganoderma essential oil；Vacuumizing can reduce boiling point, it is easier to separate impurity, be essential oil again
The method of refining；Glossy ganoderma essential oil is placed in destilling tower, ebuillition of heated, heating high temperature steam not with essential oil
Contact, but directly heat destilling tower；The gas that the boiling of glossy ganoderma essential oil produces, after condenser condenses,
The glossy ganoderma essential oil more purified；Little molecule, volatile glossy ganoderma has been obtained through steam distillation and extraction method
Essential oil；The big molecule the most volatile ganoderma lucidum essence oil that solvent extraction, resin extraction method obtain；Little molecule,
Volatile glossy ganoderma essential oil and big molecule the most volatile ganoderma lucidum essence oil obtain after vacuum distillation method purifies processing
Purer glossy ganoderma essential oil；
6th step, glossy ganoderma essential oil are allocated: little molecule, volatile glossy ganoderma essential oil and big molecule, the most volatile
Glossy ganoderma essential oil proportionally mixes after purifying glossy ganoderma essential oil, obtains pure ganoderma lucidum essence oil product, mixing ratio
Example is: 1: 0.25～5.5, has finally extracted pure glossy ganoderma essential oil.
Described steam distillation and extraction method includes: 1, live steam reclaiming process: the ganoderma lucidum fruitbody particle that will handle well
Raw material is positioned in destilling tower, then by high-temperature steam bottom destilling tower directly into ganoderma lucidum fruitbody
In grain raw material, making ganoderma lucidum fruitbody particle fully mix with high-temperature steam, seethe, boiling vapour is through condensation
Device, changes into liquid, i.e. may separate out ganoderma lucidum essence oil and the water reclaimed, i.e. obtain in oil water separator
Pure glossy ganoderma essential oil；2, indirect steam method: the ganoderma lucidum fruitbody particulate material handled well is positioned over destilling tower
In, then heat destilling tower with high-temperature steam, make ganoderma lucidum fruitbody particle produce high temperature, simultaneously glossy ganoderma
Substance particles volatilizes gas, and gas, through condenser, changes into liquid, in oil water separator
Isolate the water of glossy ganoderma essential oil and recovery, i.e. obtain pure glossy ganoderma essential oil；It is extracted into through vapor distillation method
Glossy ganoderma essential oil, main component has: ganoderma lucidum triterpene compounds, glossy ganoderma sterol (alkene), part glossy ganoderma nucleosides；
This part active ingredient compound, under the effect of high-temperature steam, is easier to evaporate, through certain
The effect of the high-temperature steam of time, this part active ingredient compound overwhelming majority can be from ganoderma lucidum fruitbody
Particle is separated；Ganoderma lucidum fruitbody particle also has the active ingredient compound that moieties is bigger then
Need to extract by common solvent method.
Described solvent extraction is: use vapor distillation method stripped ganoderma lucidum fruitbody particulate material, then
Through solvent extraction come extracting ganoderma fructification particle Middle molecule form more greatly, the most volatile effective one-tenth
Differentiation compound, so can fully extract the active ingredient in ganoderma lucidum fruitbody particle, make full use of resource；
Ganoderma lucidum fruitbody particle is positioned in extraction tower, is fully contacted with solvent, dissolve ganoderma lucidum fruitbody
Bigger molecule active ingredient compound in Li；The mixed liquor of solvent and active ingredient is transported to evaporating column,
Through heating, after solvent evaporation relatively low for boiling point, enter back into essential oil evaporating column and residual solvent is evaporated
After Laiing, i.e. obtain pure glossy ganoderma essential oil；Solvent extraction uses non-polar solven, it will usually make oil
Ether or toluene, or other solvent；Through the glossy ganoderma essential oil of common solvent method extraction, main component has:
GL-B, Amino Acid of Glossy ganoderma and polypeptide, part glossy ganoderma nucleosides, trace element, described trace element with
Organic compound form is present in glossy ganoderma.
Described resin extraction method is: owing to solvent extraction compares the consumption energy, resin extraction method consumption energy
Source is less, from the point of view of saving the energy, environmental protection, the most also with resin extraction method extracting ganoderma
Fructification particle Middle molecule forms more greatly, the most volatile active ingredient compound；The mistake of resin extraction method
Cheng You: 1, vapor distillation method stripped ganoderma lucidum fruitbody particulate material will be used to be positioned in extraction tower；
2, in extraction tower, add resin extraction agent, and ganoderma lucidum fruitbody particle is sufficiently stirred for, by ganoderma lucidum fruitbody
Particle Middle molecule forms more greatly, the most volatile active ingredient compound extracts；3, essential oil and solvent
Through filter screen filtration, filtering residue, essential oil enters solvent evaporator, Jing Guojia with the mixing liquid of solvent
Solvent is fallen in thermal evaporation, obtains pure glossy ganoderma essential oil；4, through the glossy ganoderma essential oil of common solvent method extraction, mainly
Composition with the presence of: GL-B, Amino Acid of Glossy ganoderma and polypeptide, part glossy ganoderma nucleosides, with organic form
Trace element in glossy ganoderma.
