CN105884404A - Twisted glaze and preparation method thereof - Google Patents
Twisted glaze and preparation method thereof Download PDFInfo
- Publication number
- CN105884404A CN105884404A CN201610523689.5A CN201610523689A CN105884404A CN 105884404 A CN105884404 A CN 105884404A CN 201610523689 A CN201610523689 A CN 201610523689A CN 105884404 A CN105884404 A CN 105884404A
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- glaze
- strand
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- ceramic
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Classifications
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- C—CHEMISTRY; METALLURGY
- C04—CEMENTS; CONCRETE; ARTIFICIAL STONE; CERAMICS; REFRACTORIES
- C04B—LIME, MAGNESIA; SLAG; CEMENTS; COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDING MATERIALS; ARTIFICIAL STONE; CERAMICS; REFRACTORIES; TREATMENT OF NATURAL STONE
- C04B41/00—After-treatment of mortars, concrete, artificial stone or ceramics; Treatment of natural stone
- C04B41/80—After-treatment of mortars, concrete, artificial stone or ceramics; Treatment of natural stone of only ceramics
- C04B41/81—Coating or impregnation
- C04B41/85—Coating or impregnation with inorganic materials
- C04B41/86—Glazes; Cold glazes
-
- C—CHEMISTRY; METALLURGY
- C03—GLASS; MINERAL OR SLAG WOOL
- C03C—CHEMICAL COMPOSITION OF GLASSES, GLAZES OR VITREOUS ENAMELS; SURFACE TREATMENT OF GLASS; SURFACE TREATMENT OF FIBRES OR FILAMENTS MADE FROM GLASS, MINERALS OR SLAGS; JOINING GLASS TO GLASS OR OTHER MATERIALS
- C03C8/00—Enamels; Glazes; Fusion seal compositions being frit compositions having non-frit additions
-
- C—CHEMISTRY; METALLURGY
- C04—CEMENTS; CONCRETE; ARTIFICIAL STONE; CERAMICS; REFRACTORIES
- C04B—LIME, MAGNESIA; SLAG; CEMENTS; COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDING MATERIALS; ARTIFICIAL STONE; CERAMICS; REFRACTORIES; TREATMENT OF NATURAL STONE
- C04B41/00—After-treatment of mortars, concrete, artificial stone or ceramics; Treatment of natural stone
- C04B41/45—Coating or impregnating, e.g. injection in masonry, partial coating of green or fired ceramics, organic coating compositions for adhering together two concrete elements
- C04B41/50—Coating or impregnating, e.g. injection in masonry, partial coating of green or fired ceramics, organic coating compositions for adhering together two concrete elements with inorganic materials
- C04B41/5022—Coating or impregnating, e.g. injection in masonry, partial coating of green or fired ceramics, organic coating compositions for adhering together two concrete elements with inorganic materials with vitreous materials
Abstract
The invention relates to a twisted glaze and a preparation method thereof. The twisted glaze is prepared from the following components in percentage by weight: 39 to 50.9 percent of feldspar, 15.5 to 20.3 percent of quartz, 7.8 to 10.2 percent of zirconia, 7.8 to 10.2 percent of alumina, 7.8 to 10.2 percent of kaolin, 2 to 6 percent of cellulose and 3.8 to 9.7 percent of a ceramic pigment. According to the twisted glaze, similarity between a product and a design can reach 80 to 90 percent, and the requirements of both an artistic designing and an industrial product specification can be met. The added artistic value of porcelain with the twisted glaze is improved, the large-scale production of the porcelain with twisted glaze can be implemented, and meanwhile, the rejection rate of the product can be favorably controlled.
Description
Technical field
The present invention relates to ceramic technology field, be specifically related to a kind of strand glaze and preparation method thereof.
Background technology
Strand glaze surface characteristics is similar to twist tire porcelain, but being but different from strand tire is carcass coloring, and its conventional practice is to call in colouring matter in glaze, utilizes the effect that two kinds of colorants are less soluble, imposes on slightly and reenter klining on mold after agitation.The product handed down from ancient times of tradition strand vitreous enamel are few, and its style is naturally simple.
