CN105831369A - Preparation method of chocolate with cocoa butter alternatives for 3D printing - Google Patents

Preparation method of chocolate with cocoa butter alternatives for 3D printing Download PDF

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Publication number
CN105831369A
CN105831369A CN201610171212.5A CN201610171212A CN105831369A CN 105831369 A CN105831369 A CN 105831369A CN 201610171212 A CN201610171212 A CN 201610171212A CN 105831369 A CN105831369 A CN 105831369A
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China
Prior art keywords
chocolate
agent
temperature
printing
liquid
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CN201610171212.5A
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Chinese (zh)
Inventor
覃杨华
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Guangxi Zhumeng Three Body Technology Co Ltd
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Guangxi Zhumeng Three Body Technology Co Ltd
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Priority to CN201610171212.5A priority Critical patent/CN105831369A/en
Publication of CN105831369A publication Critical patent/CN105831369A/en
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    • AHUMAN NECESSITIES
    • A23FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
    • A23GCOCOA; COCOA PRODUCTS, e.g. CHOCOLATE; SUBSTITUTES FOR COCOA OR COCOA PRODUCTS; CONFECTIONERY; CHEWING GUM; ICE-CREAM; PREPARATION THEREOF
    • A23G1/00Cocoa; Cocoa products, e.g. chocolate; Substitutes therefor
    • A23G1/30Cocoa products, e.g. chocolate; Substitutes therefor
    • A23G1/32Cocoa products, e.g. chocolate; Substitutes therefor characterised by the composition containing organic or inorganic compounds
    • A23G1/36Cocoa products, e.g. chocolate; Substitutes therefor characterised by the composition containing organic or inorganic compounds characterised by the fats used
    • AHUMAN NECESSITIES
    • A23FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
    • A23GCOCOA; COCOA PRODUCTS, e.g. CHOCOLATE; SUBSTITUTES FOR COCOA OR COCOA PRODUCTS; CONFECTIONERY; CHEWING GUM; ICE-CREAM; PREPARATION THEREOF
    • A23G1/00Cocoa; Cocoa products, e.g. chocolate; Substitutes therefor
    • A23G1/30Cocoa products, e.g. chocolate; Substitutes therefor
    • A23G1/32Cocoa products, e.g. chocolate; Substitutes therefor characterised by the composition containing organic or inorganic compounds
    • AHUMAN NECESSITIES
    • A23FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
    • A23GCOCOA; COCOA PRODUCTS, e.g. CHOCOLATE; SUBSTITUTES FOR COCOA OR COCOA PRODUCTS; CONFECTIONERY; CHEWING GUM; ICE-CREAM; PREPARATION THEREOF
    • A23G1/00Cocoa; Cocoa products, e.g. chocolate; Substitutes therefor
    • A23G1/30Cocoa products, e.g. chocolate; Substitutes therefor
    • A23G1/32Cocoa products, e.g. chocolate; Substitutes therefor characterised by the composition containing organic or inorganic compounds
    • A23G1/46Cocoa products, e.g. chocolate; Substitutes therefor characterised by the composition containing organic or inorganic compounds containing dairy products
    • AHUMAN NECESSITIES
    • A23FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
    • A23GCOCOA; COCOA PRODUCTS, e.g. CHOCOLATE; SUBSTITUTES FOR COCOA OR COCOA PRODUCTS; CONFECTIONERY; CHEWING GUM; ICE-CREAM; PREPARATION THEREOF
    • A23G2200/00COCOA; COCOA PRODUCTS, e.g. CHOCOLATE; SUBSTITUTES FOR COCOA OR COCOA PRODUCTS; CONFECTIONERY; CHEWING GUM; ICE-CREAM; PREPARATION THEREOF containing organic compounds, e.g. synthetic flavouring agents
    • A23G2200/08COCOA; COCOA PRODUCTS, e.g. CHOCOLATE; SUBSTITUTES FOR COCOA OR COCOA PRODUCTS; CONFECTIONERY; CHEWING GUM; ICE-CREAM; PREPARATION THEREOF containing organic compounds, e.g. synthetic flavouring agents containing cocoa fat if specifically mentioned or containing products of cocoa fat or containing other fats, e.g. fatty acid, fatty alcohol, their esters, lecithin, paraffins
    • AHUMAN NECESSITIES
    • A23FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
    • A23GCOCOA; COCOA PRODUCTS, e.g. CHOCOLATE; SUBSTITUTES FOR COCOA OR COCOA PRODUCTS; CONFECTIONERY; CHEWING GUM; ICE-CREAM; PREPARATION THEREOF
    • A23G2200/00COCOA; COCOA PRODUCTS, e.g. CHOCOLATE; SUBSTITUTES FOR COCOA OR COCOA PRODUCTS; CONFECTIONERY; CHEWING GUM; ICE-CREAM; PREPARATION THEREOF containing organic compounds, e.g. synthetic flavouring agents
