CN105820622A - High-temperature-resistant anti-corrosion and anti-radiation coating and preparation method thereof - Google Patents
High-temperature-resistant anti-corrosion and anti-radiation coating and preparation method thereof Download PDFInfo
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- CN105820622A CN105820622A CN201610270038.XA CN201610270038A CN105820622A CN 105820622 A CN105820622 A CN 105820622A CN 201610270038 A CN201610270038 A CN 201610270038A CN 105820622 A CN105820622 A CN 105820622A
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- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09D—COATING COMPOSITIONS, e.g. PAINTS, VARNISHES OR LACQUERS; FILLING PASTES; CHEMICAL PAINT OR INK REMOVERS; INKS; CORRECTING FLUIDS; WOODSTAINS; PASTES OR SOLIDS FOR COLOURING OR PRINTING; USE OF MATERIALS THEREFOR
- C09D1/00—Coating compositions, e.g. paints, varnishes or lacquers, based on inorganic substances
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- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09D—COATING COMPOSITIONS, e.g. PAINTS, VARNISHES OR LACQUERS; FILLING PASTES; CHEMICAL PAINT OR INK REMOVERS; INKS; CORRECTING FLUIDS; WOODSTAINS; PASTES OR SOLIDS FOR COLOURING OR PRINTING; USE OF MATERIALS THEREFOR
- C09D5/00—Coating compositions, e.g. paints, varnishes or lacquers, characterised by their physical nature or the effects produced; Filling pastes
- C09D5/08—Anti-corrosive paints
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- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09D—COATING COMPOSITIONS, e.g. PAINTS, VARNISHES OR LACQUERS; FILLING PASTES; CHEMICAL PAINT OR INK REMOVERS; INKS; CORRECTING FLUIDS; WOODSTAINS; PASTES OR SOLIDS FOR COLOURING OR PRINTING; USE OF MATERIALS THEREFOR
- C09D5/00—Coating compositions, e.g. paints, varnishes or lacquers, characterised by their physical nature or the effects produced; Filling pastes
- C09D5/18—Fireproof paints including high temperature resistant paints
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- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09D—COATING COMPOSITIONS, e.g. PAINTS, VARNISHES OR LACQUERS; FILLING PASTES; CHEMICAL PAINT OR INK REMOVERS; INKS; CORRECTING FLUIDS; WOODSTAINS; PASTES OR SOLIDS FOR COLOURING OR PRINTING; USE OF MATERIALS THEREFOR
- C09D7/00—Features of coating compositions, not provided for in group C09D5/00; Processes for incorporating ingredients in coating compositions
- C09D7/40—Additives
- C09D7/60—Additives non-macromolecular
- C09D7/61—Additives non-macromolecular inorganic
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- C09D7/00—Features of coating compositions, not provided for in group C09D5/00; Processes for incorporating ingredients in coating compositions
- C09D7/40—Additives
- C09D7/60—Additives non-macromolecular
- C09D7/63—Additives non-macromolecular organic
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- C09D7/00—Features of coating compositions, not provided for in group C09D5/00; Processes for incorporating ingredients in coating compositions
- C09D7/40—Additives
- C09D7/65—Additives macromolecular
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- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
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- C09D7/00—Features of coating compositions, not provided for in group C09D5/00; Processes for incorporating ingredients in coating compositions
- C09D7/40—Additives
- C09D7/70—Additives characterised by shape, e.g. fibres, flakes or microspheres
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Abstract
The invention provides a high-temperature-resistant anti-corrosion and anti-radiation coating. The coating comprises the following raw materials in parts by weight: 8-12 parts of aluminum sol, 10-15 parts of expanded graphite, 5-10 parts of carbon nano tube, 1-5 parts of titanium dioxide, 0.5-3 parts of hydroxypropyl methyl cellulose, 8-14 parts of glass powder, 5-10 parts of talcum powder, 20-25 parts of mica powder, 1-5 parts of methacrylic acid dicyclopentenyl-oxy-ethyl ester and 20-30 parts of water. The invention further provides a preparation method of the high-temperature-resistant anti-corrosion and anti-radiation coating. The components in the coating are mutually matched to complement the advantages each other, so that the coating has the properties of excellent corrosion resistance, radiation corrosion resistance, antibacterial property, flame retardance, high temperature resistance, cracking resistance, storage stability and the like on the premise that the adhesive force is remained.
