CN105832577A - Sunscreen rose nail polish and preparation method thereof - Google Patents
Sunscreen rose nail polish and preparation method thereof Download PDFInfo
- Publication number
- CN105832577A CN105832577A CN201610178175.0A CN201610178175A CN105832577A CN 105832577 A CN105832577 A CN 105832577A CN 201610178175 A CN201610178175 A CN 201610178175A CN 105832577 A CN105832577 A CN 105832577A
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- CN
- China
- Prior art keywords
- flos rosae
- rosae rugosae
- sun
- proof
- nial polish
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
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Classifications
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/92—Oils, fats or waxes; Derivatives thereof, e.g. hydrogenation products thereof
- A61K8/922—Oils, fats or waxes; Derivatives thereof, e.g. hydrogenation products thereof of vegetable origin
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/33—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing oxygen
- A61K8/35—Ketones, e.g. benzophenone
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/33—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing oxygen
- A61K8/37—Esters of carboxylic acids
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/40—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing nitrogen
- A61K8/42—Amides
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/72—Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds
- A61K8/73—Polysaccharides
- A61K8/731—Cellulose; Quaternized cellulose derivatives
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q17/00—Barrier preparations; Preparations brought into direct contact with the skin for affording protection against external influences, e.g. sunlight, X-rays or other harmful rays, corrosive materials, bacteria or insect stings
- A61Q17/04—Topical preparations for affording protection against sunlight or other radiation; Topical sun tanning preparations
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q3/00—Manicure or pedicure preparations
- A61Q3/02—Nail coatings
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K2800/00—Properties of cosmetic compositions or active ingredients thereof or formulation aids used therein and process related aspects
- A61K2800/40—Chemical, physico-chemical or functional or structural properties of particular ingredients
- A61K2800/42—Colour properties
- A61K2800/43—Pigments; Dyes
- A61K2800/436—Interference pigments, e.g. Iridescent, Pearlescent
Abstract
The invention discloses sunscreen rose nail polish and a preparation method thereof and belongs to the field of daily-use chemical industry. The nail polish includes a natural amide compound N-trans-feruloyloctopamine and rose essential oil. The nail polish can beautifying nails, has a refreshing flavor of rose, can prevent ultraviolet light from damaging nails and is better than a chemical sunscreen product including single component.
Description
Technical field
The present invention relates to a kind of nial polish and preparation method thereof, belong to filed of daily-use chemical industry.
Background technology
Nial polish belongs to the product of color make-up series, has and beautifies the effect modifying fingernail, but poor to the ultraviolet protection function of fingernail.
Due to environment, sunscreen product is increasingly subject to the welcome of consumer, but introduces nial polish sun-proof simultaneous with fragrance concept
In, current domestic and international market or a blank.People to the maintenance of fingernail in addition to the product such as nial polish, nail saver the most other
Without selecting, if increasing the nail polish products with sun-proof and fragrant function, not only fingernail being played and beautifying modification,
Reduce the access times of perfume, it is also possible to the injury that fingernail is caused by shielding of ultraviolet simultaneously.
The fragrance of Flos Rosae Rugosae can bring happiness, can alleviate fatigue and the regulation sentiment of people.Finger of the prior art
After nail polish is applied on fingernail, need to use organic solvent or special nail polish remover just can wash off, the most inconvenient,
And be engaged in the related works such as food and drink and have meal time health can be worked the mischief.Thus, it is easy to clean and have dulcet finger
Nail polish is increasingly pursued by people.Nial polish must possess quick-drying, gloss, adhesive force painting strong, wear-resisting, water-fast, easy and
The feature such as easily remove.Though existing product has reached certain effect the most, but it is poor to the protective capacities of ultraviolet.
The product that the present invention relates to also can be prone to complete removing with hands after drying, reaches purpose easy to use.
Therefore the present invention can enrich the function of nial polish, meets the multiple demand of people, allows and makes employment be happy to use.
