CN106190577A - A kind of preparation method of MEIGUI CHUNLU - Google Patents
A kind of preparation method of MEIGUI CHUNLU Download PDFInfo
- Publication number
- CN106190577A CN106190577A CN201610665053.4A CN201610665053A CN106190577A CN 106190577 A CN106190577 A CN 106190577A CN 201610665053 A CN201610665053 A CN 201610665053A CN 106190577 A CN106190577 A CN 106190577A
- Authority
- CN
- China
- Prior art keywords
- flos rosae
- preparation
- meigui chunlu
- rugosas pollen
- meigui
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
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Classifications
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11B—PRODUCING, e.g. BY PRESSING RAW MATERIALS OR BY EXTRACTION FROM WASTE MATERIALS, REFINING OR PRESERVING FATS, FATTY SUBSTANCES, e.g. LANOLIN, FATTY OILS OR WAXES; ESSENTIAL OILS; PERFUMES
- C11B9/00—Essential oils; Perfumes
- C11B9/02—Recovery or refining of essential oils from raw materials
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11B—PRODUCING, e.g. BY PRESSING RAW MATERIALS OR BY EXTRACTION FROM WASTE MATERIALS, REFINING OR PRESERVING FATS, FATTY SUBSTANCES, e.g. LANOLIN, FATTY OILS OR WAXES; ESSENTIAL OILS; PERFUMES
- C11B9/00—Essential oils; Perfumes
- C11B9/02—Recovery or refining of essential oils from raw materials
- C11B9/027—Recovery of volatiles by distillation or stripping
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- Chemical & Material Sciences (AREA)
- Life Sciences & Earth Sciences (AREA)
- Engineering & Computer Science (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Oil, Petroleum & Natural Gas (AREA)
- Wood Science & Technology (AREA)
- Organic Chemistry (AREA)
- Fats And Perfumes (AREA)
Abstract
The invention discloses the preparation method of a kind of MEIGUI CHUNLU, comprise the steps: that the Flos Rosae Rugosae of fresh harvesting is carried out lyophilization by (1), be 10% to average moisture content；(2) Flos Rosae Rugosae carries out pulverization process, prepares Flos Rosae Rugosas pollen；(3) by the mass ratio of Flos Rosae Rugosas pollen, Sal and water be 1:0.05:6 put into distillating still distill；(4) being cooled down by distillation, import oil water separator and separate, collect upper oil phase and lower floor's aqueous phase, lower floor's aqueous phase is described MEIGUI CHUNLU.Use the MEIGUI CHUNLU stay in grade that the method prepares, and low for equipment requirements, simple to operate, easy industrialized production.
Description
Technical field
The invention belongs to plant hydrosol extractive technique field, be specifically related to the preparation method of a kind of MEIGUI CHUNLU.
Background technology
MEIGUI CHUNLU is the side-product in Flos Rosae Rugosae quintessence oil production process, and its fragrance is simple and elegant, rich in multiple useful to human body
Composition, has the effects such as antiallergic, antiinflammatory, sterilization, is widely used in cosmetics of everyday use.Flos Rosae Rugosae quintessence oil and the preparation side of hydrosol at present
Method mainly has three kinds: (1) steam distillation；(2) carbon dioxide supercritical fluid extraction；(3) organic solvent extraction.
Conventional steam distillation, distillation time is long, and vapo(u)rizing temperature is high, and the fragrance loss of quintessence oil and hydrosol has a strong impact on
Product quality, and yield is low.
Carbon dioxide supercritical fluid extraction has ensured in terms of product yield and quality, but this extraction process is to the equipment of production
Requiring height, production cost is high.
Organic solvent extraction, causes product dissolvent residual because using organic solvent, affects product quality.
Summary of the invention
Not enough for prior art, the present invention is to provide the preparation method of a kind of MEIGUI CHUNLU.
