CN105853325A - Oolong shampoo shower gel and preparation method thereof - Google Patents

Oolong shampoo shower gel and preparation method thereof Download PDF

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Publication number
CN105853325A
CN105853325A CN201610220339.1A CN201610220339A CN105853325A CN 105853325 A CN105853325 A CN 105853325A CN 201610220339 A CN201610220339 A CN 201610220339A CN 105853325 A CN105853325 A CN 105853325A
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oolong tea
parts
oolong
preparation
oryza glutinosa
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曾海林
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Fujian Haishan Tea Industry Co Ltd
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Fujian Haishan Tea Industry Co Ltd
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    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00Cosmetics or similar toiletry preparations
    • A61K8/18Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/96Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution
    • A61K8/98Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution of animal origin
    • A61K8/987Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution of animal origin of species other than mammals or birds
    • A61K8/988Honey; Royal jelly, Propolis
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00Cosmetics or similar toiletry preparations
    • A61K8/18Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/19Cosmetics or similar toiletry preparations characterised by the composition containing inorganic ingredients
    • A61K8/26Aluminium; Compounds thereof
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00Cosmetics or similar toiletry preparations
    • A61K8/18Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/96Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution
    • A61K8/97Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution from algae, fungi, lichens or plants; from derivatives thereof
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61QSPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
    • A61Q19/00Preparations for care of the skin
    • A61Q19/10Washing or bathing preparations
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61QSPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
    • A61Q5/00Preparations for care of the hair
    • A61Q5/02Preparations for cleaning the hair

Abstract

The invention discloses an oolong shampoo shower gel and a preparation method thereof. The shampoo shower gel is prepared from oolong, glutinous rice, lemna minor, lalang grass rhizome, mulberry leaves, semen cassia, cowherb seeds, royal jelly, medical stones, ethacridine lactate, PEG-120 methyl glucose dioleate and coconut oil amphoteric diacetate disodium salt, wherein the oolong is decocted and extracted and then prepared into an essential oil and catechin extract; ozone is introduced when the sticky rice is soaked to prepare sticky rice pulp; other traditional Chinese medicinal components are decocted and then prepared into thick paste; the medical stone is crushed into the micron scale; other auxiliary materials are added to the processed raw materials and then prepared into the shampoo shower gel according to a conventional method. The oolong and effective ingredients of multiple plants are innovatively utilized; the oolong shampoo shower gel is abundant in medicine source, low in cost, simple in preparation technology, mild in cold-heat comprehensiveness from the angle of medicine compatibility, suitable for people with various skins for use, and wide in application range; and multiple small skin problems can be solved when the original skin protection and cleaning properties are kept.

Description

A kind of oolong tea shampoo used also as bath lotion and preparation method thereof
Technical field
The present invention relates to washing product field, specifically a kind of oolong tea shampoo used also as bath lotion and preparation method thereof.
Background technology
Along with improving constantly of living standard, people the most increasingly focus on the health bathing condition of self, and shampoo used also as bath lotion has become the necessary of each family, suitable with some shampoo used also as bath lotion products when having a bath, can effectively remove the oils and fats on skin and scurf, make us feeling the most comfortable;But use makes hair washing bath product with industrial chemicals more in the market, these raw materials include: cationic polymer, silicone oil, fatty alcohol polyoxyethylene ether sulfate, alkanolamide, glycine betaine, amine oxide etc., the chemical raw material majority of these chemical industry synthesis has stimulation to skin and hair, and the health of skin is harmful to by life-time service;In order to reduce the side effect of chemical raw material, people start progressively to make the transition toward natural plant raw material aspect, and natural plant raw material is applied and be there is several technical problem in shampoo used also as bath lotion: how to ensure the basic effect such as cleaning sterilization, how to propose a kind of simple and effective production technology and do not destroy plant effect;How to realize the mutual compatibility between plant to improve its effect;In the market in order to reach preferable skin protection cleaning effect, often there is problem expensive, that raw material is rare in the natural plant raw material of selection, it is impossible to meets large-scale marketization demand.
