CN105842265A - Surface treatment method of damage below machining face of carbon-fiber-reinforced composite material - Google Patents

Surface treatment method of damage below machining face of carbon-fiber-reinforced composite material Download PDF

Info

Publication number
CN105842265A
CN105842265A CN201610365481.5A CN201610365481A CN105842265A CN 105842265 A CN105842265 A CN 105842265A CN 201610365481 A CN201610365481 A CN 201610365481A CN 105842265 A CN105842265 A CN 105842265A
Authority
CN
China
Prior art keywords
exemplar
grinding
damage
sample
reinforced composite
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Granted
Application number
CN201610365481.5A
Other languages
Chinese (zh)
Other versions
CN105842265B (en
Inventor
王福吉
毕广健
宿友亮
贾振元
王小楠
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Dalian University of Technology
Original Assignee
Dalian University of Technology
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Dalian University of Technology filed Critical Dalian University of Technology
Priority to CN201610365481.5A priority Critical patent/CN105842265B/en
Publication of CN105842265A publication Critical patent/CN105842265A/en
Application granted granted Critical
Publication of CN105842265B publication Critical patent/CN105842265B/en
Active legal-status Critical Current
Anticipated expiration legal-status Critical

Links

Classifications

    • GPHYSICS
    • G01MEASURING; TESTING
    • G01NINVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
    • G01N23/00Investigating or analysing materials by the use of wave or particle radiation, e.g. X-rays or neutrons, not covered by groups G01N3/00 – G01N17/00, G01N21/00 or G01N22/00
    • G01N23/22Investigating or analysing materials by the use of wave or particle radiation, e.g. X-rays or neutrons, not covered by groups G01N3/00 – G01N17/00, G01N21/00 or G01N22/00 by measuring secondary emission from the material
    • G01N23/2202Preparing specimens therefor
    • GPHYSICS
    • G01MEASURING; TESTING
    • G01NINVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
    • G01N2223/00Investigating materials by wave or particle radiation
    • G01N2223/60Specific applications or type of materials
    • G01N2223/646Specific applications or type of materials flaws, defects

Landscapes

  • Physics & Mathematics (AREA)
  • Health & Medical Sciences (AREA)
  • Life Sciences & Earth Sciences (AREA)
  • Chemical & Material Sciences (AREA)
  • Analytical Chemistry (AREA)
  • Biochemistry (AREA)
  • General Health & Medical Sciences (AREA)
  • General Physics & Mathematics (AREA)
  • Immunology (AREA)
  • Pathology (AREA)
  • Sampling And Sample Adjustment (AREA)
  • Analysing Materials By The Use Of Radiation (AREA)

Abstract

The invention relates to a surface treatment method of damage below the machining face of carbon-fiber-reinforced composite material and belongs to the field of composite materials. The treatment method uses micro amount to remove the material layer by layer and includes: sampling; grinding, to be more specific, using a grinding machine to grinding the surface of a sample by using abrasive paper as the medium to expose the damaged surface, wherein the grinding includes coarse grinding, semi-finishing grinding and finishing grinding; cleaning, to be more specific, using an ultrasonic cleaning machine to clean the ground sample so as to remove the impurities on the surface of the material; airing; observing and evaluating. The surface treatment method has the advantages that the method is simple and easy to operate and unlimited by material shape; the surface damage of the obtained sample is clean and complete, and the problem that the damage of the machined observation sample, with the damage below the machining face, of the carbon-fiber-reinforced composite material easily expands to destroy the original shape during machining is solved.