Description
Technical field
The invention belongs to technical field of coatings, particularly relate to a kind of high-temperature resistant anti-corrosive radiation shielding coating and preparation method thereof.
Background technology
Radiation proof material has become a big problem of current material subject, and along with appearance and the extensively application of various high radiation devices, the research of radiation proof material has caused the common concern of people.The Fukushima nuclear power station crisis that the Japanese violent earthquake on March 11st, 2011 is caused, has also caused people's worry to radioprotective;And various radiation sources exist in people's life, also force people's attention to radiation proof material;Radiation is classified as the fourth-largest environomental pollution source after water source, air, noise by World Health Organization (WHO), becomes the stealth " killer " of harm human health, and protection radiation has become the task of top priority.
At present, radiation shielding coating mostly uses and adds heavy metal or rare metal powder and oxide thereof in coating composition, especially containing metallic compounds such as Ba, Pb, U, Lu, or employing composite deposite, but inevitable also bringing constructional difficulties, adhesive force is inadequate, the function defect such as not simultaneously, thus radiation shielding coating is the most only applied at some special industries and special dimension, and apply less in the field such as life of people.
Therefore the radiation shielding coating of the additional properties that exploitation has other concurrently becomes the task of top priority;The radiation shielding coating with other additional properties can meet the basic function of coating, widens again its application, also complies with that coating is multi-functional, the requirement of multi-field development.
Summary of the invention
In view of this, a kind of high-temperature resistant anti-corrosive radiation shielding coating of necessary offer and preparation method thereof, to overcome the problems referred to above.
The present invention provides a kind of high-temperature resistant anti-corrosive radiation shielding coating, and it includes the raw material of following weight portion: Alumina gel 8~12 parts, expanded graphite 10~15 parts, CNT 5~10 parts, titanium dioxide 1~5 parts, hydroxypropyl methyl cellulose 0.5~3 parts, glass dust 8~14 parts, Pulvis Talci 5~10 parts, mica powder 20~25 parts, acrylic acid double cyclopentenyl oxygen ethyl ester 1~5 parts and water 20~30 parts.
Wherein, described Alumina gel be a kind of pH value be 5~7, particle size analysis is at 60 ran, preferable, translucent to the transparent thick gel of the transparency, micelle microstructure in this Alumina gel is featheriness, positively charged, nontoxic, odorless, non-volatile, non-combustible, generate activated alumina or high purity aluminium oxide after high temperature dehydration.
Based on above-mentioned, it includes the raw material of following weight portion: Alumina gel 9~11 parts, expanded graphite 12~14 parts, CNT 7~9 parts, titanium dioxide 2~4 parts, hydroxypropyl methyl cellulose 1~2 parts, glass dust 10~12 parts, Pulvis Talci 7~9 parts, mica powder 22~24 parts, acrylic acid double cyclopentenyl oxygen ethyl ester 2~3 parts and water 23~27 parts.
Based on above-mentioned, it includes the raw material of following weight portion: Alumina gel 10 parts, expanded graphite 17 parts, 11 parts of glass dust, Pulvis Talci 8 parts, mica powder 23 parts, acrylic acid double cyclopentenyl oxygen ethyl ester 2 parts and 25 parts of water.
The present invention also provides for the preparation method of a kind of above-mentioned high-temperature resistant anti-corrosive radiation shielding coating, and it comprises the following steps:
Under conditions of 40~80 DEG C, Alumina gel, expanded graphite and water are uniformly mixed, form the first mixed solution;
Glass dust, Pulvis Talci and mica powder are joined in described first mixed solution, and ultrasonic disperse 30~40 minutes, obtain the second mixed solution;
CNT, titanium dioxide, hydroxypropyl methyl cellulose and acrylic acid double cyclopentenyl oxygen ethyl ester are added separately in described second mixed solution, and ultrasonic agitation 1~2 hours under conditions of 40~80 DEG C, prepare described high-temperature resistant anti-corrosive radiation shielding coating.
