CN105769607A - Solid shower film capable of being cut for use and preparing method thereof - Google Patents

Solid shower film capable of being cut for use and preparing method thereof Download PDF

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Publication number
CN105769607A
CN105769607A CN201610218837.2A CN201610218837A CN105769607A CN 105769607 A CN105769607 A CN 105769607A CN 201610218837 A CN201610218837 A CN 201610218837A CN 105769607 A CN105769607 A CN 105769607A
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China
Prior art keywords
weight portion
thin film
deionized water
solid
solution
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CN201610218837.2A
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Chinese (zh)
Inventor
李立
张海琳
刘晋良
雷桥
张亚琼
文艺桦
黄敏莹
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Shanghai Maritime University
Shanghai Ocean University
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Shanghai Maritime University
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Priority to CN201610218837.2A priority Critical patent/CN105769607A/en
Publication of CN105769607A publication Critical patent/CN105769607A/en
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    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00Cosmetics or similar toiletry preparations
    • A61K8/18Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/72Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds
    • A61K8/81Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds obtained by reactions involving only carbon-to-carbon unsaturated bonds
    • A61K8/8129Compositions of homopolymers or copolymers of compounds having one or more unsaturated aliphatic radicals, each having only one carbon-to-carbon double bond, and at least one being terminated by an alcohol, ether, aldehydo, ketonic, acetal or ketal radical; Compositions of hydrolysed polymers or esters of unsaturated alcohols with saturated carboxylic acids; Compositions of derivatives of such polymers, e.g. polyvinylmethylether
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00Cosmetics or similar toiletry preparations
    • A61K8/02Cosmetics or similar toiletry preparations characterised by special physical form
    • A61K8/0204Specific forms not provided for by any of groups A61K8/0208 - A61K8/14
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00Cosmetics or similar toiletry preparations
    • A61K8/18Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/30Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
    • A61K8/33Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing oxygen
    • A61K8/34Alcohols
    • A61K8/345Alcohols containing more than one hydroxy group
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00Cosmetics or similar toiletry preparations
    • A61K8/18Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/30Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
    • A61K8/40Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing nitrogen
    • A61K8/44Aminocarboxylic acids or derivatives thereof, e.g. aminocarboxylic acids containing sulfur; Salts; Esters or N-acylated derivatives thereof
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00Cosmetics or similar toiletry preparations
    • A61K8/18Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/30Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
    • A61K8/40Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing nitrogen
    • A61K8/44Aminocarboxylic acids or derivatives thereof, e.g. aminocarboxylic acids containing sulfur; Salts; Esters or N-acylated derivatives thereof
    • A61K8/442Aminocarboxylic acids or derivatives thereof, e.g. aminocarboxylic acids containing sulfur; Salts; Esters or N-acylated derivatives thereof substituted by amido group(s)
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00Cosmetics or similar toiletry preparations
    • A61K8/18Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/30Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
    • A61K8/64Proteins; Peptides; Derivatives or degradation products thereof
    • A61K8/65Collagen; Gelatin; Keratin; Derivatives or degradation products thereof
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00Cosmetics or similar toiletry preparations
    • A61K8/18Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/30Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
    • A61K8/67Vitamins
    • A61K8/678Tocopherol, i.e. vitamin E
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61QSPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
    • A61Q19/00Preparations for care of the skin
    • A61Q19/10Washing or bathing preparations
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K2800/00Properties of cosmetic compositions or active ingredients thereof or formulation aids used therein and process related aspects
    • A61K2800/40Chemical, physico-chemical or functional or structural properties of particular ingredients
    • A61K2800/48Thickener, Thickening system
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K2800/00Properties of cosmetic compositions or active ingredients thereof or formulation aids used therein and process related aspects
    • A61K2800/40Chemical, physico-chemical or functional or structural properties of particular ingredients
    • A61K2800/52Stabilizers
    • A61K2800/522Antioxidants; Radical scavengers

Abstract

A solid shower film capable of being cut for use is characterized by being prepared from PVA colloid and a shower solution which are prepared by the ratio of 4:1, the colloid is made of PVA, glycerinum and deionized water by the weight ratio of 10:1:89, and the shower solution is prepared from, by weight, 15-25 parts of green surfactant, 5-10 parts of a skin care agent, 1-2 parts of a thickening agent, 0.5-1 part of pH modifier, 0.05-0.1 part of flavoring agent, 0.05-0.1 part of antioxidant and 60-70 parts of deionized water.

