CN105776774A - Treatment method of vegetable pickling wastewater - Google Patents
Treatment method of vegetable pickling wastewater Download PDFInfo
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- CN105776774A CN105776774A CN201610312796.3A CN201610312796A CN105776774A CN 105776774 A CN105776774 A CN 105776774A CN 201610312796 A CN201610312796 A CN 201610312796A CN 105776774 A CN105776774 A CN 105776774A
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- vegetable
- waste water
- pickling waste
- processing method
- candidiasis
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- C—CHEMISTRY; METALLURGY
- C02—TREATMENT OF WATER, WASTE WATER, SEWAGE, OR SLUDGE
- C02F—TREATMENT OF WATER, WASTE WATER, SEWAGE, OR SLUDGE
- C02F9/00—Multistage treatment of water, waste water or sewage
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- C—CHEMISTRY; METALLURGY
- C02—TREATMENT OF WATER, WASTE WATER, SEWAGE, OR SLUDGE
- C02F—TREATMENT OF WATER, WASTE WATER, SEWAGE, OR SLUDGE
- C02F1/00—Treatment of water, waste water, or sewage
- C02F1/001—Processes for the treatment of water whereby the filtration technique is of importance
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- C—CHEMISTRY; METALLURGY
- C02—TREATMENT OF WATER, WASTE WATER, SEWAGE, OR SLUDGE
- C02F—TREATMENT OF WATER, WASTE WATER, SEWAGE, OR SLUDGE
- C02F1/00—Treatment of water, waste water, or sewage
- C02F1/66—Treatment of water, waste water, or sewage by neutralisation; pH adjustment
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- C—CHEMISTRY; METALLURGY
- C02—TREATMENT OF WATER, WASTE WATER, SEWAGE, OR SLUDGE
- C02F—TREATMENT OF WATER, WASTE WATER, SEWAGE, OR SLUDGE
- C02F2103/00—Nature of the water, waste water, sewage or sludge to be treated
- C02F2103/32—Nature of the water, waste water, sewage or sludge to be treated from the food or foodstuff industry, e.g. brewery waste waters
-
- C—CHEMISTRY; METALLURGY
- C02—TREATMENT OF WATER, WASTE WATER, SEWAGE, OR SLUDGE
- C02F—TREATMENT OF WATER, WASTE WATER, SEWAGE, OR SLUDGE
- C02F3/00—Biological treatment of water, waste water, or sewage
- C02F3/34—Biological treatment of water, waste water, or sewage characterised by the microorganisms used
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- Life Sciences & Earth Sciences (AREA)
- Hydrology & Water Resources (AREA)
- Engineering & Computer Science (AREA)
- Environmental & Geological Engineering (AREA)
- Water Supply & Treatment (AREA)
- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Activated Sludge Processes (AREA)
- Separation Using Semi-Permeable Membranes (AREA)
Abstract
The invention discloses a treatment method of vegetable pickling wastewater. The treatment method comprises the following steps of step 1, taking vegetable pickling wastewater, and filtering out suspended solids in the vegetable pickling wastewater; step 2, taking the vegetable pickling wastewater processed in the step 1, and regulating the pH within a range of 3.5-4.0 to 10-10.5, and removing separated solids in time during a regulation process; step 3, taking the vegetable pickling wastewater processed in the step 2, adding an antagonist, and regulating the pH to 6-7; and step 4, taking cultured candida mycoderma bacteria, and spraying temperature-resistant micro water-selective membrane on the external surfaces of the candida mycoderma bacteria, then adding the candida mycoderma bacteria into the vegetable pickling wastewater processed in the step 3, and performing aerobic treatment. The treatment method has the advantages of quickening the wastewater treatment efficiency and improving the treatment effect.
Description
Technical field
The present invention relates to field of waste water treatment, particularly to the processing method of a kind of vegetable-pickling waste water.
Background technology
Pickle is appetizing food common on China's resident's dining table, and it has inadvisable in the diet of Chinese
The status in generation.But substantial amounts of high salt acidic organic wastewater can be produced during vegetable-pickling, if vegetable-pickling waste water is directly arranged
Put structure and the nutrition being easily destroyed soil so that soil leanness, the growth of harm animal and plant, the most more and more
Cause people's concern to it.Although the Organic substance easily biological-degradable in vegetable-pickling waste water, but the sodium chloride of its middle and high concentration
But the growth of microorganism can be produced inhibitory action.