Description

The surface treatment method of damage under carbon fibre reinforced composite face
Technical field
The invention belongs to field of compound material, after relating to a kind of carbon fibre reinforced composite processing Face under damage the surface treatment method of observation.
Background technology
Carbon fibre reinforced composite product is mostly global formation after a lay solidification, is full Foot matching requirements, need further it to be carried out the machining such as drilling, trimming.But, due to Carbon fibre composite is carefully seen in fiber, resin and interface composition multi phase state, macroscopically in Multilamellar, multidirectional heterogeneous anisotropic characteristic, and fibre reinforced phase intensity, hardness are high, And it is low to be wrapped in the resin matrix phase of fiber peripheral, interface phase intensity, in machining easily because of Processing technique select improper and produce ftracture under serious face, the mechanical damage such as layering, reduce carbon The mechanical property of fiber reinforcement compound material piece.Along with carbon fibre reinforced composite is high-end Popularization and application in equipment primary load bearing component, control the strictest to its damage tolerance.Due to height Substantial load complicated and changeable, mistake is often born during holding the primary load bearing component equipped under arms Under big face, crack and damage easily extends during bearing complex load, causes component failure, Even fatal crass.Therefore, in the evaluation of multiple material product crudy, microscopic observation is passed through Under opposite, damage is quantitatively described, and then crack and damage degree and product mechanical property under acquisition face Corresponding relation between energy, processing technique, and then by Rational choice processing technique, with primary load bearing Component machining damage is control standard, selects rational processing technique reliable to guarantee that product is on active service Property.But, under face, crack and damage is positioned at the material internal of below finished surface, it is impossible to directly see Survey.Therefore, by certain means, skin-material need to be removed, make crack and damage under face the most sudden and the most violent It is exposed in scanning electron microscope visual field, and then completes accurately to measure.
But, in carbon fibre composite, the size of each composition phase is micron order, damages under machined surface Hinder scope in several microns-hundreds of micrometer range.During removing skin-material, easily Causing damage propatagtion because removal power is excessive, damage morphologies distortion, measurement result no longer has ginseng Examine value.Therefore, it is necessary to use small quantity successively to remove the mode of material, reduce as much as possible Removal power, it is to avoid damage propatagtion under the face caused by external force, keeps original damage morphologies, it is ensured that damage Hinder the accuracy of DATA REASONING.At present, have no and add for carbon fiber enhancement resin base composite material The report of work damage exemplar preparation method;" big specification titanium and the titanium of the invention such as Wang Hai, Fan second place Microstructure of the alloy preparation method of sample ", number of patent application 201310260852.X, it relates to homogenizing The preparation method of metal material metallographic exemplar, but due to observed crystal particle scale mostly in 30 μm Above, if directly using its preparation method and parameter, easily because removal power is excessive under induction face Damage propatagtion, causes exemplar to be prepared unsuccessfully.
Summary of the invention
It is an object of the invention to overcome the defect of prior art, a kind of fibre reinforced of invention is combined The surface treatment method of damage under material face, uses grinder to increase carbon fiber with sand paper for medium Strong composite carries out the grinding of different levels, to realize the trace removal of surfacing, in making Portion's injury of primary has pattern complete table to reveal, and then utilizes scanning electron microscope to damage under inside face Accurately measuring and evaluate, surface treatment method is simple to operation, do not limited by material shape. The exemplar injured surface of surface gained is the most complete.
