CN105853299A - Method of extracting daylily extract from dry daylily and application thereof - Google Patents
Method of extracting daylily extract from dry daylily and application thereof Download PDFInfo
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- CN105853299A CN105853299A CN201610353574.6A CN201610353574A CN105853299A CN 105853299 A CN105853299 A CN 105853299A CN 201610353574 A CN201610353574 A CN 201610353574A CN 105853299 A CN105853299 A CN 105853299A
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- radix hemerocalis
- hemerocalis plicatae
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/96—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution
- A61K8/97—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution from algae, fungi, lichens or plants; from derivatives thereof
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q17/00—Barrier preparations; Preparations brought into direct contact with the skin for affording protection against external influences, e.g. sunlight, X-rays or other harmful rays, corrosive materials, bacteria or insect stings
- A61Q17/005—Antimicrobial preparations
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q19/00—Preparations for care of the skin
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q19/00—Preparations for care of the skin
- A61Q19/08—Anti-ageing preparations
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K2800/00—Properties of cosmetic compositions or active ingredients thereof or formulation aids used therein and process related aspects
- A61K2800/80—Process related aspects concerning the preparation of the cosmetic composition or the storage or application thereof
- A61K2800/82—Preparation or application process involves sonication or ultrasonication
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Abstract
The invention relates to the field of plant application research, in particular to a method of extracting daylily extract from dry daylily and application thereof. The method includes the steps that the dry daylily is prepared into powder, an ultrasonic-assisted volatile solvent extraction method is adopted to extract the daylily extract, and the daylily extract can be added into cosmetics as an ingredient, and particularly can be prepared into a mask, facial cleanser, skin lotion, moisturizer, whitening cream, essence and other products. The method has the advantages of being simple in process and easy to operate, solvent is recycled, and therefore the solvent dosage is reduced; the ultrasonic-assisted technology is used, the solvent enters daylily cells more easily under the action of ultrasonic waves, and the extraction rate is high. The daylily extract contains antisepsis and anti-inflammation components and various nutrient components, the daylily extract is applied to the cosmetics, and the application range is enlarged.
Description
Technical field
The present invention relates to plant application research field, be specially a kind of extraction Radix hemerocalis plicatae extraction from dry day-lily buds
The method of thing and application thereof.
Background technology
Radix hemerocalis plicatae has another name called Flos Hemerocallis, popular name Datlily, for Liliaceae herbaceos perennial, originates in South China
Portion and Japan, its root, leaf, stem, flower have thousand of years in East Asia Region as food and traditional medicine
History.Radix hemerocalis plicatae is fresh and sweet delicious, and meat and vegetables is held concurrently excellent, in the Chinese medicine dietetic therapy history of more than 3000 year, and Radix hemerocalis plicatae
It is listed in one of conventional dietetic food.The traditional Chinese medical science thinks that Radix hemerocalis plicatae has suppressing the hyperactive liver and nourishes blood, swelling diuretic, antibacterial disappears
Scorching, stop blooding, ease pain, lactogenesis, stomach invigorating and the function calmed the nerves, hepatitis, yellow cellulitis, defecate hematochezia, sense can be treated
Emit, dysentery, urinary tract infection, dizziness, tinnitus, cardiopalmus, lumbago, edema, hypogalactia, arthralgia etc. many
Plant disease.Radix hemerocalis plicatae is nutritious, containing saccharide, protein, vitamin, inorganic salt and multiple needed by human
Aminoacid.Hemerocallis citrina Baroni Lepidium high protein, low heat value, vegetable rich in vitamin and mineral.Raw in the modern times
In work, the four big treasures that Radix hemerocalis plicatae and Lentinus Edodes, dry day-lily buds, winter bamboo shoot are collectively known as in greengrocery.Along with
The raising of people's living standard, people increasingly pay attention to finding from natural materials have medical care effect
Medicine or functional factor, for carrying out the chemical composition of domestic and international Radix hemerocalis plicatae and health-care effect research in this literary composition
Summary.