The present invention seeks to be achieved through the following technical solutions:
The preparation method of a kind of MEIGUI CHUNLU, it is characterised in that comprise the following steps:
(1) Flos Rosae Rugosae of fresh harvesting is carried out lyophilization, be 10% to average moisture content；
(2) carry out pulverization process through step (1) gained Flos Rosae Rugosae, prepare Flos Rosae Rugosas pollen；
(3) Flos Rosae Rugosas pollen, water and Sal input distillating still is distilled；
(4) distillating still distillation out in step (3) is cooled down, import oil water separator and separate, collect
Upper oil phase and lower floor's aqueous phase, lower floor's aqueous phase is described MEIGUI CHUNLU.
Preferably, step (1) cryodesiccated condition is cryogenic temperature-10～-5 DEG C, drying time 5～10 hours.
Preferably, the fineness of step (2) Flos Rosae Rugosas pollen is 10～20 mesh.
Preferably, step (3) described vapo(u)rizing temperature is 45～60 DEG C, and distillation time is 10～20 hours.
Preferably, the mass ratio of step (3) described Flos Rosae Rugosas pollen, Sal and water is 1:0.05:6.
Preferably, step (4) described chilling temperature is 10～15 DEG C.
The preparation method of the MEIGUI CHUNLU that the present invention provides, has the advantages that
(1) overcoming the MEIGUI CHUNLU that conventional hydrodistillation extracts, fragrance is the purest, the defect that impurity content is high；
(2) stability of gained MEIGUI CHUNLU is high, and active constituent content is high；
(3) this method is low for equipment requirements, simple to operate, easy industrialized production.
Detailed description of the invention
Below by the mode of specific embodiment, the present invention is further described, but scope does not limit to
In these embodiments.All based on above-mentioned technological thought, utilize amendment that ordinary skill knowledge and customary means made, replace
Change, change and belong to the scope of protection of present invention.
Embodiment 1
The preparation method of a kind of MEIGUI CHUNLU, it is characterised in that comprise the following steps:
(1) Flos Rosae Rugosae of fresh harvesting being carried out lyophilization, cryogenic temperature is-10 DEG C, 10 hours drying times, to flat
All water content are 10%；
(2) carrying out pulverization process through step (1) gained Flos Rosae Rugosae, prepare Flos Rosae Rugosas pollen, fineness is 10 mesh；
(3) Sal of the Flos Rosae Rugosas pollen of 10 weight portions, the water of 60 weight portions and 0.5 weight portion is put into distillating still to steam
Evaporating, vapo(u)rizing temperature is 45 DEG C, and distillation time is 20 hours；
(4) being cooled down by distillating still distillation out in step (3), being cooled to temperature is 15 DEG C, imports profit and divides
Separating from device, collect upper oil phase and lower floor's aqueous phase, upper oil phase is Flos Rosae Rugosae quintessence oil, and lower floor's aqueous phase is MEIGUI CHUNLU.
Embodiment 2
The preparation method of a kind of MEIGUI CHUNLU, it is characterised in that comprise the following steps:
(1) Flos Rosae Rugosae of fresh harvesting being carried out lyophilization, cryogenic temperature is-5 DEG C, and 5 hours drying times, to averagely
Water content is 10%；
(2) carrying out pulverization process through step (1) gained Flos Rosae Rugosae, prepare Flos Rosae Rugosas pollen, fineness is 20 mesh；
(3) Sal of the Flos Rosae Rugosas pollen of 10 weight portions, the water of 60 weight portions and 0.5 weight portion is put into distillating still to steam
Evaporating, vapo(u)rizing temperature is 60 DEG C, and distillation time is 10 hours；
(4) being cooled down by distillating still distillation out in step (3), being cooled to temperature is 10 DEG C, imports profit and divides
Separating from device, collect upper oil phase and lower floor's aqueous phase, upper oil phase is Flos Rosae Rugosae quintessence oil, and lower floor's aqueous phase is MEIGUI CHUNLU.