Description

A kind of solid, shaped shower thin film cutting out use and preparation method
Technical field
The invention belongs to the raw material plastifying technology field of daily use chemicals product, be specifically related to a kind of solid, shaped cutting out use and wash one's hair Bath thin film and preparation method.
Background technology
Along with the development of global economic integration, people often arrive other places and go on business, travel, then in firmly hotel, hotel During, owing to there are some defects in the traditional soap of blocks of solid shape, fancy soap, seldom by people when carrying and use Use.In order to solve the needs that people take a shower during the journey, many hotels and hotel provide the liquid bath article that some are bottled. For the liquid bath article that these are bottled, the most often there are some misgivings in guests.Such as: these bath product are No being produced by regular businessman, whether composition material therein is applicable to autologous skin?Additionally, also can take into account these pressing types How long bath gel is contained in container actually, if also in effective life?For using these bottled washing to wash one's hair use There is also for the businessman of product and cannot be used up and the very problem such as waste.In view of in recent years, the health problem in daily life is Become society and compare a big focus of concern.
Therefore, on the one hand the bath foam used in existing hotel, hotel must be strengthened the management in terms of safe and sanitary. The most how to provide a kind of easy to carry, Novel bath goods of use safety to consumer.Obviously this consumer just The new problem that daily use chemicals production firm is proposed.
Summary of the invention
The purpose of the present invention: aim to provide a kind of solid, shaped shower thin film cutting out use and the preparation side of this thin film thereof Method.
The present invention is achieved by the following technical programs:
This solid, shaped shower thin film cutting out use, it is characterised in that: it is by PVA colloid substances and body wash solution group Become;Wherein said PVA colloid substances and body wash solution press the proportions of 4:1;Described colloid substances by PVA, glycerol and go from Sub-water forms, and by PVA: glycerol: deionized water is the weight preparation of 10:1:89;Described bath foam is by green table Face activating agent, skin protectant, thickening agent, PH regulator, deodorant tune, antioxidant and deionized water composition;Described body wash solution By surfactant 15-25 weight portion, skin protectant 5-10 weight portion, thickening agent 1-2 weight portion, pH adjusting agent 0.5-1 weight portion, Deodorant tune 0.05-0.1 weight portion, antioxidant 0.05-0.1 weight portion, deionized water 60-70 weight portion are prepared.
Described green surfactant is by polyoxyethylenated alcohol sodium sulfate, cocamido propyl betaine and 12 One in alkyl betaine or two or more compounds composition.
Described skin protectant is made up of the one in propylene glycol, glycerol or both compounds.
Described natural thickener is made up of the one in pectin or gelatin or both compounds.
Described pH adjusting agent is made up of the one in EDETATE SODIUM or sodium citrate or both compounds.
Described deodorant tune is essence.
Described antioxidant is vitamin E.
This solid, shaped shower thin film cutting out use, its preparation method is as follows:
One, PVA colloid solution and body wash solution are prepared respectively;
1) with PVA, glycerol and deionized water as raw material, and by PVA: glycerol: deionized water is that the weight portion of 10:1:89 is joined The colloid solution more standby than being configured to;
2) with the green surfactant chosen, skin protectant, thickening agent, PH regulator, deodorant tune, antioxidant with go Ion is raw material, by surfactant 15-25 weight portion, skin protectant 5-10 weight portion, thickening agent 1-2 weight portion, pH adjusting agent 0.5-1 weight portion, deodorant tune 0.05-0.1 weight portion, antioxidant 0.05-0.1 weight portion, deionized water 60-70 weight portion are joined Make the body wash solution of use;Sealing, stored in containers is standby;
Two, shower thin film is made by solution curtain coating
1) ratio that 25mL body wash solution mixed by every 100mLPVA colloid solution is weighed quantitative colloid solution and takes a shower molten Liquid, and the two is stirred, is sufficiently mixed, it is thus achieved that masking mixed solution;
2) mixed solution spread upon on the pallet of drying baker, put into drying baker, under 70 DEG C of constant temperatures, dry film forming, Water solublity bath gel washing film primary products;
3) the processed machining of thin film after drying is cut into inch strips, block packaging, or is rolled into tubular, can become to be available for city The water solublity bath gel washing film commodity that field flow is logical.