Oolong tea, also known as Folium Camelliae sinensis, the pharmacological action of oolong tea, outstanding behaviours reducing fat, the aspect such as defatting beauty, oolong tea reaches kind more than 450 containing organic chemical composition, inorganic mineral element reaches kind more than 40;Organic chemical composition and inorganic mineral element in Folium Camelliae sinensis contain many nutritional labelings and active ingredient, wherein: organic chemical composition mainly has: tea polyphenols, plant alkaloid, protein, aminoacid, vitamin, pectin element, organic acid, lipopolysaccharide, saccharide, enzyme, pigment etc.;Inorganic mineral element mainly has: potassium, calcium, magnesium, cobalt, ferrum, manganese, aluminum, sodium, zinc, copper, nitrogen, phosphorus, fluorine, etc.;The health care of oolong tea includes: eliminates harm beauty treatment and healthy active oxygen, improve skin allergy, weight reducing, antitumor, pre-anti-aging;Oolong tea has the fat-reducing effect of dissolved fat, and in tea, main constituent tannic acid can speed up the quantity of heat production increase of health, promotes fat combustion, the accumulation slimmed the abdomen;There is benefit think of of refreshing oneself, allaying tiredness, diuresis of promoting the production of body fluid, antipyretic sunstroke prevention, bactericidal antiphlogistic, cold relieving are relieved the effect of alcohol, diseases prevention of detoxifying, promoting digestion greasy, defatting beauty, blood fat reducing function.
Summary of the invention
It is an object of the invention to provide a kind of compatibility proper, cost of material is low, and production technology is simple, has no side effect, have antipruritic, the oolong tea shampoo used also as bath lotion and preparation method thereof of sterilize, moisten nutrition skin, uvioresistant, anti-cancer efficacy concurrently, with the problem solving to propose in above-mentioned background technology.
For achieving the above object, the present invention provides following technical scheme:
A kind of oolong tea shampoo used also as bath lotion, includes according to the component of weight portion: oolong tea 50-60 part, Oryza glutinosa 10-20 part, Herba Spirodelae 5-10 part, Rhizoma Imperatae 5-10 part, Folium Mori 5-10 part, Semen Cassiae 2-5 part, Semen Vaccariae 2-5 part, Lac regis apis 1-2 part, Maifanitum 5-9 part, ethacridine 0.5-1 part, PEG-120 methyl glucose dioleate 1-2 part, cocos nucifera oil both sexes two acetic acid disodium salt 0.6-1 part.
As the further scheme of the present invention: described oolong tea shampoo used also as bath lotion, include according to the component of weight portion: oolong tea 53-57 part, Oryza glutinosa 14-16 part, Herba Spirodelae 7-9 part, Rhizoma Imperatae 6-8 part, Folium Mori 7-9 part, Semen Cassiae 3-4 part, Semen Vaccariae 3-4 part, Lac regis apis 1-2 part, Maifanitum 6-8 part, ethacridine 0.6-0.8 part, PEG-120 methyl glucose dioleate 1-2 part, cocos nucifera oil both sexes two acetic acid disodium salt 0.7-0.9 part.
The preparation method of described oolong tea shampoo used also as bath lotion, comprises the following steps:
1) extraction of oolong tea effective ingredient:
1.1) oolong tea raw material is weighed by formula, oolong tea and purified water are pressed 1g: 10-12ml, temperature 80-90 DEG C, the condition steaming and decocting of time 40-60min, liquid of receiving guest with tea after steaming and decocting is cooled to initial filter when 15-20 DEG C, clear filtrate, again filter, obtain oolong tea extracting solution;
1.2) oolong tea extracting solution is distilled further that to obtain oolong tea volatile oil standby;
1.3) the oolong tea extracting solution after distillation being crossed chromatographic column and polymer ceramic film, isolated catechin solution, be concentrated in vacuo by catechin solution, thickening temperature is 50-70 DEG C, and being concentrated into 1/10th of original volume, to obtain catechin extractum standby;
2) extraction of Oryza glutinosa effective ingredient: weigh Oryza glutinosa by formula, the weight ratio with 1: 1 adds purified water in the Oryza glutinosa after cleaning, and stirs with the rotating speed of 20r/min, every 20min is filled with an ozone in water, Oryza glutinosa soaking and stirring 24-30h, pulverizes and filters, and obtains Oryza glutinosa juice standby;
3) Herba Spirodelae, Rhizoma Imperatae, Folium Mori, Semen Cassiae and Semen Vaccariae are weighed by formula, the purified water adding 15 times of weight after cleaning mixing decocts extraction twice under the conditions of 95-105 DEG C, 30-40min every time, put to room temperature after merging twice extracting solution, using 300 mesh filter-cloth filterings, the Chinese medicine composition thick paste that filtrate is condensed into original solution 1/5th volume under the conditions of 45 DEG C is standby;
4) weighing Maifanitum by formula, the maifanite powder being ground into particle diameter < 10 microns is standby;
5) the maifanite powder mixing that will prepare in the Chinese medicine composition thick paste of preparation, step 4 in the Oryza glutinosa juice of preparation, step 3 in the oolong tea volatile oil prepared in step 1 and catechin extractum, step 2, add the Lac regis apis of formula ratio, ethacridine, PEG-120 methyl glucose dioleate and the stirring mixing of cocos nucifera oil both sexes two acetic acid disodium salt, make oolong tea shampoo used also as bath lotion emulsion according to a conventional method;
6) in detecting step 5, oolong tea shampoo used also as bath lotion emulsion carries out microorganism species detection, detects qualified rear sealed packaging warehouse-in, obtains finished product.
