CN105797508B - A kind of high-temperature oil gas, vapor, the easy precipitate containing carbons gaseous mixture filtering dust method - Google Patents

A kind of high-temperature oil gas, vapor, the easy precipitate containing carbons gaseous mixture filtering dust method Download PDF

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Publication number
CN105797508B
CN105797508B CN201610326539.5A CN201610326539A CN105797508B CN 105797508 B CN105797508 B CN 105797508B CN 201610326539 A CN201610326539 A CN 201610326539A CN 105797508 B CN105797508 B CN 105797508B
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gas
disengagement chamber
filter mechanism
regeneration
vapor
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CN105797508A (en
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朱书成
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Hebei Longcheng Coal Comprehensive Utilization Co ltd
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Henan Longcheng Coal Efficient Technology Application Co Ltd
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    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01DSEPARATION
    • B01D46/00Filters or filtering processes specially modified for separating dispersed particles from gases or vapours
    • B01D46/56Filters or filtering processes specially modified for separating dispersed particles from gases or vapours with multiple filtering elements, characterised by their mutual disposition
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01DSEPARATION
    • B01D46/00Filters or filtering processes specially modified for separating dispersed particles from gases or vapours
    • B01D46/10Particle separators, e.g. dust precipitators, using filter plates, sheets or pads having plane surfaces
    • B01D46/103Curved filtering elements
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01DSEPARATION
    • B01D46/00Filters or filtering processes specially modified for separating dispersed particles from gases or vapours
    • B01D46/10Particle separators, e.g. dust precipitators, using filter plates, sheets or pads having plane surfaces
    • B01D46/12Particle separators, e.g. dust precipitators, using filter plates, sheets or pads having plane surfaces in multiple arrangements
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01DSEPARATION
    • B01D46/00Filters or filtering processes specially modified for separating dispersed particles from gases or vapours
    • B01D46/66Regeneration of the filtering material or filter elements inside the filter
    • B01D46/80Chemical processes for the removal of the retained particles, e.g. by burning
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01DSEPARATION
    • B01D2267/00Multiple filter elements specially adapted for separating dispersed particles from gases or vapours
    • B01D2267/30Same type of filters

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  • Chemical & Material Sciences (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Filtering Materials (AREA)
  • Filtering Of Dispersed Particles In Gases (AREA)
  • Industrial Gases (AREA)

Abstract

The invention discloses a kind of high-temperature oil gas, vapor, the filtering dust method of the gaseous mixture of the easy precipitate containing carbons, high-temperature gas mixture passes through inlet manifold, air intake branch is passed through the closed disengagement chamber after preheating, dust filter mechanism effect under with mixed gas separation, the easy precipitate containing carbons separates out out of mixed gas simultaneously, block the stomata in filter mechanism, and make filter cake more and more thicker, when precipitate so that filter mechanism blocks and during cisco unity malfunction, disconnect the connection of high-temperature gas mixture and the closed disengagement chamber, the closed disengagement chamber being passed through after another preheating, ensure that filter process is uninterrupted;It is passed through after regeneration gas preheating in the closed disengagement chamber of cisco unity malfunction, be attached to material in filter mechanism surface and stomata at high temperature with regeneration gas slow reaction, product discharges closed disengagement chamber, it is final to realize that filter mechanism regenerates, regeneration and filtering are alternately, ensure that separation process is uninterrupted, filter efficiency and regeneration efficiency are high.