Chinese patent storehouse discloses a kind of method extracting flavone from Radix hemerocalis plicatae
(CN201410132824.4), its step is as follows: with pulverizer, Radix hemerocalis plicatae is ground into dry powder after drying,
Add extraction ethanol, soak, use and carry out supersound extraction, ultrasonic after sucking filtration, filtrate is turned
Move in volumetric flask, with constant volume ethanol constant volume.Radix hemerocalis plicatae extracting flavonoids method of the present invention, with tradition
Extracting Technique of Flavonoids is compared and is had the advantage that this method uses that solvent is few, mild condition, easily controllable, peace
Complete this method operating time reliable is short, extracts yield higher.This method low cost, simple process, easy to spread.
Chinese patent storehouse discloses a kind of health food (CN201110190260.6) for improving sleep,
It is mainly grouped into by the one-tenth of following parts by weight: Radix hemerocalis plicatae extract 10-20 part；Fructus Mori extractum 5-10 part；
Fructus Jujubae 2-6 part；Mel 1-5 part；Semen Ziziphi Spinosae extract 1-5 part.The products material that the present invention provides is natural,
Formula selection is unique, and production technology is scientific and reasonable.Compared with other similar health-care food, this product has
One the most all raw material of maximum feature belongs to natural vegetable and fruit, can be that current social day and night increases
Insomnia patient provide that a kind of effect is obvious, without any side effects, the natural functional food of mouthfeel.
The method of plant extract has a lot, and plant extract is applied primarily to the necks such as food, chemical industry, cosmetics
Territory, but extracting method and plant extract species have the biggest limitation, the most simply, safely, effectively
Extract plant, select which kind of plant, and being applied to its safety in cosmetics, protect sensitive skin, be
Problem demanding prompt solution.
Summary of the invention
For the problems referred to above, it is an object of the invention to provide a kind of extraction Radix hemerocalis plicatae extract from dry day-lily buds
Method and application, dry day-lily buds is made powder, uses and have the volatile solvent of ultrasonic assistant to extract
Method extracts Radix hemerocalis plicatae extract, and Radix hemerocalis plicatae extract can add in cosmetics as dispensing, specifically can be made into
The products such as facial film, cleansing milk, surfactant, emollient cream, skin whitener, essence.
To achieve these goals, the present invention uses below scheme
According to the first aspect of the invention, a kind of method extracting Radix hemerocalis plicatae extract from dry day-lily buds, its
Comprise the following steps:
(1) pulverizing, use pulverizer to be pulverized by dry day-lily buds, make Radix hemerocalis plicatae microgranule, particle diameter is
20-50 sieve mesh；
(2) extraction of ultrasonic assistant percolation, is placed in Radix hemerocalis plicatae microgranule in percolator, is continuously added volatilization
Property solvent so that it is penetrate Radix hemerocalis plicatae microgranule, from top to bottom from percolator bottom flow out leachate, control to ooze
Filtering speed, speed is 1-5ml/kg, at supersonic frequency 20-800KHz, ultrasound intensity 0.3-15W/cm2, carry
Under conditions of taking temperature 10-80 DEG C, extracting 1-3 hour, in percolation leaching process, liquid level to be remained is high
In raw material face 10-15cm；
(3) solvent refluxing utilizes, and leachate is heated, and solvent is condensed again after distillating and flows back in percolator
Extraction dry day-lily buds microgranule, so goes round and begins again, until the complete position of extracts active ingredients；
(4) heating precipitation, obtains leachate by step (3) and heats, isolate volatile solvent,
Obtain Radix hemerocalis plicatae extracting solution；
(5) extract concentrates, and is concentrated by Radix hemerocalis plicatae extracting solution, obtains Radix hemerocalis plicatae extract；
(6) decolorising agent or toner is selected to make required color according to the final color of Radix hemerocalis plicatae extract.