The compound method of described bath foam is:
1) by glycerol, propylene glycol and 70 80 DEG C, 20% 50% deionized water mixing of formula ratio;
2) green surfactant is added in step 1: polyoxyethylenated alcohol sodium sulfate, cocamidopropyl propyl amide Radix Betae One or more compound in alkali or empgen BB, adds remaining deionized water, is heated to temperature Being to stir 10 20min when 70 80 DEG C, temperature controls at 70 80 DEG C;
3) in the mixed solution of step 2, quantitative pectin and gelatin it are slowly added into, heated and stirred 10 30min, temperature control System is at 70 80 DEG C;
4) in the mixed solution that step 3 obtains, EDETATE SODIUM, sodium citrate, essence and vitamin E are added, 40 50 Heated and stirred 10 30min under DEG C temperature conditions, i.e. obtains required masking bath foam.
This solid, shaped shower thin film cutting out use proposed according to above technical scheme, can not only substitute at present The aqueous body wash solution commonly used, and automatically degrade after in use can meeting water due to the thin film with PVA as base material, no Any residue can be left.The most this solid, shaped shower thin film cutting out use, can cut according to the needs of user Cut out, do not result in waste, and carry also extremely convenient.
Detailed description of the invention
The present invention set forth further below, and provide embodiments of the invention.
This solid, shaped shower thin film cutting out use, it is characterised in that: it is by PVA colloid substances and body wash solution group Become;Wherein said PVA colloid substances and body wash solution press the proportions of 4:1;Described colloid substances is by by PVA, glycerol with go Ionized water forms, and by PVA: glycerol: deionized water is the weight preparation of 10:1:89;Described bath foam is by green Surfactant, skin protectant, thickening agent, PH regulator, deodorant tune, antioxidant and deionized water composition;Described shower is molten Liquid presses surfactant 15-25 weight portion, skin protectant 5-10 weight portion, thickening agent 1-2 weight portion, pH adjusting agent 0.5-1 weight Part, the preparation of deodorant tune 0.05-0.1 weight portion, antioxidant 0.05-0.1 weight portion, deionized water 60-70 weight portion.
The present invention why select PVA as make shower thin film colloidal materials, except in view of PVA (polyvinyl alcohol) A kind of macromolecule organic, white, tasteless, have that synthesis convenience, safety and low toxicity, product quality be easily controllable, low price, Outside the feature such as easy to use, it is often more important that this material water soluble, is a kind of conventional safety film former, the most not Environmental pollution can be caused.
Described green surfactant is by polyoxyethylenated alcohol sodium sulfate, cocamido propyl betaine and 12 One or more kinds of compounds composition in alkyl betaine.
Empgen BB, polyoxyethylenated alcohol sodium sulfate, cocamido propyl betaine belong to green surface and live Property agent, its each effect respectively as follows:
Empgen BB: there is excellent stain removal bactericidal, flexibility, antistatic behaviour, stability in hard water and rust-preventing characteristic, energy With various surfactants and cosmetic material compatibility, belong to zwitterionic surfactant, to skin low irritant, be and effectively Suds booster and foam stability, abundant and stable foam can be produced in body wash solution.
Polyoxyethylenated alcohol sodium sulfate: there is excellent decontamination, emulsifying, foam performance and hard water resistance performance, be not subject to The impact of the water hardness, bubbles rapidly, washing character gentle and will not injured skin, be the former of the most excellent articles for washing Material.
Cocamido propyl betaine: be a kind of zwitterionic surfactant, normal and anions and canons and non-ionic surface Activating agent use, its compatibility is good.Zest is little, soluble in water, to ph stability, strong detergency, has good rising Bubble effect, foam is fine and smooth and stable, meanwhile, has excellent thickening property, flexibility, bactericidal properties, antistatic behaviour, hard water resistance property, Performance is gentle, can significantly improve the washing softness of series products, conditioning and low-temperature stability.
Described skin protectant is made up of the one in propylene glycol, glycerol or both compounds.
Propylene glycol and glycerol belong to skin protectant, its each effect as follows:
Propylene glycol: propylene glycol can adsorb at skin surface in bathing experience, it is not easy to washes away with water.Surface moisture volatilizees Just stay layer protecting film to cover on skin later, can effectively stop or slow down the loss of internal moisture, keep the wet of skin Profit.
Glycerol: i.e. glycerol, is most common wetting agent, and moistening effect is good, can effectively prevent chapped skin.Glycerol has Water absorption, can absorb the moisture content in air thus to skin moisture-keeping, simultaneously prevented also from the moisture loss in skin.