Tradition strand glaze is with different color glaze and cosmetic soil mixed diluting, and rocks difference color glaze is stirred into irregular striped, then imposes on porcelain, then executes the difference color glaze such as clear frit or green glaze and burn till.Traditional strand glaze has the disadvantage that one, and tradition strand glaze, due to the configuration of cosmetic soil Yu glaze, can only accomplish that the color glaze strand of two kinds and three kinds is knitted, and strand vitreous enamel handed down from ancient times is substantially two kinds of color glaze and twists the porcelain knitted, and three kinds of color glaze twists knit the rarest；Its two, tradition strand glaze operating process is loaded down with trivial details, production efficiency is low, production cost is high；Its three, tradition strand glaze glaze thick, while glazing process is loaded down with trivial details, with low uncertainty, formed pattern uncontrollable, harvest rate is low；Its four, tradition strand glaze glaze color the dimest, strand vitreous enamel handed down from ancient times is substantially nothing more than three looks yellow, brown, black.
Summary of the invention
The present invention provides a kind of strand glaze and preparation method thereof, to solve the existing strand glaze strand problems such as fabric/color is few, pattern is uncontrollable.
The present invention adopts the following technical scheme that
A kind of strand glaze, this glaze is for directly executing in biscuit surface, and each component of this glaze is formed by following weight proportion: feldspar 39%～50.9%, quartz 15.5%～20.3%, zirconium oxide 7.8%～10.2%, aluminum oxide 7.8%～10.2%, kaolin 7.8%～10.2%, cellulose 2%～6%, ceramic pigment 3.8%～9.7%.
Further:
Above-mentioned ceramic pigment is one or several the combination in copper carbonate, cobalt oxide, manganese oxide, iron oxide, lead-free rare-earth colorant.
A kind of preparation method twisting glaze, comprises the following steps:
I. prepare ceramic colour glaze glaze: after being mixed respectively by the ceramic pigment after at least one ball milling, prepare color glaze compound with the crystalline ceramics glaze after ball milling, then the most by weight ratio for the color glaze compound after ball milling: cellulose solution=1:0.03～0.06 adds cellulose solution and mixes, at least one ceramic colour glaze glaze is prepared；
II. preparation strand glaze base-material: be above-mentioned crystalline ceramics glaze by weight ratio by the above-mentioned crystalline ceramics glaze through ball milling: above-mentioned cellulose solution=1:0.03～0.06 adds above-mentioned cellulose solution, and mixes, prepare and twist glaze base-material；
III. preparation strand glaze glaze: choose in the above-mentioned ceramic colour glaze glaze prepared at least one step I pours, according to design requirement, the above-mentioned strand glaze base-material prepared in step II into successively and stir, preparing strand glaze glaze；
IV: glazing: after biscuiting base substrate is soaked 5 minutes～10 minutes in water, take out above-mentioned biscuiting base substrate and spoon the above-mentioned strand glaze glaze that step III prepares, and according to design requirement, by the rotation of this biscuiting base substrate and the layout tilting to make this strand glaze glaze to form demand on biscuiting base substrate；
V: burn till: fired in the above-mentioned biscuiting base substrate after glazing in step IV is sent into tunnel cave, obtain finished product after kiln discharge cooling.
Further:
Above-mentioned steps I and the above-mentioned crystalline ceramics glaze in step II for after feldspar 50%, quartz 20%, zirconium oxide 10%, aluminum oxide 10%, kaolin 10% are mixed according to compound: water=1:0.75～0.85 adds water, and prepares after ball milling.
Above-mentioned color glaze compound in above-mentioned steps I is ball milling after being added water for ceramic pigment: water=1:0.43～1 the most by weight ratio by least one ceramic pigment, at least one ceramic pigment liquid is prepared, then the most by weight ratio for above-mentioned crystalline ceramics glaze: above-mentioned ceramic pigment liquid=1:0.12～0.25 adds above-mentioned crystalline ceramics glaze and mixes prepared after ball milling.
