CN105885751A - Preparation method of epoxy resin tung oil lime bast paste - Google Patents
Preparation method of epoxy resin tung oil lime bast paste Download PDFInfo
- Publication number
- CN105885751A CN105885751A CN201510026753.4A CN201510026753A CN105885751A CN 105885751 A CN105885751 A CN 105885751A CN 201510026753 A CN201510026753 A CN 201510026753A CN 105885751 A CN105885751 A CN 105885751A
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- CN
- China
- Prior art keywords
- epoxy resin
- calx
- glue
- verniciae fordii
- oleum verniciae
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
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- Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
- Y02—TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
- Y02P—CLIMATE CHANGE MITIGATION TECHNOLOGIES IN THE PRODUCTION OR PROCESSING OF GOODS
- Y02P20/00—Technologies relating to chemical industry
- Y02P20/141—Feedstock
Landscapes
- Adhesives Or Adhesive Processes (AREA)
- Epoxy Resins (AREA)
- Curing Cements, Concrete, And Artificial Stone (AREA)
Abstract
The invention discloses a preparation method of epoxy resin tung oil lime bast paste. Traditional tung oil lime is widely used by people in the aspects of water prevention, leakage prevention, repair and the like, however is gradually replaced by other glue due to the fact that the bonding degree is not high enough and hardness is not high enough. According to the finished product epoxy resin tung oil lime bast paste prepared through the method, on the basis of original tung oil lime, epoxy resin high-strength binding glue is introduced, so that the finished product has the high-strength waterproof performance of the original product, all the binding functions of the epoxy resin glue are achieved, the binding range is greatly enlarged, and stone, wound, steel, plastic and the like can be bound; meanwhile, the epoxy resin tung oil lime bast paste has the advantages of high temperature resistance and plasticity, thereby being capable of being used for repairing and binding in the aspects of cultural relic repair, sculpture recovery, mold molding, furniture industry, industrial art molding, radiators, hot water plastic pipes and the like.
Description
One, art
Oleum Verniciae fordii is a kind of excellent band dry vegetable oil, has that fast drying, light specific gravity, glossiness be good, attachment
The characteristics such as power is strong, heat-resisting, alkaline-resisting, antiseptic and rustproof, non-conductive, a large amount of be used as building, weapons, car and boat,
Fishing gear, electrical equipment.Oleum Verniciae fordii also has good water proofing property, typically mixes with Calx, for bonding with boiled wood oil
Object, plays waterproof, the effect of leakproof, and the present invention introduces ring on the basis of traditional Oleum Verniciae fordii Calx glue
Epoxy resins, is the raising modified model of tradition Oleum Verniciae fordii Calx.
Two, background technology
Traditional Oleum Verniciae fordii Calx glue, is mainly added Calx by Oleum Verniciae fordii and mixes by a certain percentage, in history,
It is mainly used in the plugging watertight of the utensil such as wooden barrel, tub.Along with the development of society, the most little in civilian vessel
Use wooden barrel tub, the substitute is rustless steel and plastic ware, and along with the development of technology, bonding
The field of glue also occurs in that glue miscellaneous, but is liquid, such as epoxy resin mostly, and epoxy resin is
Semifluid, although bonding force is very strong, but for the junction of bonding plane it sometimes appear that be not the most identical
Situation, such as historical relic reparation aspect, not only require height to bond degree, and need colloid to have plasticity,
Damaged part is repaired, and after molding, hardness is also higher, so only epoxy resin, it is impossible to
Meet demand.
Three, summary of the invention
Solve the technical problem that
1. Oleum Verniciae fordii Calx has the strongest water-proof repairing effect, but bonding force is not enough, adds epoxy resin, makes
Obtaining Calx therein can strongly be cemented, after molding, hardness is greatly improved.
2. epoxy adhesive is generally to be made up of epoxy resin and firming agent, when firming agent and Oleum Verniciae fordii Calx
The mixture formed after mixing, referred to as B in this literary composition, its holding time is not the longest, if not vertical
Carve and use, within general about 2 days, will harden.For extending firming agent and Oleum Verniciae fordii Calx mixed holding time,
Use the mixture reacting more relatively slow after mixing with firming agent, such as silica flour etc..And epoxy resin exists
The mixture formed after mixing with Oleum Verniciae fordii Calx, in this literary composition, referred to as A, can keep relatively long time.
Time to be used, 2 kinds are mixed in advance doughy AB glue, then use after fully mixed.
Technical scheme
1. by 1 part of epoxy resin and 1 part of Oleum Verniciae fordii again with 5 parts of Calx, the ratio of i.e. 1: 1: 5, mix homogeneously,
Form dough A.If there being different demand, epoxy resin and Oleum Verniciae fordii are constant here, and Calx can root
Cement, silica flour, porcelain powder etc. are changed into according to demand.
2. when needing bonding object, different according to the time of use:
1. if in using the same day, it is possible to according to the ratio of 1: 1: 5, by firming agent, Oleum Verniciae fordii, stone
Ash (or equivalent silica flour, cement, porcelain powder) three carries out being mixed into dough B.If it is (the dilutest
Add dry lime etc..)