Description

A kind of high-temperature oil gas, vapor, the easy precipitate containing carbons gaseous mixture filtering dust Method
Technical field
The present invention, which relates to, belongs to dedusting technical field, and in particular to a kind of high-temperature oil gas, vapor, easily separates out containing carbons The filtering dust method of the gaseous mixture of thing.
Background technology
High-temperature dusty gas is often produced in industries such as chemical industry, oil, metallurgy, particularly generates coal tar in low order pyrolysis of coal During oil gas, decomposition gas are to improve Coal Quality, coal material stirs rolling and risen, and causes coal dust in caused admixture of gas to contain Amount is very high, and easily separates out material such as tar, class bituminous material, coal ash attachment only in high temperature containing carbons in mixed gas Can exist in environment with gaseous state, temperature is slightly too low or environment is once change, and is easy for slowly separating out from gaseous mixture. Material such as tar Jiao, class bituminous material, coal ash the attachment rich product in filtering body stomata and filter cake are easily separated out containing carbons, in right amount Filter cake can allow the filter effect of filtering gas more preferable, but the easy precipitate containing carbons once gathered is excessive, on the one hand can block up The stomata of filtering body is filled in, on the one hand filter cake can be made gradually to thicken, and then loses filtering function, production is not continued.Even In the state of filter cavity continuous high temperature, the too high admixture of gas of dustiness is in filter process, because molecule liquefies, be solidifying Gu the relation between contact environment, temperature change, frequently position is being physically contacted with filtering body, can still engender and contain The phenomenon that the easy precipitate of carbons such as tar Jiao, class bituminous material, coal ash attachment separate out from gaseous mixture, is enriched in filtering body gas In hole, and filter cake is set gradually to thicken, forfeiture filtering function, and the replacing of filtering body, stopping production problem will necessarily be brought, for continuous The large chemical equipment of operation says that stop production to overhaul will necessarily bring huge economic loss.For a long time, either it is domestic still Foreign countries, high-temperature oil gas, vapor, the easy precipitate containing carbons gaseous mixture dust removal by filtration problem, particularly high Dust Capacity it is mixed Close oil gas dust removal problem to fail effectively to be solved all the time, it is impossible to form industrialized production, directly affect the entirety of our times Coal Industrial general layout, substantial amounts of low-order coal can not be utilized rapidly and efficiently.
Chinese patent CN104226028A discloses a kind of high-temperature oil gas, vapor, the gaseous mixture of the easy precipitate containing carbons Filtering dust method, by will separation gaseous mixture connect and disconnect with two or more filter plants, can be easily one Filtering mechanism works in individual filter plant for a period of time after, filter mechanism filter capacity in surface and stomata because contain carbons The combination of easy precipitate such as tar Jiao, class bituminous material and coal ash attachment, thickeies and declines to a great extent so that can not meet just Often when work, it is switched in another filter plant and goes, ensures that separation process is uninterrupted;And the filter plant being stopped Reacted by the fertile absorber with slow transitting through such as oxygen-containing gas, carbon dioxide containing gas, vapor, be by Main Ingredients and Appearance gradually The filter mechanism attachment of carbon reacts away, and becomes the gases such as carbon monoxide and is left out of filter mechanism surface and stomata, was realized The regeneration of filter structure filter capacity.Chinese patent CN104147862A discloses a kind of high-temperature oil gas, vapor, easily analysed containing carbons Go out the filtering dust system of the gaseous mixture of thing, including connect the closed disengagement chamber of admission line and discharge duct, described closed point Filter mechanism is set from intracavitary, the outer surface of the filter mechanism connects with admission line, and inner surface connects with discharge duct, institute State and filter regeneration mechanism is set in filtering dust system.The present invention by including connection admission line and discharge duct it is close Close and filter regeneration mechanism is set in disengagement chamber, can be after body running be filtered for a period of time, filtering body filter capacity is because table Tar coal ash attachment in face and stomata and decline to a great extent when can not meet normal work, by filter regeneration mechanism work Make, by filtering body it is important return to it is due it is horizontal up, repeated regeneration directly reduces the input of filtering body, also greatly improves The service life of filtering body.But these patents are not abundant enough to Btu utilization, substantial amounts of waste heat, and regeneration gas are wasted The temperature control of body is not accurate enough, it is not abundant enough to be contacted with filter mechanism, so that anti-containing the easy precipitate of carbons and regeneration gas Should be not thorough.
The content of the invention
