CN1057998A - Packaging body - Google Patents

Packaging body Download PDF

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Publication number
CN1057998A
CN1057998A CN91104601A CN91104601A CN1057998A CN 1057998 A CN1057998 A CN 1057998A CN 91104601 A CN91104601 A CN 91104601A CN 91104601 A CN91104601 A CN 91104601A CN 1057998 A CN1057998 A CN 1057998A
Authority
CN
China
Prior art keywords
space
capsule
desiccant
encapsulating film
sheeting
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Pending
Application number
CN91104601A
Other languages
Chinese (zh)
Inventor
安孙子健治
皆川史幸
篠原宽
小关贺代子
栗林淳
海老原光孝
粟野由美子
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
KANTO ISHI PHARMACEUTICAL CO Ltd
Mect Corp
Original Assignee
KANTO ISHI PHARMACEUTICAL CO Ltd
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by KANTO ISHI PHARMACEUTICAL CO Ltd filed Critical KANTO ISHI PHARMACEUTICAL CO Ltd
Publication of CN1057998A publication Critical patent/CN1057998A/en
Pending legal-status Critical Current

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Classifications

    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B65—CONVEYING; PACKING; STORING; HANDLING THIN OR FILAMENTARY MATERIAL
    • B65D—CONTAINERS FOR STORAGE OR TRANSPORT OF ARTICLES OR MATERIALS, e.g. BAGS, BARRELS, BOTTLES, BOXES, CANS, CARTONS, CRATES, DRUMS, JARS, TANKS, HOPPERS, FORWARDING CONTAINERS; ACCESSORIES, CLOSURES, OR FITTINGS THEREFOR; PACKAGING ELEMENTS; PACKAGES
    • B65D85/00—Containers, packaging elements or packages, specially adapted for particular articles or materials
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B65—CONVEYING; PACKING; STORING; HANDLING THIN OR FILAMENTARY MATERIAL
    • B65D—CONTAINERS FOR STORAGE OR TRANSPORT OF ARTICLES OR MATERIALS, e.g. BAGS, BARRELS, BOTTLES, BOXES, CANS, CARTONS, CRATES, DRUMS, JARS, TANKS, HOPPERS, FORWARDING CONTAINERS; ACCESSORIES, CLOSURES, OR FITTINGS THEREFOR; PACKAGING ELEMENTS; PACKAGES
    • B65D81/00—Containers, packaging elements, or packages, for contents presenting particular transport or storage problems, or adapted to be used for non-packaging purposes after removal of contents
    • B65D81/24—Adaptations for preventing deterioration or decay of contents; Applications to the container or packaging material of food preservatives, fungicides, pesticides or animal repellants
    • B65D81/26—Adaptations for preventing deterioration or decay of contents; Applications to the container or packaging material of food preservatives, fungicides, pesticides or animal repellants with provision for draining away, or absorbing, or removing by ventilation, fluids, e.g. exuded by contents; Applications of corrosion inhibitors or desiccators
    • B65D81/266—Adaptations for preventing deterioration or decay of contents; Applications to the container or packaging material of food preservatives, fungicides, pesticides or animal repellants with provision for draining away, or absorbing, or removing by ventilation, fluids, e.g. exuded by contents; Applications of corrosion inhibitors or desiccators for absorbing gases, e.g. oxygen absorbers or desiccants
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B65—CONVEYING; PACKING; STORING; HANDLING THIN OR FILAMENTARY MATERIAL
    • B65D—CONTAINERS FOR STORAGE OR TRANSPORT OF ARTICLES OR MATERIALS, e.g. BAGS, BARRELS, BOTTLES, BOXES, CANS, CARTONS, CRATES, DRUMS, JARS, TANKS, HOPPERS, FORWARDING CONTAINERS; ACCESSORIES, CLOSURES, OR FITTINGS THEREFOR; PACKAGING ELEMENTS; PACKAGES
    • B65D75/00—Packages comprising articles or materials partially or wholly enclosed in strips, sheets, blanks, tubes, or webs of flexible sheet material, e.g. in folded wrappers
    • B65D75/28—Articles or materials wholly enclosed in composite wrappers, i.e. wrappers formed by associating or interconnecting two or more sheets or blanks
    • B65D75/30—Articles or materials enclosed between two opposed sheets or blanks having their margins united, e.g. by pressure-sensitive adhesive, crimping, heat-sealing, or welding
    • B65D75/32—Articles or materials enclosed between two opposed sheets or blanks having their margins united, e.g. by pressure-sensitive adhesive, crimping, heat-sealing, or welding one or both sheets or blanks being recessed to accommodate contents