Preferably, dry day-lily buds microgranule in step (1), particle diameter is 35-40 sieve mesh.
Preferably, supersonic frequency 300-500KHz in step (2), ultrasound intensity 5-8W/cm2, Extracting temperature
50-60℃。
Preferably, in step (2), volatile solvent is methanol, ethanol, acetone, propylene glycol or petroleum ether.
Preferably, in step (2), volatile solvent is ethanol.
Preferably, in step (2), percolation speed is 3-5ml/kg.
Preferably, step (5) uses vacuum and low temperature concentration technique.
According to the second aspect of the invention, it is provided that the application of a kind of Radix hemerocalis plicatae extract, described Radix hemerocalis plicatae is extracted
Thing adds in cosmetics as a kind of dispensing.
Preferably, Radix hemerocalis plicatae extract is applied in the cosmetics of skin moistening, moisturizing, defying age class.
Preferably, a kind of replenishing water and preserving moisture class cosmetic combinations containing Radix hemerocalis plicatae extract, by weight, bag
Include following components: Radix hemerocalis plicatae extract 8-12 part, moisturizing agent 6-15 part, anti-sensitizer 0.5-1.2 part, whitening
Agent 1.5-3 part, transdermal enhancer 0.2-0.5 part, potassium hydroxide 0.03-0.1 part, thickening agent 0.1-0.3 part,
Emulsifying agent 0.5-1.2 part, preservative 0.2-0.6 part, deionized water 40-80 part.
The invention has the beneficial effects as follows: flow process is simple, easily operates；Solvent recycles, and saves solvent
Consumption；Using ultrasonic assistive technologies, under the effect of ultrasound wave, solvent easier entrance Radix hemerocalis plicatae is intracellular,
Extraction ratio is high；Containing anti-inflammation composition and multiple nutritional components in Radix hemerocalis plicatae extract, Radix hemerocalis plicatae is extracted
Thing is applied in cosmetics, expands range of application.
Detailed description of the invention
For the problems referred to above, it is an object of the invention to provide a kind of extraction Radix hemerocalis plicatae extract from dry day-lily buds
Method and application, dry day-lily buds is made powder, uses and have the volatile solvent of ultrasonic assistant to extract
Method extracts Radix hemerocalis plicatae extract, and Radix hemerocalis plicatae extract can add in cosmetics as dispensing, specifically can be made into
The products such as facial film, cleansing milk, surfactant, emollient cream, skin whitener, essence.
To achieve these goals, the present invention uses below scheme
According to the first aspect of the invention, a kind of method extracting Radix hemerocalis plicatae extract from dry day-lily buds, its
Comprise the following steps:
(1) pulverizing, use pulverizer to be pulverized by dry day-lily buds, make Radix hemerocalis plicatae microgranule, particle diameter is
20-50 sieve mesh；
(2) extraction of ultrasonic assistant percolation, is placed in Radix hemerocalis plicatae microgranule in percolator, is continuously added volatilization
Property solvent so that it is penetrate Radix hemerocalis plicatae microgranule, from top to bottom from percolator bottom flow out leachate, control to ooze
Filtering speed, speed is 1-5ml/kg, at supersonic frequency 20-800KHz, ultrasound intensity 0.3-15W/cm2, carries
Under conditions of taking temperature 10-80 DEG C, extracting 1-3 hour, in percolation leaching process, liquid level to be remained is high
In raw material face 10-15cm；
(3) solvent refluxing utilizes, and leachate is heated, and solvent is condensed again after distillating and flows back in percolator
Extraction dry day-lily buds microgranule, so goes round and begins again, until the complete position of extracts active ingredients；
(4) heating precipitation, obtains leachate by step (3) and heats, isolate volatile solvent,
Obtain Radix hemerocalis plicatae extracting solution；
(5) extract concentrates, and is concentrated by Radix hemerocalis plicatae extracting solution, obtains Radix hemerocalis plicatae extract；
(6) decolorising agent or toner is selected to make required color according to the final color of Radix hemerocalis plicatae extract.