The invention has the beneficial effects as follows: the present invention well solves the drawback in current glossy ganoderma using method,
And use scientific method and flow process the active ingredient in glossy ganoderma fully to be extracted, ganoderma lucidum essence oil component
Can detect, can proportioning, more scientific；Glossy ganoderma essential oil of the present invention is pure essential oil, and composition is molecular state, can
Directly to be smeared by skin, external application, it is possible to use stacte machine stacte in atmosphere, or be directly administered orally
Deng, said method fundamentally changes, has opened up people's using method to glossy ganoderma, takes full advantage of spirit
The active ingredient of sesame；Owing to the health of people is different, illness is different, therefore different for people
Somatogenic need, glossy ganoderma essential oil can also do different proportionings, makes the using effect of glossy ganoderma essential oil more preferably.This
Thinking of development and the road of glossy ganoderma industry has been opened up in invention, and the industrial value lifting for glossy ganoderma industry has
The biggest effect.
Detailed description of the invention
Below in conjunction with detailed description of the invention, the present invention is illustrated further；
Embodiment 1, a kind of glossy ganoderma essential oil and preparation method thereof, use glossy ganoderma to refine essential oil, prepared in detail
Cheng Wei: the first step, raw material screening: lucidum variety selects red sesame and purple sesame, selection maturation woodization
Ganoderma lucidum fruitbody, and go unless plant of ganoderma lucidum impurity, remove the rotten individual and individuality of form alienation；
Selection form is complete, and the glossy ganoderma of full color is individual；Second step, purification of raw materials: raw material glossy ganoderma is real
Body, separates through the screening of impurity screening machine and vibrations, the grains of sand and large granular impurity is removed；Will
Raw material ganoderma lucidum fruitbody, cleans through cleaning machine, then by little granule foreign and dust, and other impurity
Clean up；By the ganoderma lucidum fruitbody through over cleaning, it is dried process through air-dry machine, low temperature drying room；Will
Through over cleaning, it is dried the ganoderma lucidum fruitbody processed, keeps dry, low temperature storage, mildew-resistant anti-metamorphic；The
Three steps, raw material are broken: use closed disintegrating machine, entered by the ganoderma lucidum fruitbody processed through purge drying
Row break process, this crumbling method is cryogenic pulverization, and breaking temperature controls to arrive above freezing 5 at subzero 5 degrees Celsius
Between degree Celsius；The purpose of cryogenic pulverization is to produce higher temperature, thus does not results in glossy ganoderma and have
Effect composition volatilization；Broken standard controls, and the ganoderma lucidum fruitbody particle diameter after broken controls at 0.1 milli
Rice is between 1.5 millimeters；4th step, extracting ganoderma essential oil: through above-mentioned 3 steps, the spirit handled well
Sesame fructification particulate material, uses steam distillation and extraction method, solvent extraction and resin extraction method to carry out essence
Oil extracts；5th step, purification glossy ganoderma essential oil: in order to obtain purer glossy ganoderma essential oil, use vacuum to steam
Evaporate extraction, purify glossy ganoderma essential oil；Vacuumizing can reduce boiling point, it is easier to separates impurity, is essence
The method that oil refines again；Glossy ganoderma essential oil is placed in destilling tower, ebuillition of heated, heating high temperature steam not with
Essential oil contacts, but directly heats destilling tower；The gas that the boiling of glossy ganoderma essential oil produces, cold through condenser
After Ning, the glossy ganoderma essential oil more purified；Little molecule, Yi Hui has been obtained through steam distillation and extraction method
Send out glossy ganoderma essential oil；The big molecule the most volatile ganoderma lucidum essence oil that solvent extraction, resin extraction method obtain；Little
Molecule, volatile glossy ganoderma essential oil and big molecule the most volatile ganoderma lucidum essence oil purify processing through vacuum distillation method
After obtained purer glossy ganoderma essential oil；6th step, glossy ganoderma essential oil are allocated: little molecule, volatile glossy ganoderma
Essential oil and big molecule, the most volatile ganoderma lucidum essence oil proportionally mix after purifying glossy ganoderma essential oil, obtain
Pure ganoderma lucidum essence oil product, mixed proportion is: 1: 1.
Embodiment 2: little molecule volatile glossy ganoderma essential oil and the mixed proportion of big molecule the most volatile ganoderma lucidum essence oil
It is 1: 2.