    • A23G2200/12COCOA; COCOA PRODUCTS, e.g. CHOCOLATE; SUBSTITUTES FOR COCOA OR COCOA PRODUCTS; CONFECTIONERY; CHEWING GUM; ICE-CREAM; PREPARATION THEREOF containing organic compounds, e.g. synthetic flavouring agents containing dairy products
    • AHUMAN NECESSITIES
    • A23FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
    • A23VINDEXING SCHEME RELATING TO FOODS, FOODSTUFFS OR NON-ALCOHOLIC BEVERAGES AND LACTIC OR PROPIONIC ACID BACTERIA USED IN FOODSTUFFS OR FOOD PREPARATION
    • A23V2002/00Food compositions, function of food ingredients or processes for food or foodstuffs

Abstract

The invention discloses a preparation method of chocolate with cocoa butter alternatives for 3D printing and belongs to the field of a chocolate preparation technology. The chocolate with cocoa butter alternatives for 3D printing is prepared by steps of mixing, refining, sterilization, filling, sealing and the like. By the use of the chocolate, heating rate during printing, melting temperature of a model and stereo-shaping rate can be raised. The chocolate of the invention has stable fluidity, a certain viscosity and a stable shaping temperature value, has good heat resistance, and will not block holes during printing. Through the 3D printing technology, original characteristics and taste of chocolate can be maintained, and a chocolate product with a novel and beautiful shape also can be prepared.

Description

A kind of preparation method of 3D printing cocoa butter substitute type chocolate
[technical field]
The invention belongs to chocolate making technology field, be specifically related to a kind of 3D printing cocoa butter substitute type chalk The preparation method of power.
[background technology]
Chocolate is mainly made with cocoa butter for primary raw material, has fertile smooth mouthfeel and strong and only Special fragrance, is liked by consumer of various countries deeply.But, chocolate is a kind of phitosite, fat and sugar Class content is higher, and protein content is on the low side.It addition, ultra-fine microcrystalline cellulose is the natural height extracted from plant Molecular compound, nonpoisonous and tasteless, do not provide energy for human body, be a kind of low heat value, the material of high microsteping content, Itself there is oils and fats sense, the effect improving food mouthfeel can be played while reducing heat, on the other hand increase Health care in terms of chocolate dietary fiber.
3D printing technique is to design a model as source with Computerized three-dimensional, becomes with numerical control by software hierarchy is discrete Type system, successively piles up printed material bonding, final superposition molding, produces entity products.Utilize 3D Printing technique can complete varied printing in kind, from medical treatment to manufacture, from historical relic's protection to scientific research.? Closely, the feeler that 3D prints extends to again field of food, and scientist have developed and prints for the 3D of food Machine, by the raw-food material such as chocolate, butter when " ink ", prints taste and different food.
At present, the defect that chocolate of the prior art exists is the bad control of mobility of slurry, the dilutest, beats Print ratio of briquetting is low;The thickest, easy plug-hole;During printer model, fusion temperature is low.
Therefore, fusion temperature and model stereo shaping rate high, nutritious 3D when developing a kind of printer model Printing cocoa butter substitute type chocolate becomes development trend.
[summary of the invention]
The present invention provides the preparation method of a kind of 3D printing cocoa butter substitute type chocolate, to solve printer model Time fusion temperature and model stereo shaping rate low, the thickest during printing, the problem such as easy plug-hole, the chalk of the present invention Power can improve heating rate, the fusion temperature of model and stereo shaping rate during printing;The chocolate tool of the present invention There are stable mobility, certain viscosity and stable forming temperature value, heat-resist, will not plug-hole during printing; The chocolate of the present invention can pass through 3D printing technique, makes and both remains with chocolate primary characteristic and taste, again The chocolate product that modern design is attractive in appearance.