As the present invention further scheme: the filter cloth using filter opening aperture to be 150 microns in described step 1.1 carries out initial filter.
As the present invention further scheme: the oolong tea extracting solution addition Fructus Citri Limoniae acid for adjusting pH of preparation in described step 1.1 is standby to 5.8-6.2.
As the present invention further scheme: in described step 2, in soak, ozone concentration is 0.4-0.6mg/L.
In the present invention, effect of each component is as follows:
1. oolong tea: rich in multiple organic chemical composition and inorganic mineral element, containing many nutritional labelings and active ingredient, organic chemical composition mainly has: tea polyphenols, plant alkaloid, protein, aminoacid, vitamin, pectin element, organic acid, lipopolysaccharide, saccharide, enzyme, pigment etc., and inorganic mineral element mainly has: potassium, calcium, magnesium, cobalt, ferrum, manganese, aluminum, sodium, zinc, copper, nitrogen, phosphorus, fluorine, etc.;It is good that oolong Oleum Camelliae moistens moistening effect, defying age, prevention cutin hardening;Catechin can strengthen skin surface metabolism, removes skin surface free radical, protects cell membrane, and antioxidant activity is high, has radioprotective, uvioresistant, mutation effect.
2. Oryza glutinosa: containing protein, nicotinic acid, fat, saccharide, calcium, phosphorus, ferrum, vitamin B and amylopectin etc., have beauty treatment to lengthen one's life, relaxing muscles and tendons to promote blood circulation, hair care improving eyesight, lock effect such as water skin protection;Waxy big, stickiness is also big, mouthfeel is satiny, can warm taste, strengthening QI of middle-JIAO, to Deficiency and coldness of spleen and stomach, be off one's feed, abdominal distention diarrhoea has certain mitigation;There is astringent therapy effect, frequent micturition, night sweat are had preferable curative effect.
3. Herba Spirodelae: containing flavonoid and the materials such as iodine, bromine such as the water soluble vitamins such as volume vitamin B1, B2, C, luteolin-7-β-glycoside, 8-hydroxyl luteolin-8-β-glycosides, its polysaccharide is the abundant source of D-apiose.Resinous, waxiness, steroid, chlorophyll, sugar, protein, phlegmatic temperament, tannin etc.;Enter lung meridian;Diaphoresis, dispels the wind, row water, heat clearing away, removing toxic substances;Row hot carbuncle when controlling, macule is impermeable, wind heat pain rash, skin pruritus, edema, amenorrhea, skin ulcer tinea, and erysipelas is scalded;Antipyretic antibacterial;" not Lu ": the therapeutic method to keep the adverse QI flowing downwards, with piliation of taking a shower;" herbal classic ": main sudden high fever itching over the body, lower aqueous vapor, wins wine, long beard and hair, only quenches one's thirst.
4. Rhizoma Imperatae: return lung, stomach, bladder warp;Sweet in the mouth, cold in nature;Spit blood for heat in blood, epistaxis, hematuria, calentura excessive thirst, cough due to lung-heat, gastropyretic vomiting, jaundice due to damp-heat, edema oliguria, the puckery pain of pyretic stranguria;" Handbook of Prescriptions for Emergencies " is recorded, bamboo wood incarnation, and Rhizoma Imperatae burns end, leaf fat and painting, and wind enters into swollen person, the best.
