CN105879105A - Composite medical stone functional fiber surface layer material of sanitary towel and preparation method of material - Google Patents
Composite medical stone functional fiber surface layer material of sanitary towel and preparation method of material Download PDFInfo
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61L—METHODS OR APPARATUS FOR STERILISING MATERIALS OR OBJECTS IN GENERAL; DISINFECTION, STERILISATION OR DEODORISATION OF AIR; CHEMICAL ASPECTS OF BANDAGES, DRESSINGS, ABSORBENT PADS OR SURGICAL ARTICLES; MATERIALS FOR BANDAGES, DRESSINGS, ABSORBENT PADS OR SURGICAL ARTICLES
- A61L15/00—Chemical aspects of, or use of materials for, bandages, dressings or absorbent pads
- A61L15/16—Bandages, dressings or absorbent pads for physiological fluids such as urine or blood, e.g. sanitary towels, tampons
- A61L15/40—Bandages, dressings or absorbent pads for physiological fluids such as urine or blood, e.g. sanitary towels, tampons containing ingredients of undetermined constitution or reaction products thereof, e.g. plant or animal extracts
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61L—METHODS OR APPARATUS FOR STERILISING MATERIALS OR OBJECTS IN GENERAL; DISINFECTION, STERILISATION OR DEODORISATION OF AIR; CHEMICAL ASPECTS OF BANDAGES, DRESSINGS, ABSORBENT PADS OR SURGICAL ARTICLES; MATERIALS FOR BANDAGES, DRESSINGS, ABSORBENT PADS OR SURGICAL ARTICLES
- A61L15/00—Chemical aspects of, or use of materials for, bandages, dressings or absorbent pads
- A61L15/16—Bandages, dressings or absorbent pads for physiological fluids such as urine or blood, e.g. sanitary towels, tampons
- A61L15/18—Bandages, dressings or absorbent pads for physiological fluids such as urine or blood, e.g. sanitary towels, tampons containing inorganic materials
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- A—HUMAN NECESSITIES
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- A61L15/00—Chemical aspects of, or use of materials for, bandages, dressings or absorbent pads
- A61L15/16—Bandages, dressings or absorbent pads for physiological fluids such as urine or blood, e.g. sanitary towels, tampons
- A61L15/42—Use of materials characterised by their function or physical properties
- A61L15/44—Medicaments
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61L—METHODS OR APPARATUS FOR STERILISING MATERIALS OR OBJECTS IN GENERAL; DISINFECTION, STERILISATION OR DEODORISATION OF AIR; CHEMICAL ASPECTS OF BANDAGES, DRESSINGS, ABSORBENT PADS OR SURGICAL ARTICLES; MATERIALS FOR BANDAGES, DRESSINGS, ABSORBENT PADS OR SURGICAL ARTICLES
- A61L15/00—Chemical aspects of, or use of materials for, bandages, dressings or absorbent pads
- A61L15/16—Bandages, dressings or absorbent pads for physiological fluids such as urine or blood, e.g. sanitary towels, tampons
- A61L15/42—Use of materials characterised by their function or physical properties
- A61L15/46—Deodorants or malodour counteractants, e.g. to inhibit the formation of ammonia or bacteria
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61L—METHODS OR APPARATUS FOR STERILISING MATERIALS OR OBJECTS IN GENERAL; DISINFECTION, STERILISATION OR DEODORISATION OF AIR; CHEMICAL ASPECTS OF BANDAGES, DRESSINGS, ABSORBENT PADS OR SURGICAL ARTICLES; MATERIALS FOR BANDAGES, DRESSINGS, ABSORBENT PADS OR SURGICAL ARTICLES
- A61L2300/00—Biologically active materials used in bandages, wound dressings, absorbent pads or medical devices
- A61L2300/10—Biologically active materials used in bandages, wound dressings, absorbent pads or medical devices containing or releasing inorganic materials
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61L—METHODS OR APPARATUS FOR STERILISING MATERIALS OR OBJECTS IN GENERAL; DISINFECTION, STERILISATION OR DEODORISATION OF AIR; CHEMICAL ASPECTS OF BANDAGES, DRESSINGS, ABSORBENT PADS OR SURGICAL ARTICLES; MATERIALS FOR BANDAGES, DRESSINGS, ABSORBENT PADS OR SURGICAL ARTICLES
- A61L2300/00—Biologically active materials used in bandages, wound dressings, absorbent pads or medical devices
- A61L2300/20—Biologically active materials used in bandages, wound dressings, absorbent pads or medical devices containing or releasing organic materials
- A61L2300/30—Compounds of undetermined constitution extracted from natural sources, e.g. Aloe Vera
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Abstract
The invention discloses a composite medical stone functional fiber surface layer material of a sanitary towel and a preparation method of the material, and relates to the composite medical stone functional fiber surface layer material and the preparation method of the material. The material and the preparation method are aimed at solving the problems of an existing sanitary towel material without healthy high quality. The product is prepared from medical stone composite fiber, polylactic acid fiber and tencel fiber. The medical stone composite fiber is prepared from medical stone, herba leonuri, flos lonicerae, fresh ginger and viscose. The method includes the steps of firstly, preparing the medicine stone composite fiber, wherein raw materials are weighed, herba leonuri active substances are extracted, flos lonicerae active substances are extracted, fresh ginger active substances are extracted, medical stone active substances are extracted, a composite medicine stone functional extraction solution is prepared, and medical stone composite fiber is prepared; secondly, preparing the surface layer material. The product has the advantages of having functions of sterilizing, deodorizing, moisture absorbing and uterus warming, and being breathable, high in softness, free of toxin and pollution, easy to decompose biologically and the like, and an ecological material is provided for the sanitary towel surface layer manufacturing industry.