Preferably, dry day-lily buds microgranule in step (1), particle diameter is 35-40 sieve mesh.
Preferably, supersonic frequency 300-500KHz in step (2), ultrasound intensity 5-8W/cm2, Extracting temperature
50-60℃。
Preferably, in step (2), volatile solvent is methanol, ethanol, acetone, propylene glycol or petroleum ether.
Preferably, in step (2), volatile solvent is ethanol.
Preferably, in step (2), percolation speed is 3-5ml/kg.
Preferably, step (5) uses vacuum and low temperature concentration technique.
According to the second aspect of the invention, it is provided that the application of a kind of Radix hemerocalis plicatae extract, described Radix hemerocalis plicatae is extracted
Thing adds in cosmetics as a kind of dispensing.
Preferably, Radix hemerocalis plicatae extract is applied in the cosmetics of skin moistening, moisturizing, defying age class.
Preferably, a kind of replenishing water and preserving moisture class cosmetic combinations containing Radix hemerocalis plicatae extract, by weight, bag
Include following components: Radix hemerocalis plicatae extract 8-12 part, moisturizing agent 6-15 part, anti-sensitizer 0.5-1.2 part, whitening
Agent 1.5-3 part, transdermal enhancer 0.2-0.5 part, potassium hydroxide 0.03-0.1 part, thickening agent 0.1-0.3 part,
Emulsifying agent 0.5-1.2 part, preservative 0.2-0.6 part, deionized water 40-80 part.
According to compositions various in plant dissolubility in a solvent, select big to active ingredient solubility, to not
Need the solvent that dissolved element dissolubility is little, and the method that effective ingredient is dissolved out in plant tissue
Solvent extraction method.When solvent is added in plant material, solvent is due to diffusion.Cell wall is passed through in osmosis
Penetrating intracellular, dissolve solable matter, and cause the concentration difference of intraor extracellular, intracellular concentrated solution is not
Breaking to external diffusion, solvent the most constantly enters in plant tissue cell, repeatedly comes and goes, until intraor extracellular solution
When concentration reaches dynamic equilibrium, this saturated solution is leached, adds novel solvent, can be big for required composition portion
Divide dissolution.
Ultrasonic extraction is the mechanical effect utilizing ultrasound wave to have, cavitation effect and heat effect, by increasing
The movement velocity of medium molecule, increase the penetration power of medium to extract biological effective components.1, mechanical effect,
Ultrasound wave propagation in media as well can make medium particle produce vibration in its communication space, thus strengthens Jie
The diffusion of matter, propagation, here it is the mechanical effect of ultrasound wave.Ultrasound wave produces a kind of spoke in communication process
Penetrate pressure, propagate along sound wave direction, material is had the strongest destruction, cell metaplasia can be made, plant
Thing protein denaturation；Meanwhile, it can also give medium and suspended substance with different acceleration, and medium divides
The movement velocity of son is much larger than the movement velocity of suspended substance molecule.Thus produce friction between the two, this rub
Wiping power can make biomolecule depolymerization, makes the effective ingredient on cell wall be dissolved in quickly among solvent.2,
Cavitation effect, it is generally the case that media interior has dissolved some microbubbles more or less, these bubbles exist
Producing vibration under the effect of ultrasound wave, when acoustic pressure reaches certain value, bubble increases due to orientation diffusion,
Form resonant cavity, close the most suddenly, here it is the cavitation effect of ultrasound wave.The meeting when Guan Bi of this bubble
Producing the pressure of thousand of atmospheric pressure about, forming micro laser wave, it can cause plant cell wall and whole
Organism ruptures, and whole rupture process completed in moment, beneficially the dissolution of effective ingredient.3, heat
Effect, the same with other physical wave, ultrasound wave communication process in media as well be also an energy propagation and
Diffusion process, i.e. ultrasound wave is in the communication process of medium, and its acoustic energy is constantly absorbed by the particle of medium, is situated between
The energy absorbed wholly or largely is transformed into heat energy by matter, thus causes medium itself and medical material tissue temperature
The rising of degree, increases the dissolution velocity of effective ingredient.The medicine group caused due to this absorption acoustic energy
The rising knitting internal temperature is moment, and the biological activity of the composition being extracted therefore can be made to keep constant.
