CN105831369A - Preparation method of chocolate with cocoa butter alternatives for 3D printing - Google Patents
Preparation method of chocolate with cocoa butter alternatives for 3D printing Download PDFInfo
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- CN105831369A CN105831369A CN201610171212.5A CN201610171212A CN105831369A CN 105831369 A CN105831369 A CN 105831369A CN 201610171212 A CN201610171212 A CN 201610171212A CN 105831369 A CN105831369 A CN 105831369A
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- chocolate
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- printing
- liquid
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- 244000299461 Theobroma cacao Species 0.000 title claims abstract description 99
- 235000019219 chocolate Nutrition 0.000 title claims abstract description 78
- 238000010146 3D printing Methods 0.000 title claims abstract description 24
- 238000002360 preparation method Methods 0.000 title claims abstract description 15
- 235000019875 cocoa butter alternative Nutrition 0.000 title abstract 3
- 230000001954 sterilising effect Effects 0.000 claims abstract description 33
- 238000007670 refining Methods 0.000 claims abstract description 32
- 238000002156 mixing Methods 0.000 claims abstract description 25
- 238000004659 sterilization and disinfection Methods 0.000 claims abstract description 25
- 238000002844 melting Methods 0.000 claims abstract description 17
- 230000008018 melting Effects 0.000 claims abstract description 17
- 238000007789 sealing Methods 0.000 claims abstract description 17
- 238000010438 heat treatment Methods 0.000 claims abstract description 11
- 239000003795 chemical substances by application Substances 0.000 claims description 79
- 239000007788 liquid Substances 0.000 claims description 48
- 239000000843 powder Substances 0.000 claims description 39
- ZLMJMSJWJFRBEC-UHFFFAOYSA-N Potassium Chemical compound [K] ZLMJMSJWJFRBEC-UHFFFAOYSA-N 0.000 claims description 32
- 239000003963 antioxidant agent Substances 0.000 claims description 32
- 230000003078 antioxidant effect Effects 0.000 claims description 32
- 239000011591 potassium Substances 0.000 claims description 32
- 229910052700 potassium Inorganic materials 0.000 claims description 32
- 235000019879 cocoa butter substitute Nutrition 0.000 claims description 26
- 238000003756 stirring Methods 0.000 claims description 26
- 239000000796 flavoring agent Substances 0.000 claims description 25
- 239000002994 raw material Substances 0.000 claims description 25
- 230000000844 anti-bacterial effect Effects 0.000 claims description 24
- 239000003995 emulsifying agent Substances 0.000 claims description 24
- 238000005189 flocculation Methods 0.000 claims description 24
- 230000016615 flocculation Effects 0.000 claims description 24
- 235000013355 food flavoring agent Nutrition 0.000 claims description 24
- 239000000314 lubricant Substances 0.000 claims description 24
- 239000004014 plasticizer Substances 0.000 claims description 24
- 239000006184 cosolvent Substances 0.000 claims description 22
- 235000009470 Theobroma cacao Nutrition 0.000 claims description 21
- 235000013305 food Nutrition 0.000 claims description 19
- 239000003381 stabilizer Substances 0.000 claims description 19
- 239000012745 toughening agent Substances 0.000 claims description 19
- JLPULHDHAOZNQI-ZTIMHPMXSA-N 1-hexadecanoyl-2-(9Z,12Z-octadecadienoyl)-sn-glycero-3-phosphocholine Chemical compound CCCCCCCCCCCCCCCC(=O)OC[C@H](COP([O-])(=O)OCC[N+](C)(C)C)OC(=O)CCCCCCC\C=C/C\C=C/CCCCC JLPULHDHAOZNQI-ZTIMHPMXSA-N 0.000 claims description 17
- 229940083466 soybean lecithin Drugs 0.000 claims description 17
- 239000012752 auxiliary agent Substances 0.000 claims description 16
- 239000002270 dispersing agent Substances 0.000 claims description 16
- 239000004615 ingredient Substances 0.000 claims description 16
- 235000013336 milk Nutrition 0.000 claims description 16
- 239000008267 milk Substances 0.000 claims description 16
- 210000004080 milk Anatomy 0.000 claims description 16
- 235000012424 soybean oil Nutrition 0.000 claims description 16
- 239000003549 soybean oil Substances 0.000 claims description 16
- 239000000463 material Substances 0.000 claims description 14
- 239000000203 mixture Substances 0.000 claims description 9
- LDVVTQMJQSCDMK-UHFFFAOYSA-N 1,3-dihydroxypropan-2-yl formate Chemical compound OCC(CO)OC=O LDVVTQMJQSCDMK-UHFFFAOYSA-N 0.000 claims description 8
- SLNPSLWTEUJUGY-UHFFFAOYSA-N 1-(cyclopenten-1-yl)ethanone Chemical group CC(=O)C1=CCCC1 SLNPSLWTEUJUGY-UHFFFAOYSA-N 0.000 claims description 8
- OWEGMIWEEQEYGQ-UHFFFAOYSA-N 100676-05-9 Natural products OC1C(O)C(O)C(CO)OC1OCC1C(O)C(O)C(O)C(OC2C(OC(O)C(O)C2O)CO)O1 OWEGMIWEEQEYGQ-UHFFFAOYSA-N 0.000 claims description 8
- 229920001817 Agar Polymers 0.000 claims description 8
- LPIDCVUFMJNZRH-SNAWJCMRSA-N CC(C1=CC=CO1)OC(=O)/C=C/C(=O)O Chemical compound CC(C1=CC=CO1)OC(=O)/C=C/C(=O)O LPIDCVUFMJNZRH-SNAWJCMRSA-N 0.000 claims description 8
- 229920002134 Carboxymethyl cellulose Polymers 0.000 claims description 8
- 239000004375 Dextrin Substances 0.000 claims description 8
- 229920001353 Dextrin Polymers 0.000 claims description 8