5. Folium Mori: bitter in the mouth, sweet, cold in nature;Return lung, Liver Channel;Dispelling wind and heat pathogens, clearing away lung-heat and moistening for dryness, suppressing the hyperactive liver improving eyesight, cooling blood for hemostasis;" book on Chinese herbal medicine cover bamboo fish trap " is recorded: adopts and boils soup through frost person, washes eye and go lacrimation induced by wind pathogen very to win, and salt is smash deposited snakeworm Scolopendra and stung poison, steams to smash and scolds that to flutter damage blood stasis band solidifying;Decocting for tea, consumer edema foot floats, and the therapeutic method to keep the adverse QI flowing downwards makes joint profit;Grinding and dissipate, soup is adjusted;Only cholera is vomited and diarrhoea, and perspires except migratory arthralgia is ached;Process and decoct dense with Mulberry clothing, control dysentery all wounds hemostasis;" herbal classic is met former " is recorded: Folium Mori lung heat clearing stomach, goes wind improving eyesight;The frost person that learns from else's experience decocts soup, washes tear under wind-eye;Taking for a long time with Semen Sesami Nigrum honeyed pill, beard and hair is not white, the most always prolongs life;The meaning of wind pain perspiration smash in " herbal classic " speech except cold and heat perspiration, i.e. " the brightest " cook, and decocts drink profit the five internal organs, the therapeutic method to keep the adverse QI flowing downwards of getting round by bribery;Decoct wine clothes, control a wind cutting;Radix Mori ashing drenches juice, with Calx point face windward, nevus of going out, goes to dislike meat.
6. Semen Cassiae: sweet in the mouth, hardship, salty, cold nature, return liver, large intestine channel;Can clearing away heat to improve acuity of vision, loosening bowel to relieve constipation;" China's book on Chinese herbal medicine " carries and says: liver heat removing kidney tonifying, improving eyesight, diuretic relieving constipation;Curing mainly conjunctival congestion and swelling pain, photophobia tear is many, optic atrohic blindness, nyctalopia, headache and dizzy, poor vision, cirrhotic ascites, dysuria, habitual constipation;External treatment toxic swelling, tinea.
7. Semen Vaccariae: bitter in the mouth, property is put down;Return liver, stomach warp;Promoting blood circulation to restore menstrual flow, stimulating milk secretion detumescence, inducing diuresis for treating stranguria syndrome;Holy Benevolent Prescriptions records seborrheic dermatitis of the scalp: Semen Vaccariae, Radix Angelicae Dahuricae (Radix Heraclei Scabridi) decile, for end, dry mixes, and a night combs and goes;" prescriptions worth thousand gold " record all skin ulcers of carbuncle: Semen Vaccariae soup, control carbuncle acute mastitis, and lunar eclipse is the baldst, and long skin ulcer on face;Worming pain relieving: draw each five liang of Fructus Evodiae root bark with Semen Vaccariae, southeast Ramulus Persicae, east, Fructus Cnidii, Fructus Viticis Cannabifoliae, Folium Pleioblasti, each three liters of disease puncture, Semen Ricini one liter, with water two bucket half, boil and take a pipeful of, again and again wash it.
8. Lac regis apis: containing protein, fat, saccharide, vitamin A, vitamin B1, vitamin B2, abundant folic acid, pantothenic acid and inositol, and the aminoacid of multiple human body needs and bio-hormone etc.;Lac regis apis is rich in estrogen, containing the fatty acids of more than 26 kinds, 10-HAD, and content is more than 1.4%;The superoxide dismutase (SOD) detected in Lac regis apis is antioxidative main component;10-HAD and royal jelly major protein-1 can control vasodilation, reduce blood pressure;Lac regis apis has antibacterial and has the effect promoting healing to wound infection;The antimicrobial spectrum of Lac regis apis is escherichia coli, Staphylococcus aureus Bacillus typhi, streptococcus, Bacillus proteus, bacillus subtilis, tubercule bacillus, starlike Trichophyton and epidermophyton etc..
9. Maifanitum: main chemical compositions is inorganic aluminosilicate, in water, 20 various trace elements necessary to the human body such as leachable potassium, sodium, calcium, magnesium, silicon, violent, titanium, phosphorus, have two-ways regulation water ph value function, Maifanitum as Chinese medicine to dermatosis, particularly drawing out the pus, effect is fine.