To overcome drawbacks described above, it is an object of the invention to provide a kind of high-temperature oil gas, vapor, containing the easy precipitate of carbons Gaseous mixture filtering dust method.
A kind of high-temperature oil gas, vapor, the easy precipitate containing carbons gaseous mixture filtering dust method, including following step Suddenly:
(1)By 300-700 DEG C of high-temperature oil gas, vapor, the easy precipitate containing carbons gaseous mixture by inlet manifold, enter Gas branch pipe is passed through the closed disengagement chamber after preheating, and gaseous mixture is by the filter mechanism in closed disengagement chamber, and dust is in filter mechanism Effect is lower and mixed gas separation, high temperature cleaning gaseous mixture pass sequentially through exhaust branch pipe, exhaust main discharge;
(2)With the progress of filtering, gradually have containing the easy precipitate of carbons for example tar, class bituminous material, coal ash attachment from Separated out in mixed gas, block the stomata in filter mechanism, and make filter cake more and more thicker;
(3)When precipitate so that filter mechanism blocks and during cisco unity malfunction, disconnect high-temperature oil gas, vapor, carbon containing The connection of the gaseous mixture of the easy precipitate of class and the closed disengagement chamber, the closed disengagement chamber being passed through after another preheating, ensured It is uninterrupted to filter journey;
(4)After regeneration gas is preheated to 450-500 DEG C, it is passed through in the closed disengagement chamber of cisco unity malfunction, duration of ventilation 5-10h, the material being attached in filter mechanism surface and stomata are close with regeneration gas slow reaction, product discharge at high temperature Disengagement chamber is closed, finally realizes that filter mechanism regenerates;
(5)When the closed disengagement chamber in work can not work because filter mechanism blocks, high-temperature oil gas, vapor, contain The closed disengagement chamber that the gaseous mixture of the easy precipitate of carbons is switched to after regeneration again works on, the like, realize multiple closed The periodicity alternation of disengagement chamber and regeneration.
Preferably, the regeneration gas is oxygen-containing gas or vapor.
Preferably, described oxygen-containing gas is that air forms through the dilution of carbon dioxide, nitrogen or vapor, oxygen Volume content is 3-8%.
Preferably, described oxygen-containing gas is that air forms through vapor dilution.
Preferably, the filter mechanism is several arcs of recesses screen packs arranged side by side, to filtration system inlet manifold direction Depression.
The positive beneficial effect of the present invention:
1. filtering dust system filter mechanism of the present invention is several arcs of recesses filters arranged side by side, filter is to filtering System inlet manifold direction is recessed, high-temperature gas mixture resistance reduces, and is easy to flow, and high-temperature gas mixture and filter mechanism connect Contacting surface product is big, thorough to filtering dust, and filter efficiency is high.
2. regeneration gas of the present invention is preheated to 450-500 DEG C, temperature is high, and oxidation reaction is abundant, favorable regeneration effect, extends The usage time of filtration system, and regeneration rate is fast, present invention filtering and regeneration alternately, ensure between separation process not Disconnected, filter efficiency and regeneration efficiency are high.
Formed 3. oxygen-containing gas of the present invention is air through vapor dilution, wherein oxygen and vapor can mix with high temperature Close the tar in gas, class bituminous material, coal ash attachment and oxidation reaction occurs, realize the regeneration of filter mechanism, favorable regeneration effect.
Brief description of the drawings
Fig. 1 is high-temperature oil gas of the present invention, the filtering dust device structure of the gaseous mixture of vapor, the easy precipitate containing carbons shows It is intended to;
In figure:The closed disengagement chambers of 1-, 2- air intake branches, 3- inlet manifold, 4- exhaust branch pipes, 5- exhaust mains, 6- valves, 7- filter mechanisms, 8- regeneration gas air inlets.
Embodiment
With reference to some specific embodiments, the present invention is further described.
Embodiment 1
Referring to Fig. 1, filtration system used by filter method of the present invention, including multiple closed disengagement chambers 1 in parallel, it is described Closed disengagement chamber 1 connects inlet manifold 3 by air intake branch 2, and exhaust main 5, the air intake branch are connected by exhaust branch pipe 4 2 and exhaust branch pipe 4 in be respectively equipped with valve 6, filter mechanism 7 and regeneration gas air inlet 8 are set in the closed disengagement chamber 1, The filter mechanism 7 is several arcs of recesses screen packs arranged side by side, is recessed to the direction of filtration system inlet manifold 3, regeneration gas It is passed through by regeneration gas air inlet 8 in closed disengagement chamber 1.
A kind of high-temperature oil gas, vapor, the easy precipitate containing carbons gaseous mixture filtering dust method, including following step Suddenly:
(1)By 300-700 DEG C of high-temperature oil gas, vapor, the easy precipitate containing carbons gaseous mixture be passed through preheating after it is close Disengagement chamber 1 is closed, gaseous mixture is by the filter mechanism 7 in closed disengagement chamber 1, and dust is under the effect of filter mechanism 7 with mixing qi leel From high temperature cleaning gaseous mixture passes sequentially through exhaust branch pipe 4, exhaust main 5 is discharged;