- 239000004593 Epoxy Substances 0.000 claims description 8
- GUBGYTABKSRVRQ-PICCSMPSSA-N Maltose Natural products O[C@@H]1[C@@H](O)[C@H](O)[C@@H](CO)O[C@@H]1O[C@@H]1[C@@H](CO)OC(O)[C@H](O)[C@H]1O GUBGYTABKSRVRQ-PICCSMPSSA-N 0.000 claims description 8
- 239000004368 Modified starch Substances 0.000 claims description 8
- 229920000881 Modified starch Polymers 0.000 claims description 8
- 229920002125 Sokalan® Polymers 0.000 claims description 8
- 239000008272 agar Substances 0.000 claims description 8
- 235000010419 agar Nutrition 0.000 claims description 8
- 239000001768 carboxy methyl cellulose Substances 0.000 claims description 8
- 235000010948 carboxy methyl cellulose Nutrition 0.000 claims description 8
- 239000008112 carboxymethyl-cellulose Substances 0.000 claims description 8
- -1 compatilizer Substances 0.000 claims description 8
- 235000019425 dextrin Nutrition 0.000 claims description 8
- 235000014113 dietary fatty acids Nutrition 0.000 claims description 8
- 238000004821 distillation Methods 0.000 claims description 8
- 239000000194 fatty acid Substances 0.000 claims description 8
- 229930195729 fatty acid Natural products 0.000 claims description 8
- 150000004665 fatty acids Chemical class 0.000 claims description 8
- 239000011344 liquid material Substances 0.000 claims description 8
- 235000019426 modified starch Nutrition 0.000 claims description 8
- 239000004584 polyacrylic acid Substances 0.000 claims description 8
- 229920000036 polyvinylpyrrolidone Polymers 0.000 claims description 8
- 239000001267 polyvinylpyrrolidone Substances 0.000 claims description 8
- 235000013855 polyvinylpyrrolidone Nutrition 0.000 claims description 8
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims description 8
- 239000000230 xanthan gum Substances 0.000 claims description 8
- 235000010493 xanthan gum Nutrition 0.000 claims description 8
- 229920001285 xanthan gum Polymers 0.000 claims description 8
- 229940082509 xanthan gum Drugs 0.000 claims description 8
- 125000003071 maltose group Chemical group 0.000 claims 1
- 229920002401 polyacrylamide Polymers 0.000 claims 1
- 235000007686 potassium Nutrition 0.000 claims 1
- 235000010408 potassium alginate Nutrition 0.000 claims 1
- 239000000737 potassium alginate Substances 0.000 claims 1
- MZYRDLHIWXQJCQ-YZOKENDUSA-L potassium alginate Chemical compound [K+].[K+].O1[C@@H](C([O-])=O)[C@@H](OC)[C@H](O)[C@H](O)[C@@H]1O[C@@H]1[C@@H](C([O-])=O)O[C@@H](O)[C@@H](O)[C@H]1O MZYRDLHIWXQJCQ-YZOKENDUSA-L 0.000 claims 1
- 238000007639 printing Methods 0.000 abstract description 8
- 238000007493 shaping process Methods 0.000 abstract description 6
- 238000005516 engineering process Methods 0.000 abstract description 5
- 238000011049 filling Methods 0.000 abstract 1
- HRPVXLWXLXDGHG-UHFFFAOYSA-N Acrylamide Chemical compound NC(=O)C=C HRPVXLWXLXDGHG-UHFFFAOYSA-N 0.000 description 7
- 239000000783 alginic acid Substances 0.000 description 7
- 235000010443 alginic acid Nutrition 0.000 description 7
- 229920000615 alginic acid Polymers 0.000 description 7
- 229960001126 alginic acid Drugs 0.000 description 7
- 150000004781 alginic acids Chemical class 0.000 description 7
- 238000000034 method Methods 0.000 description 6
- 230000004927 fusion Effects 0.000 description 4
- MOVRNJGDXREIBM-UHFFFAOYSA-N aid-1 Chemical group O=C1NC(=O)C(C)=CN1C1OC(COP(O)(=O)OC2C(OC(C2)N2C3=C(C(NC(N)=N3)=O)N=C2)COP(O)(=O)OC2C(OC(C2)N2C3=C(C(NC(N)=N3)=O)N=C2)COP(O)(=O)OC2C(OC(C2)N2C3=C(C(NC(N)=N3)=O)N=C2)COP(O)(=O)OC2C(OC(C2)N2C(NC(=O)C(C)=C2)=O)COP(O)(=O)OC2C(OC(C2)N2C3=C(C(NC(N)=N3)=O)N=C2)COP(O)(=O)OC2C(OC(C2)N2C3=C(C(NC(N)=N3)=O)N=C2)COP(O)(=O)OC2C(OC(C2)N2C3=C(C(NC(N)=N3)=O)N=C2)COP(O)(=O)OC2C(OC(C2)N2C(NC(=O)C(C)=C2)=O)COP(O)(=O)OC2C(OC(C2)N2C3=C(C(NC(N)=N3)=O)N=C2)COP(O)(=O)OC2C(OC(C2)N2C3=C(C(NC(N)=N3)=O)N=C2)COP(O)(=O)OC2C(OC(C2)N2C3=C(C(NC(N)=N3)=O)N=C2)COP(O)(=O)OC2C(OC(C2)N2C(NC(=O)C(C)=C2)=O)COP(O)(=O)OC2C(OC(C2)N2C3=C(C(NC(N)=N3)=O)N=C2)COP(O)(=O)OC2C(OC(C2)N2C3=C(C(NC(N)=N3)=O)N=C2)COP(O)(=O)OC2C(OC(C2)N2C3=C(C(NC(N)=N3)=O)N=C2)CO)C(O)C1 MOVRNJGDXREIBM-UHFFFAOYSA-N 0.000 description 3
- 238000000465 moulding Methods 0.000 description 2
- 241000196324 Embryophyta Species 0.000 description 1
- 229920000168 Microcrystalline cellulose Polymers 0.000 description 1
- 235000014121 butter Nutrition 0.000 description 1
- 239000001913 cellulose Substances 0.000 description 1
- 229920002678 cellulose Polymers 0.000 description 1
- 235000010980 cellulose Nutrition 0.000 description 1
- 229940110456 cocoa butter Drugs 0.000 description 1
- 235000019868 cocoa butter Nutrition 0.000 description 1
- 150000001875 compounds Chemical class 0.000 description 1
- 230000007547 defect Effects 0.000 description 1
- 238000004512 die casting Methods 0.000 description 1
- 235000013325 dietary fiber Nutrition 0.000 description 1
- 239000006185 dispersion Substances 0.000 description 1
- 230000000694 effects Effects 0.000 description 1
- 239000003925 fat Substances 0.000 description 1
- 235000019197 fats Nutrition 0.000 description 1
- 235000019634 flavors Nutrition 0.000 description 1
- 239000003205 fragrance Substances 0.000 description 1
- 238000000227 grinding Methods 0.000 description 1