At above-mentioned high-temperature resistant anti-corrosive radiation shielding coating, expanded graphite not only remains the advantageous properties such as high temperature resistant, corrosion-resistant, radiation hardness, the electric conductivity of native graphite, but also has the characteristics such as flexibility, resilience, autohension, impermeability, adsorptivity and low-density.CNT be particle diameter at a kind of one-dimensional material of 10~50nm, there is the performances such as excellent heat-conductivity conducting and electronic shield.The diameter of titanium dioxide is below 100 nanometers, and product appearance is fluffy white powder;There is the performance such as anti-line, antibacterial, self-cleaning, aging resistance, weatherability.Expanded graphite, CNT and titanium dioxide interact at dispersant so that described environment-friendly type thermostable radiation shielding coating has fire-retardant, radioprotective and the function such as antibacterial.Hydroxypropyl methyl cellulose primarily serves the effect of dispersant, additionally has the features such as the low ashes of salt tolerance, pH stability, water-retaining property, dimensional stability, excellent film property and the most resistance to enzyme, thickening property and caking property.Acrylic acid double cyclopentenyl oxygen ethyl ester can carry out being polymerized and cross-linking as coalescents in the environment of film forming automatically, becomes a composition part for paint film, it is possible to makes up volume contraction in film forming procedure compared with problem big, that paint film is easy to crack.
Glass dust, Pulvis Talci and mica powder are mainly used as the implant of above-mentioned high-temperature resistant anti-corrosive radiation shielding coating.Glass dust is white powder, has the advantages such as transparency good, hardness is high, even particle size distribution, good dispersion, and paint film is good without blue light, recoatability, improves the anti scuffing performance of paint film, has photoextinction, can improve the weatherability of paint film.Pulvis Talci linear expansion coefficient is the biggest, the coefficient of expansion brushing base material close to described high-temperature resistant anti-corrosive radiation shielding coating, but its volumetric expansion dilution is the least, the most talcous interpolation can change the linear expansion coefficient of coating, anti-be full of cracks performance under the alternating hot and cold performance of raising coating and high temperature, sedimentation when coating stores can be slowed down simultaneously, and coating flowing hanging can be prevented, improve the resistance to water of film, wearability.Mica powder can significantly improve paint film strength and resistance to chalking.
Therefore, cooperate between each component in the high-temperature resistant anti-corrosive radiation shielding coating that the present invention provides, have complementary advantages, on the premise of making this coating keep good adhesion, there is the characteristics such as the anticorrosion of excellence, anti-radiation and antibacterial, fire-retardant, tolerance high temperature, anti-be full of cracks, cold-hot alternation, storage stability, have a extensive future at special dimensions such as petroleum and petrochemical industry, metallurgy, electric power, national defence.The preparation method of the above-mentioned high-temperature resistant anti-corrosive radiation shielding coating that the present invention provides is easy and simple to handle, easily realizes.
Detailed description of the invention
Below by detailed description of the invention, technical scheme is described in further detail.
Embodiment 1
The embodiment of the present invention 1 provides a kind of high-temperature resistant anti-corrosive radiation shielding coating, it includes the raw material of following weight portion: Alumina gel 8 parts, expanded graphite 10 parts, CNT 5 parts, titanium dioxide 1 part, hydroxypropyl methyl cellulose 0.5 part, 8 parts of glass dust, Pulvis Talci 5 parts, mica powder 20 parts, acrylic acid double cyclopentenyl oxygen ethyl ester 1 part and 20 parts of water, wherein, each raw material in this embodiment is technical grade.