Embodiment 3
The preparation method of a kind of MEIGUI CHUNLU, it is characterised in that comprise the following steps:
(1) Flos Rosae Rugosae of fresh harvesting being carried out lyophilization, cryogenic temperature is-8 DEG C, and 8 hours drying times, to averagely
Water content is 10%；
(2) carrying out pulverization process through step (1) gained Flos Rosae Rugosae, prepare Flos Rosae Rugosas pollen, fineness is 15 mesh；
(3) Sal of the Flos Rosae Rugosas pollen of 10 weight portions, the water of 60 weight portions and 0.5 weight portion is put into distillating still to steam
Evaporating, vapo(u)rizing temperature is 50 DEG C, and distillation time is 18 hours；
(4) being cooled down by distillating still distillation out in step (3), being cooled to temperature is 15 DEG C, imports profit and divides
Separating from device, collect upper oil phase and lower floor's aqueous phase, upper oil phase is Flos Rosae Rugosae quintessence oil, and lower floor's aqueous phase is MEIGUI CHUNLU.
Carrying out effect test by embodiment 1-3 gained MEIGUI CHUNLU, test data are as follows:
Physical and chemical index:
(1) fragrance: there is the distinctive happy delicate fragrance of Flos Rosae Rugosae, soft aroma and pure, free from extraneous odour；
(2) outward appearance and impurity: uniform transparency liquid, free from foreign meter；
(3) arsenic content (mg/L, in terms of As) :≤0.5；
(4) lead content (mg/L, in terms of Pb) :≤0.1
(5) mercury content (mg/L, in terms of Hg) :≤0.05.
Microbiological indicator:
Claims (6)
1. the preparation method of a MEIGUI CHUNLU, it is characterised in that comprise the following steps:
(1) Flos Rosae Rugosae of fresh harvesting is carried out lyophilization, be 10% to average moisture content；
(2) carry out pulverization process through step (1) gained Flos Rosae Rugosae, prepare Flos Rosae Rugosas pollen；
(3) Flos Rosae Rugosas pollen, water and Sal input distillating still is distilled；
(4) distillating still distillation out in step (3) is cooled down, import oil water separator and separate, collect upper strata
Oil phase and lower floor's aqueous phase, lower floor's aqueous phase is described MEIGUI CHUNLU.
The preparation method of MEIGUI CHUNLU the most according to claim 1, it is characterised in that described step (1) is cryodesiccated
Condition is cryogenic temperature-10～-5 DEG C, drying time 5～10 hours.
The preparation method of MEIGUI CHUNLU the most according to claim 1, it is characterised in that described step (2) Flos Rosae Rugosas pollen
Fineness is 10～20 mesh.
The preparation method of MEIGUI CHUNLU the most according to claim 1, it is characterised in that step (3) described vapo(u)rizing temperature is
45～60 DEG C, distillation time is 10～20 hours.
The preparation method of MEIGUI CHUNLU the most according to claim 1, it is characterised in that step (3) described Flos Rosae Rugosas pollen, food
The mass ratio of salt and water is 1:0.05:6.
The preparation method of MEIGUI CHUNLU the most according to claim 1, it is characterised in that step (4) described chilling temperature is
10～15 DEG C.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201610665053.4A CN106190577A (en) | 2016-08-12 | 2016-08-12 | A kind of preparation method of MEIGUI CHUNLU |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201610665053.4A CN106190577A (en) | 2016-08-12 | 2016-08-12 | A kind of preparation method of MEIGUI CHUNLU |
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| Publication Number | Publication Date |
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| CN106190577A true CN106190577A (en) | 2016-12-07 |
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| CN201610665053.4A Pending CN106190577A (en) | 2016-08-12 | 2016-08-12 | A kind of preparation method of MEIGUI CHUNLU |
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Cited By (8)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN106398872A (en) * | 2016-11-19 | 2017-02-15 | 陈桂龙 | Extraction method of rose oil |