For the technical scheme making those skilled in the art be better understood from the application, below in conjunction with reality
Execute example technical scheme is clearly and completely described, it is clear that described embodiment is only
Being only a part of embodiment of the application, based on the embodiment in the application, those of ordinary skill in the art exist
Do not make the every other embodiment obtained under creative work premise, all should belong to the application protection
Scope.
Embodiment 1
A kind of method extracting Radix hemerocalis plicatae extract from dry day-lily buds, it comprises the following steps:
Dry day-lily buds quality: 10KG, solvent is methanol；
(1) pulverizing, use pulverizer to be pulverized by dry day-lily buds, make Radix hemerocalis plicatae microgranule, particle diameter is
30 sieve meshes；
(2) extraction of ultrasonic assistant percolation, is placed in Radix hemerocalis plicatae microgranule in percolator, is continuously added volatilization
Property solvent so that it is penetrate Radix hemerocalis plicatae microgranule, from top to bottom from percolator bottom flow out leachate, percolation speed
Degree is 4ml/kg, at supersonic frequency 200KHz, ultrasound intensity 6W/cm2, under conditions of Extracting temperature 55 DEG C,
Extracting 2 hours, in percolation leaching process, liquid level to be remained is higher than raw material face 10cm；
(3) solvent refluxing utilizes, and leachate is heated, and solvent is condensed again after distillating and flows back in percolator
Extraction dry day-lily buds microgranule, so goes round and begins again, until the complete position of extracts active ingredients；
(4) heating precipitation, obtains leachate by step (3) and heats, isolate volatile solvent,
Obtain Radix hemerocalis plicatae extracting solution；
(5) extract concentrates, and is concentrated by Radix hemerocalis plicatae extracting solution, obtains Radix hemerocalis plicatae extract；
(6) decolorising agent or toner is selected to make required color according to the final color of Radix hemerocalis plicatae extract.
Embodiment 2
A kind of method extracting Radix hemerocalis plicatae extract from dry day-lily buds, it comprises the following steps:
Dry day-lily buds quality: 50KG, solvent is alcohol；
(1) pulverizing, use pulverizer to be pulverized by dry day-lily buds, make Radix hemerocalis plicatae microgranule, particle diameter is
40 sieve meshes；
(2) extraction of ultrasonic assistant percolation, is placed in Radix hemerocalis plicatae microgranule in percolator, is continuously added volatilization
Property solvent so that it is penetrate Radix hemerocalis plicatae microgranule, from top to bottom from percolator bottom flow out leachate, percolation speed
Degree is 3.5ml/kg, at supersonic frequency 300KHz, ultrasound intensity 5W/cm2, condition that Extracting temperature is 60 DEG C
Under, extract 2 hours, in percolation leaching process, liquid level to be remained is higher than raw material face 12cm；
(3) solvent refluxing utilizes, and leachate is heated, and solvent is condensed again after distillating and flows back in percolator
Extraction dry day-lily buds microgranule, so goes round and begins again, until the complete position of extracts active ingredients；
(4) heating precipitation, obtains leachate by step (3) and heats, isolate volatile solvent,
Obtain Radix hemerocalis plicatae extracting solution；
(5) extract concentrates, and is concentrated by Radix hemerocalis plicatae extracting solution, obtains Radix hemerocalis plicatae extract；
(6) decolorising agent or toner is selected to make required color according to the final color of Radix hemerocalis plicatae extract.