Described natural thickener is made up of the one in pectin or gelatin or both compounds.
Pectin and gelatin belong to natural thickener, its each effect as follows:
Pectin: pectin platymiscium polysaccharide material, can form the resilient gel of tool, increase liquid viscosity.
Gelatin: gelatin is the mixture of victory peptide and collagenic protein partial hydrolysis, and effect is similar with pectin.
Described pH adjusting agent is made up of the one in EDETATE SODIUM or sodium citrate or both compounds.
EDETATE SODIUM and sodium citrate belong to PH regulator, its each effect as follows:
EDETATE SODIUM: be a kind of chelating agen, can effectively regulate the pH value of bath gel product, maintains skin acid balance, fall Other the chemical substances low zest to skin.
Sodium citrate: be a kind of organic compound, belong to weak acid strong alkali salt, there is good pH regulator and shock-absorbing capacity, energy Effectively regulate the pH value of bath gel product, maintain skin acid balance, reduce other chemical substances zest to skin.
Described deodorant tune is essence.
Essence is a kind of is imitated fruit and the concentration aromatic oil of natural perfume material abnormal smells from the patient by synthetic, adds bath gel product In in order to improve the abnormal smells from the patient of product.
Described antioxidant is vitamin E.
Vitamin E belongs to antioxidant, is a kind of fatsoluble vitamin, and its hydrolyzate is tocopherol, is topmost antioxygen One of agent, can keep skin health state with anti-oxidation protection body cell from the murder by poisoning of free radical.
This solid, shaped shower thin film cutting out use, its preparation method is as follows:
One, PVA colloid solution and body wash solution are prepared respectively;
1) with PVA, glycerol and deionized water raw material, and it is molten to be configured to standby colloid by the weight of 10:1:89 Liquid;
2) with the green surfactant chosen, skin protectant, thickening agent, PH regulator, deodorant tune, antioxidant with go Ion is raw material, by surfactant 15-25 weight portion, skin protectant 5-10 weight portion, thickening agent 1-2 weight portion, pH adjusting agent 0.5-1 weight portion, deodorant tune 0.05-0.1 weight portion, antioxidant 0.05-0.1 weight portion, deionized water 60-70 weight portion are joined Make the body wash solution of use;Sealing, stored in containers is standby;
Two, shower thin film is made by solution curtain coating
1) ratio that 25mL body wash solution mixed by every 100mLPVA colloid solution is weighed quantitative colloid solution and takes a shower molten Liquid, and the two is stirred, is sufficiently mixed, it is thus achieved that masking mixed solution;
2) mixed solution spread upon on the pallet of drying baker, put into drying baker, under 70 DEG C of constant temperatures, dry film forming, Water solublity bath gel washing film primary products;
3) the processed machining of thin film after drying, cuts into inch strips, block packaging, or is rolled into tubular, can become to be available for The water solublity bath gel washing film commodity of market circulation.
The compound method of described bath foam is:
1) by glycerol, propylene glycol and 70 80 DEG C, 20% 50% deionized water mixing of formula ratio;
2) green surfactant is added in step 1: polyoxyethylenated alcohol sodium sulfate, cocamidopropyl propyl amide Radix Betae One or more compound in alkali or empgen BB, adds remaining deionized water, is heated to temperature Being to stir 10 20min when 70 80 DEG C, temperature controls at 70 80 DEG C;
3) in the mixed solution of step 2, quantitative pectin and gelatin it are slowly added into, heated and stirred 10 30min, temperature control System is at 70 80 DEG C;
4) in the mixed solution that step 3 obtains, EDETATE SODIUM, sodium citrate, essence and vitamin E are added, 40 50 Heated and stirred 10 30min under DEG C temperature conditions, i.e. obtains required masking bath foam.
Embodiment 1
PVA 10 weight portion;
Glycerol 1 weight portion;
Deionized water 89 weight portion;
PVA colloid solution 100 weight portion is prepared according to said ratio.
Sealing, stored in containers is standby.