Summary of the invention
For the deficiencies in the prior art, the technical problem to be solved is to provide after one is smeared with rose scent, and
Easily remove and have the nial polish of sun-screening function.
The present invention solves firmness and the technical problem of glossiness difference of existing nial polish the most simultaneously, it is provided that one has well
Glossiness and the nial polish of firmness.
The present invention is achieved by the following technical solutions:
This sun-proof Flos Rosae Rugosae nial polish includes the N-trans Resina Ferulae nor-Neosynephrine of acyl group, Flos Rosae Rugosae quintessence oil.
Wherein, by weight, the described N-trans Resina Ferulae nor-Neosynephrine of acyl group is 0.2-0.6 part, and Flos Rosae Rugosae quintessence oil is 2-6 part.
It addition, described sun-proof Flos Rosae Rugosae nial polish includes pharmaceutically acceptable carrier or composition.
Preferably, by weight, described sun-proof Flos Rosae Rugosae nial polish also includes the ethyl acetate of 20-40 part, the nitro of 5-15 part
Cellulose, the Camphora of 0.5-1.5 part, the pearl essence of 0.1-0.3 part, the pigment of 1-3 part.
The invention also discloses the preparation method of described sun-proof Flos Rosae Rugosae nial polish, the preparation method of described sun-proof Flos Rosae Rugosae nial polish is as follows:
By ethyl acetate and Flos Rosae Rugosae quintessence oil, after mixing and stirring, under stirring, add NC Nitroncellulose in above-mentioned mixed liquor
In, stir 10min at 1500 rpm；It is subsequently adding the N-trans Resina Ferulae nor-Neosynephrine of acyl group, under 1500rpm, stirs 10min.
Finally Camphora, pearl essence, pigment are added thereto, stir 10min at 1500 rpm；200 mesh screen make solution,
In 0-4 DEG C of cold preservation 4-5 hour, finally encapsulate and i.e. obtain sun-proof Flos Rosae Rugosae nial polish.
The present invention is compared with prior art: this nial polish is without formaldehyde, organic solvent and poisonous heavy metal, environment friendly and pollution-free,
And it is easy to user removal；And the addition of Flos Rosae Rugosae quintessence oil improves nial polish to fingernail bond properties, it is not necessary to add spice, just
It is provided with the faint scent of Flos Rosae Rugosae；Simultaneously can the injury of complete barrier ultraviolet, make nial polish have outstanding sun-proof function, carry
The high SPF (sun protection factor) of nial polish, is better than the effect of single chemicals, fingernail plays very effective protection and repair.And
And preparation technology simplifies, practical function highly significant, and be suitable to industrialized production.
Accompanying drawing explanation
Fig. 1 is the measurement result of sun-proof Flos Rosae Rugosae nial polish UVResistant effect.
Detailed description of the invention
Below in conjunction with specific embodiment, technical scheme is described in further detail, but protection scope of the present invention is not limited to
Described embodiment.
The preparation of the embodiment 1 N-trans Resina Ferulae nor-Neosynephrine of acyl group
Synthetic method is for first synthesizing Ferulic acid, then forms amide, concrete steps with chapter amine by amido link
With reference to journal article: Zhengrong Wu, Lifang Zheng, Yang Li, et al.Synthesis and
structure–activity relationships and effects of phenylpropanoid amides of
octopamine and dopamine on tyrosinase inhibition and antioxidation,Food
Chemistry.134(2012)1128-1131.