Embodiment 3
A kind of method extracting Radix hemerocalis plicatae extract from dry day-lily buds, it comprises the following steps:
Dry day-lily buds quality: 100KG, solvent is acetone；
(1) pulverizing, use pulverizer to be pulverized by dry day-lily buds, make Radix hemerocalis plicatae microgranule, particle diameter is
45 sieve meshes；
(2) extraction of ultrasonic assistant percolation, is placed in Radix hemerocalis plicatae microgranule in percolator, is continuously added volatilization
Property solvent so that it is penetrate Radix hemerocalis plicatae microgranule, from top to bottom from percolator bottom flow out leachate, percolation speed
Degree is 3ml/kg, at supersonic frequency 400KHz, ultrasound intensity 8W/cm2, under conditions of Extracting temperature 70 DEG C,
Extracting 2.5 hours, in percolation leaching process, liquid level to be remained is higher than raw material face 15cm；
(3) solvent refluxing utilizes, and leachate is heated, and solvent is condensed again after distillating and flows back in percolator
Extraction dry day-lily buds microgranule, so goes round and begins again, until the complete position of extracts active ingredients；
(4) heating precipitation, obtains leachate by step (3) and heats, isolate volatile solvent,
Obtain Radix hemerocalis plicatae extracting solution；
(5) extract concentrates, and is concentrated by Radix hemerocalis plicatae extracting solution, obtains Radix hemerocalis plicatae extract；
(6) decolorising agent or toner is selected to make required color according to the final color of Radix hemerocalis plicatae extract.
Finally illustrate, above example only in order to technical scheme to be described and unrestricted, ability
Other amendment or equivalents that technical scheme is made by territory those of ordinary skill, as long as not taking off
From the spirit and scope of technical solution of the present invention, all should contain in the middle of scope of the presently claimed invention.
Claims (9)
1. the method extracting Radix hemerocalis plicatae extract from dry day-lily buds, it is characterised in that it includes following
Step:
(1) pulverizing, use pulverizer to be pulverized by dry day-lily buds, make Radix hemerocalis plicatae microgranule, particle diameter is
20-50 sieve mesh；
(2) extraction of ultrasonic assistant percolation, is placed in Radix hemerocalis plicatae microgranule in percolator, is continuously added volatilization
Property solvent so that it is penetrate Radix hemerocalis plicatae microgranule, from top to bottom from percolator bottom flow out leachate, control to ooze
Filtering speed, speed is 1-5ml/kg, at supersonic frequency 20-800KHz, ultrasound intensity 0.3-15W/cm2, carries
Under conditions of taking temperature 10-80 DEG C, extract 1-3 hour, liquid to be remained in percolation leaching process
Face is higher than raw material face 10-15cm；
(3) solvent refluxing utilizes, and leachate is heated, and solvent is condensed again after distillating and flows back in percolator
Extraction dry day-lily buds microgranule, so goes round and begins again, until the complete position of extracts active ingredients；
(4) heating precipitation, obtains leachate by step (3) and heats, isolate volatile solvent,
Obtain Radix hemerocalis plicatae extracting solution；
(5) extract concentrates, and is concentrated by Radix hemerocalis plicatae extracting solution, obtains Radix hemerocalis plicatae extract；
(6) decolorising agent or toner is selected to make required color according to the final color of Radix hemerocalis plicatae extract.
A kind of method extracting Radix hemerocalis plicatae extract from dry day-lily buds the most according to claim 1, its
Being characterised by, dry day-lily buds microgranule in step (1), particle diameter is 35-40 sieve mesh.
A kind of method extracting Radix hemerocalis plicatae extract from dry day-lily buds the most according to claim 1, its
It is characterised by, supersonic frequency 300-500KHz in step (2), ultrasound intensity 5-8W/cm2, carry
Take temperature 50-60 DEG C.
A kind of method extracting Radix hemerocalis plicatae extract from dry day-lily buds the most according to claim 1, its
Being characterised by, in step (2), volatile solvent is methanol, ethanol, acetone, propylene glycol or petroleum ether.