For solve above technical problem, the present invention by the following technical solutions:
The preparation method of a kind of 3D printing cocoa butter substitute type chocolate, comprises the following steps:
S1, mixing: by cocoa powder, milk powder, soybean lecithin water proof heating means melt be flowing liquid, Melting temperature is 46-49 DEG C, stirs during melting, and the speed of stirring is 20-200r/min, and stirring is to liquid material Till fineness is 21-24 μm;
S2, refine: by mixed for step S1 material add toughener, plasticizer, compatilizer, lubricant, Cosolvent, levelling agent, dispersant, emulsifying agent are 200-300W at ultrasonic power, and temperature is 45-50 DEG C, stirs Mixing speed is menophania refining 0.5-1.5h under conditions of 300-400r/min, it is thus achieved that menophania refining feed liquid, then refines to menophania Feed liquid is added stabilizer, antioxidant, flocculation aid, antibacterial, tasty agents, flavouring agent, sweeting agent ultrasonic Power is 100-200W, and temperature is 35-40 DEG C, and mixing speed is menophania refining under conditions of 200-300r/min 0.4-0.8h, obtains chocolate liquid;
S3, sterilizing: chocolate liquid step S2 prepared uses 100-200 eye mesh screen to filter, after completing Carrying out sterilization treatment, condition: temperature is 98-102 DEG C, pressure is 210-230KPa, and sterilization time is 10-20s;
S4, fill, sealing: in vacuum be by the chocolate liquid of step S3 sterilization treatment 0.09-0.099Mpa, temperature carries out fill, sealing at being 40-50 DEG C, the most prepared after being cooled to temperature≤25 DEG C 3D prints with cocoa butter substitute type chocolate;
Described toughener is LG-DOW 8402;Described plasticizer is epoxy soybean oil;Described lubricant is food Use wax;Described cosolvent is polyvinylpyrrolidone;Described levelling agent is epoxidized soybean oil fatty acid;Described point Powder consists of the following composition: potassium carboxymethylcellulose, agar, modified starch, polyacrylic acid potassium, alginic acid Potassium, dextrin;Described compatilizer is Dupont EEA2112AC;Described emulsifying agent is distillation monoglyceride;Institute Stating stabilizer is xanthan gum;Described antioxidant is food grade antioxidant MSK-NE150;Described flocculation aid is poly- Acrylamide;Described antibacterial is methyl-furfuryl fumarate;Described tasty agents is guanyl potassium;Described sweeting agent For maltose;Described flavouring agent is methyl cyclopentenyl ketone;
Preferably, described 3D printing cocoa butter substitute type chocolate, in units of weight portion, including following Raw material: major ingredient 70-100 part, auxiliary agent 20-30 part, described major ingredient is in units of weight portion, including following former Material: cocoa powder 45-60 part, soybean lecithin 10-20 part, milk powder 15-20 part;Described auxiliary agent is with weight Part is unit, including following raw material: toughener 1-2 part, plasticizer 1-2 part, lubricant 1-2 part, hydrotropy Agent 1-2 part, levelling agent 1-1.5 part, dispersant 1-1.5 part, compatilizer 1-1.5 part, emulsifying agent 1-1.5 part, Stabilizer 1-1.5 part, antioxidant 1-1.2 part, flocculation aid 1-1.2 part, antibacterial 1-1.2 part, tasty agents 1-1.2 Part, flavouring agent 1-1.2 part, sweeting agent 6-10 part.
The method have the advantages that
(1) the 3D printing cocoa butter substitute type chocolate of the present invention contains potassium composition, when can improve printing Heating rate, improves fusing point;
(2) the 3D printing cocoa butter substitute type chocolate of the present invention contains the cellulose components of soybean lecithin, Model stereo shaping rate can be improved;
(3) present invention does not carry out homoiothermic use by tradition after conching, but direct quantitative is canned, Convenient store and transport, and can ready access upon use, make the 3D of chocolate print and leave factory and realize strange land and print, Use easy to operate;
(4) present invention carries out fine grinding and combines refining process to process material chocolate mass, reduces material Particle size, improves the smooth mouth-feel of chocolate, and prepared chocolate dissolves rear good fluidity, uses as raw material When 3D prints will not plug-hole, and the chocolate product printed is difficult to grow dim and turns white, and can realize creative making Diversification, in high precision, complex-curved, the chocolate product of moulding uniqueness, overturn traditional die casting pattern, It is completely free of mould constraint, meets the customized market of personalization of people.
[detailed description of the invention]
For ease of being more fully understood that the present invention, being illustrated by following instance, these examples belong to the present invention's Protection domain, but it is not intended to protection scope of the present invention.