    • B65D75/325—Articles or materials enclosed between two opposed sheets or blanks having their margins united, e.g. by pressure-sensitive adhesive, crimping, heat-sealing, or welding one or both sheets or blanks being recessed to accommodate contents one sheet being recessed, and the other being a flat not- rigid sheet, e.g. puncturable or peelable foil
    • B65D75/327—Articles or materials enclosed between two opposed sheets or blanks having their margins united, e.g. by pressure-sensitive adhesive, crimping, heat-sealing, or welding one or both sheets or blanks being recessed to accommodate contents one sheet being recessed, and the other being a flat not- rigid sheet, e.g. puncturable or peelable foil and forming several compartments
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B65—CONVEYING; PACKING; STORING; HANDLING THIN OR FILAMENTARY MATERIAL
    • B65D—CONTAINERS FOR STORAGE OR TRANSPORT OF ARTICLES OR MATERIALS, e.g. BAGS, BARRELS, BOTTLES, BOXES, CANS, CARTONS, CRATES, DRUMS, JARS, TANKS, HOPPERS, FORWARDING CONTAINERS; ACCESSORIES, CLOSURES, OR FITTINGS THEREFOR; PACKAGING ELEMENTS; PACKAGES
    • B65D75/00—Packages comprising articles or materials partially or wholly enclosed in strips, sheets, blanks, tubes, or webs of flexible sheet material, e.g. in folded wrappers
    • B65D75/28—Articles or materials wholly enclosed in composite wrappers, i.e. wrappers formed by associating or interconnecting two or more sheets or blanks
    • B65D75/30—Articles or materials enclosed between two opposed sheets or blanks having their margins united, e.g. by pressure-sensitive adhesive, crimping, heat-sealing, or welding
    • B65D75/32—Articles or materials enclosed between two opposed sheets or blanks having their margins united, e.g. by pressure-sensitive adhesive, crimping, heat-sealing, or welding one or both sheets or blanks being recessed to accommodate contents
    • B65D75/325—Articles or materials enclosed between two opposed sheets or blanks having their margins united, e.g. by pressure-sensitive adhesive, crimping, heat-sealing, or welding one or both sheets or blanks being recessed to accommodate contents one sheet being recessed, and the other being a flat not- rigid sheet, e.g. puncturable or peelable foil
    • B65D75/327—Articles or materials enclosed between two opposed sheets or blanks having their margins united, e.g. by pressure-sensitive adhesive, crimping, heat-sealing, or welding one or both sheets or blanks being recessed to accommodate contents one sheet being recessed, and the other being a flat not- rigid sheet, e.g. puncturable or peelable foil and forming several compartments
    • B65D75/328—Articles or materials enclosed between two opposed sheets or blanks having their margins united, e.g. by pressure-sensitive adhesive, crimping, heat-sealing, or welding one or both sheets or blanks being recessed to accommodate contents one sheet being recessed, and the other being a flat not- rigid sheet, e.g. puncturable or peelable foil and forming several compartments the compartments being interconnected, e.g. by small channels

Landscapes

  • Engineering & Computer Science (AREA)
  • Mechanical Engineering (AREA)
  • Chemical & Material Sciences (AREA)
  • Composite Materials (AREA)
  • Food Science & Technology (AREA)
  • Packages (AREA)
  • Medical Preparation Storing Or Oral Administration Devices (AREA)

Abstract

A capsule is made of not wet thoroughly sheeting and not wet thoroughly encapsulating film, and encapsulating film is sealedly connected on the said sheeting.Capsule has first space that comprises the article that will encapsulate respectively, comprises second space of desiccant respectively, and the connected space that is communicated with first and second spaces between sheeting and encapsulating film respectively, and connected space has little cross-sectional area.Article that encapsulate and desiccant are included in respectively in first, second space, place between each connected space and keep not contacting mutually.