| CN107189858A (en) * | 2017-04-27 | 2017-09-22 | 陶发助 | A kind of preparation method of yulan magnolia hydrosol |
| CN107788314A (en) * | 2017-11-08 | 2018-03-13 | 苏州星圣娜玫瑰园艺有限公司 | The preparation method of rose |
| CN107898733A (en) * | 2017-12-30 | 2018-04-13 | 广州市中通生化制品有限公司 | A kind of after-sun composition and preparation method and application |
| CN110669589A (en) * | 2019-11-12 | 2020-01-10 | 高治伟 | Preparation process of rose essential oil |
| CN111925869A (en) * | 2020-07-28 | 2020-11-13 | 庐江县璟泰玫瑰花种植有限责任公司 | Preparation method of rose syrup |
| CN113337343A (en) * | 2021-05-18 | 2021-09-03 | 中农实创(北京)环境工程技术有限公司 | Rose hydrolat prepared from new variety of roses and preparation method of rose hydrolat |
| CN115161114A (en) * | 2022-06-07 | 2022-10-11 | 厦门健康工程与创新研究院 | Method for extracting hydrolat from spliced roses of different varieties |
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| CN1557521A (en) * | 2004-01-19 | 2004-12-29 | 中 孟 | Extraction method of wild rose under supercritical CO2 condition |
| CN101280243A (en) * | 2008-06-04 | 2008-10-08 | 杨利民 | Method for extracting rose essence oil and rose absolute by water vapor water distillation technology |
| CN103614241A (en) * | 2013-12-13 | 2014-03-05 | 北京市门头沟区科技开发实验基地 | Method for preparing rose essential oil and product thereof |
| CN103642592A (en) * | 2013-11-01 | 2014-03-19 | 西安银能科技发展有限责任公司 | Full utilization technology of rose flower |
| JP2015218120A (en) * | 2014-05-15 | 2015-12-07 | 白井松新薬株式会社 | Tyrosinase inhibitor and manufacturing method thereof |
| CN205152181U (en) * | 2015-11-25 | 2016-04-13 | 四川省盛祥玫瑰生态农业开发有限公司 | A oil -water separator for producing rose hydrosol |
| CN205152180U (en) * | 2015-11-25 | 2016-04-13 | 四川省盛祥玫瑰生态农业开发有限公司 | A distillation plant for producing rose hydrosol |
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2016
- 2016-08-12 CN CN201610665053.4A patent/CN106190577A/en active Pending
Patent Citations (7)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN1557521A (en) * | 2004-01-19 | 2004-12-29 | 中 孟 | Extraction method of wild rose under supercritical CO2 condition |
| CN101280243A (en) * | 2008-06-04 | 2008-10-08 | 杨利民 | Method for extracting rose essence oil and rose absolute by water vapor water distillation technology |
| CN103642592A (en) * | 2013-11-01 | 2014-03-19 | 西安银能科技发展有限责任公司 | Full utilization technology of rose flower |
| CN103614241A (en) * | 2013-12-13 | 2014-03-05 | 北京市门头沟区科技开发实验基地 | Method for preparing rose essential oil and product thereof |
| JP2015218120A (en) * | 2014-05-15 | 2015-12-07 | 白井松新薬株式会社 | Tyrosinase inhibitor and manufacturing method thereof |
| CN205152181U (en) * | 2015-11-25 | 2016-04-13 | 四川省盛祥玫瑰生态农业开发有限公司 | A oil -water separator for producing rose hydrosol |
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Cited By (8)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN106398872A (en) * | 2016-11-19 | 2017-02-15 | 陈桂龙 | Extraction method of rose oil |
| CN107189858A (en) * | 2017-04-27 | 2017-09-22 | 陶发助 | A kind of preparation method of yulan magnolia hydrosol |
| CN107788314A (en) * | 2017-11-08 | 2018-03-13 | 苏州星圣娜玫瑰园艺有限公司 | The preparation method of rose |
| CN107898733A (en) * | 2017-12-30 | 2018-04-13 | 广州市中通生化制品有限公司 | A kind of after-sun composition and preparation method and application |
| CN110669589A (en) * | 2019-11-12 | 2020-01-10 | 高治伟 | Preparation process of rose essential oil |
| CN111925869A (en) * | 2020-07-28 | 2020-11-13 | 庐江县璟泰玫瑰花种植有限责任公司 | Preparation method of rose syrup |
| CN113337343A (en) * | 2021-05-18 | 2021-09-03 | 中农实创(北京)环境工程技术有限公司 | Rose hydrolat prepared from new variety of roses and preparation method of rose hydrolat |
| CN115161114A (en) * | 2022-06-07 | 2022-10-11 | 厦门健康工程与创新研究院 | Method for extracting hydrolat from spliced roses of different varieties |
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Application publication date: 20161207 |