(2)With the progress of filtering, gradually have containing the easy precipitate of carbons such as tar Jiao, class bituminous material, coal ash attachment Separated out out of mixed gas, block the stomata in filter mechanism 7, and make filter cake more and more thicker;
(3)When precipitate so that filter mechanism 7 blocks and during cisco unity malfunction, disconnect high-temperature oil gas, vapor, carbon containing The connection of the gaseous mixture of the easy precipitate of class and the closed disengagement chamber 1, the closed disengagement chamber 1 being passed through after another preheating, ensures Filter process is uninterrupted;
(4)After regeneration gas is preheated to 450 DEG C, the closed separation of cisco unity malfunction is passed through by regeneration gas air inlet 8 Chamber 1, the regeneration gas are oxygen-containing gas, and oxygen-containing gas is that air forms through vapor dilution, and oxygen volume content is 5%, is led to Gas time 6h, the material being attached in the surface of filter mechanism 7 and stomata are arranged with regeneration gas slow reaction, product at high temperature Go out closed disengagement chamber 1, finally realize that filter mechanism 7 regenerates;
(5)When the closed disengagement chamber 1 in work because filter mechanism 7 block can not work when, high-temperature oil gas, vapor, The gaseous mixture of the easy precipitate containing carbons be switched to again regeneration after closed disengagement chamber 1 work on, the like, realize two it is close Close the periodicity alternation and regeneration of disengagement chamber 1.
Embodiment 2
The present embodiment filter method is similar with the filter method of embodiment 1, and same section does not repeat, and somewhat different is:Institute State regeneration gas and be preheated to 460 DEG C.
Embodiment 3
The present embodiment filter method is similar with the filter method of embodiment 1, and same section does not repeat, and somewhat different is:Institute State regeneration gas and be preheated to 440 DEG C.
Embodiment 4
The present embodiment filter method is similar with the filter method of embodiment 1, and same section does not repeat, and somewhat different is:Institute It is oxygen-containing gas to state regeneration gas, and oxygen-containing gas is that air forms through vapor dilution, and oxygen volume content is 6%.
Embodiment 5
The present embodiment filter method is similar with the filter method of embodiment 1, and same section does not repeat, and somewhat different is:Institute It is oxygen-containing gas to state regeneration gas, and oxygen-containing gas is that air forms through vapor dilution, and oxygen volume content is 4%.
Embodiment 6
The present embodiment filter method is similar with the filter method of embodiment 1, and same section does not repeat, and somewhat different is:Institute State regeneration gas and be preheated to 470 DEG C, duration of ventilation 8h, the regeneration gas is oxygen-containing gas, and oxygen-containing gas is air through dioxy Change carbon gas dilution to form, oxygen volume content is 8%.
Embodiment 7
The present embodiment filter method is similar with the filter method of embodiment 1, and same section does not repeat, and somewhat different is:Institute State regeneration gas and be preheated to 480 DEG C, duration of ventilation 7h, the regeneration gas is vapor.
Embodiment 8
The present embodiment filter method is similar with the filter method of embodiment 1, and same section does not repeat, and somewhat different is:Institute State regeneration gas and be preheated to 490 DEG C, duration of ventilation 5h, the regeneration gas is oxygen-containing gas, and oxygen-containing gas is air through dioxy Change carbon dilution to form, oxygen volume content is 4%.
Embodiment 9
The present embodiment filter method is similar with the filter method of embodiment 1, and same section does not repeat, and somewhat different is:Institute State regeneration gas and be preheated to 500 DEG C, duration of ventilation 10h, the regeneration gas is oxygen-containing gas, and oxygen-containing gas is air through nitrogen Dilution forms, and oxygen volume content is 3%.
Application test
The high temperature of Co., Ltd is applied using 1-9 of embodiment of the present invention filter method processing Henan dragon coal-forming high efficiency technical Oil gas, vapor, the gaseous mixture of the easy precipitate containing carbons, the results are shown in Table 1.
The 1-9 results of the embodiment of the present invention of table 1
As can be seen from Table 1:Processing effect of the preheating temperature of 1-9 of embodiment of the present invention regeneration gas to high-temperature gas mixture Fruit has a great influence, and when the regeneration gas preheating temperature of embodiment 1 is 450 DEG C, regeneration gas is that air forms through vapor dilution, oxygen Air volume content is 5%, and the treatment effeciency of tar and dust is respectively 83% and 99.8%, and treatment effeciency is high.
Finally illustrate, the above embodiments are merely illustrative of the technical solutions of the present invention and it is unrestricted, this area is common Other modifications or equivalent substitution that technical staff is made to technical scheme, without departing from technical solution of the present invention Spirit and scope, all should cover among scope of the presently claimed invention.