The technical solution used in the present invention is to damage under a kind of carbon fibre reinforced composite face Surface treatment method, it is characterised in that processing method uses small quantity successively to remove the side of material Formula, the method includes sampling, grinds, cleans, dries, observes evaluation;The concrete step of method Rapid as follows:
The first step: sampling, is the carbon fibre reinforced composite sample after utilizing sawing machine Cutting indexes Sample 1;Then saddle weight 2 is heated, utilize the Cera Flava of fusing that exemplar 1 is bonded at saddle weight 2 On, after cooling, exemplar 1 is fixed on saddle weight 2, and the quantity of the most fixing exemplar 1 must not Less than three;
Second step: grind, grinds with face lapping mill, enters exemplar 1 for medium with sand paper 3 Row grinds, and carries out respectively roughly grinding, partly refines, refines three steps operations;Choose corase grind, half fine grinding, Sand paper 3 model that fine grinding is used, and abrasive disk 6 is right in corase grind, partly fine grinding, fine grinding institute The rotating speed answered;Parameter for each step is chosen, and sand paper 3 granularity is the biggest, and rotating speed is the biggest, grinds Mill speed is the fastest, and milling time to shorten relatively;Sand paper 3 granularity is the least, and rotating speed is the lowest, grinds Mill speed is the slowest, and milling time to increase relatively, makes surface quality increase;
3rd step: clean, is first placed on saddle weight 2 to add and heats in hot plate, melted by wax, After exemplar 1 is taken off from saddle weight 2, put into the water in the beaker filling clear water, in beaker Want submergence exemplar 1;Again beaker is put in ultrasonic washing unit, ground exemplar 1 is entered Row is cleaned multiple times, and removes the impurity of material surface;Clean after terminating, by the water in beaker every time It is changed to clear water;
4th step: dry, dries cleaned exemplar 1, makes moisture evaporate completely;
5th step: observation is evaluated, and is that the exemplar 1 after drying collects with sample sack, and Carry out labelling, utilize scanning electron microscope to be observed through surface-treated exemplar, Observe and under face, damage original pattern, and evaluate accurately.
The invention has the beneficial effects as follows that surface treatment method is simple to operation, do not limited by material shape System, the exemplar injured surface of surface gained is totally complete, completely remains the original of machining damage Pattern, including fiber bending, fibrous fracture, fibrous matrix Interface Cracking etc..Processing method solution Determine and under carbon fibre reinforced composite face, damage observation exemplar preparation process has been damaged after processing The problem easily extended and destroy original pattern.
Accompanying drawing explanation
Fig. 1 is the grinding mechanism schematic diagram of the present invention, in figure: 1. exemplar, 2. saddle weight, 3. Sand paper, 4. bolt, 5. annulus, 6. abrasive disk,
Fig. 2 is to damage under the face using the inventive method to utilize scanning electronic microscope observation to arrive Situation, in figure: 7-fibrous fracture, 8-fiber bending, 9-fibrous matrix Interface Cracking
Detailed description of the invention
Being embodied as of the embodiment of the present invention is described in detail below in conjunction with technical scheme and accompanying drawing.
Accompanying drawing 1 is the grinding mechanism schematic diagram of the present invention, a kind of carbon fibre reinforced composite face The surface treatment method of lower damage observation, including sampling, grind, clean, dry, observe step Suddenly.As a example by unidirectional carbon fiber reinforced composite material laminate after processing, specifically comprise the following steps that
The first step: sampling, after utilizing sawing machine sawing to be about 20mm × 20mm processing Carbon fibre reinforced composite exemplar 1, is careful not to when sawing destroy machined surface.With Time with sand paper by clean for the sanding burr at exemplar 1 edge, if exemplar 1 marginal existence adds man-hour The projection caused, the most also polishes off the material of projection with sand paper, it is ensured that exemplar 1 surface Flatness.