1) by glycerol, propylene glycol and 70 80 DEG C, 20% 50% deionized water mixing of formula ratio;
2) green surfactant is added in step 1: polyoxyethylenated alcohol sodium sulfate, cocamidopropyl propyl amide Radix Betae One in alkali or empgen BB or more than one compound, add remaining deionized water, be heated to temperature Being to stir 10 20min when 70 80 DEG C, temperature controls at 70 80 DEG C;
3) in the mixed solution of step 2, quantitative pectin and gelatin it are slowly added into, heated and stirred 10 30min, temperature control System is at 70 80 DEG C;
4) in the mixed solution that step 3 obtains, EDETATE SODIUM, sodium citrate, essence and Wei Sheng are added
Element E, heated and stirred 10 30min under 40 50 DEG C of temperature conditionss, i.e. obtain required masking bath foam;And Sealing stored in containers is standby.
Embodiment 2
PVA 10 weight portion;
Glycerol 1 weight portion;
Deionized water 89 weight portion;
PVA colloid solution 100 weight portion is prepared according to said ratio.
The green surfactant that chooses with above-mentioned, skin protectant, thickening agent, PH regulator, deodorant tune, antioxidant and Deionization is the body wash solution that parts by weight of raw materials is configured to use;Sealing, stored in containers is standby.
1) by glycerol, propylene glycol and 70 80 DEG C, 20% 50% deionized water mixing of formula ratio;
2) green surfactant is added in step 1: polyoxyethylenated alcohol sodium sulfate, cocamidopropyl propyl amide Radix Betae A kind of or a kind of, above compound in alkali or empgen BB, adds remaining deionized water, is heated to temperature Being to stir 10 20min when 70 80 DEG C, temperature controls at 70 80 DEG C;
3) in the mixed solution of step 2, quantitative pectin and gelatin it are slowly added into, heated and stirred 10 30min, temperature control System is at 70 80 DEG C;
4) in the mixed solution that step 3 obtains, EDETATE SODIUM, sodium citrate, essence and vitamin E are added, 40 50 Heated and stirred 10 30min under DEG C temperature conditions, i.e. obtains required masking bath foam;And it is standby sealing stored in containers.
Embodiment 3
PVA 10 weight portion;
Glycerol 1 weight portion;
Deionized water 89 weight portion;
PVA colloid solution 100 weight portion is prepared according to said ratio.
The green surfactant that chooses with above-mentioned, skin protectant, thickening agent, PH regulator, deodorant tune, antioxidant and Deionization is the body wash solution that parts by weight of raw materials is configured to use;Sealing, stored in containers is standby.
1) by glycerol, propylene glycol and 70 80 DEG C, 20% 50% deionized water mixing of formula ratio;
2) green surfactant is added in step 1: polyoxyethylenated alcohol sodium sulfate, cocamidopropyl propyl amide Radix Betae One in alkali or empgen BB or more than one compound, add remaining deionized water, be heated to temperature Being to stir 10 20min when 70 80 DEG C, temperature controls at 70 80 DEG C;
3) in the mixed solution of step 2, quantitative pectin and gelatin it are slowly added into, heated and stirred 10 30min, temperature control System is at 70 80 DEG C;
4) in the mixed solution that step 3 obtains, EDETATE SODIUM, sodium citrate, essence and vitamin E are added, 40 50 Heated and stirred 10 30min under DEG C temperature conditions, i.e. obtains required masking bath foam;And it is standby sealing stored in containers.
Embodiment 4
PVA 10 weight portion;
Glycerol 1 weight portion;
Deionized water 89 weight portion;
PVA colloid solution 100 weight portion is prepared according to said ratio.
The green surfactant that chooses with above-mentioned, skin protectant, thickening agent, PH regulator, deodorant tune, antioxidant and Deionization is the body wash solution that parts by weight of raw materials is configured to use;Sealing, stored in containers is standby.
1) by glycerol, propylene glycol and 70 80 DEG C, 20% 50% deionized water mixing of formula ratio;
2) green surfactant is added in step 1: polyoxyethylenated alcohol sodium sulfate, cocamidopropyl propyl amide Radix Betae One or more compound in alkali or empgen BB, adds remaining deionized water, is heated to temperature Being to stir 10 20min when 70 80 DEG C, temperature controls at 70 80 DEG C;
3) in the mixed solution of step 2, quantitative pectin and gelatin it are slowly added into, heated and stirred 10 30min, temperature control System is at 70 80 DEG C;
4) in the mixed solution that step 3 obtains, EDETATE SODIUM, sodium citrate, essence and vitamin E are added, 40 50 Heated and stirred 10 30min under DEG C temperature conditions, i.e. obtains required masking bath foam;And it is standby sealing stored in containers.