Preparation method: under conditions of 40 DEG C, uniformly mixes Alumina gel, expanded graphite and water, forms the first mixed solution;Glass dust, Pulvis Talci and mica powder are joined in described first mixed solution, and ultrasonic disperse 30 minutes, obtain the second mixed solution;CNT, titanium dioxide, hydroxypropyl methyl cellulose and acrylic acid double cyclopentenyl oxygen ethyl ester are added separately in described second mixed solution, and ultrasonic agitation 1 hour under conditions of 40 DEG C, prepare the high-temperature resistant anti-corrosive radiation shielding coating described in the present embodiment.
Embodiment 2
The embodiment of the present invention 2 provides a kind of high-temperature resistant anti-corrosive radiation shielding coating, it includes the raw material of following weight portion: Alumina gel 9 parts, expanded graphite 12 parts, CNT 7 parts, titanium dioxide 2 parts, hydroxypropyl methyl cellulose 1 part, 10 parts of glass dust, Pulvis Talci 7 parts, mica powder 22 parts, acrylic acid double cyclopentenyl oxygen ethyl ester 2 parts and 23 parts of water, wherein, each raw material in this embodiment is technical grade.
Preparation method: under conditions of 50 DEG C, uniformly mixes Alumina gel, expanded graphite and water, forms the first mixed solution;Glass dust, Pulvis Talci and mica powder are joined in described first mixed solution, and ultrasonic disperse 30 minutes, obtain the second mixed solution;CNT, titanium dioxide, hydroxypropyl methyl cellulose and acrylic acid double cyclopentenyl oxygen ethyl ester are added separately in described second mixed solution, and under conditions of 50 DEG C ultrasonic agitation 1.5 hours, prepare high-temperature resistant anti-corrosive radiation shielding coating described in the present embodiment.
Embodiment 3
The embodiment of the present invention 3 provides a kind of high-temperature resistant anti-corrosive radiation shielding coating, it includes the raw material of following weight portion: Alumina gel 10 parts, expanded graphite 13 parts, CNT 8 parts, titanium dioxide 3 parts, hydroxypropyl methyl cellulose 1.5 parts, 11 parts of glass dust, Pulvis Talci 8 parts, mica powder 23 parts, acrylic acid double cyclopentenyl oxygen ethyl ester 2 parts and 25 parts of water, wherein, each raw material in this embodiment is technical grade.
Preparation method: under conditions of 60 DEG C, uniformly mixes Alumina gel, expanded graphite and water, forms the first mixed solution;Glass dust, mica powder and Pulvis Talci are joined in described first mixed solution, and ultrasonic disperse 35 minutes, obtain the second mixed solution;CNT, titanium dioxide, hydroxypropyl methyl cellulose and acrylic acid double cyclopentenyl oxygen ethyl ester are added separately in described second mixed solution, and under conditions of 60 DEG C ultrasonic agitation 1.5 hours, prepare high-temperature resistant anti-corrosive radiation shielding coating described in the present embodiment.
Embodiment 4
The embodiment of the present invention 4 provides a kind of high-temperature resistant anti-corrosive radiation shielding coating, it includes the raw material of following weight portion: Alumina gel 11 parts, expanded graphite 14 parts, CNT 9 parts, titanium dioxide 4 parts, hydroxypropyl methyl cellulose 2 parts, 12 parts of glass dust, Pulvis Talci 9 parts, mica powder 24 parts, acrylic acid double cyclopentenyl oxygen ethyl ester 3 parts and 27 parts of water, wherein, each raw material in this embodiment is technical grade.
Preparation method: under conditions of 70 DEG C, uniformly mixes Alumina gel, expanded graphite and water, forms the first mixed solution;Glass dust, mica powder and Pulvis Talci are joined in described first mixed solution, and ultrasonic disperse 40 minutes, obtain the second mixed solution;CNT, titanium dioxide, hydroxypropyl methyl cellulose and acrylic acid double cyclopentenyl oxygen ethyl ester are added separately in described second mixed solution, and ultrasonic agitation 2 hours under conditions of 70 DEG C, prepare the high-temperature resistant anti-corrosive radiation shielding coating described in the present embodiment.