Embodiment 3: little molecule volatile glossy ganoderma essential oil and the mixed proportion of big molecule the most volatile ganoderma lucidum essence oil
It is 1: 3.
Embodiment 4: little molecule volatile glossy ganoderma essential oil and the mixed proportion of big molecule the most volatile ganoderma lucidum essence oil
It is 1: 4.
Embodiment 5: little molecule volatile glossy ganoderma essential oil and the mixed proportion of big molecule the most volatile ganoderma lucidum essence oil
It is 2: 1.
Embodiment 6: little molecule volatile glossy ganoderma essential oil and the mixed proportion of big molecule the most volatile ganoderma lucidum essence oil
It is 3: 1.
Embodiment 7: little molecule volatile glossy ganoderma essential oil and the mixed proportion of big molecule the most volatile ganoderma lucidum essence oil
It is 4: 1.
Last it is noted that obvious, above-described embodiment is only by clearly demonstrating what the present invention was made
Citing, and not restriction to embodiment.For those of ordinary skill in the field, upper
State bright on the basis of can also make other changes in different forms, that is thus extended out is aobvious
And the change being clear to or variation still in protection scope of the present invention among.
Claims (4)
1. glossy ganoderma essential oil and preparation method thereof, feature is to use glossy ganoderma to refine essential oil, detailed preparation process
For: the first step, raw material screening: lucidum variety selects red sesame and purple sesame, selection maturation wood
The ganoderma lucidum fruitbody changed, and go, unless plant of ganoderma lucidum impurity, to remove rotten individual and form alienation
Individual；Selection form is complete, and the glossy ganoderma of full color is individual；Second step, purification of raw materials: by former
Material ganoderma lucidum fruitbody, separates through the screening of impurity screening machine and vibrations, by the grains of sand and big
Grain impurity removes；By raw material ganoderma lucidum fruitbody, clean through cleaning machine, then by little granule foreign and
Dust, and other impurity cleans up；By the ganoderma lucidum fruitbody through over cleaning, through air-dry machine,
Low temperature drying room is dried process；By through over cleaning, be dried process ganoderma lucidum fruitbody, keep be dried,
Low temperature stores, mildew-resistant anti-metamorphic；3rd step, raw material are broken: use closed disintegrating machine, will be through
The ganoderma lucidum fruitbody crossing purge drying process carries out break process, and this crumbling method is cryogenic pulverization,
Breaking temperature controls between subzero 5 degrees Celsius to 5 degrees Celsius above freezing；The purpose of cryogenic pulverization exists
In producing higher temperature, thus do not result in effective component of glossy ganoderma volatilization；Broken standard controls,
Ganoderma lucidum fruitbody particle diameter after broken controls between 0.1 millimeter to 1.5 millimeter；The
Four steps, extracting ganoderma essential oil: through above-mentioned 3 steps, the ganoderma lucidum fruitbody granular raw handled well
Material, uses steam distillation and extraction method, solvent extraction and resin extraction method to carry out extraction of essential oil；The
Five steps, purification glossy ganoderma essential oil: in order to obtain purer glossy ganoderma essential oil, use vacuum distillation extraction
Method, purifies glossy ganoderma essential oil；Vacuumizing can reduce boiling point, it is easier to separates impurity, is essential oil
The method refined again；Being placed in destilling tower by glossy ganoderma essential oil, ebuillition of heated, heating high temperature steam is not
Contact with essential oil, but directly heat destilling tower；The gas that the boiling of glossy ganoderma essential oil produces, through supercooling
After condenser condensation, the glossy ganoderma essential oil more purified；Obtain little through steam distillation and extraction method
Molecule, volatile glossy ganoderma essential oil；The big molecule that solvent extraction, resin extraction method obtain is difficult to wave
Send out glossy ganoderma essential oil；Little molecule, volatile glossy ganoderma essential oil and big molecule the most volatile ganoderma lucidum essence oil pass through
Vacuum distillation method has obtained purer glossy ganoderma essential oil after purifying processing；6th step, glossy ganoderma essential oil are adjusted
Join: little molecule, volatile glossy ganoderma essential oil and big molecule, the most volatile ganoderma lucidum essence oil are through purifying spirit
Proportionally mixing after sesame essential oil, obtain pure ganoderma lucidum essence oil product, mixed proportion is: 1: 0.25～5.5；
Finally extract pure glossy ganoderma essential oil.