Publication No. CN101586084A, publication date are that the Chinese patent on November 25th, 2009 provides a strain guarantor
Hide numbered CGMCC No.3000, vegetable-pickling waste water can be carried out the candidiasis G70 of weak basification
(Gandida thaimueangensis) and utilize the method that this bacterial strain carries out weak basification to vegetable-pickling waste water.
Research finds, although this candidiasis G70 can be by the metabolic activity of self by vegetable-pickling waste water
Acidity is removed completely, but owing to the speed used time limiting this process of salinity is longer；And the effect of this process and efficiency
All Effects of Salinities by pickling waste water are bigger.
Summary of the invention
It is an object of the invention to provide the processing method of a kind of vegetable-pickling waste water, which solve and process at candidiasis
The speed of vegetable waste water and effect, by the bigger problem of Effects of Salinity, have quickening waste water treatment efficiency and improve treatment effect
Advantage.
The above-mentioned technical purpose of the present invention has the technical scheme that
The processing method of a kind of vegetable-pickling waste water, comprises the steps:
Step 1, takes vegetable-pickling waste water, the float being filtered to remove in vegetable-pickling waste water；
Step 2, the vegetable-pickling waste water that step 1 of learning from else's experience processes, between pH 3.5-4.0 to 10-10.5, carry out pH regulator, adjust
The solid separated out is removed in time during joint；
Step 3, the vegetable-pickling waste water that step 2 of learning from else's experience processes, add antagonist, regulate pH to 6-7；
Step 4, takes cultured candidiasis, sprays the micro-water permeable membrane of heatproof at its outer surface, is added to afterwards through step 3
In the vegetable-pickling waste water processed, Aerobic Process for Treatment.
Use said structure, first, the pH of vegetable-pickling waste water be adjusted between 3.5-4.0 to 10-10.5,
Change the pH condition of vegetable-pickling waste water, in multiple pH condition, polymorphic type impurity is carried out precipitation process, reduce in waste water
Impurity content；Under different pH regulator, system is carried out recrystallization crystallize, the salinity in regulation waste water, makes in waste water
Salinity condition be applicable to candidiasis waste water process；
Secondly, having the micro-water permeable membrane of heatproof at candidiasis trypsin method, candidiasis progresses in waste water system by this film,
Candidiasis is selected the superior and eliminated the inferior in this process, can improve the disposal ability of candidiasis；This film is to candida mycoderma simultaneously
Bacterium plays the effect of protection, and in the waste water entrance film outside film, the candida mycoderma in rear tunicle quickly processes, and the water after process is to film
Neighbouring pickling waste water plays certain diluting effect, and the disposal ability of the candida mycoderma near raising film, carries further further
The treatment effect of high pickling waste water；
Research proves, the applicable salinity being processed vegetable-pickling waste water by the present processes is 0.5-10.0%, and its treatment effect
All effectively improve with efficiency.
More preferably: concretely comprising the following steps of described step 2: the vegetable-pickling waste water that step 1 of learning from else's experience processes, adjust
Joint pH to 3.5-4.0 stirring makes it separate out solid, is filtered to remove impurity；First gradually heighten the pH of vegetable-pickling waste water extremely
10-10.5, more gradually turn down the pH to 3.5-4.0 of vegetable-pickling waste water, by 0.5 governing speed regulation of pH/ time, and
After regulation pH, stirring makes it separate out solid every time, is filtered to remove impurity.
Use said structure, gradually regulate, the situation that the partial impurities that too fast regulation causes eliminates the most completely can be reduced,
Regulate between pH3.5-10.5 simultaneously, the microorganism survival of the fittest originally existed in vegetable-pickling waste water can be improved, make excellent
The microorganism of matter enters the waste water in later stage and processes, and improves its waste treatment capacity further；It was verified that when described regulation speed
When degree is 0.5 pH/ time, the waste treatment capacity in its later stage can obtain stability contorting, it is adaptable to big production application.