- 238000004519 manufacturing process Methods 0.000 description 1
- 235000019813 microcrystalline cellulose Nutrition 0.000 description 1
- 239000008108 microcrystalline cellulose Substances 0.000 description 1
- 229940016286 microcrystalline cellulose Drugs 0.000 description 1
- 235000008935 nutritious Nutrition 0.000 description 1
- 235000014593 oils and fats Nutrition 0.000 description 1
- 239000002245 particle Substances 0.000 description 1
- 239000002002 slurry Substances 0.000 description 1
- 239000002904 solvent Substances 0.000 description 1
- 230000009967 tasteless effect Effects 0.000 description 1
Classifications
-
- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23G—COCOA; COCOA PRODUCTS, e.g. CHOCOLATE; SUBSTITUTES FOR COCOA OR COCOA PRODUCTS; CONFECTIONERY; CHEWING GUM; ICE-CREAM; PREPARATION THEREOF
- A23G1/00—Cocoa; Cocoa products, e.g. chocolate; Substitutes therefor
- A23G1/30—Cocoa products, e.g. chocolate; Substitutes therefor
- A23G1/32—Cocoa products, e.g. chocolate; Substitutes therefor characterised by the composition containing organic or inorganic compounds
- A23G1/36—Cocoa products, e.g. chocolate; Substitutes therefor characterised by the composition containing organic or inorganic compounds characterised by the fats used
-
- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23G—COCOA; COCOA PRODUCTS, e.g. CHOCOLATE; SUBSTITUTES FOR COCOA OR COCOA PRODUCTS; CONFECTIONERY; CHEWING GUM; ICE-CREAM; PREPARATION THEREOF
- A23G1/00—Cocoa; Cocoa products, e.g. chocolate; Substitutes therefor
- A23G1/30—Cocoa products, e.g. chocolate; Substitutes therefor
- A23G1/32—Cocoa products, e.g. chocolate; Substitutes therefor characterised by the composition containing organic or inorganic compounds
-
- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23G—COCOA; COCOA PRODUCTS, e.g. CHOCOLATE; SUBSTITUTES FOR COCOA OR COCOA PRODUCTS; CONFECTIONERY; CHEWING GUM; ICE-CREAM; PREPARATION THEREOF
- A23G1/00—Cocoa; Cocoa products, e.g. chocolate; Substitutes therefor
- A23G1/30—Cocoa products, e.g. chocolate; Substitutes therefor
- A23G1/32—Cocoa products, e.g. chocolate; Substitutes therefor characterised by the composition containing organic or inorganic compounds
- A23G1/46—Cocoa products, e.g. chocolate; Substitutes therefor characterised by the composition containing organic or inorganic compounds containing dairy products
-
- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23G—COCOA; COCOA PRODUCTS, e.g. CHOCOLATE; SUBSTITUTES FOR COCOA OR COCOA PRODUCTS; CONFECTIONERY; CHEWING GUM; ICE-CREAM; PREPARATION THEREOF
- A23G2200/00—COCOA; COCOA PRODUCTS, e.g. CHOCOLATE; SUBSTITUTES FOR COCOA OR COCOA PRODUCTS; CONFECTIONERY; CHEWING GUM; ICE-CREAM; PREPARATION THEREOF containing organic compounds, e.g. synthetic flavouring agents
- A23G2200/08—COCOA; COCOA PRODUCTS, e.g. CHOCOLATE; SUBSTITUTES FOR COCOA OR COCOA PRODUCTS; CONFECTIONERY; CHEWING GUM; ICE-CREAM; PREPARATION THEREOF containing organic compounds, e.g. synthetic flavouring agents containing cocoa fat if specifically mentioned or containing products of cocoa fat or containing other fats, e.g. fatty acid, fatty alcohol, their esters, lecithin, paraffins
-
- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23G—COCOA; COCOA PRODUCTS, e.g. CHOCOLATE; SUBSTITUTES FOR COCOA OR COCOA PRODUCTS; CONFECTIONERY; CHEWING GUM; ICE-CREAM; PREPARATION THEREOF
- A23G2200/00—COCOA; COCOA PRODUCTS, e.g. CHOCOLATE; SUBSTITUTES FOR COCOA OR COCOA PRODUCTS; CONFECTIONERY; CHEWING GUM; ICE-CREAM; PREPARATION THEREOF containing organic compounds, e.g. synthetic flavouring agents
- A23G2200/12—COCOA; COCOA PRODUCTS, e.g. CHOCOLATE; SUBSTITUTES FOR COCOA OR COCOA PRODUCTS; CONFECTIONERY; CHEWING GUM; ICE-CREAM; PREPARATION THEREOF containing organic compounds, e.g. synthetic flavouring agents containing dairy products
-
- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23V—INDEXING SCHEME RELATING TO FOODS, FOODSTUFFS OR NON-ALCOHOLIC BEVERAGES AND LACTIC OR PROPIONIC ACID BACTERIA USED IN FOODSTUFFS OR FOOD PREPARATION
- A23V2002/00—Food compositions, function of food ingredients or processes for food or foodstuffs
Abstract
The invention discloses a preparation method of chocolate with cocoa butter alternatives for 3D printing and belongs to the field of a chocolate preparation technology. The chocolate with cocoa butter alternatives for 3D printing is prepared by steps of mixing, refining, sterilization, filling, sealing and the like. By the use of the chocolate, heating rate during printing, melting temperature of a model and stereo-shaping rate can be raised. The chocolate of the invention has stable fluidity, a certain viscosity and a stable shaping temperature value, has good heat resistance, and will not block holes during printing. Through the 3D printing technology, original characteristics and taste of chocolate can be maintained, and a chocolate product with a novel and beautiful shape also can be prepared.
Description
[technical field]
The invention belongs to chocolate making technology field, be specifically related to a kind of 3D printing cocoa butter substitute type chalk
The preparation method of power.