Glossy ganoderma essential oil the most according to claim 1 and tool preparation method, is characterized in that described steam distillation
1., live steam reclaiming process extraction includes:: be positioned over by the ganoderma lucidum fruitbody particulate material handled well
In destilling tower, then by high-temperature steam bottom destilling tower directly into ganoderma lucidum fruitbody particulate material
In, make ganoderma lucidum fruitbody particle fully mix with high-temperature steam, seethe, boiling vapour through condenser,
Change into liquid, oil water separator i.e. may separate out ganoderma lucidum essence oil and the water reclaimed, i.e. obtain
Pure glossy ganoderma essential oil；2., indirect steam method: the ganoderma lucidum fruitbody particulate material handled well is positioned over
In destilling tower, then heat destilling tower with high-temperature steam, make ganoderma lucidum fruitbody particle produce high temperature,
Ganoderma lucidum fruitbody particle volatilizes gas simultaneously, and gas, through condenser, changes into liquid, at oil
Separator i.e. may separate out ganoderma lucidum essence oil and the water reclaimed, i.e. obtain pure glossy ganoderma essential oil；Pass through
The glossy ganoderma essential oil that vapor distillation method is extracted into, main component has: ganoderma lucidum triterpene compounds, glossy ganoderma
Sterol, part glossy ganoderma nucleosides；This part active ingredient compound under the effect of high-temperature steam, than
It is easier to evaporate, through the effect of the high-temperature steam of certain time, this part active ingredient
The compound overwhelming majority can be separated from ganoderma lucidum fruitbody particle；In ganoderma lucidum fruitbody particle also
The active ingredient compound having moieties bigger then needs to extract by common solvent method.
Glossy ganoderma essential oil the most according to claim 1 and preparation method thereof, is characterized in that described solvent extraction
Method is: use vapor distillation method stripped ganoderma lucidum fruitbody particulate material, then through solvent extraction
Method come extracting ganoderma fructification particle Middle molecule form more greatly, the most volatile active ingredient chemical combination
Thing, so can fully extract the active ingredient in ganoderma lucidum fruitbody particle, make full use of resource；Will
Ganoderma lucidum fruitbody particle is positioned in extraction tower, is fully contacted with solvent, dissolves ganoderma lucidum fruitbody
Bigger molecule active ingredient compound in particle；The mixed liquor of solvent and active ingredient is transported to
Evaporating column, through heating, after solvent evaporation relatively low for boiling point, enters back into essential oil evaporating column by residual
After remaining solvent is evaporated, i.e. obtain pure glossy ganoderma essential oil；Solvent extraction uses nonpolar molten
Agent, it will usually make petroleum ether or toluene, or other solvent；Spirit through the extraction of common solvent method
Sesame essential oil, main component has: GL-B, Amino Acid of Glossy ganoderma and polypeptide, part glossy ganoderma nucleosides,
Trace element, described trace element is present in glossy ganoderma with organic compound form.
Glossy ganoderma essential oil the most according to claim 1 and preparation method thereof, is characterized in that described resin extraction
Method is: owing to solvent extraction compares the consumption energy, it is less, from joint that resin extraction method consumes the energy
About from the point of view of the energy, environmental protection, the most also by resin extraction method extracting ganoderma fructification
Grain Middle molecule forms more greatly, the most volatile active ingredient compound；The process of resin extraction method has:
1., vapor distillation method stripped ganoderma lucidum fruitbody particulate material will be used to be positioned in extraction tower；
2., in extraction tower, add resin extraction agent, and ganoderma lucidum fruitbody particle is sufficiently stirred for, by glossy ganoderma
Fructification particle Middle molecule forms more greatly, the most volatile active ingredient compound extracts；③、
Essential oil and solvent, through filter screen filtration, filter residue, and essential oil enters solvent with the mixing liquid of solvent
Evaporating column, falls solvent through heating evaporation, obtains pure glossy ganoderma essential oil；4., through common solvent method
The glossy ganoderma essential oil of extraction, main component has: GL-B, Amino Acid of Glossy ganoderma and polypeptide, part spirit
Sesame nucleosides, the trace element being present in glossy ganoderma with organic form.
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| CN106590937A (en) * | 2017-02-09 | 2017-04-26 | 陈亚海 | Process of extracting ganoderma lucidum essential oil by virtue of leaching method |
| CN107686774A (en) * | 2017-10-24 | 2018-02-13 | 安徽恒达药业有限公司 | A kind of extracting method of Peppermint essential oil |
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| 陈世珍: "天然香精油的萃取方法及其应用", 《精细与专用化学》 * |
Cited By (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN106590937A (en) * | 2017-02-09 | 2017-04-26 | 陈亚海 | Process of extracting ganoderma lucidum essential oil by virtue of leaching method |
| CN107686774A (en) * | 2017-10-24 | 2018-02-13 | 安徽恒达药业有限公司 | A kind of extracting method of Peppermint essential oil |
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Application publication date: 20160824 |