In an embodiment, described 3D printing cocoa butter substitute type chocolate, in units of weight portion, including with Lower raw material: major ingredient 70-100 part, auxiliary agent 20-30 part, described major ingredient is in units of weight portion, including following Raw material: cocoa powder 45-60 part, soybean lecithin 10-20 part, milk powder 15-20 part;Described auxiliary agent is with weight Amount part is unit, including following raw material: toughener 1-2 part, plasticizer 1-2 part, lubricant 1-2 part, help Solvent 1-2 part, levelling agent 1-1.5 part, dispersant 1-1.5 part, compatilizer 1-1.5 part, emulsifying agent 1-1.5 Part, stabilizer 1-1.5 part, antioxidant 1-1.2 part, flocculation aid 1-1.2 part, antibacterial 1-1.2 part, delicate flavour Agent 1-1.2 part, flavouring agent 1-1.2 part, sweeting agent 6-10 part;
Described toughener is LG-DOW 8402;Described plasticizer is epoxy soybean oil;Described lubricant is food Use wax;Described cosolvent is polyvinylpyrrolidone;Described levelling agent is epoxidized soybean oil fatty acid;Described point Powder consists of the following composition: potassium carboxymethylcellulose, agar, modified starch, polyacrylic acid potassium, alginic acid Potassium, dextrin;Described compatilizer is Dupont EEA2112AC;Described emulsifying agent is distillation monoglyceride;Institute Stating stabilizer is xanthan gum;Described antioxidant is food grade antioxidant MSK-NE150;Described flocculation aid is poly- Acrylamide;Described antibacterial is methyl-furfuryl fumarate;Described tasty agents is guanyl potassium;Described sweeting agent For maltose;Described flavouring agent is methyl cyclopentenyl ketone;
Described 3D printing cocoa butter substitute type chocolate, its preparation method comprises the following steps:
S1, mixing: by cocoa powder, milk powder, soybean lecithin water proof heating means melt be flowing liquid, Melting temperature is 46-49 DEG C, stirs during melting, and the speed of stirring is 20-200r/min, and stirring is to liquid material Till fineness is 21-24 μm;
S2, refine: by mixed for step S1 material add toughener, plasticizer, compatilizer, lubricant, Cosolvent, levelling agent, dispersant, emulsifying agent are 200-300W at ultrasonic power, and temperature is 45-50 DEG C, stirs Mixing speed is menophania refining 0.5-1.5h under conditions of 300-400r/min, it is thus achieved that menophania refining feed liquid, then refines to menophania Feed liquid is added stabilizer, antioxidant, flocculation aid, antibacterial, tasty agents, flavouring agent, sweeting agent ultrasonic Power is 100-200W, and temperature is 35-40 DEG C, and mixing speed is menophania refining under conditions of 200-300r/min 0.4-0.8h, obtains chocolate liquid;
S3, sterilizing: chocolate liquid step S2 prepared uses 100-200 eye mesh screen to filter, after completing Carrying out sterilization treatment, condition: temperature is 98-102 DEG C, pressure is 210-230KPa, and sterilization time is 10-20s;
S4, fill, sealing: in vacuum be by the chocolate liquid of step S3 sterilization treatment 0.09-0.099Mpa, temperature carries out fill, sealing at being 40-50 DEG C, the most prepared after being cooled to temperature≤25 DEG C 3D prints with cocoa butter substitute type chocolate.
Below by more specifically embodiment, the present invention will be described.
Embodiment 1
A kind of 3D prints with cocoa butter substitute type chocolate, in units of weight portion, including following raw material: major ingredient 70 parts, auxiliary agent 20 parts, described major ingredient is in units of weight portion, including following raw material: cocoa powder 45 parts, Soybean lecithin 10 parts, milk powder 15 parts;Described auxiliary agent is in units of weight portion, including following raw material: increase Tough dose 1 part, plasticizer 1 part, lubricant 1 part, cosolvent 1 part, levelling agent 1 part, dispersant 1 part, Compatilizer 1 part, emulsifying agent 1 part, stabilizer 1 part, 1 part of antioxidant, flocculation aid 1 part, antibacterial 1 part, Tasty agents 1 part, flavouring agent 1 part, sweeting agent 6 parts;
Described toughener is LG-DOW 8402;Described plasticizer is epoxy soybean oil;Described lubricant is food Use wax;Described cosolvent is polyvinylpyrrolidone;Described levelling agent is epoxidized soybean oil fatty acid;Described point Powder consists of the following composition: potassium carboxymethylcellulose, agar, modified starch, polyacrylic acid potassium, alginic acid Potassium, dextrin;Described compatilizer is Dupont EEA2112AC;Described emulsifying agent is distillation monoglyceride;Institute Stating stabilizer is xanthan gum;Described antioxidant is food grade antioxidant MSK-NE150;Described flocculation aid is poly- Acrylamide;Described antibacterial is methyl-furfuryl fumarate;Described tasty agents is guanyl potassium;Described sweeting agent For maltose;Described flavouring agent is methyl cyclopentenyl ketone;
Described 3D printing cocoa butter substitute type chocolate, its preparation method comprises the following steps:
S1, mixing: by cocoa powder, milk powder, soybean lecithin water proof heating means melt be flowing liquid, Melting temperature is 46 DEG C, stirs during melting, and the speed of stirring is 200r/min, and stirring is to liquid material fineness Till 21-24 μm;
S2, refine: by mixed for step S1 material add toughener, plasticizer, compatilizer, lubricant, Cosolvent, levelling agent, dispersant, emulsifying agent are 200W at ultrasonic power, and temperature is 45 DEG C, mixing speed For menophania refining 1.5h under conditions of 300r/min, it is thus achieved that menophania refining feed liquid, then add steady in menophania refining feed liquid Determining agent, antioxidant, flocculation aid, antibacterial, tasty agents, flavouring agent, sweeting agent is 100W at ultrasonic power, Temperature is 35 DEG C, and mixing speed is menophania refining 0.8h under conditions of 200r/min, obtains chocolate liquid;
S3, sterilizing: use 100 eye mesh screens to filter the chocolate liquid that step S2 prepares, carry out after completing Sterilization treatment, condition: temperature is 98 DEG C, pressure is 210KPa, and sterilization time is 20s;
S4, fill, sealing: be 0.09Mpa in vacuum by the chocolate liquid of step S3 sterilization treatment, Temperature is to carry out fill, sealing at 40 DEG C, is cooled to after temperature is 25 DEG C i.e. prepare 3D and prints with for cocoa Epoxy-type chocolate.