[background technology]
Chocolate is mainly made with cocoa butter for primary raw material, has fertile smooth mouthfeel and strong and only
Special fragrance, is liked by consumer of various countries deeply.But, chocolate is a kind of phitosite, fat and sugar
Class content is higher, and protein content is on the low side.It addition, ultra-fine microcrystalline cellulose is the natural height extracted from plant
Molecular compound, nonpoisonous and tasteless, do not provide energy for human body, be a kind of low heat value, the material of high microsteping content,
Itself there is oils and fats sense, the effect improving food mouthfeel can be played while reducing heat, on the other hand increase
Health care in terms of chocolate dietary fiber.
3D printing technique is to design a model as source with Computerized three-dimensional, becomes with numerical control by software hierarchy is discrete
Type system, successively piles up printed material bonding, final superposition molding, produces entity products.Utilize 3D
Printing technique can complete varied printing in kind, from medical treatment to manufacture, from historical relic's protection to scientific research.?
Closely, the feeler that 3D prints extends to again field of food, and scientist have developed and prints for the 3D of food
Machine, by the raw-food material such as chocolate, butter when " ink ", prints taste and different food.
At present, the defect that chocolate of the prior art exists is the bad control of mobility of slurry, the dilutest, beats
Print ratio of briquetting is low;The thickest, easy plug-hole;During printer model, fusion temperature is low.
Therefore, fusion temperature and model stereo shaping rate high, nutritious 3D when developing a kind of printer model
Printing cocoa butter substitute type chocolate becomes development trend.
[summary of the invention]
The present invention provides the preparation method of a kind of 3D printing cocoa butter substitute type chocolate, to solve printer model
Time fusion temperature and model stereo shaping rate low, the thickest during printing, the problem such as easy plug-hole, the chalk of the present invention
Power can improve heating rate, the fusion temperature of model and stereo shaping rate during printing;The chocolate tool of the present invention
There are stable mobility, certain viscosity and stable forming temperature value, heat-resist, will not plug-hole during printing;
The chocolate of the present invention can pass through 3D printing technique, makes and both remains with chocolate primary characteristic and taste, again
The chocolate product that modern design is attractive in appearance.
For solve above technical problem, the present invention by the following technical solutions:
The preparation method of a kind of 3D printing cocoa butter substitute type chocolate, comprises the following steps:
S1, mixing: by cocoa powder, milk powder, soybean lecithin water proof heating means melt be flowing liquid,
Melting temperature is 46-49 DEG C, stirs during melting, and the speed of stirring is 20-200r/min, and stirring is to liquid material
Till fineness is 21-24 μm;
S2, refine: by mixed for step S1 material add toughener, plasticizer, compatilizer, lubricant,
Cosolvent, levelling agent, dispersant, emulsifying agent are 200-300W at ultrasonic power, and temperature is 45-50 DEG C, stirs
Mixing speed is menophania refining 0.5-1.5h under conditions of 300-400r/min, it is thus achieved that menophania refining feed liquid, then refines to menophania
Feed liquid is added stabilizer, antioxidant, flocculation aid, antibacterial, tasty agents, flavouring agent, sweeting agent ultrasonic
Power is 100-200W, and temperature is 35-40 DEG C, and mixing speed is menophania refining under conditions of 200-300r/min
0.4-0.8h, obtains chocolate liquid;
S3, sterilizing: chocolate liquid step S2 prepared uses 100-200 eye mesh screen to filter, after completing
Carrying out sterilization treatment, condition: temperature is 98-102 DEG C, pressure is 210-230KPa, and sterilization time is 10-20s;
S4, fill, sealing: in vacuum be by the chocolate liquid of step S3 sterilization treatment
0.09-0.099Mpa, temperature carries out fill, sealing at being 40-50 DEG C, the most prepared after being cooled to temperature≤25 DEG C
3D prints with cocoa butter substitute type chocolate;
Described toughener is LG-DOW 8402;Described plasticizer is epoxy soybean oil;Described lubricant is food
Use wax;Described cosolvent is polyvinylpyrrolidone;Described levelling agent is epoxidized soybean oil fatty acid;Described point
Powder consists of the following composition: potassium carboxymethylcellulose, agar, modified starch, polyacrylic acid potassium, alginic acid
Potassium, dextrin;Described compatilizer is Dupont EEA2112AC;Described emulsifying agent is distillation monoglyceride;Institute
Stating stabilizer is xanthan gum;Described antioxidant is food grade antioxidant MSK-NE150;Described flocculation aid is poly-
Acrylamide;Described antibacterial is methyl-furfuryl fumarate;Described tasty agents is guanyl potassium;Described sweeting agent
For maltose;Described flavouring agent is methyl cyclopentenyl ketone;
Preferably, described 3D printing cocoa butter substitute type chocolate, in units of weight portion, including following
Raw material: major ingredient 70-100 part, auxiliary agent 20-30 part, described major ingredient is in units of weight portion, including following former
Material: cocoa powder 45-60 part, soybean lecithin 10-20 part, milk powder 15-20 part;Described auxiliary agent is with weight
Part is unit, including following raw material: toughener 1-2 part, plasticizer 1-2 part, lubricant 1-2 part, hydrotropy
Agent 1-2 part, levelling agent 1-1.5 part, dispersant 1-1.5 part, compatilizer 1-1.5 part, emulsifying agent 1-1.5 part,
Stabilizer 1-1.5 part, antioxidant 1-1.2 part, flocculation aid 1-1.2 part, antibacterial 1-1.2 part, tasty agents 1-1.2
Part, flavouring agent 1-1.2 part, sweeting agent 6-10 part.
The method have the advantages that
(1) the 3D printing cocoa butter substitute type chocolate of the present invention contains potassium composition, when can improve printing
Heating rate, improves fusing point;
(2) the 3D printing cocoa butter substitute type chocolate of the present invention contains the cellulose components of soybean lecithin,
Model stereo shaping rate can be improved;
(3) present invention does not carry out homoiothermic use by tradition after conching, but direct quantitative is canned,
Convenient store and transport, and can ready access upon use, make the 3D of chocolate print and leave factory and realize strange land and print,
Use easy to operate;
(4) present invention carries out fine grinding and combines refining process to process material chocolate mass, reduces material
Particle size, improves the smooth mouth-feel of chocolate, and prepared chocolate dissolves rear good fluidity, uses as raw material
When 3D prints will not plug-hole, and the chocolate product printed is difficult to grow dim and turns white, and can realize creative making
Diversification, in high precision, complex-curved, the chocolate product of moulding uniqueness, overturn traditional die casting pattern,
It is completely free of mould constraint, meets the customized market of personalization of people.