Description
Technical field
The present invention relates to a kind of compound Chinese medicinal stone functional fibre skin-material and preparation method thereof.
Background technology
Menstruation reflects the physical condition of women to a certain extent.With menstruation accompany occur dysmenorrhea, stomachache, waist
The symptoms such as acid annoying many women.The women in the whole world 80% has gynaecopathia in various degree, wherein gynecological's disease of 63%
Disease causes owing to women employs sanitary towel inferior at intermenstrual period.So sanitary towel's material of the healthy high-quality of research and development has
Very big significance.
Summary of the invention
The problem that the invention aims to solve to lack now sanitary towel's material of healthy high-quality, and a kind of sanitary towel is provided
Compound Chinese medicinal stone functional fibre skin-material and preparation method thereof.
The compound Chinese medicinal stone functional fibre skin-material of a kind of sanitary towel of the present invention is by Maifanitum composite fibre, acid fiber by polylactic
It is prepared from according to mass ratio 1:1:1 with tencel fiber；Described Maifanitum composite fibre presses mass fraction by 9～11 parts
Maifanitum, 7～8 parts of Herba Leonuris, 6～8 portions of Flos Loniceraes, 3～5 portions of Rhizoma Zingiberis Recenss and 2～4 parts of viscoses are prepared from.
The preparation method of the compound Chinese medicinal stone functional fibre skin-material of a kind of sanitary towel of the present invention sequentially includes the following steps:
One, the preparation of Maifanitum composite fibre:
1. weigh raw material: by mass fraction weigh 9～11 parts of Maifanitums, 7～8 parts of Herba Leonuris, 6～8 portions of Flos Loniceraes, 3～5 parts
Rhizoma Zingiberis Recens and 2～4 parts of viscoses, standby；
2. Herba Leonuri active substance extracts: 7～8 parts of Herba Leonuris step 1. weighed, boiling three times, each 2h,
Every time amount of water flooded Herba Leonuri surface 1cm～1.5cm, once filtered after merging three decoction liquor, then will once mistake
The filtrate of filter concentrates, and obtains once concentration liquid, be subsequently adding and the ethanol of once concentration liquid equivalent, stir evenly standing after cooling,
Obtaining secondary filtrate and filtering residue after secondary filter, filtering residue, by the washing with alcohol of 40%～50%, obtains cleaning mixture, then will wash
Washing liquid and secondary filtrate merges, being evaporated to density is 1.10～1.30, obtains Herba Leonuri activity extract；
3. honey suckle active material extracts: 6～8 portions of Flos Loniceraes step 1. weighed, boiling three times, each 2h,
Amount of water flooded Flos Lonicerae surface 1cm～1.5cm every time, merged three decoction liquor, and after being cooled to room temperature, regulation pH value is to 3.0,
Then filtering, gained filtrate is adsorbed with macroporous adsorptive resins, and flow velocity is 2.5BV/h～3.5BV/h, then enters with water
Row eluting, flow velocity be flow velocity be 2.5BV/h～3.5BV/h, eluting 20min～40min, more successively with 10% ethanol, 25%
Ethanol and 45% ethanol carry out eluting, flow velocity is 2.5BV/h～3.5BV/h, and elution time is 50minmin～70min,
Merge four gained eluents, obtain honey suckle active extract；
4. Rhizoma Zingiberis Recens active substance extracts: 3～5 portions of Rhizoma Zingiberis Recenss step 1. weighed are divided into three parts, use surname extraction respectively
Device carries out reflux, extract, reflux, extract, 20min～40min to three portions of Rhizoma Zingiberis Recenss, merges three parts of extracting solution, steams with Rotary Evaporators
Dry, obtain active substance, be subsequently adding the ethanol of 50% and be configured to the solution that mass concentration is 20%～30% of active substance,
Obtain Rhizoma Zingiberis Recens activity extract；Wherein said reflux, extract, parameter is: extractant is the ethanol of 80%, uses every time and carries
The mass ratio of the quality and every portion of Rhizoma Zingiberis Recens that take agent is 4～6:1；
5. China medicinal stone active material extracts: 9～11 parts of Maifanitums step 1. weighed mix with deionized water, are placed in boiling water
In bath, water carries twice, and each solid-liquid ratio is 1:5, and each water carries the time and is 20min～40min, and water goes to after carrying respectively
Carrying out homogenizing in homogenizer, each homogenizing time is 20min～40min, after merging Aqueous extracts in rotating speed is
Under conditions of 3500rpm/min～4500rpm/min, centrifugal 10min～20min, takes supernatant thing, obtains China medicinal stone active and extracts
Thing；
6. compound Chinese medicinal stone function extracting solution is prepared: the gold that 3. the Herba Leonuri activity extract that step 2. obtained, step obtain
Rhizoma Zingiberis Recens activity extract that 4. Flos Lonicerae activity extract, step obtain and the China medicinal stone active extract that 5. step obtains mixing are all
Even, obtain compound Chinese medicinal stone function extracting solution；
7. Maifanitum composite fibre is prepared: in the compound Chinese medicinal stone function extracting solution that 6. step obtains, add what 1. step weighed
2～4 parts of viscoses, stir 10min～20min under conditions of rotating speed is 700rpm/min～900rpm/min, obtain Maifanitum
Composite fibre；
Two, skin-material is prepared: Maifanitum composite fibre, acid fiber by polylactic and the tencel fiber step one prepared are according to matter
Amount ratio makes yarn for 1:1:1 blending, then according to yarn is interweaved on four satin weave once by the weave of satin weave
Tissue, obtains sanitary towel's compound Chinese medicinal stone functional fibre skin-material.