Embodiment 2
A kind of 3D prints with cocoa butter substitute type chocolate, in units of weight portion, including following raw material: major ingredient 100 parts, auxiliary agent 30 parts, described major ingredient is in units of weight portion, including following raw material: cocoa powder 60 parts, Soybean lecithin 20 parts, milk powder 20 parts;Described auxiliary agent is in units of weight portion, including following raw material: increase Tough dose 2 parts, plasticizer 2 parts, lubricant 2 parts, cosolvent 2 parts, levelling agent 1.5 parts, dispersant 1.5 Part, compatilizer 1.5 parts, emulsifying agent 1.5 parts, stabilizer 1.5 parts, 1.2 parts of antioxidant, flocculation aid 1.2 parts, Antibacterial 1.2 parts, tasty agents 1.2 parts, flavouring agent 1.2 parts, sweeting agent 10 parts;
Described toughener is LG-DOW 8402;Described plasticizer is epoxy soybean oil;Described lubricant is food Use wax;Described cosolvent is polyvinylpyrrolidone;Described levelling agent is epoxidized soybean oil fatty acid;Described point Powder consists of the following composition: potassium carboxymethylcellulose, agar, modified starch, polyacrylic acid potassium, alginic acid Potassium, dextrin;Described compatilizer is Dupont EEA2112AC;Described emulsifying agent is distillation monoglyceride;Institute Stating stabilizer is xanthan gum;Described antioxidant is food grade antioxidant MSK-NE150;Described flocculation aid is poly- Acrylamide;Described antibacterial is methyl-furfuryl fumarate;Described tasty agents is guanyl potassium;Described sweeting agent For maltose;Described flavouring agent is methyl cyclopentenyl ketone;
Described 3D printing cocoa butter substitute type chocolate, its preparation method comprises the following steps:
S1, mixing: by cocoa powder, milk powder, soybean lecithin water proof heating means melt be flowing liquid, Melting temperature is 49 DEG C, stirs during melting, and the speed of stirring is 20r/min, and stirring to liquid material fineness is Till 21-24 μm;
S2, refine: by mixed for step S1 material add toughener, plasticizer, compatilizer, lubricant, Cosolvent, levelling agent, dispersant, emulsifying agent are 300W at ultrasonic power, and temperature is 50 DEG C, mixing speed For menophania refining 0.5h under conditions of 400r/min, it is thus achieved that menophania refining feed liquid, then add steady in menophania refining feed liquid Determining agent, antioxidant, flocculation aid, antibacterial, tasty agents, flavouring agent, sweeting agent is 200W at ultrasonic power, Temperature is 40 DEG C, and mixing speed is menophania refining 0.4h under conditions of 300r/min, obtains chocolate liquid;
S3, sterilizing: use 200 eye mesh screens to filter the chocolate liquid that step S2 prepares, carry out after completing Sterilization treatment, condition: temperature is 102 DEG C, pressure is 230KPa, and sterilization time is 10s;
S4, fill, sealing: be 0.099Mpa in vacuum by the chocolate liquid of step S3 sterilization treatment, Temperature is to carry out fill, sealing at 50 DEG C, is cooled to after temperature is 23 DEG C i.e. prepare 3D and prints with for cocoa Epoxy-type chocolate.