The concentration of above-mentioned cellulose solution is 60%～70%.
The agitating mode being stirred the above-mentioned strand glaze base-material being mixed into above-mentioned ceramic colour glaze glaze for carrying out 180 °～360 ° stirrings counterclockwise after first carrying out 180 °～360 ° stirrings clockwise again in above-mentioned steps III, for being twisted into above-mentioned strand glaze glaze by this immiscible ceramic colour glaze glaze.
The firing temperature of above-mentioned steps V is 1200 DEG C～1300 DEG C.
Above-mentioned steps V also includes with being filled the sponge of water by above-mentioned strand glaze glaze unnecessary bottom the above-mentioned biscuiting base substrate after glazing in above-mentioned steps IV.
From the above-mentioned description of this invention, compared to the prior art, present invention have the advantage that
First, the strand vitreous enamel of the present invention can realize the similarity of product and design and reach 80%～90%, and no matter from the realization of Art Design or the angle of the code requirement of industrial products, the present invention can meet.The present invention is improving the strand artistic surcharge of vitreous enamel and is making the large-scale industrial production twisting vitreous enamel additionally aid the control of percent defective of product while being possibly realized.
Second, the strand glaze preparation method of the present invention achieves a strand time glazing of glaze and gets final product kiln-firing, it is not necessary to execute strand glaze and other color glaze such as clear frit or green glaze respectively, the easy production process of strand vitreous enamel, improves production efficiency and saves production cost.
3rd, the present invention strand glaze glaze setting time short and by the inclination of this biscuiting base substrate, rotate can realize twist glaze striped on biscuiting base substrate, form specific pattern.
4th, the crystalline ceramics glaze of the present invention and being equipped with of ceramic colour glaze glaze, up to tens kinds color glaze strand can be realized knit, color select more so that more strand glaze pattern be designed to possibility, add the value of strand vitreous enamel and improve the competitiveness twisting glaze porcelain products.
5th, the present invention is by the use of the cellulose of this kind of ratio and the agitating mode that matches therewith, make ceramic colour glaze glaze can exist in this crystalline ceramics glaze immisciblely, while being conducive to strand glaze to be formed, this strand glaze glaze making composition has reached optimum efficiency in lubrication with viscosity, so that strand glaze striped has optimal adhesion property and mobile performance to this biscuiting base substrate, and then allow the invention to the inclination by biscuiting base substrate, rotate make to twist glaze glaze can controllably on biscuiting base substrate stream dynamic, thus draw specific pattern.
Detailed description of the invention
As the preferred embodiments of the present invention, a kind of preparation method twisting glaze, comprise the following steps:
I. prepare crystalline ceramics glaze: according to compound after feldspar 50%, quartz 20%, zirconium oxide 10%, aluminum oxide 10%, kaolin 10% being mixed: water=1:0.8 adds water, prepare after ball milling.
II. preparing cellulose solution: by cellulose grain according to cellulose grain: water=1:0.5 adds temperature and is about 40 DEG C～the warm water of 60 DEG C, stirring prepares after dissolving completely to cellulose grain.
III. preparation strand glaze base-material: be crystalline ceramics glaze by weight ratio by above-mentioned crystalline ceramics glaze and above-mentioned cellulose solution: cellulose solution=1:0.06 adds above-mentioned cellulose solution, and mixes, prepared twists glaze base-material.
VI. prepare ceramic colour glaze glaze: by the ceramic pigment of three kinds of different colours the most by weight ratio for ceramic pigment: water=1:0.8 add water after ball milling, three kinds of ceramic pigment liquid are prepared after ball milling, then the most by weight ratio for above-mentioned crystalline ceramics glaze: this ceramic pigment liquid=1:0.2 adds above-mentioned crystalline ceramics glaze and mixes prepared three kinds of color glaze compounds, then the most by weight ratio for above-mentioned color glaze compound: above-mentioned cellulose solution=1:0.06 adds cellulose solution and mixes, the ceramic colour glaze glaze that three kinds of colors are different is prepared.