Embodiment 5
PVA 10 weight portion;
Glycerol 1 weight portion;
Deionized water 89 weight portion;
PVA colloid solution 100 weight portion is prepared according to said ratio.
The green surfactant that chooses with above-mentioned, skin protectant, thickening agent, PH regulator, deodorant tune, antioxidant and Deionization is the body wash solution that parts by weight of raw materials is configured to use;Sealing, stored in containers is standby.
1) by glycerol, propylene glycol and 70 80 DEG C, 20% 50% deionized water mixing of formula ratio;
2) green surfactant is added in step 1: polyoxyethylenated alcohol sodium sulfate, cocamidopropyl propyl amide Radix Betae One or more compound in alkali or empgen BB, adds remaining deionized water, is heated to temperature Being to stir 10 20min when 70 80 DEG C, temperature controls at 70 80 DEG C;
3) in the mixed solution of step 2, quantitative pectin and gelatin it are slowly added into, heated and stirred 10 30min, temperature control System is at 70 80 DEG C;
4) in the mixed solution that step 3 obtains, EDETATE SODIUM, sodium citrate, essence and vitamin E are added, 40 50 Heated and stirred 10 30min under DEG C temperature conditions, i.e. obtains required masking bath foam;And it is standby sealing stored in containers.
Embodiment 6
PVA 10 weight portion;
Glycerol 1 weight portion;
Deionized water 89 weight portion;
PVA colloid solution 100 weight portion is prepared according to said ratio.
The green surfactant that chooses with above-mentioned, skin protectant, thickening agent, PH regulator, deodorant tune, antioxidant and Deionization is the body wash solution that parts by weight of raw materials is configured to use;Sealing, stored in containers is standby.
1) by glycerol, propylene glycol and 70 80 DEG C, 20% 50% deionized water mixing of formula ratio;
2) green surfactant is added in step 1: polyoxyethylenated alcohol sodium sulfate, cocamidopropyl propyl amide Radix Betae One or more compound in alkali or empgen BB, adds remaining deionized water, is heated to temperature Being to stir 10 20min when 70 80 DEG C, temperature controls at 70 80 DEG C;
3) in the mixed solution of step 2, quantitative pectin and gelatin it are slowly added into, heated and stirred 10 30min, temperature control System is at 70 80 DEG C;
4) in the mixed solution that step 3 obtains, EDETATE SODIUM, sodium citrate, essence and Wei Sheng are added
Element E, heated and stirred 10 30min under 40 50 DEG C of temperature conditionss, i.e. obtain required masking bath foam;And Sealing stored in containers is standby.
Embodiment 7
PVA 10 weight portion;
Glycerol 1 weight portion;
Deionized water 89 weight portion;
PVA colloid solution 100 weight portion is prepared according to said ratio.
The green surfactant that chooses with above-mentioned, skin protectant, thickening agent, PH regulator, deodorant tune, antioxidant and Deionization is the body wash solution that parts by weight of raw materials is configured to use;Sealing, stored in containers is standby.
1) by glycerol, propylene glycol and 70 80 DEG C, 20% 50% deionized water mixing of formula ratio;
2) in step 1) in add green surfactant: polyoxyethylenated alcohol sodium sulfate, cocamidopropyl propyl amide are sweet One in dish alkali or empgen BB or more than one compound, add remaining deionized water, be heated to temperature Degree is to stir 10 20min when 70 80 DEG C, and temperature controls at 70 80 DEG C;
3) in step 2) mixed solution in be slowly added into quantitative pectin and gelatin, heated and stirred 10 30min, temperature Control at 70 80 DEG C;
4) in step 3) mixed solution that obtains adds EDETATE SODIUM, sodium citrate, essence and vitamin E, 40 50 Heated and stirred 10 30min under DEG C temperature conditions, i.e. obtains required masking bath foam;And it is standby sealing stored in containers.
Show through experimental use: according to this solid, shaped shower thin film cutting out use of above fabrication techniques, no Only there is the washing function identical with existing frequently-used liquid type bath foam, easy to carry, and owing to PVA has degraded automatically Function, thus without the problem such as sewer pipe and waste that results in blockage.
Be only more than the applicant according to substantially creating the embodiment provided, any according to this intention make without essence Property intention improvement, be regarded as thinking with the technical program similar, belong to the category of present invention protection.