Compared with prior art, the invention has the beneficial effects as follows: the employing oolong tea of novelty of the present invention is aided with other several pars, crude drug or plant as main component and is prepared as shampoo used also as bath lotion, prescription is natural to have no side effect, volatile oil in oolong tea can play lock water, moisten effect, polyphenols, catechin are provided that stronger antioxidation, increase skin toxin expelling metabolism, coordinate with remaining several component, sterilization, antiinflammatory, skin moistening skin protection, hair-growing and hair care, regulation skin and the function of scalp water and oil balance can be realized;Catechin in oolong tea can also strengthen the lipase inhibitory action of Semen Cassiae, strengthens Lac regis apis, the antiinflammation of Semen Vaccariae, strengthens the itching-relieving action of Folium Mori, reduces Oryza glutinosa anaphylactogen, improves the soft degree of product, uses safer, non-stimulated;From the point of view of compatibility of drugs angle, cold and heat are comprehensive flat, the people being suitable for various skin quality uses, the auxiliary property of medicine plus Maifanitum and ethacridine, the shampoo used also as bath lotion making the present invention can solve multiple skin minor issue while keeping its script skin protection clean-up performance, anti-inflammation and sterilization effect more persistently effectively, has efficiently, wide spectrum, low drug resistance and the high feature of safety coefficient;Shampoo used also as bath lotion of the present invention makes full use of the effective ingredient of oolong tea and various plants, and medicine source is abundant, advantage of lower cost, and the extraction of effective ingredient all uses extract at low temperature, can ensure the activity of each effective ingredient to greatest extent, simple to operate, applied range.
Detailed description of the invention
Below in conjunction with detailed description of the invention, the technical scheme of this patent is described in more detail.
Embodiment 1
A kind of oolong tea shampoo used also as bath lotion, includes according to the component of weight portion: oolong tea 50 parts, 10 parts of Oryza glutinosa, 5 parts of Herba Spirodelae, Rhizoma Imperatae 5 parts, 5 parts of Folium Mori, Semen Cassiae 2 parts, Semen Vaccariae 2 parts, Lac regis apis 1 part, Maifanitum 5 parts, ethacridine 0.5 part, PEG-120 methyl glucose dioleate 1 part, cocos nucifera oil both sexes two acetic acid disodium salt 0.6 part.
Embodiment 2
A kind of oolong tea shampoo used also as bath lotion, includes according to the component of weight portion: oolong tea 60 parts, 20 parts of Oryza glutinosa, 10 parts of Herba Spirodelae, Rhizoma Imperatae 10 parts, 10 parts of Folium Mori, Semen Cassiae 5 parts, Semen Vaccariae 5 parts, Lac regis apis 2 parts, Maifanitum 9 parts, ethacridine 1 part, PEG-120 methyl glucose dioleate 2 parts, cocos nucifera oil both sexes two acetic acid disodium salt 1 part.
Embodiment 3
A kind of oolong tea shampoo used also as bath lotion, includes according to the component of weight portion: oolong tea 53 parts, 14 parts of Oryza glutinosa, 7 parts of Herba Spirodelae, Rhizoma Imperatae 6 parts, 7 parts of Folium Mori, Semen Cassiae 3 parts, Semen Vaccariae 3 parts, Lac regis apis 1 part, Maifanitum 6 parts, ethacridine 0.6 part, PEG-120 methyl glucose dioleate 1 part, cocos nucifera oil both sexes two acetic acid disodium salt 0.7 part.
Embodiment 4
A kind of oolong tea shampoo used also as bath lotion, includes according to the component of weight portion: oolong tea 57 parts, 16 parts of Oryza glutinosa, 9 parts of Herba Spirodelae, Rhizoma Imperatae 8 parts, 9 parts of Folium Mori, Semen Cassiae 4 parts, Semen Vaccariae 4 parts, Lac regis apis 2 parts, Maifanitum 8 parts, ethacridine 0.8 part, PEG-120 methyl glucose dioleate 2 parts, cocos nucifera oil both sexes two acetic acid disodium salt 0.9 part.
Embodiment 5
A kind of oolong tea shampoo used also as bath lotion, includes according to the component of weight portion: oolong tea 55 parts, 15 parts of Oryza glutinosa, 7.5 parts of Herba Spirodelae, Rhizoma Imperatae 7.5 parts, 7.5 parts of Folium Mori, Semen Cassiae 3.5 parts, Semen Vaccariae 3.5 parts, Lac regis apis 1.5 parts, Maifanitum 7 parts, ethacridine 0.8 part, PEG-120 methyl glucose dioleate 1.5 parts, cocos nucifera oil both sexes two acetic acid disodium salt 0.8 part.