Beneficial effects of the present invention:
The present invention relates to the preparation of the compound Chinese medicinal stone functional fibre skin-material of a kind of sanitary towel.Containing Maifanitum, Herba Leonuri,
The material such as Flos Lonicerae and Rhizoma Zingiberis Recens.Herba Leonuri merit is apt to promoting blood flow to regulate menstruation, and blood stasis dispelling stimulates the menstrual flow, and controls dysmenorrhea due to blood stasis, amenorrhea, dislikes for puerperal
Dew is not to the utmost, the stagnant stomachache of the stasis of blood has mitigation, and can protect uterus；Flos Lonicerae has broad-spectrum antibacterial action, can carry out
Gynaecopathia has prevention and treatment, to gynecological inflammation swelling in early days, and the chemotactic of the leukocyte in mid-term and swimming out of, the fibre in late period
Dimension connective tissue proliferation has significant curative effect.And Rhizoma Zingiberis Recens as the representative of " warm palace " Chinese medicine have the most antipyretic, antibacterial, antiinflammatory,
Kill trichomonas vaginitis effect, the growth and breeding of multiple pathomycete pathogen is also had inhibitory action.Meanwhile, Maifanitum can be held
Continue to human body trace element supplement, supplement the trace element such as the zinc of needed by human body, selenium, molybdenum, calcium in time.Because this fabric
It is fiber blend yarn healthy, green, environmental and ecological, so having special permanent function, not only useful to health,
The fabric prepared also has good adsorption function, can process the peroxide rubbish that human body is harmful, keeps human normal
Metabolism and physiological equilibrium, regulation human body balance.And have sterilization concurrently, deodorization, moisture absorption, palace ventilative, warm, skin connect
Touch that property is splendid, pliability is high, nontoxic pollution-free, biological easily decomposition, good springiness, anti pilling, easy dyeing, the merit such as nonflammable
Can and characteristic, provide multiple functional health, green, ecological material for sanitary towel top layer manufacturing.
Detailed description of the invention
Detailed description of the invention one: the compound Chinese medicinal stone functional fibre skin-material of a kind of sanitary towel of present embodiment is by Maifanitum
Composite fibre, acid fiber by polylactic and tencel fiber are prepared from according to mass ratio 1:1:1；Described Maifanitum composite fibre
By mass fraction by 9～11 parts of Maifanitums, 7～8 parts of Herba Leonuris, 6～8 portions of Flos Loniceraes, 3～5 portions of Rhizoma Zingiberis Recenss and 2～4 parts of viscose systems
For forming.
Detailed description of the invention two: present embodiment is unlike detailed description of the invention one: described Maifanitum composite fibre is pressed
Mass fraction is prepared from by 10 parts of Maifanitums, 8 parts of Herba Leonuris, 7 portions of Flos Loniceraes, 4 portions of Rhizoma Zingiberis Recenss and 3 parts of viscoses.Other
Step and parameter are identical with detailed description of the invention one.