Wherein: ceramic pigment is by one or several the combination in copper carbonate, cobalt oxide, manganese oxide, iron oxide, high temperature cerise lead-free rare-earth colorant, orange red lead-free rare-earth colorant, lilac lead-free rare-earth colorant, vanadium blueness lead-free rare-earth colorant and zirconium-iron pink lead-free rare-earth colorant.
V. preparation strand glaze glaze: by three kinds of steps VI prepare above-mentioned ceramic colour glaze glaze according to design requirement pour into successively step III prepare above-mentioned strand glaze base-material in and stir, this stirring be first carry out clockwise 180 ° stirring after carry out again counterclockwise 360 ° stirring agitating modes, this ceramic colour glaze glaze that three kinds are immiscible is twisted into the strand glaze glaze that the stranded lines with on layout is substantially uniform.
Wherein: in above-mentioned strand glaze glaze, the above-mentioned ceramic colour glaze glaze that three kinds of steps VI prepare respectively accounts for 10%, and above-mentioned strand glaze base-material accounts for 70%.
VI. glazing: after biscuiting base substrate is soaked 10 minutes in water, take out above-mentioned biscuiting base substrate and spoon the above-mentioned strand glaze glaze that step V prepares, and according to design requirement, by the rotation of this biscuiting base substrate and the layout tilting to make this strand glaze glaze to form demand on biscuiting base substrate.Finally with being filled the sponge of water by strand glaze glaze unnecessary bottom the above-mentioned biscuiting base substrate after glazing.
VII. burn till: having fired in the above-mentioned biscuiting base substrate after glazing in step VI is sent into tunnel cave, firing temperature is 1200 DEG C～1300 DEG C, after kiln discharge cooling, obtain finished product.
In the present embodiment, coordinate agitating mode by various ceramic pigments, the strand glaze glaze close with the strand weavy grain road of layout can be prepared, then on biscuiting base substrate, form target pattern by the flowing of strand glaze glaze.Biscuiting base substrate spoon strand glaze glaze time, can as required from the top of biscuiting base substrate down water pouring or in the middle part of biscuiting base substrate, bottom water pouring.
Above are only the detailed description of the invention of the present invention, but the design concept of the present invention is not limited thereto, all changes utilizing this design that the present invention carries out unsubstantiality, the behavior invading scope all should be belonged to.
Claims (9)
1. a strand glaze, this glaze is for directly executing in biscuit surface, it is characterised in that: each component of described glaze is formed by following weight proportion: feldspar 39%～50.9%, quartz 15.5%～20.3%, zirconium oxide 7.8%～10.2%, aluminum oxide 7.8%～10.2%, kaolin 7.8%～10.2%, cellulose 2%～6%, ceramic pigment 3.8%～9.7%.
A kind of strand glaze the most according to claim 1, it is characterised in that: described ceramic pigment is one or several the combination in copper carbonate, cobalt oxide, manganese oxide, iron oxide, lead-free rare-earth colorant.
3. the preparation method twisting glaze, it is characterised in that: described preparation method comprises the following steps:
I. prepare ceramic colour glaze glaze: after being mixed respectively by the ceramic pigment after at least one ball milling, prepare color glaze compound with the crystalline ceramics glaze after ball milling, then the most by weight ratio for the color glaze compound after ball milling: cellulose solution=1:0.03～0.06 adds cellulose solution and mixes, at least one ceramic colour glaze glaze is prepared；
II. preparation strand glaze base-material: be described crystalline ceramics glaze by weight ratio by the described crystalline ceramics glaze through ball milling: described cellulose solution=1:0.03～0.06 adds described cellulose solution, and mixes, prepare and twist glaze base-material；
III. preparation strand glaze glaze: choose in the described ceramic colour glaze glaze prepared at least one step I pours, according to design requirement, the described strand glaze base-material prepared in step II into successively and stir, preparing strand glaze glaze；
IV: glazing: after biscuiting base substrate is soaked 5 minutes～10 minutes in water, take out described biscuiting base substrate and spoon the described strand glaze glaze that step III prepares, and according to design requirement, by the rotation of this biscuiting base substrate and the layout tilting to make this strand glaze glaze to form demand on biscuiting base substrate；
V: burn till: fired in the described biscuiting base substrate after glazing in step IV is sent into tunnel cave, obtain finished product after kiln discharge cooling.