Spectral data is as follows: the N-trans Resina Ferulae nor-Neosynephrine of acyl group: pale yellow powder, fusing point: 183-185 DEG C；IR(KBr,
cm-1):3361,3020-2930,1653,1594-1514,1268-1213；1H NMR(CD3OD-d4,400MHz).δ:
3.43 (dd, J=13.6,8.0Hz, 1H), 3.52 (dd, J=13.6,5.2Hz, 1H), 3.88 (s, 3H), 4.72
(dd, J=7.6,5.2Hz, 1H), 6.46 (d, J=15.6Hz, 1H), 6.76 (d, J=8.8Hz, 2H), 6.78
(d, J=8.5Hz, 1H), 7.02 (dd, J=8.4,1.2Hz, 1H), 7.12 (s, 1H), 7.23 (d, J=8.5Hz,
2H), 7.44 (d, J=15.6Hz, 1H)；13C NMR(CD3OD-d4,100MHz)δ:169.5,158.1,149.9,
149.3,142.2,134.7,128.5,128.3,123.3,118.7,116.5,116.1,111.6,73.4,56.4,
48.3；HRMS:m/z 352.1149(calcd for C18H19NO5+Na,352.1155)。
The preparation of embodiment 2 sun-proof Flos Rosae Rugosae nial polish
The formula of the most sun-proof Flos Rosae Rugosae nial polish
Formula 1
The N-trans Resina Ferulae nor-Neosynephrine of acyl group of 2g, the Flos Rosae Rugosae quintessence oil of 20g, the ethyl acetate of 200g, the nitrocellulose of 50g
Element, the Camphora of 5g, the pearl essence of 1g, the pigment of 10g.
Formula 2
The N-trans Resina Ferulae nor-Neosynephrine of acyl group of 4g, the Flos Rosae Rugosae quintessence oil of 40g, the ethyl acetate of 300g, the nitro of 100g is fine
Dimension element, the Camphora of 10g, the pearl essence of 2g, the pigment of 20g.
Formula 3
The N-trans Resina Ferulae nor-Neosynephrine of acyl group of 6g, the Flos Rosae Rugosae quintessence oil of 60g, the ethyl acetate of 400g, the nitro of 150g is fine
Dimension element, the Camphora of 15g, the pearl essence of 3g, the pigment of 30g.
The preparation method of the most sun-proof Flos Rosae Rugosae nial polish
By ethyl acetate and Flos Rosae Rugosae quintessence oil, after mixing and stirring, under stirring, add NC Nitroncellulose in above-mentioned mixed liquor
In, stir 10min at 1500 rpm；It is subsequently adding the sunscreen N-trans Resina Ferulae nor-Neosynephrine of acyl group, stirs under 1500rpm
Mix 10min.Finally Camphora, pearl essence, pigment are added thereto, stir 10min at 1500 rpm；200 mesh screen
Make solution, and 0-4 DEG C of cold preservation 4-5 hour, finally encapsulate and i.e. obtain sun-proof Flos Rosae Rugosae nial polish finished product.
The performance test of embodiment 3 sun-proof Flos Rosae Rugosae nial polish
1. the preparation of laboratory sample
(1) sun-proof Flos Rosae Rugosae nial polish
The N-trans Resina Ferulae nor-Neosynephrine of acyl group of formula: 2g, the Flos Rosae Rugosae quintessence oil of 20g, the ethyl acetate of 200g, the nitre of 50g
Base cellulose, the Camphora of 5g, the pearl essence of 1g, the pigment of 10g.
Preparation method:
By ethyl acetate and Flos Rosae Rugosae quintessence oil, after mixing and stirring, NC Nitroncellulose is incorporated in above-mentioned mixing under stirring
In liquid, stir 10min at 1500 rpm；It is subsequently adding the N-trans Resina Ferulae nor-Neosynephrine of acyl group, under 1500rpm, stirs 10
min.Finally according to the above ratio Camphora, pearl essence, pigment are added thereto, stir 10min at 1500 rpm；200 mesh sieves
Solution is made in filtration, in 0-4 DEG C of cold preservation 4-5 hour, finally encapsulates and i.e. obtains sun-proof Flos Rosae Rugosae nial polish finished product.
(2) rhodamine toner line of oils
The Flos Rosae Rugosae quintessence oil of formula: 20g, the ethyl acetate of 200g, the NC Nitroncellulose of 50g, the Camphora of 5g, the pearl essence of 1g,
The pigment of 10g.