Detailed description of the invention three: the preparation side of the compound Chinese medicinal stone functional fibre skin-material of a kind of sanitary towel of present embodiment
Method sequentially includes the following steps:
One, the preparation of Maifanitum composite fibre:
1. weigh raw material: by mass fraction weigh 9～11 parts of Maifanitums, 7～8 parts of Herba Leonuris, 6～8 portions of Flos Loniceraes, 3～5 parts
Rhizoma Zingiberis Recens and 2～4 parts of viscoses, standby；
2. Herba Leonuri active substance extracts: 7～8 parts of Herba Leonuris step 1. weighed, boiling three times, each 2h,
Every time amount of water flooded Herba Leonuri surface 1cm～1.5cm, once filtered after merging three decoction liquor, then will once mistake
The filtrate of filter concentrates, and obtains once concentration liquid, be subsequently adding and the ethanol of once concentration liquid equivalent, stir evenly standing after cooling,
Obtaining secondary filtrate and filtering residue after secondary filter, filtering residue, by the washing with alcohol of 40%～50%, obtains cleaning mixture, then will wash
Washing liquid and secondary filtrate merges, being evaporated to density is 1.10～1.30, obtains Herba Leonuri activity extract；
3. honey suckle active material extracts: 6～8 portions of Flos Loniceraes step 1. weighed, boiling three times, each 2h,
Amount of water flooded Flos Lonicerae surface 1cm～1.5cm every time, merged three decoction liquor, and after being cooled to room temperature, regulation pH value is to 3.0,
Then filtering, gained filtrate is adsorbed with macroporous adsorptive resins, and flow velocity is 2.5BV/h～3.5BV/h, then enters with water
Row eluting, flow velocity be flow velocity be 2.5BV/h～3.5BV/h, eluting 20min～40min, more successively with 10% ethanol, 25%
Ethanol and 45% ethanol carry out eluting, flow velocity is 2.5BV/h～3.5BV/h, and elution time is 50minmin～70min,
Merge four gained eluents, obtain honey suckle active extract；
4. Rhizoma Zingiberis Recens active substance extracts: 3～5 portions of Rhizoma Zingiberis Recenss step 1. weighed are divided into three parts, use surname extraction respectively
Device carries out reflux, extract, reflux, extract, 20min～40min to three portions of Rhizoma Zingiberis Recenss, merges three parts of extracting solution, steams with Rotary Evaporators
Dry, obtain active substance, be subsequently adding the ethanol of 50% and be configured to the solution that mass concentration is 20%～30% of active substance,
Obtain Rhizoma Zingiberis Recens activity extract；Wherein said reflux, extract, parameter is: extractant is the ethanol of 80%, uses every time and carries
The mass ratio of the quality and every portion of Rhizoma Zingiberis Recens that take agent is 4～6:1；
5. China medicinal stone active material extracts: 9～11 parts of Maifanitums step 1. weighed mix with deionized water, are placed in boiling water
In bath, water carries twice, and each solid-liquid ratio is 1:5, and each water carries the time and is 20min～40min, and water goes to after carrying respectively
Carrying out homogenizing in homogenizer, each homogenizing time is 20min～40min, after merging Aqueous extracts in rotating speed is
Under conditions of 3500rpm/min～4500rpm/min, centrifugal 10min～20min, takes supernatant thing, obtains China medicinal stone active and extracts
Thing；
6. compound Chinese medicinal stone function extracting solution is prepared: the gold that 3. the Herba Leonuri activity extract that step 2. obtained, step obtain
Rhizoma Zingiberis Recens activity extract that 4. Flos Lonicerae activity extract, step obtain and the China medicinal stone active extract that 5. step obtains mixing are all
Even, obtain compound Chinese medicinal stone function extracting solution；
7. Maifanitum composite fibre is prepared: in the compound Chinese medicinal stone function extracting solution that 6. step obtains, add what 1. step weighed
2～4 parts of viscoses, stir 10min～20min under conditions of rotating speed is 700rpm/min～900rpm/min, obtain Maifanitum
Composite fibre；
Two, skin-material is prepared: Maifanitum composite fibre, acid fiber by polylactic and the tencel fiber step one prepared are according to matter
Amount ratio makes yarn for 1:1:1 blending, then according to yarn is interweaved on four satin weave once by the weave of satin weave
Tissue, obtains sanitary towel's compound Chinese medicinal stone functional fibre skin-material.
Detailed description of the invention four: present embodiment is unlike detailed description of the invention three: step one 1. in claim by mass fraction
Take 10 parts of Maifanitums, 8 parts of Herba Leonuris, 7 portions of Flos Loniceraes, 4 portions of Rhizoma Zingiberis Recenss and 3 parts of viscoses, standby.Other steps and parameter
Identical with detailed description of the invention three.
Detailed description of the invention five: present embodiment is unlike detailed description of the invention three or four: step one 2. in by step 1.
7～the 8 parts of Herba Leonuris weighed, boiling three times, each 2h, each amount of water flooded Herba Leonuri surface 1.5cm, closed
And once filter after three decoction liquor, then the filtrate once filtered is concentrated, obtain once concentration liquid after cooling, so
Rear addition and the ethanol of once concentration liquid equivalent, stir evenly standing, obtain secondary filtrate and filtering residue after secondary filter, and filtering residue is used
The washing with alcohol of 45%, obtains cleaning mixture, then cleaning mixture and secondary filtrate is merged, and being evaporated to density is 1.20,
Obtain Herba Leonuri activity extract.Other steps and parameter are identical with detailed description of the invention three or four.