[detailed description of the invention]
For ease of being more fully understood that the present invention, being illustrated by following instance, these examples belong to the present invention's
Protection domain, but it is not intended to protection scope of the present invention.
In an embodiment, described 3D printing cocoa butter substitute type chocolate, in units of weight portion, including with
Lower raw material: major ingredient 70-100 part, auxiliary agent 20-30 part, described major ingredient is in units of weight portion, including following
Raw material: cocoa powder 45-60 part, soybean lecithin 10-20 part, milk powder 15-20 part;Described auxiliary agent is with weight
Amount part is unit, including following raw material: toughener 1-2 part, plasticizer 1-2 part, lubricant 1-2 part, help
Solvent 1-2 part, levelling agent 1-1.5 part, dispersant 1-1.5 part, compatilizer 1-1.5 part, emulsifying agent 1-1.5
Part, stabilizer 1-1.5 part, antioxidant 1-1.2 part, flocculation aid 1-1.2 part, antibacterial 1-1.2 part, delicate flavour
Agent 1-1.2 part, flavouring agent 1-1.2 part, sweeting agent 6-10 part;
Described toughener is LG-DOW 8402;Described plasticizer is epoxy soybean oil;Described lubricant is food
Use wax;Described cosolvent is polyvinylpyrrolidone;Described levelling agent is epoxidized soybean oil fatty acid;Described point
Powder consists of the following composition: potassium carboxymethylcellulose, agar, modified starch, polyacrylic acid potassium, alginic acid
Potassium, dextrin;Described compatilizer is Dupont EEA2112AC;Described emulsifying agent is distillation monoglyceride;Institute
Stating stabilizer is xanthan gum;Described antioxidant is food grade antioxidant MSK-NE150;Described flocculation aid is poly-
Acrylamide;Described antibacterial is methyl-furfuryl fumarate;Described tasty agents is guanyl potassium;Described sweeting agent
For maltose;Described flavouring agent is methyl cyclopentenyl ketone;
Described 3D printing cocoa butter substitute type chocolate, its preparation method comprises the following steps:
S1, mixing: by cocoa powder, milk powder, soybean lecithin water proof heating means melt be flowing liquid,
Melting temperature is 46-49 DEG C, stirs during melting, and the speed of stirring is 20-200r/min, and stirring is to liquid material
Till fineness is 21-24 μm;
S2, refine: by mixed for step S1 material add toughener, plasticizer, compatilizer, lubricant,
Cosolvent, levelling agent, dispersant, emulsifying agent are 200-300W at ultrasonic power, and temperature is 45-50 DEG C, stirs
Mixing speed is menophania refining 0.5-1.5h under conditions of 300-400r/min, it is thus achieved that menophania refining feed liquid, then refines to menophania
Feed liquid is added stabilizer, antioxidant, flocculation aid, antibacterial, tasty agents, flavouring agent, sweeting agent ultrasonic
Power is 100-200W, and temperature is 35-40 DEG C, and mixing speed is menophania refining under conditions of 200-300r/min
0.4-0.8h, obtains chocolate liquid;
S3, sterilizing: chocolate liquid step S2 prepared uses 100-200 eye mesh screen to filter, after completing
Carrying out sterilization treatment, condition: temperature is 98-102 DEG C, pressure is 210-230KPa, and sterilization time is 10-20s;
S4, fill, sealing: in vacuum be by the chocolate liquid of step S3 sterilization treatment
0.09-0.099Mpa, temperature carries out fill, sealing at being 40-50 DEG C, the most prepared after being cooled to temperature≤25 DEG C
3D prints with cocoa butter substitute type chocolate.
Below by more specifically embodiment, the present invention will be described.
Embodiment 1
A kind of 3D prints with cocoa butter substitute type chocolate, in units of weight portion, including following raw material: major ingredient
70 parts, auxiliary agent 20 parts, described major ingredient is in units of weight portion, including following raw material: cocoa powder 45 parts,
Soybean lecithin 10 parts, milk powder 15 parts;Described auxiliary agent is in units of weight portion, including following raw material: increase
Tough dose 1 part, plasticizer 1 part, lubricant 1 part, cosolvent 1 part, levelling agent 1 part, dispersant 1 part,
Compatilizer 1 part, emulsifying agent 1 part, stabilizer 1 part, 1 part of antioxidant, flocculation aid 1 part, antibacterial 1 part,
Tasty agents 1 part, flavouring agent 1 part, sweeting agent 6 parts;
Described toughener is LG-DOW 8402;Described plasticizer is epoxy soybean oil;Described lubricant is food
Use wax;Described cosolvent is polyvinylpyrrolidone;Described levelling agent is epoxidized soybean oil fatty acid;Described point
Powder consists of the following composition: potassium carboxymethylcellulose, agar, modified starch, polyacrylic acid potassium, alginic acid
Potassium, dextrin;Described compatilizer is Dupont EEA2112AC;Described emulsifying agent is distillation monoglyceride;Institute
Stating stabilizer is xanthan gum;Described antioxidant is food grade antioxidant MSK-NE150;Described flocculation aid is poly-
Acrylamide;Described antibacterial is methyl-furfuryl fumarate;Described tasty agents is guanyl potassium;Described sweeting agent
For maltose;Described flavouring agent is methyl cyclopentenyl ketone;
Described 3D printing cocoa butter substitute type chocolate, its preparation method comprises the following steps:
S1, mixing: by cocoa powder, milk powder, soybean lecithin water proof heating means melt be flowing liquid,
Melting temperature is 46 DEG C, stirs during melting, and the speed of stirring is 200r/min, and stirring is to liquid material fineness
Till 21-24 μm;
S2, refine: by mixed for step S1 material add toughener, plasticizer, compatilizer, lubricant,
Cosolvent, levelling agent, dispersant, emulsifying agent are 200W at ultrasonic power, and temperature is 45 DEG C, mixing speed
For menophania refining 1.5h under conditions of 300r/min, it is thus achieved that menophania refining feed liquid, then add steady in menophania refining feed liquid
Determining agent, antioxidant, flocculation aid, antibacterial, tasty agents, flavouring agent, sweeting agent is 100W at ultrasonic power,
Temperature is 35 DEG C, and mixing speed is menophania refining 0.8h under conditions of 200r/min, obtains chocolate liquid;
S3, sterilizing: use 100 eye mesh screens to filter the chocolate liquid that step S2 prepares, carry out after completing
Sterilization treatment, condition: temperature is 98 DEG C, pressure is 210KPa, and sterilization time is 20s;
S4, fill, sealing: be 0.09Mpa in vacuum by the chocolate liquid of step S3 sterilization treatment,
Temperature is to carry out fill, sealing at 40 DEG C, is cooled to after temperature is 25 DEG C i.e. prepare 3D and prints with for cocoa
Epoxy-type chocolate.