Preparation method: by ethyl acetate and Flos Rosae Rugosae quintessence oil, after mixing and stirring, under stirring add NC Nitroncellulose in
In above-mentioned mixed liquor, stir 10min at 1500 rpm.Finally Camphora according to the above ratio, pearl essence, pigment are added it
In, stir 10min at 1500 rpm；200 mesh screen, in 0-4 DEG C of cold preservation 4-5 hour and get final product.
(3) N-trans Resina Ferulae acyl group nor-Neosynephrine group
The N-trans Resina Ferulae nor-Neosynephrine of acyl group of formula: 2g, the Flos Rosae Rugosae quintessence oil of 20g, the ethyl acetate of 200g, the nitre of 50g
Base cellulose, the Camphora of 5g, the pearl essence of 1g, the pigment of 10g.
Preparation method: ethyl acetate is mixed with entering NC Nitroncellulose, stirs 10min at 1500 rpm；It is subsequently adding N-
The trans nor-Neosynephrine of Resina Ferulae acyl group, stirs 10min under 1500rpm.Last according to the above ratio by Camphora, pearl essence, pigment
It is added thereto, stirs 10min at 1500 rpm；200 mesh screen, in 0-4 DEG C of cold preservation 4-5 hour and get final product.
2. the preparation of comparison
The ethyl acetate of formula: 200g, the NC Nitroncellulose of 50g, the Camphora of 5g, the pearl essence of 1g, the pigment of 10g.
Preparation method:
Ethyl acetate is mixed with NC Nitroncellulose, stirs 10min at 1500 rpm；Again Camphora, pearl essence, pigment are pressed
Ratio adds in above-mentioned solution, stirs 10min at 1500 rpm；200 mesh screen, in 0-4 DEG C of cold preservation within 4-5 hour, be
?.
The most sun-proof Flos Rosae Rugosae nial polish performance test
(1) outward appearance: full color, light, there is moist feeling.
(2) abnormal smells from the patient and remove easy degree: there is rose scent taste, easily remove with hands.
(3) 3M adhesive tape method measures its UVResistant effect.
The present embodiment uses 3M adhesive tape method to measure the sun-proof result of the sun-proof Flos Rosae Rugosae nial polish made.
1cm × 4cm size will be cut into by 3M medical air-permeable adhesive tape, be pasted onto quartz colorimetric utensil transparent side surface.Accurately claim for examination
Product 35mg, by test sample uniform application on quartz colorimetric utensil transparent surface, is placed in 35 DEG C of drying baker, is dried 30 minutes.So
With ultraviolet spectrophotometer at detection wavelength it is afterwards
285nm, 290nm, 295nm, 300nm, 305nm, 310nm, 315nm, 320nm detect, and each test sample sets
Put five parallel, measure OD value, OD value is the biggest, the best to the protection effect of UVB.
By Fig. 1 result it can be seen that under same concentration, the OD value of sun-proof Flos Rosae Rugosae nial polish disclosed by the invention is apparently higher than right
According to group, rhodamine toner line of oils and N-trans Resina Ferulae acyl group nor-Neosynephrine group, show to contain the trans Resina Ferulae acyl group containing N-nor-pungent simultaneously
The sun-proof Flos Rosae Rugosae nial polish prescription uvioresistant effect/anti-sunlight function of Fu Lin and Flos Rosae Rugosae quintessence oil is significantly higher than individually containing Flos Rosae Rugosae quintessence oil
Experimental group and the independent effect containing N-trans Resina Ferulae acyl group nor-Neosynephrine experimental group, Flos Rosae Rugosae quintessence oil Resina Ferulae trans with N-acyl group goes
There is between first Neosynephrine the effect of Synergistic.