Detailed description of the invention six: present embodiment is unlike one of detailed description of the invention three to five: step one is 3. middle will step
The rapid 6～8 portions of Flos Loniceraes 1. weighed, boiling three times, each 2h, each amount of water flooded Flos Lonicerae surface 1.5cm,
Merging three decoction liquor, after being cooled to room temperature, regulation pH value is to 3.0, then filters, gained filtrate macroporous adsorbent resin
Post adsorbs, and flow velocity is 3BV/h, then carries out eluting with water, flow velocity be flow velocity be 3BV/h, eluting 30min, then
Carrying out eluting with the ethanol of the ethanol of 10%, the ethanol of 25% and 45% successively, flow velocity is 3BV/h, and elution time is
60min, merges four gained eluents, obtains honey suckle active extract.Other steps and parameter and detailed description of the invention
One of three to five identical.
Detailed description of the invention seven: present embodiment is unlike one of detailed description of the invention three to six: step one is 4. middle will step
The rapid 3～5 portions of Rhizoma Zingiberis Recenss 1. weighed are divided into three parts, with apparatus,Soxhlet's, three portions of Rhizoma Zingiberis Recenss are carried out reflux, extract, respectively, return
Stream extracts 30min, merges three parts of extracting solution, is evaporated with Rotary Evaporators, obtains active substance, be subsequently adding the second of 50%
Alcohol is configured to the solution that mass concentration is 25% of active substance, obtains Rhizoma Zingiberis Recens activity extract.Other steps and parameter with
One of detailed description of the invention three to six is identical.
Detailed description of the invention eight: present embodiment is unlike one of detailed description of the invention three to seven: step one 4. in every time
Using the quality of extractant is 5:1 with the mass ratio of every portion of Rhizoma Zingiberis Recens.Other steps and parameter and detailed description of the invention three to seven
One of identical.
Detailed description of the invention nine: present embodiment is unlike one of detailed description of the invention three to eight: step one is 5. middle will step
The rapid 9～11 parts of Maifanitums 1. weighed mix with deionized water, are placed in water in boiling water bath and carry twice, and each solid-liquid ratio is 1:5,
Every time water carries the time and is 30min, and water goes to carry out in homogenizer homogenizing respectively after carrying, each homogenizing time is 30min,
Under conditions of rotating speed is 4000rpm/min, it is centrifuged 15min after merging Aqueous extracts, takes supernatant thing, obtain China medicinal stone active and carry
Take thing.Other steps and parameter are identical with one of detailed description of the invention three to eight.
Detailed description of the invention ten: present embodiment is unlike one of detailed description of the invention three to nine: step one 7. in step
The rapid compound Chinese medicinal stone function extracting solution 6. obtained adds 2～4 parts of viscoses that 1. step weighs, is 800rpm/min at rotating speed
Under conditions of stir 15min.Other steps and parameter are identical with one of detailed description of the invention three to nine.
By following verification experimental verification beneficial effects of the present invention
Test one, the compound Chinese medicinal stone functional fibre skin-material of a kind of sanitary towel of this test are pressed mass fraction and are answered by Maifanitum
Condensating fiber, acid fiber by polylactic and tencel fiber are prepared from according to mass ratio 1:1:1；Described Maifanitum composite fibre is pressed
Mass fraction is prepared from by 10 parts of Maifanitums, 8 parts of Herba Leonuris, 7 portions of Flos Loniceraes, 4 portions of Rhizoma Zingiberis Recenss and 3 parts of viscoses.
Test two, preparation are tested the compound Chinese medicinal stone functional fibre skin-material of a kind of sanitary towel of the present invention as described in
Preparation method sequentially includes the following steps:
One, the preparation of Maifanitum composite fibre:
1. raw material is weighed: weigh 10 parts of Maifanitums, 8 portions of Herba Leonuris, 7 portions of Flos Loniceraes, 4 portions of Rhizoma Zingiberis Recenss and 3 by mass fraction
Part viscose, standby；
2. Herba Leonuri active substance extracts: 8 parts of Herba Leonuris step 1. weighed, boiling three times, each 2h, often
Secondary amount of water flooded Herba Leonuri surface 1.5cm, once filtered, the filter then will once filtered after merging three decoction liquor
Liquid concentrates, and obtains once concentration liquid, is subsequently adding and the ethanol of once concentration liquid equivalent, stir evenly standing, secondary mistake after cooling
Obtaining secondary filtrate and filtering residue after filter, filtering residue, by the washing with alcohol of 45%, obtains cleaning mixture, then by cleaning mixture and secondary
Filtrate merges, and being evaporated to density is 1.20, obtains Herba Leonuri activity extract；
3. honey suckle active material extracts: 7 portions of Flos Loniceraes step 1. weighed, boiling three times, each 2h, often