Description

Packaging body
The present invention relates to a kind of encapsulation (Paekage) technology, specially refer to the encapsulation technology of under desirable water balance condition, preserving medicine and food.
In general, the capsule shown in Fig. 6 is used to encapsulate the medicine of capsule or sheet.Promptly as shown in Figure 6, a plurality of capsules 100 are contained in one as the article that will encapsulate are known as PTP(Press Through Pack) in the bag pressure capsule 101, this capsule is made up of the saturating wet-sheet of the moisture permeable encapsulating film and with the dished portion that is used to hold capsule, is coming the encapsulation film by heating on saturating wet-sheet.Capsule 101 is comprised in the bag 102 with desiccant 103, and bag 102 is made by aluminium etc.
Yet, in this encapsulation, found some problems, that is:
1) owing to the moisture permeable property of encapsulating film, when bag 102 was staved, moisture was invaded by encapsulating film, and the water balance of capsule 100 has just departed from desirable value as a result.
2) because 1) the result, state the occasion of packing forms in the use, when being used to have hygroscopic Powdered inhalant medicine (powderg inhafant drug), the distributive law of medicine is because the absorption of moisture and reduce rapidly and become at short notice and be lower than standard value after bag 102 is opened, thereby the Keeping life of moisture capsule 100 is very short.Similarly, can not keep designed encapsulation characteristic with other moisture absorption products that will encapsulate.
3) because 1) and 2) the result, for medicine that is easy to the absorption level and food, the threat of a kind of negative consequence as going bad just arranged.
Thereby, an object of the present invention is to provide encapsulation technology, by this technology, can keep desirable water balance or aridity, can regulate the aridity of packaged product reliably, even the not sealing of outer bag.
Another object of the present invention provides the encapsulation technology that can reliably keep packaged product design.
A further object of the present invention provides encapsulation technology easily, and packaged here article can carry by one unit.
Another object of the present invention provides encapsulation technology, can be easily sends out medicine in the pharmacy etc. with this technology.
Another object of the present invention provides a kind of making and prevents that eating desiccant becomes possible encapsulation technology by mistake.
A further object of the invention provides a kind of encapsulation technology that can suppress the cost rising.
In these inventions, representative invention is as follows with summary description:
That is, capsule of the present invention is made up of not saturating wet sheet-materials and not wet thoroughly encapsulating film, and this film is sealed on the sheet material.Between tablet material and encapsulating film, capsule has first space that comprises the article of wanting packed respectively, and capsule also has second space that comprises desiccant respectively, and respectively with first space and the connected space that is communicated with between second space is mutual.
Above-mentioned according to encapsulation of the present invention by selecting the kind of desiccant, size and shape are regulated its drying capacity changeably, and regulate and/or keep the water balance and the aridity of packed product reliably.
Not only sheeting but also encapsulating film, they have constituted capsule, all are wet thoroughly, and moisture can not be invaded the inside of capsule like this, just has been prevented from because water absorbs the rotten of packaged articles that causes, even take out the packaging bag of capsule outside conduct bag.Thereby, according to encapsulation of the present invention can be easily with in addition the one unit of packaged articles and desiccant carry.
In addition, can eliminate the situation that mistake is eaten desiccant, because packaged article and desiccant are contained in the space of separating between mutually.
Above-mentioned and other target of the present invention and novel characteristics can be more obvious in the description that links together with reference to following and accompanying drawing, in the accompanying drawings:
Fig. 1 is the amplification profile according to one unit among the encapsulation embodiment of the present invention;
Fig. 2 is according to a scheme drawing that encapsulation is implemented of the present invention;
Fig. 3 is that a diagram of curves shows according to encapsulation of the present invention and the comparison of the preservation effect of technology in the past;
Fig. 4 is according to the amplification profile of another encapsulation embodiment of the present invention;
Fig. 5 according to of the present invention another encapsulate the amplification profile of embodiment;
Fig. 6 is the scheme drawing that encapsulated in the former technology.
Embodiment 1
Referring to accompanying drawing, accompanying drawing 1 is the amplification profile according to one unit among the encapsulation embodiment of the present invention.Fig. 2 is the scheme drawing of this encapsulation embodiment among the present invention.Fig. 3 is that a diagram of curves shows according to encapsulation of the present invention and former technology preservation effect relatively.