The preparation method of the oolong tea shampoo used also as bath lotion described in embodiment 1-5, comprises the following steps:
1) extraction of oolong tea effective ingredient:
1.1) oolong tea raw material is weighed by formula, oolong tea and purified water are pressed 1g: 10-12ml, temperature 80-90 DEG C, the condition steaming and decocting of time 40-60min, the filter cloth using filter opening aperture to be 150 microns when liquid of receiving guest with tea after steaming and decocting is cooled to 15-20 DEG C carries out initial filter, clear filtrate, again filter, obtain oolong tea extracting solution, add Fructus Citri Limoniae acid for adjusting pH standby to 5.8-6.2;
1.2) oolong tea extracting solution is distilled further that to obtain oolong tea volatile oil standby;
1.3) the oolong tea extracting solution after distillation being crossed chromatographic column and polymer ceramic film, isolated catechin solution, be concentrated in vacuo by catechin solution, thickening temperature is 50-70 DEG C, and being concentrated into 1/10th of original volume, to obtain catechin extractum standby;
2) extraction of Oryza glutinosa effective ingredient: weigh Oryza glutinosa by formula, weight ratio with 1: 1 adds purified water in the Oryza glutinosa after cleaning, stir with the rotating speed of 20r/min, every 20min is filled with an ozone in water, in soak, ozone concentration is 0.4-0.6mg/L, Oryza glutinosa soaking and stirring 24-30h, pulverizes and filters, and obtains Oryza glutinosa juice standby;
3) Herba Spirodelae, Rhizoma Imperatae, Folium Mori, Semen Cassiae and Semen Vaccariae are weighed by formula, the purified water adding 15 times of weight after cleaning mixing decocts extraction twice under the conditions of 95-105 DEG C, 30-40min every time, put to room temperature after merging twice extracting solution, using 300 mesh filter-cloth filterings, the Chinese medicine composition thick paste that filtrate is condensed into original solution 1/5th volume under the conditions of 45 DEG C is standby;
4) weighing Maifanitum by formula, the maifanite powder being ground into particle diameter < 10 microns is standby;
5) the maifanite powder mixing that will prepare in the Chinese medicine composition thick paste of preparation, step 4 in the Oryza glutinosa juice of preparation, step 3 in the oolong tea volatile oil prepared in step 1 and catechin extractum, step 2, add the Lac regis apis of formula ratio, ethacridine, PEG-120 methyl glucose dioleate and the stirring mixing of cocos nucifera oil both sexes two acetic acid disodium salt, make oolong tea shampoo used also as bath lotion emulsion according to a conventional method;
6) in detecting step 5, oolong tea shampoo used also as bath lotion emulsion carries out microorganism species detection, detects qualified rear sealed packaging warehouse-in, obtains finished product.
Below in conjunction with experimental data or detection data, effect of the present invention is further elaborated.
1) present invention is carried out the mensuration of antiinflammatory fungistatic effect, specific as follows:
1.1) aerobe fungistatic effect measures:
Use the oolong tea shampoo used also as bath lotion of the embodiment of the present invention 5 preparation as experimental drug, respectively the bacterial strains such as known staphylococcus aureus, shigella flexneri, escherichia coli, dysentery bacterium, streptococcus faecalis are made fungistatic effect test, result of the test such as following table, and bacterial strain is test strain in following table, without specific requirements, and conventional method isolated can be passed through:
Strains tested Staphylococcus aureus Shigella flexneri Escherichia coli Dysentery bacterium Streptococcus faecalis
Inhibition zone diameter (mm) 10.5 10.0 10.2 10.3 10.5
1.2) measurement result of minimum inhibitory concentration is as follows:
Being drawn by above experiment, the present invention all at more than 10mm to above-mentioned bacterial strains inhibition zone diameter, has long-acting lasting fungistatic effect, and determines minimum inhibitory concentration.