More preferably: in step 2, regulation pH adjusting agent used by pH is selected from K2CO3、KOH、Ca(HCO3)2、Ca(OH)2、HCl、H2CO3。
Using said structure, the impurity of introducing not only processes without interference with waste water, moreover it is possible to reduce Na+Suppression to microorganism
Effect.
More preferably: described antagonist is selected from K+、Ca2+、Fe3+、Fe2+、Mg2+、Al3+In at least one.
Use said structure, its energy and Na+Effect, reduces Na+Inhibitory action to microorganism；It uses these simultaneously
The antagonist of type, its energy and Cl-Effect, reduces salinity and reduces the salinity altercation impact on microbial treatments waste water.
More preferably: described candidiasis is selected from candidiasis G70.
Using said structure, its cellularity is unique, has wider pH growth scope and high organic composite tolerance,
It has corresponding salt tolerance.
More preferably: the micro-water permeable membrane of described heatproof includes polyethers, polyolefin copolymers and polyester acid copolymer；
And the micro-water permeable membrane of heatproof includes that the weight ratio of polyethers, polyolefin copolymers and polyester acid copolymer is 1: 5-10: 5-10.
Using said structure, triple combination acts on, and has preferable acid-fast alkali-proof temperature tolerance, and three entwines into tool simultaneously
There is more areolate micro-water permeable membrane, can supply water and the turnover of a small amount of candidiasis.
Research finds, the weight ratio of described candidiasis and the micro-water permeable membrane of heatproof is 1: 0.5-2, the micro-water permeable membrane pair of heatproof
Protection and the facilitation of candidiasis are most suitable.
More preferably: the micro-water permeable membrane of described heatproof also includes adhesive hybrid resin；And described polyethers and compound tree
The weight ratio of fat binding agent is 1: 0.1-0.5.
Using said structure, first, micro-for heatproof water permeable membrane and candidiasis are bonded together by adhesive hybrid resin,
Both annexations can be improved further；Secondly, the biological activity of candidiasis and the impact of diffusion velocity can be neglected by it
Slightly disregard；It addition, micro-permeable and candidiasis the effect of the micro-water permeable membrane of heatproof is not affected by.
More preferably: described spraying uses fluidized bed gas suspension method.
Use said structure, the micro-water permeable membrane of the heatproof outside candidiasis can be made evenly, it is ensured that the micro-water permeable membrane of heatproof
Protective effect.
In sum, the method have the advantages that
1. the processing method of a kind of vegetable-pickling waste water of the application of the application is less by the Effects of Salinity of vegetable-pickling waste water, is suitable for
In salinity at the vegetable-pickling waste water of 0.5-10.0%, its highly effective, it is adaptable to large-scale production；
2. utilizing the processing method of a kind of vegetable-pickling waste water of the application, run 30 days continuously, CODcr clearance reaches 54%,
Its Aerobic Process for Treatment time is short, and treatment effeciency is high.
Detailed description of the invention
This specific embodiment is only explanation of the invention, and it is not limitation of the present invention, people in the art
The present embodiment can be made after reading this specification by member as required does not has the amendment of creative contribution, but as long as at this
All protected by Patent Law in the right of invention.
Embodiment 1: candidiasis G70 separation screening
Embodiment 1 with reference to Publication No. CN101586084A separates candidiasis G70, and it concretely comprises the following steps:
Take Zhejiang Cixi hot pickled mustard tube factory Sewage outlet mud sample 2g, be placed in the filtered preserved szechuan pickle waste water of 50ml, add bead vibration
Break up, take supernatant 5ml and join in the filtered preserved szechuan pickle waste water of 50ml, temperature 30 DEG C, rotating speed 160rpm, shaking table
Enrichment culture 4 days；
Being coated with preserved szechuan pickle waste water culture medium flat plate after the preserved szechuan pickle waste water gradient dilution after the filtration of enrichment culture bacterium solution, sterilizing, 30 DEG C quiet
Put cultivation 4 days；According to the different single colony inoculation of colonial morphology picking in preserved szechuan pickle waste water to filtering, after sterilizing, temperature
30 DEG C, rotating speed 160rpm, shaking table is cultivated 48hr, is screened the bacterial strain that preserved szechuan pickle waste water can be made to alkalize；
Carrying out streak culture by the bacterial strain that preserved szechuan pickle waste water can be made to alkalize, obtain monoclonal, line still uses preserved szechuan pickle waste water culture medium flat plate；
Picking monoclonal is transferred in the preserved szechuan pickle waste water after filtration, sterilizing, temperature 30 DEG C, rotating speed 160rpm, and shaking table is cultivated；Treat
Bacterium solution grows to OD600During for 0.3-0.6, it is forwarded to equipped with 300ml filtration sterilization hot pickled mustard tube by the inoculum concentration of 2% (v/v)
In the conical flask of waste water, temperature 30 DEG C, rotating speed 160rpm, shaking table is cultivated 48hr, every 6hr and is taken sample mensuration bacterium solution pH
With COD (bacterium solution 6000rpm collects supernatant after being centrifuged 10min), screening obtains alkalize effect and COD removal effect
Best bacterial strain candida mycoderma G70.