Secondary amount of water flooded Flos Lonicerae surface 1.5cm, merged three decoction liquor, and after being cooled to room temperature, regulation pH value is to 3.0, then
Filtering, gained filtrate is adsorbed with macroporous adsorptive resins, and flow velocity is 3BV/h, then carries out eluting with water, and flow velocity is
Flow velocity is 3BV/h, eluting 30min, then carries out eluting with the ethanol of the ethanol of 10%, the ethanol of 25% and 45% successively,
Flow velocity is 3BV/h, and elution time is 60min, merges four gained eluents, obtains honey suckle active extract；
4. Rhizoma Zingiberis Recens active substance extracts: 4 portions of Rhizoma Zingiberis Recenss step 1. weighed are divided into three parts, respectively with apparatus,Soxhlet's pair
Three portions of Rhizoma Zingiberis Recenss carry out reflux, extract, reflux, extract, 30min, merge three parts of extracting solution, are evaporated with Rotary Evaporators, are lived
Property material, be subsequently adding the ethanol of 50% and be configured to the solution that mass concentration is 25% of active substance, obtain Rhizoma Zingiberis Recens activity
Extract；Wherein said reflux, extract, parameter is: extractant is the ethanol of 80%, use every time the quality of extractant with
The mass ratio of every portion of Rhizoma Zingiberis Recens is 5:1；
5. China medicinal stone active material extracts: 10 parts of Maifanitums step 1. weighed mix with deionized water, are placed in boiling water bath
Middle water carries twice, and each solid-liquid ratio is 1:5, and each water carries the time and is 30min, and water goes in homogenizer after carrying respectively
Carrying out homogenizing, each homogenizing time is 30min, centrifugal under conditions of rotating speed is 4000rpm/min after merging Aqueous extracts
15min, takes supernatant thing, obtains China medicinal stone active extract；
6. compound Chinese medicinal stone function extracting solution is prepared: the gold that 3. the Herba Leonuri activity extract that step 2. obtained, step obtain
Rhizoma Zingiberis Recens activity extract that 4. Flos Lonicerae activity extract, step obtain and the China medicinal stone active extract that 5. step obtains mixing are all
Even, obtain compound Chinese medicinal stone function extracting solution；
7. Maifanitum composite fibre is prepared: in the compound Chinese medicinal stone function extracting solution that 6. step obtains, add what 1. step weighed
3 parts of viscoses, stir 15min under conditions of rotating speed is 800rpm/min and obtain Maifanitum composite fibre；
Two, skin-material is prepared: Maifanitum composite fibre, acid fiber by polylactic and the tencel fiber step one prepared are according to matter
Amount ratio makes yarn for 1:1:1 blending, then according to yarn is interweaved on four satin weave once by the weave of satin weave
Tissue, obtains sanitary towel's compound Chinese medicinal stone functional fibre skin-material.
(1) efficacy assessments of the compound Chinese medicinal stone sanitary towel of this test: gonococcus inhibition test finds the Maifanitum of this test
Sanitary towel has the woods autumn Neisseria causing gynaecopathia antibacterial and sterilizing ability is relatively strong, with equal price like product on the market
Comparing, sterilization ratio improves 12.3%；The average decrement of infusorian is 21.1%.
(2) safety evaluation of the compound Chinese medicinal stone sanitary towel of this test: acute dermal toxicity test finds percutaneous primary coating
After tested material, animal does not occurs Health cost effect in a short time.Rat performance without exception (behavior and clinical characteristics are without exception)；
What after acute skin irritation experimental rabbits cutaneous application facial film, local produced changes and tissue injury without inflammatory, without erythema, water
Swollen；After acute ocular irritation test rabbit eyeball surface contact tested material, institute is without inflammatory change and tissue injury.Cornea is without ulcer
Formed or muddy, iris normal, refer to palpebral conjunctiva and bulbar conjunctiva position blood vessel is normal, without edema；Skin allergy test is surveyed
Examination guinea pig skin is without erythema and edema, and sensitization rate 0.003% is in tolerance interval, without asthma, astasia or shock etc.
Severe allergy phenomenon.
Claims (10)
1. the compound Chinese medicinal stone functional fibre skin-material of a sanitary towel, it is characterised in that the compound Chinese medicinal stone of a kind of sanitary towel
Functional fibre skin-material by Maifanitum composite fibre, acid fiber by polylactic and tencel fiber according to mass ratio 1:1:1 preparation and
Become；Described Maifanitum composite fibre press mass fraction by 9～11 parts of Maifanitums, 7～8 parts of Herba Leonuris, 6～8 portions of Flos Loniceraes,
3～5 portions of Rhizoma Zingiberis Recenss and 2～4 parts of viscoses are prepared from.
The compound Chinese medicinal stone functional fibre skin-material of a kind of sanitary towel the most according to claim 1, it is characterised in that institute
The Maifanitum composite fibre stated by mass fraction by 10 parts of Maifanitums, 8 portions of Herba Leonuris, 7 portions of Flos Loniceraes, 4 portions of Rhizoma Zingiberis Recenss and 3
Part viscose is prepared from.