Second step: grind, is to be fixed on by the exemplar 1 of sawing on circular saddle weight 2, every time Fixing exemplar 1 quantity must not be less than three.The method of fixing exemplar 1 is: by saddle weight 2 It is placed on warm table heating, when being heated to about 80 DEG C, smears Huang at saddle weight 2 upper surface During wax, Cera Flava melts, and is bonded on Cera Flava by exemplar 1, by exemplar 1 machined surface face phase during operation The center of circle, pushes away exemplar 1 from the center of circle to saddle weight 2 edge, for making wax can not infiltrate at machined surface Edge, affects the observation of machined surface.Exemplar 1 same at circular saddle weight 2 upper surface as far as possible On the center of circle, in order to during grinding, exemplar grinding rate one causes surfacing.Exemplar will be well placed Saddle weight 2 is placed in water, for making saddle weight 2 fast cooling, notices that water can have solid simultaneously The surface of random sample part 1.After saddle weight 2 temperature reduces, after Cera Flava solidification, exemplar 1 is fixed on On saddle weight 2 surface.
Then, use grinder that exemplar is ground, grind schematic diagram as it is shown in figure 1, divide Do not carry out roughly grinding, partly refine, refine three steps operations.Choose corase grind, partly fine grinding, fine grinding is made The model of sand paper 3, and abrasive disk 6 is turning corresponding to corase grind, half fine grinding, fine grinding Speed.
1) corase grind, first fixes P320 or P400 on the abrasive disk 6 be threaded hole Sand paper 3, it is ensured that sand paper 3 is smooth lay on abrasive disk 6, then by tighting a bolt 4 Compress and be positioned at the annulus 5 on sand paper 3, thus utilize the thrust of annulus 5 by solid for sand paper 3 Fixed.Again the ballast 2 pieces fixing exemplar 1 is put on abrasive disk 6, make exemplar 1 surface with Sand paper 3 contacts, and abrasive disk 6 rotates counterclockwise, and adjusts the angle revising wheel, so that revising Wheel can drive exemplar rotation, exemplar 1 to make relative operation friction with abrasive disk 6, thus reach The purpose ground.Adding appropriate clear water when grinding, abrasive disk 6 rotating speed is 20r/min, The corase grind time is about 10min.Purpose is quickly to remove sample surface material.
2) half fine grinding, after having roughly ground, rinses well exemplar 1 with clear water, then by upper Stating operation and sand paper 3 is changed to the sand paper of P600, this step abrasive disk 6 rotating speed is 18r/min, half The fine grinding time is about 30min.Purpose is to remove the sample surface material that corase grind destroys.
3) fine grinding, after half has refined, rinses well exemplar 1 with clear water, still by upper Stating operation and sand paper 3 is changed to the sand paper of P800, the rotating speed of this step abrasive disk 6 is 13r/min, The fine grinding time is about 30min.Purpose is to remove the material surface that half fine grinding destroys, and makes processing Damage under the face of Shi Zaocheng and be not damaged, show really.After having refined, use clear water Exemplar 1 is rinsed well, can observe that ground exemplar 1 surface roughness is the least, friction Face reflective is fine.
Parameter for each step is chosen, and sand paper granularity is the biggest, and rotating speed is the biggest, and grinding rate is more Hurry up, milling time to shorten relatively;Sand paper granularity is the least, and rotating speed is the lowest, and grinding rate is the slowest, Milling time to increase relatively, but surface quality is higher than the former.
3rd step: clean, is to be placed on saddle weight 2 to add to heat in hot plate, it is therefore an objective to melted by wax Changing, then exemplar 1 just can be taken off from saddle weight 2.The exemplar 1 taken off is put into Filling in the beaker of clear water, the water in beaker wants submergence exemplar.Next step, put into super by beaker In sound wave cleaning machine, exemplar 1 is carried out.Carry out 3 times altogether to clean, clean every time and terminate After, the water in beaker is changed to clear water.
4th step: dry, is that exemplar 1 tweezers after cleaning take out from beaker, is placed on Dry in dust removing cloth.Ground sample surface is not pressed from both sides when noting with tweezers folder exemplar, in order to avoid Destroy original damage.
5th step: observe and evaluate, is that the exemplar 1 after drying collects with sample sack, And carry out labelling, damage observation can be carried out by scanning electron microscope at any time, observe exemplar 1 Damage original pattern under face, and evaluate accurately.Can clearly see in fig 2 To 1 lower degree of impairment of exemplar: fibrous fracture 7, fiber bending 8 and fibrous matrix interface are opened Split 9.