The preserved szechuan pickle waste water pH 4.5 selected, salinity is 3.4% (in terms of NaCl), and solid medium adds 6% agar；Go out
Bacterium is adjusted to 120 DEG C, 0.1MPa and 30min.
Embodiment 2: candidiasis G70 cultivates
Embodiment 2 with reference to Publication No. CN101586084A cultivates candidiasis G70, and it concretely comprises the following steps:
The candidiasis G70 of the embodiment 1 after activation is forwarded to Fructus Hordei Germinatus by the inoculum concentration of 2% (v/v) and leaches powder culture medium
(dried malt leach powder 0.3%, cerevisin 0.3%), temperature 30 DEG C, rotating speed 160rpm, shaking table cultivate, 12 hours
I.e. to exponential phase.
The relevant information statistics of bacterial strain involved by table 1 the application
| Bacterial strain name | Public strain storehouse preserving number |
| Candida thaimueangensis | CGMCC No.3000 |
Embodiment 3-7: the processing method of a kind of vegetable-pickling waste water, comprises the steps:
Step 1, takes vegetable-pickling waste water, the float being filtered to remove in vegetable-pickling waste water；
Step 2, the vegetable-pickling waste water that step 1 of learning from else's experience processes, make it separate out with pH adjusting agent regulation pH to 3.5-4.0 stirring
Solid, is filtered to remove impurity；First gradually heighten the pH to 10-10.5 of vegetable-pickling waste water, more gradually turn down vegetable-pickling
The pH to 3.5-4.0 of waste water, governing speed is 0.5 pH/ time, and after each regulation pH, stirring makes it separate out solid,
It is filtered to remove impurity；
Step 3, the vegetable-pickling waste water that step 2 of learning from else's experience processes, add antagonist, regulate pH to 6-7 by pH adjusting agent；
Step 4, takes cultured candidiasis G70, uses fluidized bed gas suspension method organic on its outer surface sprays successively
Polymer binder and the micro-water permeable membrane of heatproof, added in the vegetable-pickling waste water that step 3 processes, Aerobic Process for Treatment afterwards；
Wherein the micro-water permeable membrane of heatproof includes polyethers, polyolefin copolymers and polyester acid copolymer；
The raw material information that embodiment 3-7 uses is as shown in table 2-3；
Water quality before and after processing embodiment 3-7 and the Aerobic Process for Treatment time in step 4 are monitored, and its result is as shown in table 3.
The raw material information used in table 2 embodiment 3-7
In table 3 embodiment 3-7 raw material consumption information and process Information Statistics
Running 30 days continuously, CODcr clearance reaches more than 54%.
Claims (9)
1. the processing method of a vegetable-pickling waste water, it is characterised in that comprise the steps:
Step 1, takes vegetable-pickling waste water, the float being filtered to remove in vegetable-pickling waste water；
Step 2, the vegetable-pickling waste water that step 1 of learning from else's experience processes, between pH 3.5-4.0 to 10-10.5, carry out pH regulator, during regulation, remove the solid separated out in time；
Step 3, the vegetable-pickling waste water that step 2 of learning from else's experience processes, add antagonist, regulate pH to 6-7；
Step 4, takes cultured candidiasis, sprays the micro-water permeable membrane of heatproof at its outer surface, is added to afterwards in the vegetable-pickling waste water that step 3 processes, Aerobic Process for Treatment.