In this embodiment, capsule 1 is by wet thoroughly sheeting 2, and wet thoroughly encapsulating film 3 formations, and sheeting 2 is by laminating such as an aluminum slice or a plastic film, and encapsulating film 3 is sealedly connected on the sheeting 2, such as connecting by thermosealed method.
Encapsulating film 3 is by forming such as not wet thoroughly plastic film, and is preferably transparent or semitransparent.For example, encapsulating film 3 can the polychloroethylene film of extensive water-based constitutes as having not by transparent resin.
As illustrated in fig. 1 and 2, encapsulating film 3 among the embodiment has space 5(first space of concave shape), the capsule 4 as the article that will encapsulate is contained in this space respectively, be used for comprising respectively space 7(second space of desiccant 6) and the connected space 8 that respectively space 5 and space 7 is interconnected, and encapsulating film 3 all parts except these spaces 5,7 and 8 all are sealedly connected on the sheeting 2.
Tablet material 2 can be staved, and staves as the finger nail of choosing, and takes out capsule 4.
Connected space 8 as depicted in figs. 1 and 2, in height is lower than space 5 and 7, is narrower than space 7 and 7 on width, determines a crevice, and the cross-sectional plane of connected space 8 is less than the outside dimension of capsule 4 and desiccant 6.Thereby be received in the space 7 or 5 that capsule 4 in space 5 or 7 and desiccant 6 can not move to connection from its space 5 or 7, not only capsule 4 but also desiccant 6 all are included in space 5 or 7 and do not contact mutually separately independently.
In addition, capsule 1 is in this embodiment engraved defiber interrupted cut-off rule or continuous recess line is determined each unit 19 so that can easily a capsule 4 be separated as one unit 19 and other unit 19 mutually with the combination of a desiccant 6 such as resembling.In this embodiment, contain 10 unit 19 in capsule 1 of purpose for example, yet this does not also mean that qualification agent 10.Therefore, owing to can easily separate each unit 19, be very easily so separate and take one or more unit away.
Whole capsule 1 is included in the bag 10, and as outer bag, bag 10 is made of a moisture impermeability material such as aluminum slice etc.
Next step explains the method for production and the operation of this embodiment.
At first, under the situation of the capsule 1 of producing this embodiment, contain the space 5 of capsule, the space 7 and the connected space 8 that contain desiccant all are to make with the not wet thoroughly encapsulating film 3 that the concave shape is made with a plastic film.
Then, stipulated that big or small capsule 4 and desiccant 6 are placed into space 5 that comprises capsule and the space 7 that comprises desiccant respectively.In this state, be that method with heated sealant is sealed on the wet thoroughly sheeting 2 except all parts of space 5,7 and 8 outer package films 3.Next step provides defiber such as interrupted line of cut or continuous recess line to capsule 1, and the combination that makes each capsule 5 and a desiccant 6 is as one unit 1a.
For the reason of selling etc., the capsule of being produced 1 is comprised in the bag 10 as outer bag, has stipulated the number of unit 1a in every bag, and such as 10 unit, bag 10 has watertightness.
In addition, above-mentioned production process can be carried out along waterline by not shown automatic production, come down to full automation production operation.
According to present embodiment, the space 5 that comprises capsule 4 is connected with the space 7 that comprises desiccant 6 by connected space 8, not only sheeting 2 but also encapsulating film 3, mutual heat seal between them, has watertightness, thereby, the drying of capsule 4 etc. only control by desiccant 6 in addition outside bag to open the back be like this, capsule 4 does not absorb any moisture from the external world.Therefore, when suitably having selected desiccant to obtain the best aridity of capsule 4 with its kind, amount, size and shape, capsule 4 and desiccant 6 are sent into its oneself space 5 and 7 respectively, thereby always capsule is remained on optimum drying degree or water balance, capsule 4 content that unfavorable phenomenon causes as the intrusion by moisture rotten or since breaking of the over-drying capsule that causes 4 all can avoid taking place.
In addition, the bag 1 among this embodiment is made of wet thoroughly dense seal unit such as 1a unit, thus on defiber 9 each unit and to take these separative elements away be very easily separately.
In addition, in the present embodiment, capsule 4 agent 6 that can not be dried is polluted, because connected space 8 has the cross-sectional plane less than the outside dimension of capsule 4 and desiccant 6, and the space 5 and 7 that is comprising capsule 4 and desiccant 6 respectively is communicated with non-touching form.In addition, eat the accident of desiccant 6 rather than capsule 4 and can prevent, because staved when taking out capsule 4 with comprising space 5 corresponding parts when sheeting 2, desiccant 6 can't take out simultaneously with capsule 4.