Claims (1)

1. a surface treatment method for damage, its feature under carbon fibre reinforced composite face Being, processing method uses small quantity successively to remove the mode of material, the method include sampling, Grind, clean, dry, observe evaluation;Method specifically comprises the following steps that
The first step: sampling, is the carbon fibre reinforced composite sample after utilizing sawing machine Cutting indexes Sample (1);Then saddle weight (2) is heated, utilize the Cera Flava of fusing to be bonded at by exemplar (1) On saddle weight (2), after cooling, exemplar (1) is fixed on saddle weight (2), fixes every time The quantity of exemplar (1) must not be less than three;
Second step: grind, grinds with face lapping mill, is that medium is to exemplar with sand paper (3) (1) it is ground, carries out respectively roughly grinding, partly refine, refine three steps operations;Choose corase grind, Half fine grinding, refine used sand paper (3) model, and abrasive disk (6) roughly grinding, partly Rotating speed corresponding to fine grinding, fine grinding;Each step parameter is chosen, sand paper (3) granularity The biggest, grinding rate is the fastest, and milling time shortens relatively;Sand paper (3) granularity is the least, grinds Mill speed is the slowest, and milling time increases relatively, makes surface quality increase;
3rd step: clean, is first placed on saddle weight (2) to add and heats in hot plate, melted by wax, After exemplar (1) is taken off from saddle weight (2), put in the beaker filling clear water, burn Water in Bei wants submergence exemplar;Again beaker is put in ultrasonic washing unit, to ground sample Part (1) is cleaned multiple times, and removes the impurity of material surface;Clean after terminating every time, will Water in beaker is changed to clear water;
4th step: dry, dries cleaned exemplar (1), makes moisture evaporate completely;
5th step: observation is evaluated, and the exemplar (1) after drying collects with sample sack, And carry out labelling, utilize scanning electron microscope to enter through surface-treated exemplar (1) Row observation, observes and damages original pattern under face, and evaluate accurately.
CN201610365481.5A 2016-05-30 2016-05-30 The surface treatment method damaged under carbon fibre reinforced composite face Active CN105842265B (en)

Priority Applications (1)

Application Number Priority Date Filing Date Title
CN201610365481.5A CN105842265B (en) 2016-05-30 2016-05-30 The surface treatment method damaged under carbon fibre reinforced composite face

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
CN201610365481.5A CN105842265B (en) 2016-05-30 2016-05-30 The surface treatment method damaged under carbon fibre reinforced composite face

Publications (2)

Publication Number Publication Date
CN105842265A true CN105842265A (en) 2016-08-10
CN105842265B CN105842265B (en) 2018-12-18

Family

ID=56595917

Family Applications (1)

Application Number Title Priority Date Filing Date
CN201610365481.5A Active CN105842265B (en) 2016-05-30 2016-05-30 The surface treatment method damaged under carbon fibre reinforced composite face

Country Status (1)

Country Link
CN (1) CN105842265B (en)

Cited By (4)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN109580683A (en) * 2018-11-23 2019-04-05 广东工业大学 A kind of fiberglass reinforced PTFE plate half bore microsection manufacture method
CN111390654A (en) * 2020-03-30 2020-07-10 中国科学院宁波材料技术与工程研究所 Treatment method for surface of carbon fiber resin matrix composite material
CN112748115A (en) * 2020-12-23 2021-05-04 沈阳航空航天大学 Evaluation method for subsurface damage of fiber reinforced composite material hole making
CN115615782A (en) * 2022-11-10 2023-01-17 大连理工大学 Evaluation and prediction method for fiber reinforced composite subsurface damage

Family Cites Families (5)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN101319974B (en) * 2008-07-18 2010-08-25 昆明理工大学 Method for preparing aluminum/lead system laminar composite material metallic phase example and display organization
CN101825587B (en) * 2010-04-15 2012-02-08 哈尔滨飞机工业集团有限责任公司 Fiber volume content test method of glass fiber laminated board
CN103163133B (en) * 2013-02-05 2015-04-08 华东理工大学 Continuous filament reinforced plastic impregnation uniformity evaluation method
CN103994910B (en) * 2014-06-09 2016-08-31 上海华力微电子有限公司 Small sample level minimizing technology
CN104669071B (en) * 2015-01-22 2016-11-30 湖南大学 A kind of polishing processing technique of composite