Embodiment 3
A kind of 3D prints with cocoa butter substitute type chocolate, in units of weight portion, including following raw material: major ingredient 85 parts, auxiliary agent 25 parts, described major ingredient is in units of weight portion, including following raw material: cocoa powder 52 parts, Soybean lecithin 15 parts, milk powder 18 parts;Described auxiliary agent is in units of weight portion, including following raw material: increase Tough dose 1.5 parts, plasticizer 1.5 parts, lubricant 1.5 parts, cosolvent 1.5 parts, levelling agent 1.2 parts, dispersion Agent 1.2 parts, compatilizer 1.2 parts, emulsifying agent 1.2 parts, stabilizer 1.2 parts, 1 part of antioxidant, flocculation aid 1 Part, antibacterial 1 part, tasty agents 1 part, flavouring agent 1 part, sweeting agent 8 parts;
Described toughener is LG-DOW 8402;Described plasticizer is epoxy soybean oil;Described lubricant is food Use wax;Described cosolvent is polyvinylpyrrolidone;Described levelling agent is epoxidized soybean oil fatty acid;Described point Powder consists of the following composition: potassium carboxymethylcellulose, agar, modified starch, polyacrylic acid potassium, alginic acid Potassium, dextrin;Described compatilizer is Dupont EEA2112AC;Described emulsifying agent is distillation monoglyceride;Institute Stating stabilizer is xanthan gum;Described antioxidant is food grade antioxidant MSK-NE150;Described flocculation aid is poly- Acrylamide;Described antibacterial is methyl-furfuryl fumarate;Described tasty agents is guanyl potassium;Described sweeting agent For maltose;Described flavouring agent is methyl cyclopentenyl ketone;
Described 3D printing cocoa butter substitute type chocolate, its preparation method comprises the following steps:
S1, mixing: by cocoa powder, milk powder, soybean lecithin water proof heating means melt be flowing liquid, Melting temperature is 48 DEG C, stirs during melting, and the speed of stirring is 150r/min, and stirring is to liquid material fineness Till 21-24 μm;
S2, refine: by mixed for step S1 material add toughener, plasticizer, compatilizer, lubricant, Cosolvent, levelling agent, dispersant, emulsifying agent are 250W at ultrasonic power, and temperature is 48 DEG C, mixing speed For menophania refining 1h under conditions of 350r/min, it is thus achieved that menophania refining feed liquid, then add stable in menophania refining feed liquid Agent, antioxidant, flocculation aid, antibacterial, tasty agents, flavouring agent, sweeting agent are 150W at ultrasonic power, Temperature is 38 DEG C, and mixing speed is menophania refining 0.6h under conditions of 250r/min, obtains chocolate liquid;
S3, sterilizing: use 150 eye mesh screens to filter the chocolate liquid that step S2 prepares, carry out after completing Sterilization treatment, condition: temperature is 100 DEG C, pressure is 220KPa, and sterilization time is 15s;
S4, fill, sealing: be 0.095Mpa in vacuum by the chocolate liquid of step S3 sterilization treatment, Temperature is to carry out fill, sealing at 45 DEG C, is cooled to after temperature is 22 DEG C i.e. prepare 3D and prints with for cocoa Epoxy-type chocolate.
Embodiment 4
A kind of 3D prints with cocoa butter substitute type chocolate, in units of weight portion, including following raw material: major ingredient 75 parts, auxiliary agent 20 parts, described major ingredient is in units of weight portion, including following raw material: cocoa powder 50 parts, Soybean lecithin 10 parts, milk powder 15 parts;Described auxiliary agent is in units of weight portion, including following raw material: increase Tough dose 1 part, plasticizer 1 part, lubricant 1 part, cosolvent 1 part, levelling agent 1 part, dispersant 1 part, Compatilizer 1 part, emulsifying agent 1 part, stabilizer 1 part, 1 part of antioxidant, flocculation aid 1 part, antibacterial 1 part, Tasty agents 1 part, flavouring agent 1 part, sweeting agent 6 parts;
Described toughener is LG-DOW 8402;Described plasticizer is epoxy soybean oil;Described lubricant is food Use wax;Described cosolvent is polyvinylpyrrolidone;Described levelling agent is epoxidized soybean oil fatty acid;Described point Powder consists of the following composition: potassium carboxymethylcellulose, agar, modified starch, polyacrylic acid potassium, alginic acid Potassium, dextrin;Described compatilizer is Dupont EEA2112AC;Described emulsifying agent is distillation monoglyceride;Institute Stating stabilizer is xanthan gum;Described antioxidant is food grade antioxidant MSK-NE150;Described flocculation aid is poly- Acrylamide;Described antibacterial is methyl-furfuryl fumarate;Described tasty agents is guanyl potassium;Described sweeting agent For maltose;Described flavouring agent is methyl cyclopentenyl ketone;
Described 3D printing cocoa butter substitute type chocolate, its preparation method comprises the following steps:
S1, mixing: by cocoa powder, milk powder, soybean lecithin water proof heating means melt be flowing liquid, Melting temperature is 47 DEG C, stirs during melting, and the speed of stirring is 200r/min, and stirring is to liquid material fineness Till 21-24 μm;
S2, refine: by mixed for step S1 material add toughener, plasticizer, compatilizer, lubricant, Cosolvent, levelling agent, dispersant, emulsifying agent are 200W at ultrasonic power, and temperature is 45 DEG C, mixing speed For menophania refining 1.5h under conditions of 300r/min, it is thus achieved that menophania refining feed liquid, then add steady in menophania refining feed liquid Determining agent, antioxidant, flocculation aid, antibacterial, tasty agents, flavouring agent, sweeting agent is 200W at ultrasonic power, Temperature is 40 DEG C, and mixing speed is menophania refining 0.4h under conditions of 300r/min, obtains chocolate liquid;
S3, sterilizing: use 200 eye mesh screens to filter the chocolate liquid that step S2 prepares, carry out after completing Sterilization treatment, condition: temperature is 102 DEG C, pressure is 230KPa, and sterilization time is 10s;
S4, fill, sealing: be 0.099Mpa in vacuum by the chocolate liquid of step S3 sterilization treatment, Temperature is to carry out fill, sealing at 50 DEG C, is cooled to after temperature is 25 DEG C i.e. prepare 3D and prints with for cocoa Epoxy-type chocolate.