2.1) anaerobe fungistatic effect mensuration
Use the oolong tea shampoo used also as bath lotion of the embodiment of the present invention 5 preparation as experimental drug, bacillus perfringens, clostridium tetani, the black bacteroid of product, bacteroides fragilis, propionibacterium acnes and common Candida albicans etc. to anaerobism makees fungistatic effect test respectively, result of the test such as following table, and bacterial strain is test strain in following table, without specific requirements, and conventional method isolated can be passed through:
2.2) measurement result of minimum inhibitory concentration is as follows:
Being drawn by above experiment, antiinflammatory inhibiting-bacteria preparation of the present invention all at more than 10mm to above-mentioned bacterial strains inhibition zone diameter, has long-acting lasting fungistatic effect, and determines minimum inhibitory concentration.
3) nutrient measures:
In the present invention, amino acid classes is: aspartic acid, glutamic acid, serine, histidine, glycine, threonine, arginine, alanine, tyrosine, valine, methionine, phenylalanine, isoleucine, leucine, lysine, proline, total content 88.7mg/100g;Polysaccharide 3.58g/100ml, and containing vitamin B1, B2, C, K, E etc., especially with vitamin B1, B2, E for many, rich in SOD.
Rich in several amino acids, vitamin, polysaccharide in the present invention, to strengthening skin, mucosa resistance and nutrition skin, there is remarkable efficacy.
4) safety toxicity test
The product using the embodiment of the present invention 5 preparation carries out acute toxicity test, local skin test and mucosa stimulation test.
4.1) acute toxicity test
The product embodiment of the present invention 5 prepared uses kunming mice body weight 20-25 gram 20, male and female half and half, tests by abdomen injection and administration by gavage.
Experimental result is as follows:
A. intraperitoneal injection: LD 50=2.018g/kg;Average fiducial limit=2.018 ± 0.1437k/kg
B. administration by gavage: mouse stomach, no abnormality seen are reacted with the product 2 times/day prepared more than the embodiment of the present invention 5 of ten multiple doses.
4.2) local skin test
The product using the embodiment of the present invention 5 preparation carries out to animal that local skin is excitatory, sensitization and absorption test, experimental result is as follows: the present invention is to Cavia porcellus is complete and damaged skin is without excitatory, the most nontoxic and sensitization, can not be absorbed by complete and damaged skin and be caused and be poisoned to death.
4.3) mucomembranous irritant test
Use the embodiment of the present invention 5 preparation product rabbit and doggie are carried out wound surface mucosa stimulation test, result is as follows: the present invention to mucosa without irritating, also without pathologic lesion.
Above-mentioned toxicological test confirm the present invention be a kind of harmless, nontoxic, have no side effect, the washing product that non-stimulated, safety coefficient is big;In sum, the present invention have efficiently, broad-spectrum antibacterial effect;Drug resistance is low;Skin, mucosa resistance and nutrition skin can be strengthened;And safety coefficient is high, harmless, nontoxic, have no side effect, non-stimulated.
Above the better embodiment of this patent is explained in detail, but this patent is not limited to above-mentioned embodiment, in the ken that one skilled in the relevant art is possessed, it is also possible to various changes can be made on the premise of without departing from this patent objective.

Claims (7)

1. an oolong tea shampoo used also as bath lotion, it is characterised in that include according to the component of weight portion: oolong tea 50-60 part, Oryza glutinosa 10-20 part, Herba Spirodelae 5-10 part, Rhizoma Imperatae 5-10 part, Folium Mori 5-10 part, Semen Cassiae 2-5 part, Semen Vaccariae 2-5 part, Lac regis apis 1-2 part, Maifanitum 5-9 part, ethacridine 0.5-1 part, PEG-120 methyl glucoside two oleic acid Ester 1-2 part, cocos nucifera oil both sexes two acetic acid disodium salt 0.6-1 part.
Oolong tea shampoo used also as bath lotion the most according to claim 1, it is characterised in that include according to the component of weight portion: Oolong tea 53-57 part, Oryza glutinosa 14-16 part, Herba Spirodelae 7-9 part, Rhizoma Imperatae 6-8 part, Folium Mori 7-9 part, Semen Cassiae 3-4 Part, Semen Vaccariae 3-4 part, Lac regis apis 1-2 part, Maifanitum 6-8 part, ethacridine 0.6-0.8 part, PEG-120 first Base glucose dioleates 1-2 part, cocos nucifera oil both sexes two acetic acid disodium salt 0.7-0.9 part.