Claims (9)

1. the solid, shaped shower thin film that can cut out use, it is characterised in that: it is made up of PVA colloid substances and body wash solution; Wherein said PVA colloid substances and body wash solution press the proportions of 4:1;Described colloid substances is by by PVA, glycerol and deionization Water forms, and presses the weight preparation of 10:1:89;Described bath foam is by green surfactant, skin protectant, thickening Agent, PH regulator, deodorant tune, antioxidant and deionized water composition;Described body wash solution presses surfactant 15-25 weight Part, skin protectant 5-10 weight portion, thickening agent 1-2 weight portion, pH adjusting agent 0.5-1 weight portion, deodorant tune 0.05-0.1 weight portion, Antioxidant 0.05-0.1 weight portion, deionized water 60-70 weight portion are prepared.
A kind of solid, shaped shower thin film cutting out use, it is characterised in that: described green table Face activating agent by the one in polyoxyethylenated alcohol sodium sulfate, cocamido propyl betaine and empgen BB or The compound composition that person is two or more.
A kind of solid, shaped shower thin film cutting out use, it is characterised in that: described skin protectant It is made up of a kind of in propylene glycol, glycerol or both compounds.
A kind of solid, shaped shower thin film cutting out use, it is characterised in that: described natural increasing Thick dose is made up of a kind of in pectin or gelatin or both compounds.
A kind of solid, shaped shower thin film cutting out use, it is characterised in that: described pH regulator Agent is made up of a kind of in EDETATE SODIUM or sodium citrate or both compounds.
A kind of solid, shaped shower thin film cutting out use, it is characterised in that: described deodorant tune For essence.
A kind of solid, shaped shower thin film cutting out use, it is characterised in that: described antioxidation Agent is vitamin E.
A kind of solid, shaped shower thin film cutting out use, its preparation method is as follows:
One, PVA colloid solution and body wash solution are prepared respectively;
1) with PVA, glycerol and deionized water raw material, and it is configured to standby colloid solution by the weight of 10:1:89;
2) with the green surfactant chosen, skin protectant, thickening agent, PH regulator, deodorant tune, antioxidant and deionization For raw material, by surfactant 15-25 weight portion, skin protectant 5-10 weight portion, thickening agent 1-2 weight portion, pH adjusting agent 0.5-1 Weight portion, deodorant tune 0.05-0.1 weight portion, antioxidant 0.05-0.1 weight portion, deionized water 60-70 weight portion are configured to The body wash solution used;Sealing, stored in containers is standby;
Two, shower thin film is made by solution curtain coating
1) ratio that 25mL body wash solution mixed by every 100mLPVA colloid solution is weighed quantitative colloid solution and body wash solution, and The two is stirred, is sufficiently mixed, it is thus achieved that masking mixed solution;
2) mixed solution is spread upon on the pallet of drying baker, put into drying baker, under 70 DEG C of constant temperatures, dry film forming, Water solublity bath gel washing film primary products;
3) the processed machinery of thin film after drying carries out cutting into inch strips, block packaging, or is rolled into tubular, can become to be available for city's field flow Logical water solublity bath gel washing film commodity.
A kind of preparation method of the solid, shaped shower thin film cutting out use, it is characterised in that: institute The compound method stating bath foam is:
1) by glycerol, propylene glycol and 70 80 DEG C, 20% 50% deionized water mixing of formula ratio;
2) add green surfactant in step 1: polyoxyethylenated alcohol sodium sulfate, cocamido propyl betaine or One in empgen BB or more than one compound, add remaining deionized water, is heated to temperature and is Stirring 10 20min when 70 80 DEG C, temperature controls at 70 80 DEG C;
3) being slowly added into quantitative pectin and gelatin in the mixed solution of step 2, heated and stirred 10 30min, temperature controls 70‐80℃;
4) in the mixed solution that step 3 obtains, EDETATE SODIUM, sodium citrate, essence and vitamin E are added, 40 50 DEG C of temperature Heated and stirred 10 30min under the conditions of degree, i.e. obtains required masking bath foam.
CN201610218837.2A 2016-04-11 2016-04-11 Solid shower film capable of being cut for use and preparing method thereof Pending CN105769607A (en)

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CN1268558A (en) * 1999-03-24 2000-10-04 尹小林 Multifunctional disposable cleaning film
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CN1268558A (en) * 1999-03-24 2000-10-04 尹小林 Multifunctional disposable cleaning film
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Application publication date: 20160720