A kind of preparation method twisting glaze the most according to claim 3, it is characterized in that: described step I and the described crystalline ceramics glaze in step II for after feldspar 50%, quartz 20%, zirconium oxide 10%, aluminum oxide 10%, kaolin 10% are mixed according to compound: water=1:0.75～0.85 adds water, and prepares after ball milling.
A kind of preparation method twisting glaze the most according to claim 4, it is characterized in that: the described color glaze compound in described step I is ball milling after being added water for ceramic pigment: water=1:0.43～1 the most by weight ratio by least one ceramic pigment, at least one ceramic pigment liquid is prepared, then the most by weight ratio for described crystalline ceramics glaze: described ceramic pigment liquid=1:0.12～0.25 adds described crystalline ceramics glaze and mixes prepared after ball milling.
6. according to the arbitrary described a kind of preparation method twisting glaze of claim 3 to 5, it is characterised in that: the concentration of described cellulose solution is 60%～70%.
A kind of preparation method twisting glaze the most according to claim 3, it is characterized in that: the agitating mode described strand glaze base-material being mixed into described ceramic colour glaze glaze being stirred for carrying out 180 °～360 ° stirrings counterclockwise after first carrying out 180 °～360 ° stirrings clockwise again in described step III, for this immiscible ceramic colour glaze glaze is twisted into described strand glaze glaze.
A kind of preparation method twisting glaze the most according to claim 3, it is characterised in that: the firing temperature of described step V is 1200 DEG C～1300 DEG C.
A kind of preparation method twisting glaze the most according to claim 3, it is characterised in that: described step V also includes with being filled the sponge of water by described strand glaze glaze unnecessary bottom the described biscuiting base substrate after glazing in described step IV.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201610523689.5A CN105884404B (en) | 2016-07-06 | 2016-07-06 | A kind of strand glaze and preparation method thereof |
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| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201610523689.5A CN105884404B (en) | 2016-07-06 | 2016-07-06 | A kind of strand glaze and preparation method thereof |
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| CN105884404A true CN105884404A (en) | 2016-08-24 |
| CN105884404B CN105884404B (en) | 2019-01-18 |
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Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN111099922A (en) * | 2019-12-27 | 2020-05-05 | 广西南山瓷器有限公司 | Ceramic decorative soil and use method thereof |
Citations (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN103288418A (en) * | 2013-05-13 | 2013-09-11 | 王洪新 | Glazed ceramic technique |
| CN103588418A (en) * | 2012-08-15 | 2014-02-19 | 张桂兰 | Microlite with twistable glaze, and production method and special-purpose equipment |
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2016
- 2016-07-06 CN CN201610523689.5A patent/CN105884404B/en active Active
Patent Citations (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN103588418A (en) * | 2012-08-15 | 2014-02-19 | 张桂兰 | Microlite with twistable glaze, and production method and special-purpose equipment |
| CN103288418A (en) * | 2013-05-13 | 2013-09-11 | 王洪新 | Glazed ceramic technique |
Non-Patent Citations (1)
| Title |
|---|
| 王浩: "浅谈古代绞胎瓷与"绞釉"瓷", 《中国陶瓷工业》 * |
Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN111099922A (en) * | 2019-12-27 | 2020-05-05 | 广西南山瓷器有限公司 | Ceramic decorative soil and use method thereof |
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| CN105884404B (en) | 2019-01-18 |
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Effective date of registration: 20200423 Address after: 521000. A2-10 block north of Ruyi Road, Ruyi Industrial Park, maple, Chaozhou, Guangdong Patentee after: GUANGDONG BENING CERAMICS INDUSTRIES Co.,Ltd. Address before: 521031, Guangdong Province, Chaozhou Province town of maple Creek former village, Xie Industrial Zone Road, the middle Patentee before: Wu Yonglong |
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