Claims (5)

  1. A kind of 1. filtering dust method of the gaseous mixture of high-temperature oil gas, vapor, the easy precipitate containing carbons, it is characterised in that bag Include following steps:
    (1)The gaseous mixture of 300-700 DEG C of high-temperature oil gas, vapor, the easy precipitate containing carbons is passed through into inlet manifold, air inlet branch Pipe is passed through the closed disengagement chamber after preheating, and gaseous mixture is acted on by the filter mechanism in closed disengagement chamber, dust in filter mechanism Lower and mixed gas separation, high temperature cleaning gaseous mixture pass sequentially through exhaust branch pipe, exhaust main discharge;The filter mechanism is some Individual arcs of recesses screen pack arranged side by side, screen pack are recessed to filtration system inlet manifold direction;
    (2)With the progress of filtering, gradually there is the easy precipitate containing carbons to be separated out out of mixed gas, block the gas in filter mechanism Hole, and make filter cake more and more thicker;
    (3)When precipitate so that filter mechanism blocks and during cisco unity malfunction, disconnect high-temperature oil gas, vapor, easy containing carbons The connection of the gaseous mixture of precipitate and the closed disengagement chamber, the closed disengagement chamber being passed through after another preheating, ensures filtered Journey is uninterrupted;
    (4)After regeneration gas is preheated to 450-500 DEG C, it is passed through in the closed disengagement chamber of cisco unity malfunction, duration of ventilation 5- 10h, the material being attached in filter mechanism surface and stomata are closed with regeneration gas slow reaction, product discharge at high temperature Disengagement chamber, finally realize that filter mechanism regenerates;
    (5)When the closed disengagement chamber in work can not work because filter mechanism blocks, high-temperature oil gas, vapor, containing carbons The closed disengagement chamber that the gaseous mixture of easy precipitate is switched to after regeneration again works on, the like, realize multiple closed separation The periodicity alternation of chamber and regeneration.
  2. 2. filtering dust method according to claim 1, it is characterised in that the regeneration gas is oxygen-containing gas or water Steam.
  3. 3. filtering dust method according to claim 2, it is characterised in that described oxygen-containing gas is air through titanium dioxide Carbon gas, nitrogen or vapor dilution form, and oxygen volume content is 3-8%.
  4. 4. filtering dust method according to claim 3, it is characterised in that described oxygen-containing gas is air through vapor Dilution forms.
  5. 5. filtering dust method according to claim 1, it is characterised in that the easy precipitate of carbons that contains is tar, class Bituminous material or coal ash attachment.
CN201610326539.5A 2016-05-17 2016-05-17 A kind of high-temperature oil gas, vapor, the easy precipitate containing carbons gaseous mixture filtering dust method Active CN105797508B (en)

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CN107126773A (en) * 2017-04-27 2017-09-05 舒尔环保科技(合肥)有限公司 A kind of Combined air filter
CN107081016A (en) * 2017-05-31 2017-08-22 四川建源节能科技有限公司 A kind of filter membrane
CN111135650B (en) * 2019-12-31 2022-04-12 中国化学工程第十三建设有限公司 Tail gas treatment device for gasification furnace
CN111482015A (en) * 2020-04-18 2020-08-04 钟辉 Industrial waste gas particle filters with exempting from to change formula and endow magnetism filter layer
CN111991949A (en) * 2020-08-26 2020-11-27 郑少伟 Air filter for coal-fired power generation and mounting assembly thereof
CN112138479B (en) * 2020-09-30 2022-04-01 格鼎机电有限公司 Variable air duct dust remover convenient to maintain

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JPS6053165B2 (en) * 1981-03-16 1985-11-25 株式会社豊田中央研究所 Internal combustion engine exhaust smoke collection device
US4502874A (en) * 1982-10-08 1985-03-05 Pneumafil Corporation Continuous filtration
US6077490A (en) * 1999-03-18 2000-06-20 Mcdermott Technology, Inc. Method and apparatus for filtering hot syngas
JP2001329830A (en) * 2000-03-15 2001-11-30 Ibiden Co Ltd Regeneration device for exhaust gas purifying filter, and filter regeneration method, regeneration program for exhaust gas purifying filter, and recording medium storing program
CN103644014B (en) * 2013-12-23 2016-04-20 苏州赛菲集团有限公司 A kind of regenerative aluminum-containing silicon carbide fiber felt microparticle catcher and manufacture method thereof

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