Oolong tea shampoo used also as bath lotion the most according to claim 2, it is characterised in that include according to the component of weight portion: Oolong tea 55 parts, 15 parts of Oryza glutinosa, 7.5 parts of Herba Spirodelae, Rhizoma Imperatae 7.5 parts, 7.5 parts of Folium Mori, Semen Cassiae 3.5 parts, king Do not stay row 3.5 parts, Lac regis apis 1.5 parts, Maifanitum 7 parts, ethacridine 0.8 part, PEG-120 methyl glucoside two oil Acid esters 1.5 parts, cocos nucifera oil both sexes two acetic acid disodium salt 0.8 part.
4. the preparation method of an oolong tea shampoo used also as bath lotion as claimed in claim 1, it is characterised in that include following step Rapid:
1) extraction of oolong tea effective ingredient:
1.1) weigh oolong tea raw material by formula, oolong tea and purified water are pressed 1g: 10-12ml, temperature 80-90 DEG C, time Between the condition steaming and decocting of 40-60min, liquid of receiving guest with tea after steaming and decocting is cooled to initial filter when 15-20 DEG C, clear filtrate, again filters, To oolong tea extracting solution;
1.2) oolong tea extracting solution is distilled further that to obtain oolong tea volatile oil standby;
1.3) the oolong tea extracting solution after distillation is crossed chromatographic column and polymer ceramic film, isolated catechin solution, will Catechin solution is concentrated in vacuo, and thickening temperature is 50-70 DEG C, and being concentrated into 1/10th of original volume, to obtain catechin extractum standby With;
2) extraction of Oryza glutinosa effective ingredient: weigh Oryza glutinosa by formula, the weight ratio with 1: 1 adds in the Oryza glutinosa after cleaning Purified water, stirs with the rotating speed of 20r/min, and every 20min is filled with an ozone in water, Oryza glutinosa soaking and stirring 24-30h, Pulverize and filter, obtain Oryza glutinosa juice standby;
3) weigh Herba Spirodelae, Rhizoma Imperatae, Folium Mori, Semen Cassiae and Semen Vaccariae by formula, after cleaning mixing, add 15 times of weight Purified water under the conditions of 95-105 DEG C, decoct extraction twice, each 30-40min, put to room temperature after merging twice extracting solution, Using 300 mesh filter-cloth filterings, the Chinese medicine composition thick paste that filtrate is condensed into original solution 1/5th volume under the conditions of 45 DEG C is standby With;
4) weighing Maifanitum by formula, the maifanite powder being ground into particle diameter < 10 microns is standby;
5) by the Oryza glutinosa juice of preparation, step 3 in the oolong tea volatile oil prepared in step 1 and catechin extractum, step 2 The Chinese medicine composition thick paste of middle preparation, step 4 prepare maifanite powder mixing, add formula ratio Lac regis apis, Ethacridine, PEG-120 methyl glucose dioleate and the stirring mixing of cocos nucifera oil both sexes two acetic acid disodium salt, according to a conventional method Make oolong tea shampoo used also as bath lotion emulsion;
6) in detecting step 5, oolong tea shampoo used also as bath lotion emulsion carries out microorganism species detection, detects qualified rear sealed packaging Warehouse-in, obtains finished product.
The preparation method of oolong tea shampoo used also as bath lotion the most according to claim 4, it is characterised in that described step 1.1 Middle employing filter opening aperture is that the filter cloth of 150 microns carries out initial filter.
The preparation method of oolong tea shampoo used also as bath lotion the most according to claim 4, it is characterised in that described step 1.1 It is standby to 5.8-6.2 that the oolong tea extracting solution of middle preparation adds Fructus Citri Limoniae acid for adjusting pH.
The preparation method of oolong tea shampoo used also as bath lotion the most according to claim 4, it is characterised in that in described step 2 In soak, ozone concentration is 0.4-0.6mg/L.
CN201610220339.1A 2016-04-11 2016-04-11 Oolong shampoo shower gel and preparation method thereof Pending CN105853325A (en)

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CN108578331A (en) * 2018-07-25 2018-09-28 啵噜噜(广州)婴儿用品科技有限公司 A kind of child bubble shower cream
CN108578341A (en) * 2018-05-31 2018-09-28 贵州盛达生植物发展有限公司 A kind of dendrobium candidum shower cream and preparation method thereof

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Publication number Priority date Publication date Assignee Title
CN108578341A (en) * 2018-05-31 2018-09-28 贵州盛达生植物发展有限公司 A kind of dendrobium candidum shower cream and preparation method thereof
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