Embodiment 2
A kind of 3D prints with cocoa butter substitute type chocolate, in units of weight portion, including following raw material: major ingredient
100 parts, auxiliary agent 30 parts, described major ingredient is in units of weight portion, including following raw material: cocoa powder 60 parts,
Soybean lecithin 20 parts, milk powder 20 parts;Described auxiliary agent is in units of weight portion, including following raw material: increase
Tough dose 2 parts, plasticizer 2 parts, lubricant 2 parts, cosolvent 2 parts, levelling agent 1.5 parts, dispersant 1.5
Part, compatilizer 1.5 parts, emulsifying agent 1.5 parts, stabilizer 1.5 parts, 1.2 parts of antioxidant, flocculation aid 1.2 parts,
Antibacterial 1.2 parts, tasty agents 1.2 parts, flavouring agent 1.2 parts, sweeting agent 10 parts;
Described toughener is LG-DOW 8402;Described plasticizer is epoxy soybean oil;Described lubricant is food
Use wax;Described cosolvent is polyvinylpyrrolidone;Described levelling agent is epoxidized soybean oil fatty acid;Described point
Powder consists of the following composition: potassium carboxymethylcellulose, agar, modified starch, polyacrylic acid potassium, alginic acid
Potassium, dextrin;Described compatilizer is Dupont EEA2112AC;Described emulsifying agent is distillation monoglyceride;Institute
Stating stabilizer is xanthan gum;Described antioxidant is food grade antioxidant MSK-NE150;Described flocculation aid is poly-
Acrylamide;Described antibacterial is methyl-furfuryl fumarate;Described tasty agents is guanyl potassium;Described sweeting agent
For maltose;Described flavouring agent is methyl cyclopentenyl ketone;
Described 3D printing cocoa butter substitute type chocolate, its preparation method comprises the following steps:
S1, mixing: by cocoa powder, milk powder, soybean lecithin water proof heating means melt be flowing liquid,
Melting temperature is 49 DEG C, stirs during melting, and the speed of stirring is 20r/min, and stirring to liquid material fineness is
Till 21-24 μm;
S2, refine: by mixed for step S1 material add toughener, plasticizer, compatilizer, lubricant,
Cosolvent, levelling agent, dispersant, emulsifying agent are 300W at ultrasonic power, and temperature is 50 DEG C, mixing speed
For menophania refining 0.5h under conditions of 400r/min, it is thus achieved that menophania refining feed liquid, then add steady in menophania refining feed liquid
Determining agent, antioxidant, flocculation aid, antibacterial, tasty agents, flavouring agent, sweeting agent is 200W at ultrasonic power,
Temperature is 40 DEG C, and mixing speed is menophania refining 0.4h under conditions of 300r/min, obtains chocolate liquid;
S3, sterilizing: use 200 eye mesh screens to filter the chocolate liquid that step S2 prepares, carry out after completing
Sterilization treatment, condition: temperature is 102 DEG C, pressure is 230KPa, and sterilization time is 10s;
S4, fill, sealing: be 0.099Mpa in vacuum by the chocolate liquid of step S3 sterilization treatment,
Temperature is to carry out fill, sealing at 50 DEG C, is cooled to after temperature is 23 DEG C i.e. prepare 3D and prints with for cocoa
Epoxy-type chocolate.
Embodiment 3
A kind of 3D prints with cocoa butter substitute type chocolate, in units of weight portion, including following raw material: major ingredient
85 parts, auxiliary agent 25 parts, described major ingredient is in units of weight portion, including following raw material: cocoa powder 52 parts,
Soybean lecithin 15 parts, milk powder 18 parts;Described auxiliary agent is in units of weight portion, including following raw material: increase
Tough dose 1.5 parts, plasticizer 1.5 parts, lubricant 1.5 parts, cosolvent 1.5 parts, levelling agent 1.2 parts, dispersion
Agent 1.2 parts, compatilizer 1.2 parts, emulsifying agent 1.2 parts, stabilizer 1.2 parts, 1 part of antioxidant, flocculation aid 1
Part, antibacterial 1 part, tasty agents 1 part, flavouring agent 1 part, sweeting agent 8 parts;
Described toughener is LG-DOW 8402;Described plasticizer is epoxy soybean oil;Described lubricant is food
Use wax;Described cosolvent is polyvinylpyrrolidone;Described levelling agent is epoxidized soybean oil fatty acid;Described point
Powder consists of the following composition: potassium carboxymethylcellulose, agar, modified starch, polyacrylic acid potassium, alginic acid
Potassium, dextrin;Described compatilizer is Dupont EEA2112AC;Described emulsifying agent is distillation monoglyceride;Institute
Stating stabilizer is xanthan gum;Described antioxidant is food grade antioxidant MSK-NE150;Described flocculation aid is poly-
Acrylamide;Described antibacterial is methyl-furfuryl fumarate;Described tasty agents is guanyl potassium;Described sweeting agent
For maltose;Described flavouring agent is methyl cyclopentenyl ketone;
Described 3D printing cocoa butter substitute type chocolate, its preparation method comprises the following steps:
S1, mixing: by cocoa powder, milk powder, soybean lecithin water proof heating means melt be flowing liquid,
Melting temperature is 48 DEG C, stirs during melting, and the speed of stirring is 150r/min, and stirring is to liquid material fineness
Till 21-24 μm;
S2, refine: by mixed for step S1 material add toughener, plasticizer, compatilizer, lubricant,
Cosolvent, levelling agent, dispersant, emulsifying agent are 250W at ultrasonic power, and temperature is 48 DEG C, mixing speed
For menophania refining 1h under conditions of 350r/min, it is thus achieved that menophania refining feed liquid, then add stable in menophania refining feed liquid
Agent, antioxidant, flocculation aid, antibacterial, tasty agents, flavouring agent, sweeting agent are 150W at ultrasonic power,
Temperature is 38 DEG C, and mixing speed is menophania refining 0.6h under conditions of 250r/min, obtains chocolate liquid;
S3, sterilizing: use 150 eye mesh screens to filter the chocolate liquid that step S2 prepares, carry out after completing
Sterilization treatment, condition: temperature is 100 DEG C, pressure is 220KPa, and sterilization time is 15s;
S4, fill, sealing: be 0.095Mpa in vacuum by the chocolate liquid of step S3 sterilization treatment,
Temperature is to carry out fill, sealing at 45 DEG C, is cooled to after temperature is 22 DEG C i.e. prepare 3D and prints with for cocoa
Epoxy-type chocolate.