The processing method of a kind of vegetable-pickling waste water the most according to claim 1, it is characterised in that concretely comprising the following steps of described step 2: the vegetable-pickling waste water that step 1 of learning from else's experience processes, regulation pH to 3.5-4.0 stirring makes it separate out solid, is filtered to remove impurity；First gradually heighten the pH to 10-10.5 of vegetable-pickling waste water, more gradually turn down the pH to 3.5-4.0 of vegetable-pickling waste water, by 0.5 governing speed regulation of pH/ time, and stir after regulation pH every time and make it separate out solid, be filtered to remove impurity.
The processing method of a kind of vegetable-pickling waste water the most according to claim 1, it is characterised in that in step 2, regulation pH adjusting agent used by pH is selected from K2CO3, KOH, Ca(HCO3)2, Ca(OH)2、HCl、H2CO3。
The processing method of a kind of vegetable-pickling waste water the most according to claim 1, it is characterised in that described antagonist is selected from K+、Ca2+、Fe3+、Fe2+、Mg2+、Al3+In at least one.
The processing method of a kind of vegetable-pickling waste water the most according to claim 1, it is characterised in that described candidiasis is selected from candidiasis G70.
The processing method of a kind of vegetable-pickling waste water the most according to claim 1, it is characterised in that the micro-water permeable membrane of described heatproof includes polyethers, polyolefin copolymers and polyester acid copolymer；And the micro-water permeable membrane of heatproof includes that the weight ratio of polyethers, polyolefin copolymers and polyester acid copolymer is 1:5-10:5-10.
The processing method of a kind of vegetable-pickling waste water the most according to claim 1, it is characterised in that the weight ratio of described candidiasis and the micro-water permeable membrane of heatproof is 1:0.5-2.
The processing method of a kind of vegetable-pickling waste water the most according to claim 6, it is characterised in that the micro-water permeable membrane of described heatproof also includes adhesive hybrid resin；And the weight ratio of described polyethers and adhesive hybrid resin is 1:0.1-0.5.
The processing method of a kind of vegetable-pickling waste water the most according to claim 1, it is characterised in that described spraying uses fluidized bed gas suspension method.
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Citations (5)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN101475909A (en) * | 2009-01-22 | 2009-07-08 | 房华江 | Method for cultivating halophilic bacteria and method for treating salting wastewater by using halophilic bacteria cultivated thereby |
| CN101481184A (en) * | 2009-02-10 | 2009-07-15 | 杭州水处理技术研究开发中心有限公司 | Novel membrane processing and salt recycling method for hot pickled mustard tube cleaning wastewater |
| CN101586084A (en) * | 2009-05-14 | 2009-11-25 | 浙江大学 | Yeast and application thereof in the weak alkaline treatment of vegetable-pickling waste water |
| CN102849857A (en) * | 2012-04-10 | 2013-01-02 | 南京大学 | Method for treating high-salinity high-concentration ammonia-nitrogen wastewater |
| CN105152356A (en) * | 2015-08-27 | 2015-12-16 | 武汉沃田生态科技有限公司 | Microcapsule complex microbial inoculant and preparation method thereof |
-
2016
- 2016-05-12 CN CN201610312796.3A patent/CN105776774B/en active Active
Patent Citations (5)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN101475909A (en) * | 2009-01-22 | 2009-07-08 | 房华江 | Method for cultivating halophilic bacteria and method for treating salting wastewater by using halophilic bacteria cultivated thereby |
| CN101481184A (en) * | 2009-02-10 | 2009-07-15 | 杭州水处理技术研究开发中心有限公司 | Novel membrane processing and salt recycling method for hot pickled mustard tube cleaning wastewater |
| CN101586084A (en) * | 2009-05-14 | 2009-11-25 | 浙江大学 | Yeast and application thereof in the weak alkaline treatment of vegetable-pickling waste water |
| CN102849857A (en) * | 2012-04-10 | 2013-01-02 | 南京大学 | Method for treating high-salinity high-concentration ammonia-nitrogen wastewater |
| CN105152356A (en) * | 2015-08-27 | 2015-12-16 | 武汉沃田生态科技有限公司 | Microcapsule complex microbial inoculant and preparation method thereof |
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