2. if not using the same day, the mixture in terms of firming agent the most should not select Calx, because Oleum Verniciae fordii
Can only keep a couple of days with the mixture of Calx, can be the most solid after a couple of days, should select and firming agent and paulownia
Oil reacts relatively slow, slow to meeting the resting period, or the material not reacted, such as silica flour
Deng, it is then passed through being thoroughly mixed to form mixture B1, ready during for using later.
4. when using, by A and B/B1 of above mix homogeneously the most with 4: 1 ratio, i.e. 4 parts mixture A
Carry out mixed once again with 1 part of mixture B/ or B1, thoroughly uniformly after, so that it may make epoxy resin Oleum Verniciae fordii stone
Ash, bonding for carrying out.
5. for convenience of using, in case take out direct bonding object when needing later, can be in advance A and B1
With the ratio of 4: 1, being combined and make cylindric, outer layer vast scale A is annulus, the B1 of middle small scale
In cylinder, owing to being all dough, being not easy each other directly to react, such holding time is relatively permanent,
When needing bonding object, laterally cut out appropriate, after being sufficiently mixed, epoxy resin Oleum Verniciae fordii Calx glue,
The most just can be used directly.
Beneficial effect
This invention, on the basis of traditional Oleum Verniciae fordii Calx, substantially increases bonding custom, add robustness,
Water proofing property and plasticity, its application is quite varied.
1., owing to having the powerful cementability of epoxy resin, breach the tradition bonded scope of Oleum Verniciae fordii Calx,
Can be used for bonding timber, steel, stone material, sculpture, plastics etc. epoxy resin can bonding field, example
Such as upholstery, decorations, auto repair, industrial art and modelling etc..
2. and owing to introducing the powder such as Calx, silica flour, cement, its powder is by epoxy resin combination drying
The mixture hardness ratio of rear formation is higher, be suitable for stone material, sculpture repair bonding.
3. add its resistant to elevated temperatures feature, in conjunction with the water proofing property of Oleum Verniciae fordii, can be used for radiator, water container
Ware, the mending-leakage of industrial pond.
4. this mixture plasticity is strong.In the case of bonding two object junctions are not the most identical, can
According to circumstances carry out moulding, after waiting mixture dry, the most fixed-type.For repairing damaged historical relic, damaged carving
Mould and there is the advantage that liquid glue does not has.
Four, specific embodiments
Manufacture method:
1. the ratio of 1: 1: 5 is used, i.e. 1 part epoxy resin, a Oleum Verniciae fordii, 5 parts of Calx (or other powder
Shape thing, such as quartz sand, cement, Pulvis Talci, porcelain powder etc.) carry out full and uniform mixing, formed mixed
Compound A,
2. the ratio of 1: 1: 5 is used, i.e. 1 part firming agent, a Oleum Verniciae fordii, 5 parts of Calx (or other powderies
Thing, such as quartz sand, cement, Pulvis Talci, porcelain powder etc.) carry out full and uniform mixing, form mixing
Thing B/B1;
When 3. using, 4 parts of A and a B/B1 are mixed again, after mix homogeneously, i.e. make asphalt mixtures modified by epoxy resin
Fat Oleum Verniciae fordii Calx glue.
For convenience of using, in case take out direct bonding object when needing later, can in advance mixture A and
Mixture B1, with the ratio of 4: 1, is combined and makes cylindric, and outer layer vast scale A is annulus, middle little
The B1 of ratio is cylinder, owing to being all dough, is not easy each other directly to react, such holding time
Relatively permanent, when needing bonding object, laterally cut out appropriate, after being sufficiently mixed, epoxy resin
Oleum Verniciae fordii Calx glue, the most just can be used directly.
The most just can carry out bonding as required, object can be timber, steel, stone material, plastics etc., also may be used
Carry out repairing reparation to damaged historical relic, damaged sculpture and radiator etc..
Claims (5)
1. a manufacture method for epoxy resin Oleum Verniciae fordii Calx glue, its step is as follows
1. the ratio of 1: 1: 5 is used, i.e. 1 part epoxy resin, a Oleum Verniciae fordii, 5 parts of Calx (or other powderies
Thing, such as quartz sand, cement, Pulvis Talci, porcelain powder etc.) carry out full and uniform mixing, form mixture,
Referred to as A in this literary composition;
2. simultaneously, with the ratio of 1: 1: 5, i.e. 1 part firming agent, a Oleum Verniciae fordii, 5 parts of Calx (or other powder
Shape thing, such as quartz sand, cement, Pulvis Talci, porcelain powder etc.) carry out full and uniform mixing, form mixing
Thing, referred to as B/B1 in this literary composition;
When 3. using, 4 parts of A and a B/B1 are mixed again, after mix homogeneously, i.e. make epoxy resin paulownia
Oilstone ash glue.