Cited By (6)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN109580683A (en) * 2018-11-23 2019-04-05 广东工业大学 A kind of fiberglass reinforced PTFE plate half bore microsection manufacture method
CN109580683B (en) * 2018-11-23 2021-03-02 广东工业大学 Manufacturing method of glass fiber reinforced PTFE plate half-hole section
CN111390654A (en) * 2020-03-30 2020-07-10 中国科学院宁波材料技术与工程研究所 Treatment method for surface of carbon fiber resin matrix composite material
CN112748115A (en) * 2020-12-23 2021-05-04 沈阳航空航天大学 Evaluation method for subsurface damage of fiber reinforced composite material hole making
CN112748115B (en) * 2020-12-23 2022-08-30 沈阳航空航天大学 Evaluation method for subsurface damage of fiber reinforced composite material hole making
CN115615782A (en) * 2022-11-10 2023-01-17 大连理工大学 Evaluation and prediction method for fiber reinforced composite subsurface damage

Also Published As

Publication number Publication date
CN105842265B (en) 2018-12-18

Similar Documents

Publication Publication Date Title
CN105842265A (en) Surface treatment method of damage below machining face of carbon-fiber-reinforced composite material
Yang et al. Vibration coupling effects and machining behavior of ultrasonic vibration plate device for creep-feed grinding of Inconel 718 nickel-based superalloy
Dold et al. A study on laser touch dressing of electroplated diamond wheels using pulsed picosecond laser sources
Wu et al. Prediction of grinding force for brittle materials considering co-existing of ductility and brittleness
Solhtalab et al. Cup wheel grinding-induced subsurface damage in optical glass BK7: an experimental, theoretical and numerical investigation
Zhou et al. Surface integrity of titanium part by ultrasonic magnetic abrasive finishing
CN108318304A (en) A kind of the aerospace preparation of PCBA effective sections and damage detecting method
CN101700594A (en) On-site unstressed surfacing repairing process of large rotor journal sealing bush abrasion part
Dong et al. Investigation on grinding force and machining quality during rotary ultrasonic grinding deep-small hole of fluorophlogopite ceramics
CN104568545A (en) Manufacturing method of shale rock lamina
Feng et al. Prediction of grinding force in microgrinding of ceramic materials by cohesive zone-based finite element method
Xu et al. An experimental investigation of grinding force and energy in laser thermal shock-assisted grinding of zirconia ceramics
Qu et al. Realization of high efficiency and low damage machining of anisotropic KDP crystal by grinding
Li et al. Analysis on the effects of grinding wheel speed on removal behavior of brittle optical materials
CN108982275B (en) Ultrasonic-assisted high-speed single-point scratch test device and test method
CN101704152A (en) In-situ stress-free resurfacing welding repair process of abrasion of large-sized rotor journal
Chen et al. Study on the characteristics of zirconia ceramic in three-dimensional ultrasonic vibration-assisted ELID internal grinding
CN103231302A (en) Method for obtaining super-smooth surface low-sub-surface-damage crystal
Li et al. Coupling stress caused by thermal and slicing force in KDP crystal slicing with fixed abrasive wire saw
Jackson A review of the design of grinding wheels operating at excessive speeds
CN101367185A (en) Polishing mould for optical element and manufacturing method thereof
Chen et al. Experimental research on wear mechanism of diamond wheels for grinding Cf/SiC composites grooves
Zhao et al. Grinding damage of BK7 using copper-resin bond coarse-grained diamond wheel
Qiu et al. On the grinding performance of alumina wheels in ultrasonic vibration–assisted grinding of hardened GCr15 steel
He et al. A new monitor model to detect damages in surface and subsurface during cup grinding process of BK7 optical glass: a new optimization model for energy damage

Legal Events

Date Code Title Description
C06 Publication
PB01 Publication
C10 Entry into substantive examination
SE01 Entry into force of request for substantive examination
GR01 Patent grant
GR01 Patent grant