Embodiment 4
A kind of 3D prints with cocoa butter substitute type chocolate, in units of weight portion, including following raw material: major ingredient
75 parts, auxiliary agent 20 parts, described major ingredient is in units of weight portion, including following raw material: cocoa powder 50 parts,
Soybean lecithin 10 parts, milk powder 15 parts;Described auxiliary agent is in units of weight portion, including following raw material: increase
Tough dose 1 part, plasticizer 1 part, lubricant 1 part, cosolvent 1 part, levelling agent 1 part, dispersant 1 part,
Compatilizer 1 part, emulsifying agent 1 part, stabilizer 1 part, 1 part of antioxidant, flocculation aid 1 part, antibacterial 1 part,
Tasty agents 1 part, flavouring agent 1 part, sweeting agent 6 parts;
Described toughener is LG-DOW 8402;Described plasticizer is epoxy soybean oil;Described lubricant is food
Use wax;Described cosolvent is polyvinylpyrrolidone;Described levelling agent is epoxidized soybean oil fatty acid;Described point
Powder consists of the following composition: potassium carboxymethylcellulose, agar, modified starch, polyacrylic acid potassium, alginic acid
Potassium, dextrin;Described compatilizer is Dupont EEA2112AC;Described emulsifying agent is distillation monoglyceride;Institute
Stating stabilizer is xanthan gum;Described antioxidant is food grade antioxidant MSK-NE150;Described flocculation aid is poly-
Acrylamide;Described antibacterial is methyl-furfuryl fumarate;Described tasty agents is guanyl potassium;Described sweeting agent
For maltose;Described flavouring agent is methyl cyclopentenyl ketone;
Described 3D printing cocoa butter substitute type chocolate, its preparation method comprises the following steps:
S1, mixing: by cocoa powder, milk powder, soybean lecithin water proof heating means melt be flowing liquid,
Melting temperature is 47 DEG C, stirs during melting, and the speed of stirring is 200r/min, and stirring is to liquid material fineness
Till 21-24 μm;
S2, refine: by mixed for step S1 material add toughener, plasticizer, compatilizer, lubricant,
Cosolvent, levelling agent, dispersant, emulsifying agent are 200W at ultrasonic power, and temperature is 45 DEG C, mixing speed
For menophania refining 1.5h under conditions of 300r/min, it is thus achieved that menophania refining feed liquid, then add steady in menophania refining feed liquid
Determining agent, antioxidant, flocculation aid, antibacterial, tasty agents, flavouring agent, sweeting agent is 200W at ultrasonic power,
Temperature is 40 DEG C, and mixing speed is menophania refining 0.4h under conditions of 300r/min, obtains chocolate liquid;
S3, sterilizing: use 200 eye mesh screens to filter the chocolate liquid that step S2 prepares, carry out after completing
Sterilization treatment, condition: temperature is 102 DEG C, pressure is 230KPa, and sterilization time is 10s;
S4, fill, sealing: be 0.099Mpa in vacuum by the chocolate liquid of step S3 sterilization treatment,
Temperature is to carry out fill, sealing at 50 DEG C, is cooled to after temperature is 25 DEG C i.e. prepare 3D and prints with for cocoa
Epoxy-type chocolate.
Embodiment 5
A kind of 3D prints with cocoa butter substitute type chocolate, in units of weight portion, including following raw material: major ingredient
95 parts, auxiliary agent 30 parts, described major ingredient is in units of weight portion, including following raw material: cocoa powder 60 parts,
Soybean lecithin 20 parts, milk powder 15 parts;Described auxiliary agent is in units of weight portion, including following raw material: increase
Tough dose 2 parts, plasticizer 2 parts, lubricant 2 parts, cosolvent 2 parts, levelling agent 1.5 parts, dispersant 1.5
Part, compatilizer 1.5 parts, emulsifying agent 1.5 parts, stabilizer 1.5 parts, 1.2 parts of antioxidant, flocculation aid 1.2 parts,
Antibacterial 1.2 parts, tasty agents 1.2 parts, flavouring agent 1.2 parts, sweeting agent 10 parts;
Described toughener is LG-DOW 8402;Described plasticizer is epoxy soybean oil;Described lubricant is food
Use wax;Described cosolvent is polyvinylpyrrolidone;Described levelling agent is epoxidized soybean oil fatty acid;Described point
Powder consists of the following composition: potassium carboxymethylcellulose, agar, modified starch, polyacrylic acid potassium, alginic acid
Potassium, dextrin;Described compatilizer is Dupont EEA2112AC;Described emulsifying agent is distillation monoglyceride;Institute
Stating stabilizer is xanthan gum;Described antioxidant is food grade antioxidant MSK-NE150;Described flocculation aid is poly-
Acrylamide;Described antibacterial is methyl-furfuryl fumarate;Described tasty agents is guanyl potassium;Described sweeting agent
For maltose;Described flavouring agent is methyl cyclopentenyl ketone;
Described 3D printing cocoa butter substitute type chocolate, its preparation method comprises the following steps:
S1, mixing: by cocoa powder, milk powder, soybean lecithin water proof heating means melt be flowing liquid,
Melting temperature is 49 DEG C, stirs during melting, and the speed of stirring is 20r/min, and stirring to liquid material fineness is
Till 21-24 μm;
S2, refine: by mixed for step S1 material add toughener, plasticizer, compatilizer, lubricant,
Cosolvent, levelling agent, dispersant, emulsifying agent are 300W at ultrasonic power, and temperature is 50 DEG C, mixing speed
For menophania refining 0.5h under conditions of 400r/min, it is thus achieved that menophania refining feed liquid, then add steady in menophania refining feed liquid
Determining agent, antioxidant, flocculation aid, antibacterial, tasty agents, flavouring agent, sweeting agent is 200W at ultrasonic power,
Temperature is 40 DEG C, and mixing speed is menophania refining 0.4h under conditions of 300r/min, obtains chocolate liquid;
S3, sterilizing: use 200 eye mesh screens to filter the chocolate liquid that step S2 prepares, carry out after completing
Sterilization treatment, condition: temperature is 102 DEG C, pressure is 230KPa, and sterilization time is 10s;
S4, fill, sealing: be 0.099Mpa in vacuum by the chocolate liquid of step S3 sterilization treatment,
Temperature is to carry out fill, sealing at 50 DEG C, is cooled to after temperature is 23 DEG C i.e. prepare 3D and prints with for cocoa
Epoxy-type chocolate.