2. the manufacture method of a kind of epoxy resin Oleum Verniciae fordii Calx glue described in claim 1, is characterised by: institute
Method of stating, can be different according to the emphasis of glue in manufacturing process, select different Calx substitutes,
Such as silica flour, porcelain powder, cement etc..
3. the manufacture method of a kind of epoxy resin Oleum Verniciae fordii Calx glue described in claim 1, is characterised by: institute
State the finished product that method makes, be to integrate epoxy resin and the advantage of Oleum Verniciae fordii Calx, existing the most bonding
Property, also have the characteristics such as thermostability, water proofing property, plasticity, molding are firm.
4. the manufacture method of a kind of epoxy resin Oleum Verniciae fordii Calx glue described in claim 1, is characterised by: institute
State the finished product that method makes, itself be i.e. bonded glue, be also filling chink or repairing breakage
The succedaneum at place.
5. the manufacture method of a kind of epoxy resin Oleum Verniciae fordii Calx glue described in claim 1, is characterised by: can
In advance A and B1 with the ratio of 4: 1, being combined and make cylindric, outer layer vast scale A is annulus, in
Between the B1 of small scale be cylinder, laterally cut out appropriate during use, can use after mix homogeneously.
Priority Applications (1)
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CN201510026753.4A CN105885751B (en) | 2015-01-20 | 2015-01-20 | A kind of production method of epoxy resin tung oil lime glue |
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CN201510026753.4A CN105885751B (en) | 2015-01-20 | 2015-01-20 | A kind of production method of epoxy resin tung oil lime glue |
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CN105885751A true CN105885751A (en) | 2016-08-24 |
CN105885751B CN105885751B (en) | 2019-11-29 |
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Cited By (2)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN106927783A (en) * | 2017-04-11 | 2017-07-07 | 广州智弘建筑物检测与鉴定技术有限公司 | A kind of preparation method of the tung oil ash of renovation |
CN108585717A (en) * | 2018-04-02 | 2018-09-28 | 广州灰塑文化发展有限公司 | A method of preparing grey moulding material |
Citations (5)
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CN1040212A (en) * | 1989-05-03 | 1990-03-07 | 山西省水利科学研究所 | Castor-oil hydraulic adhesive and manufacture method |
WO2003062306A1 (en) * | 2002-01-25 | 2003-07-31 | Perstorp Specialty Chemicals Ab | Chain extended dendritic polyether |
CN101696349A (en) * | 2009-11-03 | 2010-04-21 | 中国西电集团公司 | Adhesive, preparation method thereof, and epoxy glass fabric prepared from adhesive |
CN102559134A (en) * | 2012-01-06 | 2012-07-11 | 中国工程物理研究院化工材料研究所 | Tung oil based material for solar battery packaging and packaging method and application thereof |
CN103992764A (en) * | 2014-04-29 | 2014-08-20 | 天长永泰密封材料有限公司 | High viscosity rapid room temperature curing sealant |
-
2015
- 2015-01-20 CN CN201510026753.4A patent/CN105885751B/en active Active
Patent Citations (5)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN1040212A (en) * | 1989-05-03 | 1990-03-07 | 山西省水利科学研究所 | Castor-oil hydraulic adhesive and manufacture method |
WO2003062306A1 (en) * | 2002-01-25 | 2003-07-31 | Perstorp Specialty Chemicals Ab | Chain extended dendritic polyether |
CN101696349A (en) * | 2009-11-03 | 2010-04-21 | 中国西电集团公司 | Adhesive, preparation method thereof, and epoxy glass fabric prepared from adhesive |
CN102559134A (en) * | 2012-01-06 | 2012-07-11 | 中国工程物理研究院化工材料研究所 | Tung oil based material for solar battery packaging and packaging method and application thereof |
CN103992764A (en) * | 2014-04-29 | 2014-08-20 | 天长永泰密封材料有限公司 | High viscosity rapid room temperature curing sealant |
Non-Patent Citations (2)
Title |
---|
杨富巍: "《无机胶凝材料在不可移动文物保护中的应用》", 《中国博士学位论文全文数据库 哲学与人文科学辑》 * |
赵鹏: "《桐油-石灰传统灰浆的性能与作用机理》", 《硅酸盐学报》 * |
Cited By (2)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN106927783A (en) * | 2017-04-11 | 2017-07-07 | 广州智弘建筑物检测与鉴定技术有限公司 | A kind of preparation method of the tung oil ash of renovation |
CN108585717A (en) * | 2018-04-02 | 2018-09-28 | 广州灰塑文化发展有限公司 | A method of preparing grey moulding material |
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Effective date of registration: 20191031 Address after: 510663 room 701, 9 Kehui 1st Street, science Avenue, Huangpu District, Guangzhou City, Guangdong Province Applicant after: Guangzhou Baojie electronic Mstar Technology Ltd Address before: High tech Zone Xiaojiahe street Chengdu city Sichuan province 610018 No. 55-2 Applicant before: Ma Xingyue |
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