A kind of method extracting Radix hemerocalis plicatae extract from dry day-lily buds the most according to claim 1, its
Being characterised by, in step (2), percolation speed is 3-5ml/kg.
A kind of method extracting Radix hemerocalis plicatae extract from dry day-lily buds the most according to claim 1, its
It is characterised by, step (5) uses vacuum and low temperature concentration technique.
7. the application of a Radix hemerocalis plicatae extract, it is characterised in that described Radix hemerocalis plicatae extract is joined as one
Material adds in cosmetics.
The application of a kind of Radix hemerocalis plicatae extract the most according to claim 7, it is characterised in that by Hemerocallis citrina Baroni
Dish extract is applied in the cosmetics of skin moistening, moisturizing, defying age class.
9. according to the application of a kind of Radix hemerocalis plicatae extract described in claim 7 or 8, it is characterised in that a kind of
Replenishing water and preserving moisture class cosmetic combinations containing Radix hemerocalis plicatae extract, by weight, including following components: Hemerocallis citrina Baroni
Dish extract 8-12 part, moisturizing agent 6-15 part, anti-sensitizer 0.5-1.2 part, whitening agent 1.5-3 part,
Transdermal enhancer 0.2-0.5 part, potassium hydroxide 0.03-0.1 part, thickening agent 0.1-0.3 part,
Emulsifying agent 0.5-1.2 part, preservative 0.2-0.6 part, deionized water 40-80 part.
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| CN201610353574.6A CN105853299A (en) | 2016-05-24 | 2016-05-24 | Method of extracting daylily extract from dry daylily and application thereof |
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| CN201610353574.6A CN105853299A (en) | 2016-05-24 | 2016-05-24 | Method of extracting daylily extract from dry daylily and application thereof |
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Cited By (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN112057399A (en) * | 2020-09-11 | 2020-12-11 | 祁东纯之绿食品有限公司 | A facial mask containing flos Hemerocallis extract |
| CN112438935A (en) * | 2020-12-10 | 2021-03-05 | 上海应用技术大学 | Hemerocallis fulva leaf extracting solution and preparation method and application thereof |
| CN112662197A (en) * | 2021-01-19 | 2021-04-16 | 上海应用技术大学 | Method for extracting water-soluble pigment from day lily flower |
| CN112675248A (en) * | 2019-10-18 | 2021-04-20 | 大江生医股份有限公司 | Application of flos Hemerocallis extract in regulating gene expression level, caring skin, resisting depression and protecting cerebrovascular |
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| CN102210800A (en) * | 2008-07-31 | 2011-10-12 | 倪健 | New application of citron daylily and citron daylily general flavone |
| CN102488819A (en) * | 2011-12-12 | 2012-06-13 | 倪健 | Preparing method for daylily flower extract |
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| CN102210800A (en) * | 2008-07-31 | 2011-10-12 | 倪健 | New application of citron daylily and citron daylily general flavone |
| CN102488819A (en) * | 2011-12-12 | 2012-06-13 | 倪健 | Preparing method for daylily flower extract |
Cited By (5)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN112675248A (en) * | 2019-10-18 | 2021-04-20 | 大江生医股份有限公司 | Application of flos Hemerocallis extract in regulating gene expression level, caring skin, resisting depression and protecting cerebrovascular |
| CN112057399A (en) * | 2020-09-11 | 2020-12-11 | 祁东纯之绿食品有限公司 | A facial mask containing flos Hemerocallis extract |
| CN112438935A (en) * | 2020-12-10 | 2021-03-05 | 上海应用技术大学 | Hemerocallis fulva leaf extracting solution and preparation method and application thereof |
| CN112662197A (en) * | 2021-01-19 | 2021-04-16 | 上海应用技术大学 | Method for extracting water-soluble pigment from day lily flower |
| CN112662197B (en) * | 2021-01-19 | 2022-06-28 | 上海应用技术大学 | Method for extracting water-soluble pigment from hemerocallis fulva flowers |
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Application publication date: 20160817 |