The present inventor compares the result of use of capsule 1 according to the present invention and the former technology shown in Fig. 6, has obtained result as shown in Figure 3.This relatively in, for each capsule, by at bag 10 and 102(by the distrib distribution radio of KI-III onto stage-2+3+4 of MLI as outer bag) open after along with the MLI(Multi-stage Liquid Impinger multistage liquid of time collides)-distributive law of 2+3+4 stage KI-III evaluate be stored in 25 ℃-83%RH(relative humidity) under the stability of powdery inhalant in capsule.According to this relatively, bag 1 demonstrated enough stability by whole 28 days, and in the former technology, and one day apportionment ratio after opening from bag descended and demonstrated the value that is significantly less than standard value (30%) in the time of 3 days.By this relatively, prove that comparing us with common capsule has obtained complete favourable stability in capsule of the present invention.
Embodiment 2
Amplification profile according to another encapsulation embodiment of the present invention has been shown among Fig. 4.This embodiment 2 is except comprising space 5a(first space at each tablet) in comprise such as tablet 4a rather than capsule as the article that will encapsulate, other is substantially the same manner as Example 1.
In this embodiment 2,, can select the characteristic that comprises size, kind and shape of desiccant 6 according to the desirable dryness factor of tablet 9.
In embodiment 1 the good various results of use of explanation also can be in this embodiment 2 second space, reach the connected space that between sheeting and packaging film, respectively first and second space is interconnected together, so that pass through desiccant, even after bag is opened outside, the aridity of packed article or water balance always remain under the felicity condition, when the excellent quality of article can be retained to it and is used.
2) according to 1), can be by selecting size, the kind of desiccant, amount and shape are regulated its drying capacity in advance, effectively prevent the rotten of the packed article that caused by dry deficiency and are broken by the over-drying packed article that cause.
3) according to 1), and remove 1) in addition, because any unfavorable accident that packaged article and desiccant direct contact cause can be eliminated, because the cross-sectional plane of connected space is less than packed article not only but also less than the outside dimension of desiccant, they are included in first and second spaces respectively and do not contact mutually.
4) according to 1) or 3), packed article always remain under the best conditions, even are taking the occasion of one or several unit away, because capsule all has the dense seal unit of moisture impermeability by each unit but constitutes, this is very useful and easily.
5) according to 4), the mode of capsule is cut apart in use, with in addition the form of one or more unit to fetch and deliver or store be more easily, because each combination of first, second space 12 connected spaces provides in said encapsulating film, the defiber that each combination is separated as a unit provides in encapsulating film and light sheet material.
6) according to 1) can prevent the trouble that mistake is got desiccant, because desiccant can not taken out,, the corresponding part of sheeting and packaged article takes out article even being staved from capsule.
7) according to 1) medicine can be in the pharmacy etc. locates easily to distribute.
8) according to 1), the capsule with good performance can only obtain drying by increasing by one.
Embodiment 3
Illustrated among Fig. 5 according to of the present invention another encapsulate the amplification profile of embodiment.Capsule 1 in the present embodiment 3 is an example, and powder 4b is placed into as the article that will encapsulate among the powder packaging 4c with moisture permeable property in this example, and it is comprised in a powder and comprises (first space) among the 5b of space then.
In this embodiment 3, also can obtain and above-mentioned example 1, example 2 essentially identical good results of use.
In addition, powder bag 4c can take out the back with it and eat and get inner powder 4b by taking out powder packaging 4e itself staving the tablet material with nail by form people such as edible film in this embodiment 3.
Resemble above-describedly, the invention of being made by the present inventor is to be that the basis illustrates with embodiment.Yet this is interpreted as the present invention and is not limited to the foregoing description; Do not leaving scope of the present invention, it all is possible that many kinds change.
For example, be used for the shape and the configuration of the shape in space of packed article and desiccant and configuration or connected space and can't help embodiment and limit.The composition material of sheeting 2 and encapsulating film 3 also can be selected changeably.
Top description is that such occasion is made, in these occasions, the present invention is applied to drug capsules, tablet and powder, yet the present invention is not confined to these occasions, and for example it can be applicable to other food that resembles the shape of product of bead shape, agriculture chemistry or the like.
Can be summarized as follows by the above-mentioned representative effect that the present invention obtained.
1) capsule is formed by not wet thoroughly sheeting and with the not wet thoroughly encapsulating film that sheeting is tightly connected, it has first space that comprises packed article respectively, the agent that comprises desiccant respectively is provided to the manufacturing line on the common capsule production technology and changes space that mould is formed for packed article and desiccant to be also had connected space and obtains, thereby has suppressed the increase of productive costs.