Embodiment 5
A kind of 3D prints with cocoa butter substitute type chocolate, in units of weight portion, including following raw material: major ingredient 95 parts, auxiliary agent 30 parts, described major ingredient is in units of weight portion, including following raw material: cocoa powder 60 parts, Soybean lecithin 20 parts, milk powder 15 parts;Described auxiliary agent is in units of weight portion, including following raw material: increase Tough dose 2 parts, plasticizer 2 parts, lubricant 2 parts, cosolvent 2 parts, levelling agent 1.5 parts, dispersant 1.5 Part, compatilizer 1.5 parts, emulsifying agent 1.5 parts, stabilizer 1.5 parts, 1.2 parts of antioxidant, flocculation aid 1.2 parts, Antibacterial 1.2 parts, tasty agents 1.2 parts, flavouring agent 1.2 parts, sweeting agent 10 parts;
Described toughener is LG-DOW 8402;Described plasticizer is epoxy soybean oil;Described lubricant is food Use wax;Described cosolvent is polyvinylpyrrolidone;Described levelling agent is epoxidized soybean oil fatty acid;Described point Powder consists of the following composition: potassium carboxymethylcellulose, agar, modified starch, polyacrylic acid potassium, alginic acid Potassium, dextrin;Described compatilizer is Dupont EEA2112AC;Described emulsifying agent is distillation monoglyceride;Institute Stating stabilizer is xanthan gum;Described antioxidant is food grade antioxidant MSK-NE150;Described flocculation aid is poly- Acrylamide;Described antibacterial is methyl-furfuryl fumarate;Described tasty agents is guanyl potassium;Described sweeting agent For maltose;Described flavouring agent is methyl cyclopentenyl ketone;
Described 3D printing cocoa butter substitute type chocolate, its preparation method comprises the following steps:
S1, mixing: by cocoa powder, milk powder, soybean lecithin water proof heating means melt be flowing liquid, Melting temperature is 49 DEG C, stirs during melting, and the speed of stirring is 20r/min, and stirring to liquid material fineness is Till 21-24 μm;
S2, refine: by mixed for step S1 material add toughener, plasticizer, compatilizer, lubricant, Cosolvent, levelling agent, dispersant, emulsifying agent are 300W at ultrasonic power, and temperature is 50 DEG C, mixing speed For menophania refining 0.5h under conditions of 400r/min, it is thus achieved that menophania refining feed liquid, then add steady in menophania refining feed liquid Determining agent, antioxidant, flocculation aid, antibacterial, tasty agents, flavouring agent, sweeting agent is 200W at ultrasonic power, Temperature is 40 DEG C, and mixing speed is menophania refining 0.4h under conditions of 300r/min, obtains chocolate liquid;
S3, sterilizing: use 200 eye mesh screens to filter the chocolate liquid that step S2 prepares, carry out after completing Sterilization treatment, condition: temperature is 102 DEG C, pressure is 230KPa, and sterilization time is 10s;
S4, fill, sealing: be 0.099Mpa in vacuum by the chocolate liquid of step S3 sterilization treatment, Temperature is to carry out fill, sealing at 50 DEG C, is cooled to after temperature is 23 DEG C i.e. prepare 3D and prints with for cocoa Epoxy-type chocolate.
Above content is it cannot be assumed that the present invention is embodied as being confined to these explanations, for technology belonging to the present invention For the those of ordinary skill in field, without departing under present inventive concept premise, it is also possible to make and some simply pushing away Drill or replace, all should be considered as belonging to the scope of patent protection that the present invention is determined by the claims submitted to.