3. the preparation method of the compound Chinese medicinal stone functional fibre skin-material of a sanitary towel, it is characterised in that the method is by following
Step is carried out:
One, the preparation of Maifanitum composite fibre:
1. weigh raw material: by mass fraction weigh 9～11 parts of Maifanitums, 7～8 parts of Herba Leonuris, 6～8 portions of Flos Loniceraes, 3～5 parts
Rhizoma Zingiberis Recens and 2～4 parts of viscoses, standby；
2. Herba Leonuri active substance extracts: 7～8 parts of Herba Leonuris step 1. weighed, boiling three times, each 2h, often
Secondary amount of water flooded Herba Leonuri surface 1cm～1.5cm, once filters, then will once filter after merging three decoction liquor
Filtrate concentrate, obtain once concentration liquid after cooling, be subsequently adding and the ethanol of once concentration liquid equivalent, stir evenly standing, two
Obtaining secondary filtrate and filtering residue after secondary filtration, filtering residue, by the washing with alcohol of 40%～50%, obtains cleaning mixture, then by cleaning mixture
Merging with secondary filtrate, being evaporated to density is 1.10～1.30, obtains Herba Leonuri activity extract；
3. honey suckle active material extracts: 6～8 portions of Flos Loniceraes step 1. weighed, boiling three times, each 2h, often
Secondary amount of water flooded Flos Lonicerae surface 1cm～1.5cm, merged three decoction liquor, and after being cooled to room temperature, regulation pH value is to 3.0,
Then filtering, gained filtrate is adsorbed with macroporous adsorptive resins, and flow velocity is 2.5BV/h～3.5BV/h, then carries out with water
Eluting, flow velocity be flow velocity be 2.5BV/h～3.5BV/h, eluting 20min～40min, more successively with 10% ethanol, 25%
Ethanol and 45% ethanol carry out eluting, flow velocity is 2.5BV/h～3.5BV/h, and elution time is 50minmin～70min,
Merge four gained eluents, obtain honey suckle active extract；
4. Rhizoma Zingiberis Recens active substance extracts: 3～5 portions of Rhizoma Zingiberis Recenss step 1. weighed are divided into three parts, use apparatus,Soxhlet's respectively
Three portions of Rhizoma Zingiberis Recenss are carried out reflux, extract, reflux, extract, 20min～40min, merge three parts of extracting solution, be evaporated with Rotary Evaporators,
Obtain active substance, be subsequently adding the ethanol of 50% and be configured to the solution that mass concentration is 20%～30% of active substance, obtain
Rhizoma Zingiberis Recens activity extract；Wherein said reflux, extract, parameter is: extractant is the ethanol of 80%, uses extractant every time
Quality is 4～6:1 with the mass ratio of every portion of Rhizoma Zingiberis Recens；
5. China medicinal stone active material extracts: 9～11 parts of Maifanitums step 1. weighed mix with deionized water, are placed in boiling water bath
Middle water carries twice, and each solid-liquid ratio is 1:5, and each water carries the time and is 20min～40min, and water goes to homogenizing after carrying respectively
Carrying out homogenizing in machine, each homogenizing time is 20min～40min, after merging Aqueous extracts in rotating speed is
Under conditions of 3500rpm/min～4500rpm/min, centrifugal 10min～20min, takes supernatant thing, obtains China medicinal stone active extract；
6. compound Chinese medicinal stone function extracting solution is prepared: the gold that 3. the Herba Leonuri activity extract that step 2. obtained, step obtain
Rhizoma Zingiberis Recens activity extract that 4. Flos Lonicerae activity extract, step obtain and the China medicinal stone active extract that 5. step obtains mixing are all
Even, obtain compound Chinese medicinal stone function extracting solution；
7. Maifanitum composite fibre is prepared: in the compound Chinese medicinal stone function extracting solution that 6. step obtains, add what 1. step weighed
2～4 parts of viscoses, stir 10min～20min under conditions of rotating speed is 700rpm/min～900rpm/min, obtain Maifanitum multiple
Condensating fiber；
Two, skin-material is prepared: Maifanitum composite fibre, acid fiber by polylactic and the tencel fiber step one prepared are according to matter
Amount ratio makes yarn for 1:1:1 blending, then according to yarn is interweaved on four satin weave group once by the weave of satin weave
Knit, obtain sanitary towel's compound Chinese medicinal stone functional fibre skin-material.
The preparation method of the compound Chinese medicinal stone functional fibre skin-material of a kind of sanitary towel the most according to claim 3, its
It is characterised by weighing 10 parts of Maifanitums, 8 portions of Herba Leonuris, 7 portions of Flos Loniceraes, 4 portions of Rhizoma Zingiberis Recenss and 3 by mass fraction during step one is 1.
Part viscose, standby.
The preparation method of the compound Chinese medicinal stone functional fibre skin-material of a kind of sanitary towel the most according to claim 3, its
It is characterised by during step one is 2. 7～8 parts of Herba Leonuris step 1. weighed, boiling three times, each 2h, each amount of water
Flooded Herba Leonuri surface 1.5cm, once filtered after merging three decoction liquor, then the filtrate once filtered was concentrated,
Obtain once concentration liquid after cooling, be subsequently adding and the ethanol of once concentration liquid equivalent, stir evenly standing, obtain after secondary filter
Secondary filtrate and filtering residue, filtering residue, by the washing with alcohol of 45%, obtains cleaning mixture, then cleaning mixture and secondary filtrate is merged,
Being evaporated to density is 1.20, obtains Herba Leonuri activity extract.