Claims (6)

1, a capsule is made up of the not wet thoroughly encapsulating film that not wet thoroughly sheeting and sealing are connected on the sheeting, it is characterized in that:
Between sheeting and encapsulating film, provide first space that comprises respectively by package dress article, the connected space that comprises second space of desiccant respectively and respectively first space and second space are interconnected.
2, according to the capsule of claim 1, it is characterized in that:
Said first space, said second space and said connected space are formed on the said encapsulating film with the concave shape.
3, according to the encapsulation of claim 1, it is characterized in that:
Said connected space has the cross-sectional area less than the outside dimension of said packed article and said desiccant, and
In the middle of being included in respectively, packed article and desiccant be inserted with non-touching each other said first space and said second space of connected space.
4, according to the encapsulation of claim 1, it is characterized in that:
Said first space is provided on said encapsulating film, a plurality of combinations of said second space and said connected space, and
Not only providing defiber on said encapsulating film but also the said sheeting, so that can separate as one unit each combination.
5, according to the encapsulation of claim 1, it is characterized by:
Said capsule is made of a transparent resin.
6, according to the encapsulation of claim 1, it is characterized by:
Said encapsulating film is made of the polychloroethylene film with moisture impermeability.
CN91104601A 1990-07-10 1991-07-10 Packaging body Pending CN1057998A (en)

Applications Claiming Priority (2)

Application Number Priority Date Filing Date Title
JP181784/90 1990-07-10
JP2181784A JPH0471560A (en) 1990-07-10 1990-07-10 Packing body

Publications (1)

Publication Number Publication Date
CN1057998A true CN1057998A (en) 1992-01-22

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Family Applications (1)

Application Number Title Priority Date Filing Date
CN91104601A Pending CN1057998A (en) 1990-07-10 1991-07-10 Packaging body

Country Status (13)

Country Link
EP (1) EP0466068A3 (en)
JP (1) JPH0471560A (en)
KR (1) KR920002443A (en)
CN (1) CN1057998A (en)
AU (1) AU643536B2 (en)
BR (1) BR9102914A (en)
CA (1) CA2046375A1 (en)
HU (1) HU210152B (en)
IL (1) IL98722A0 (en)
NO (1) NO912688L (en)
NZ (1) NZ238829A (en)
RO (1) RO108641B1 (en)
RU (1) RU2018470C1 (en)

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NO912688L (en) 1992-01-13
RU2018470C1 (en) 1994-08-30
AU8031191A (en) 1992-01-16
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JPH0471560A (en) 1992-03-06
JPH0581266B2 (en) 1993-11-12
BR9102914A (en) 1992-02-11
EP0466068A2 (en) 1992-01-15
HU210152B (en) 1995-02-28
CA2046375A1 (en) 1992-01-11
HU912321D0 (en) 1991-12-30
NO912688D0 (en) 1991-07-09
KR920002443A (en) 1992-02-28
EP0466068A3 (en) 1992-12-09
IL98722A0 (en) 1992-07-15
AU643536B2 (en) 1993-11-18
RO108641B1 (en) 1994-07-29

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