Embodiment 5
The embodiment of the present invention 5 provides a kind of high-temperature resistant anti-corrosive radiation shielding coating, it includes the raw material of following weight portion: Alumina gel 12 parts, expanded graphite 15 parts, CNT 10 parts, titanium dioxide 5 parts, hydroxypropyl methyl cellulose 3 parts, 14 parts of glass dust, Pulvis Talci 10 parts, mica powder 25 parts, acrylic acid double cyclopentenyl oxygen ethyl ester 5 parts and 30 parts of water, wherein, each raw material in this embodiment is technical grade.
Preparation method: under conditions of 80 DEG C, uniformly mixes Alumina gel, expanded graphite and water, forms the first mixed solution;Glass dust, mica powder and Pulvis Talci are joined in described first mixed solution, and ultrasonic disperse 35 minutes, obtain the second mixed solution;CNT, titanium dioxide, hydroxypropyl methyl cellulose and acrylic acid double cyclopentenyl oxygen ethyl ester are added separately in described second mixed solution, and ultrasonic agitation 2 hours under conditions of 80 DEG C, prepare the high-temperature resistant anti-corrosive radiation shielding coating described in the present embodiment.
High-temperature resistant anti-corrosive radiation shielding coating embodiment 1 to embodiment 5 provided is coated on surface cleaning, dry sheet metal, carries out the test of correlated performance after the most at room temperature placing solidification in 24 hours.Wherein, the sheet metal used in this test be smooth, without the mechanical defect such as impression and pit, a size of 50 × 120 × 1mm(by GB GB1735-79), and through oil removing, processing of rust removing, it is ensured that this surface of thin steel sheet cleaning, dry.
Storage stability, adhesive force (by GB GB1720-89), impact strength (by GB GB/T1732-1993), drying time (by GB GB1728-1979) etc. all test according to concerned countries standard.
Heat-resisting quantity is tested: is put in Muffle furnace by model, is warmed up to 800 degree, takes out after placing 10 hours, is cooled to room temperature, observes specimen surface situation, as without pull-away, be full of cracks situation, illustrated that paint film heat resistance is good (by GB GB1735-89).
Cold-hot alternation performance test: be put in Muffle furnace by model, is warmed up to 800 degree, is incubated 10 hours, takes out, and puts in cold water and soaks 1 hour, is 1 cycle.In 5 cycles repeatedly, observe paint film change.As without pull-away, be full of cracks situation, illustrated that paint film cold-hot alternation is functional.
Whether corrosion resistance is tested: model is put into salt fog machine, does spray testing with the sodium chloride solution of 5%, observation model bubbling, get rusty (by GB GB/T1771-91).
By above method of testing, embodiment 1 to embodiment 5 result of the test is as shown in the table:
Test result table
Therefore, high-temperature resistant anti-corrosive radiation shielding coating corrosion resistance under normal temperature cure, paint film base material adhesive force, anti-be full of cracks, cold-hot alternation, high temperature that the embodiment of the present invention provides, storage property etc. is all had outstanding performance, and is a kind of well fire-resistant anticorrosion paint;Meanwhile, expanded graphite, CNT and titanium dioxide make above-mentioned coating also have radioprotective, the function such as fire-retardant, antibacterial.The production of this coating is relatively easy, saves the energy.It has a extensive future at special dimensions such as petroleum and petrochemical industry, metallurgy, electric power, national defence.
Finally should be noted that: above example is only in order to illustrate that technical scheme is not intended to limit;Although being described in detail the present invention with reference to preferred embodiment, those of ordinary skill in the field are it is understood that still can modify to the detailed description of the invention of the present invention or portion of techniques feature is carried out equivalent;Without deviating from the spirit of technical solution of the present invention, it all should be contained in the middle of the technical scheme scope that the present invention is claimed.
Claims (4)
1. a high-temperature resistant anti-corrosive radiation shielding coating, it is characterized in that, it includes the raw material of following weight portion: Alumina gel 8~12 parts, expanded graphite 10~15 parts, CNT 5~10 parts, titanium dioxide 1~5 parts, hydroxypropyl methyl cellulose 0.5~3 parts, glass dust 8~14 parts, Pulvis Talci 5~10 parts, mica powder 20~25 parts, acrylic acid double cyclopentenyl oxygen ethyl ester 1~5 parts and water 20~30 parts.