Claims (2)

1. a 3D prints by the preparation method of cocoa butter substitute type chocolate, it is characterised in that comprise the following steps:
S1, mixing: by cocoa powder, milk powder, soybean lecithin water proof heating means melt be flowing liquid, melting temperature is 46-49 DEG C, during melting stir, the speed of stirring is 20-200r/min, stirring be 21-24 μm to liquid material fineness;
S2, refine: mixed for step S1 material is added toughener, plasticizer, compatilizer, lubricant, cosolvent, levelling agent, dispersant, emulsifying agent is 200-300W at ultrasonic power, temperature is 45-50 DEG C, mixing speed is menophania refining 0.5-1.5h under conditions of 300-400r/min, obtain menophania refining feed liquid, stabilizer is added again in menophania refining feed liquid, antioxidant, flocculation aid, antibacterial, tasty agents, flavouring agent, sweeting agent is 100-200W at ultrasonic power, temperature is 35-40 DEG C, mixing speed is menophania refining 0.4-0.8h under conditions of 200-300r/min, obtain chocolate liquid;
S3, sterilizing: chocolate liquid step S2 prepared uses 100-200 eye mesh screen to filter, and carries out sterilization treatment, condition: temperature is 98-102 DEG C after completing, and pressure is 210-230KPa, and sterilization time is 10-20s;
S4, fill, sealing: be 0.09-0.099Mpa in vacuum by the chocolate liquid of step S3 sterilization treatment, temperature carries out fill, sealing at being 40-50 DEG C, i.e. prepares 3D printing cocoa butter substitute type chocolate after being cooled to temperature≤25 DEG C;
Described toughener is LG-DOW 8402;Described plasticizer is epoxy soybean oil;Described lubricant is edible wax;Described cosolvent is polyvinylpyrrolidone;Described levelling agent is epoxidized soybean oil fatty acid;Described dispersant consists of the following composition: potassium carboxymethylcellulose, agar, modified starch, polyacrylic acid potassium, potassium alginate, dextrin;Described compatilizer is Dupont EEA2112AC;Described emulsifying agent is distillation monoglyceride;Described stabilizer is xanthan gum;Described antioxidant is food grade antioxidant MSK-NE150;Described flocculation aid is polyacrylamide;Described antibacterial is methyl-furfuryl fumarate;Described tasty agents is guanyl potassium;Described sweeting agent is maltose;Described flavouring agent is methyl cyclopentenyl ketone.
The preparation method of 3D printing cocoa butter substitute type chocolate the most according to claim 1, it is characterized in that, described 3D printing cocoa butter substitute type chocolate, in units of weight portion, including following raw material: major ingredient 70-100 part, auxiliary agent 20-30 part, described major ingredient is in units of weight portion, including following raw material: cocoa powder 45-60 part, soybean lecithin 10-20 part, milk powder 15-20 part;Described auxiliary agent is in units of weight portion, including following raw material: toughener 1-2 part, plasticizer 1-2 part, lubricant 1-2 part, cosolvent 1-2 part, levelling agent 1-1.5 part, dispersant 1-1.5 part, compatilizer 1-1.5 part, emulsifying agent 1-1.5 part, stabilizer 1-1.5 part, antioxidant 1-1.2 part, flocculation aid 1-1.2 part, antibacterial 1-1.2 part, tasty agents 1-1.2 part, flavouring agent 1-1.2 part, sweeting agent 6-10 part.
CN201610171212.5A 2016-03-24 2016-03-24 Preparation method of chocolate with cocoa butter alternatives for 3D printing Withdrawn CN105831369A (en)

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CN104543269A (en) * 2014-12-31 2015-04-29 青岛奥德莱三维打印有限公司 Three-dimensional printing supplies and production method thereof
CN104938738A (en) * 2015-07-02 2015-09-30 杭州天舜食品有限公司 Cocoa butter substitute chocolate for 3D (three-dimensional printing) printing and preparation method thereof
CN104996691A (en) * 2015-07-02 2015-10-28 杭州天舜食品有限公司 Pure cocoa butter type chocolate for 3D printing and preparation method of palmin type chocolate

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CN104543269A (en) * 2014-12-31 2015-04-29 青岛奥德莱三维打印有限公司 Three-dimensional printing supplies and production method thereof
CN104938738A (en) * 2015-07-02 2015-09-30 杭州天舜食品有限公司 Cocoa butter substitute chocolate for 3D (three-dimensional printing) printing and preparation method thereof
CN104996691A (en) * 2015-07-02 2015-10-28 杭州天舜食品有限公司 Pure cocoa butter type chocolate for 3D printing and preparation method of palmin type chocolate

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