Claims (5)
1. a sun-proof Flos Rosae Rugosae nial polish, it is characterised in that described sun-proof Flos Rosae Rugosae nial polish includes that N-trans Resina Ferulae acyl group is nor-
Neosynephrine, Flos Rosae Rugosae quintessence oil.
Sun-proof Flos Rosae Rugosae nial polish the most according to claim 1, it is characterised in that by weight, described N-trans Ah
Wei, the nor-Neosynephrine of acyl group was 0.2-0.6 part, and Flos Rosae Rugosae quintessence oil is 2-6 part.
Sun-proof Flos Rosae Rugosae nial polish the most according to claim 1 and 2, it is characterised in that described sun-proof Flos Rosae Rugosae nial polish bag
Include pharmaceutically acceptable carrier or composition.
Sun-proof Flos Rosae Rugosae nial polish the most according to claim 3, it is characterised in that by weight, described sun-proof Flos Rosae Rugosae refers to
Nail polish also includes the ethyl acetate of 20-40 part, the NC Nitroncellulose of 5-15 part, the Camphora of 0.5-1.5 part, the pearly-lustre of 0.1-0.3 part
Powder, the pigment of 1-3 part.
Sun-proof Flos Rosae Rugosae nial polish the most according to claim 4, it is characterised in that the preparation side of described sun-proof Flos Rosae Rugosae nial polish
Method is as follows:
By ethyl acetate and Flos Rosae Rugosae quintessence oil, after mixing and stirring, under stirring, add NC Nitroncellulose in above-mentioned mixed liquor
In, stir 10min at 1500 rpm；It is subsequently adding the N-trans Resina Ferulae nor-Neosynephrine of acyl group, under 1500rpm, stirs 10min,
Finally Camphora, pearl essence, pigment are added thereto, stir 10min at 1500 rpm；200 mesh screen make solution,
In 0-4 DEG C of cold preservation 4-5 hour, finally encapsulate and i.e. obtain sun-proof Flos Rosae Rugosae nial polish.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201610178175.0A CN105832577B (en) | 2016-03-25 | 2016-03-25 | A kind of sun-proof rose nail polish and preparation method thereof |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201610178175.0A CN105832577B (en) | 2016-03-25 | 2016-03-25 | A kind of sun-proof rose nail polish and preparation method thereof |
Publications (2)
| Publication Number | Publication Date |
|---|---|
| CN105832577A true CN105832577A (en) | 2016-08-10 |
| CN105832577B CN105832577B (en) | 2018-01-05 |
Family
ID=56583567
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN201610178175.0A Active CN105832577B (en) | 2016-03-25 | 2016-03-25 | A kind of sun-proof rose nail polish and preparation method thereof |
Country Status (1)
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Citations (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN1596872A (en) * | 2003-09-17 | 2005-03-23 | 杜洪良 | Formula of sun screen fingernail oil |
| JP2005154361A (en) * | 2003-11-27 | 2005-06-16 | Shiseido Co Ltd | Manicure preparation |
| CN103655277A (en) * | 2013-11-20 | 2014-03-26 | 青岛晨讯通商贸有限公司 | Light fragrance long-acting nail polish |
-
2016
- 2016-03-25 CN CN201610178175.0A patent/CN105832577B/en active Active
Patent Citations (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN1596872A (en) * | 2003-09-17 | 2005-03-23 | 杜洪良 | Formula of sun screen fingernail oil |
| JP2005154361A (en) * | 2003-11-27 | 2005-06-16 | Shiseido Co Ltd | Manicure preparation |
| CN103655277A (en) * | 2013-11-20 | 2014-03-26 | 青岛晨讯通商贸有限公司 | Light fragrance long-acting nail polish |
Non-Patent Citations (1)
| Title |
|---|
| ZHENGRONG WU等: "Synthesis and structure–activity relationships and effects of phenylpropanoid amides of octopamine and dopamine on tyrosinase inhibition and antioxidation", 《FOOD CHEMISTRY》 * |
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| CN105832577B (en) | 2018-01-05 |
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