The preparation method of the compound Chinese medicinal stone functional fibre skin-material of a kind of sanitary towel the most according to claim 3, its
It is characterised by during step one is 3. 6～8 portions of Flos Loniceraes step 1. weighed, boiling three times, each 2h, each amount of water
Flooding Flos Lonicerae surface 1.5cm, and merged three decoction liquor, after being cooled to room temperature, regulation pH value is to 3.0, then filters, institute
Obtaining filtrate to adsorb with macroporous adsorptive resins, flow velocity is 3BV/h, then carries out eluting with water, and flow velocity is that flow velocity is
3BV/h, eluting 30min, then carry out eluting with the ethanol of the ethanol of 10%, the ethanol of 25% and 45% successively, flow velocity is
3BV/h, elution time is 60min, merges four gained eluents, obtains honey suckle active extract.
The preparation method of the compound Chinese medicinal stone functional fibre skin-material of a kind of sanitary towel the most according to claim 3, its
It is characterised by during step one is 4. that 3～5 portions of Rhizoma Zingiberis Recenss step 1. weighed are divided into three parts, respectively with apparatus,Soxhlet's to three parts
Rhizoma Zingiberis Recens carries out reflux, extract, reflux, extract, 30min, merges three parts of extracting solution, is evaporated with Rotary Evaporators, obtains active matter
Matter, is subsequently adding the ethanol of 50% and is configured to the solution that mass concentration is 25% of active substance, obtain Rhizoma Zingiberis Recens activity extract.
The preparation method of the compound Chinese medicinal stone functional fibre skin-material of a kind of sanitary towel the most according to claim 3, its
It is characterised by during step one is 4. that use the quality of extractant and the mass ratio of every portion of Rhizoma Zingiberis Recens is 5:1 every time.
The preparation method of the compound Chinese medicinal stone functional fibre skin-material of a kind of sanitary towel the most according to claim 3, its
It is characterised by during step one is 5. that 9～11 parts of Maifanitums step 1. weighed mix with deionized water, is placed in water in boiling water bath and carries two
Secondary, each solid-liquid ratio is 1:5, and each water carries the time and is 30min, and water goes to carry out in homogenizer homogenizing respectively after carrying,
Homogenizing time is 30min every time, is centrifuged 15min, takes after merging Aqueous extracts under conditions of rotating speed is 4000rpm/min
Clear thing, obtains China medicinal stone active extract.
The preparation method of the compound Chinese medicinal stone functional fibre skin-material of a kind of sanitary towel the most according to claim 3,
It is characterized in that in the compound Chinese medicinal stone function extracting solution that 6. step obtains, during step one is 7., add 2～4 parts that 1. step weighs
Viscose, stirs 15min under conditions of rotating speed is 800rpm/min.
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Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN113995573A (en) * | 2021-11-05 | 2022-02-01 | 广东德鑫制药有限公司 | Sanitary towel with odor removing and bacteria inhibiting functions and manufacturing method thereof |
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| Publication number | Priority date | Publication date | Assignee | Title |
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| CN102691153A (en) * | 2012-06-18 | 2012-09-26 | 绍兴县舒丽乐纺织品有限公司 | Medical stone fiber multi-component ecological home textile fabric |
| CN102733096A (en) * | 2012-06-13 | 2012-10-17 | 嘉兴学院 | Non-allergenic fully-degradable medical and hygienic non-woven material capable of adjusting moisture |
| CN102813956A (en) * | 2012-08-17 | 2012-12-12 | 天津市中科健新材料技术有限公司 | Thermal skin warming agent composition for disposable hygienic product and preparation method of thermal skin warming agent |
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Patent Citations (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN102733096A (en) * | 2012-06-13 | 2012-10-17 | 嘉兴学院 | Non-allergenic fully-degradable medical and hygienic non-woven material capable of adjusting moisture |
| CN102691153A (en) * | 2012-06-18 | 2012-09-26 | 绍兴县舒丽乐纺织品有限公司 | Medical stone fiber multi-component ecological home textile fabric |
| CN102813956A (en) * | 2012-08-17 | 2012-12-12 | 天津市中科健新材料技术有限公司 | Thermal skin warming agent composition for disposable hygienic product and preparation method of thermal skin warming agent |
Cited By (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN113995573A (en) * | 2021-11-05 | 2022-02-01 | 广东德鑫制药有限公司 | Sanitary towel with odor removing and bacteria inhibiting functions and manufacturing method thereof |
| CN113995573B (en) * | 2021-11-05 | 2022-07-22 | 广东德鑫制药有限公司 | Sanitary towel with functions of removing odor and inhibiting bacteria and manufacturing method thereof |
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