High-temperature resistant anti-corrosive radiation shielding coating the most according to claim 1, it is characterized in that, it includes the raw material of following weight portion: Alumina gel 9~11 parts, expanded graphite 12~14 parts, CNT 7~9 parts, titanium dioxide 2~4 parts, hydroxypropyl methyl cellulose 1~2 parts, glass dust 10~12 parts, Pulvis Talci 7~9 parts, mica powder 22~24 parts, acrylic acid double cyclopentenyl oxygen ethyl ester 2~3 parts and water 23~27 parts.
Described high-temperature resistant anti-corrosive radiation shielding coating the most according to claim 2, it is characterized in that, it includes the raw material of following weight portion: Alumina gel 10 parts, expanded graphite 13 parts, CNT 8 parts, titanium dioxide 3 parts, hydroxypropyl methyl cellulose 1.5 parts, 11 parts of glass dust, Pulvis Talci 8 parts, mica powder 23 parts, acrylic acid double cyclopentenyl oxygen ethyl ester 2 parts and 25 parts of water.
4. a preparation method for the high-temperature resistant anti-corrosive radiation shielding coating described in any one of claims 1 to 3, it comprises the following steps:
Under conditions of 40~80 DEG C, Alumina gel, expanded graphite and water are uniformly mixed, form the first mixed solution;
Glass dust, Pulvis Talci, mica powder are joined in described first mixed solution, and ultrasonic disperse 30~40 minutes, obtain the second mixed solution;
CNT, titanium dioxide, hydroxypropyl methyl cellulose and acrylic acid double cyclopentenyl oxygen ethyl ester are added separately in described second mixed solution, and ultrasonic agitation 1~2 hours under conditions of 40~80 DEG C, prepare described high-temperature resistant anti-corrosive radiation shielding coating.
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Cited By (2)
Publication number | Priority date | Publication date | Assignee | Title |
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CN107163723A (en) * | 2017-05-26 | 2017-09-15 | 张家港市沙源检测技术有限公司 | A kind of preparation method of electric lighting water paint |
CN107286769A (en) * | 2017-05-26 | 2017-10-24 | 张家港市沙源检测技术有限公司 | A kind of LED decorations water paint |
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CN103113768A (en) * | 2013-03-08 | 2013-05-22 | 苏州纳迪微电子有限公司 | High temperature resistant coating for engine exhaust system |
CN103740284A (en) * | 2014-01-06 | 2014-04-23 | 武汉双虎涂料有限公司 | High temperature-resistant composite inorganic binder, as well as preparation method and application thereof |
CN104087034A (en) * | 2014-07-18 | 2014-10-08 | 关锦池 | Inorganic high-temperature resistant and anti-electrostatic coating material |
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CN102585570A (en) * | 2012-01-09 | 2012-07-18 | 武汉理工大学 | Water-soluble non-combustible ceramic anti-radiation coating and preparation method thereof |
CN103113768A (en) * | 2013-03-08 | 2013-05-22 | 苏州纳迪微电子有限公司 | High temperature resistant coating for engine exhaust system |
CN103740284A (en) * | 2014-01-06 | 2014-04-23 | 武汉双虎涂料有限公司 | High temperature-resistant composite inorganic binder, as well as preparation method and application thereof |
CN104087034A (en) * | 2014-07-18 | 2014-10-08 | 关锦池 | Inorganic high-temperature resistant and anti-electrostatic coating material |
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Publication number | Priority date | Publication date | Assignee | Title |
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CN107163723A (en) * | 2017-05-26 | 2017-09-15 | 张家港市沙源检测技术有限公司 | A kind of preparation method of electric lighting water paint |
CN107286769A (en) * | 2017-05-26 | 2017-10-24 | 张家港市沙源检测技术有限公司 | A kind of LED decorations water paint |
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Application publication date: 20160803 |