Above content is it cannot be assumed that the present invention is embodied as being confined to these explanations, for technology belonging to the present invention
For the those of ordinary skill in field, without departing under present inventive concept premise, it is also possible to make and some simply pushing away
Drill or replace, all should be considered as belonging to the scope of patent protection that the present invention is determined by the claims submitted to.
Claims (2)
1. a 3D prints by the preparation method of cocoa butter substitute type chocolate, it is characterised in that comprise the following steps:
S1, mixing: by cocoa powder, milk powder, soybean lecithin water proof heating means melt be flowing liquid, melting temperature is 46-49 DEG C, during melting stir, the speed of stirring is 20-200r/min, stirring be 21-24 μm to liquid material fineness;
S2, refine: mixed for step S1 material is added toughener, plasticizer, compatilizer, lubricant, cosolvent, levelling agent, dispersant, emulsifying agent is 200-300W at ultrasonic power, temperature is 45-50 DEG C, mixing speed is menophania refining 0.5-1.5h under conditions of 300-400r/min, obtain menophania refining feed liquid, stabilizer is added again in menophania refining feed liquid, antioxidant, flocculation aid, antibacterial, tasty agents, flavouring agent, sweeting agent is 100-200W at ultrasonic power, temperature is 35-40 DEG C, mixing speed is menophania refining 0.4-0.8h under conditions of 200-300r/min, obtain chocolate liquid;
S3, sterilizing: chocolate liquid step S2 prepared uses 100-200 eye mesh screen to filter, and carries out sterilization treatment, condition: temperature is 98-102 DEG C after completing, and pressure is 210-230KPa, and sterilization time is 10-20s;
S4, fill, sealing: be 0.09-0.099Mpa in vacuum by the chocolate liquid of step S3 sterilization treatment, temperature carries out fill, sealing at being 40-50 DEG C, i.e. prepares 3D printing cocoa butter substitute type chocolate after being cooled to temperature≤25 DEG C;
Described toughener is LG-DOW 8402;Described plasticizer is epoxy soybean oil;Described lubricant is edible wax;Described cosolvent is polyvinylpyrrolidone;Described levelling agent is epoxidized soybean oil fatty acid;Described dispersant consists of the following composition: potassium carboxymethylcellulose, agar, modified starch, polyacrylic acid potassium, potassium alginate, dextrin;Described compatilizer is Dupont EEA2112AC;Described emulsifying agent is distillation monoglyceride;Described stabilizer is xanthan gum;Described antioxidant is food grade antioxidant MSK-NE150;Described flocculation aid is polyacrylamide;Described antibacterial is methyl-furfuryl fumarate;Described tasty agents is guanyl potassium;Described sweeting agent is maltose;Described flavouring agent is methyl cyclopentenyl ketone.
The preparation method of 3D printing cocoa butter substitute type chocolate the most according to claim 1, it is characterized in that, described 3D printing cocoa butter substitute type chocolate, in units of weight portion, including following raw material: major ingredient 70-100 part, auxiliary agent 20-30 part, described major ingredient is in units of weight portion, including following raw material: cocoa powder 45-60 part, soybean lecithin 10-20 part, milk powder 15-20 part;Described auxiliary agent is in units of weight portion, including following raw material: toughener 1-2 part, plasticizer 1-2 part, lubricant 1-2 part, cosolvent 1-2 part, levelling agent 1-1.5 part, dispersant 1-1.5 part, compatilizer 1-1.5 part, emulsifying agent 1-1.5 part, stabilizer 1-1.5 part, antioxidant 1-1.2 part, flocculation aid 1-1.2 part, antibacterial 1-1.2 part, tasty agents 1-1.2 part, flavouring agent 1-1.2 part, sweeting agent 6-10 part.
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CN104543269A (en) * | 2014-12-31 | 2015-04-29 | 青岛奥德莱三维打印有限公司 | Three-dimensional printing supplies and production method thereof |
CN104938738A (en) * | 2015-07-02 | 2015-09-30 | 杭州天舜食品有限公司 | Cocoa butter substitute chocolate for 3D (three-dimensional printing) printing and preparation method thereof |
CN104996691A (en) * | 2015-07-02 | 2015-10-28 | 杭州天舜食品有限公司 | Pure cocoa butter type chocolate for 3D printing and preparation method of palmin type chocolate |
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2016
- 2016-03-24 CN CN201610171212.5A patent/CN105831369A/en not_active Withdrawn
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CN104543269A (en) * | 2014-12-31 | 2015-04-29 | 青岛奥德莱三维打印有限公司 | Three-dimensional printing supplies and production method thereof |
CN104938738A (en) * | 2015-07-02 | 2015-09-30 | 杭州天舜食品有限公司 | Cocoa butter substitute chocolate for 3D (three-dimensional printing) printing and preparation method thereof |
CN104996691A (en) * | 2015-07-02 | 2015-10-28 | 杭州天舜食品有限公司 | Pure cocoa butter type chocolate for 3D printing and preparation method of palmin type chocolate |
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