CN105767971A - Method for accelerating ageing of pericarpium citri reticulatae - Google Patents
Method for accelerating ageing of pericarpium citri reticulatae Download PDFInfo
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Abstract
The invention discloses a method for accelerating ageing of pericarpium citri reticulatae.According to the method, orange peels washed clean are dried to a little moisture, the dried orange peels are placed in a high-temperature and high-humidity environment to be treated for some time, the orange peels are then placed in a low-temperature and low humidity environment to be treated for some time, and high-temperature and high-humidity treatment and low-temperature and low-humidity treatment are carried out alternately and repeatedly.The method overcomes the defects that in the prior art, the ageing process of pericarpium citri reticulatae is long, and the product quality is not stable.By means of the method, rapid ageing of pericarpium citri reticulatae by manual work is achieved, and physical methods are mainly used for promoting chemical reactions of effective substances in orange peels; in a short time, the ageing quality reaches that of natural ageing for 3-5 years, no additives are added, and the product quality is safe.
Description
Technical field
The present invention relates to the processing technique field of Pericarpium Citri Reticulatae, particularly relate to a kind of method accelerating Pericarpium Citri Reticulatae ageing.
Background technology
Pericarpium Citri Reticulatae is the dry mature skin of rutaceae orange (CitrusreticulataBlanco) its variety.Originate in the ground such as Guangdong, Fujian, Sichuan, Chongqing, Zhejiang, Jiangxi, Hunan, wherein good with Xinhui of Guangdong Province, four meetings, the suburbs, Guangzhou product person's matter, big with the ground such as Sichuan, Chongqing yield.
Pericarpium Citri Reticulatae has effect of regulating qi-flowing for strengthening spleen, drying dampness to eliminate phlegm, and along with growth in the living standard, people's health care consciousness strengthens gradually, and Pericarpium Citri Reticulatae is because of mellow time of its flavour is sweet, CHENXIANG is unique fine quality and its special health-care effect to human body, the deep favor by consumer.
All the time, Pericarpium Citri Reticulatae is with Chen Jiuzhe for good, and there are proverb " Pericarpium Citri Reticulatae in thousand, century-old Pericarpium Citri Reticulatae ", " one or two Pericarpium Citri Reticulatae one or two gold medals, century-old Pericarpium Citri Reticulatae victory gold " etc. in Guangdong.In the field of circulation, the more old Pericarpium Citri Reticulatae market price is more high, and also has a lot of collector to collect year Pericarpium Citri Reticulatae of a specified duration.Pericarpium Citri Reticulatae ageing is the natural fermentation process of Pericarpium Citri Reticulatae, and ageing is Pericarpium Citri Reticulatae development fragrance, consolidates and improve the master operation of kind, and the distinctive quality of Pericarpium Citri Reticulatae and CHENXIANG are formed in ageing process.In ageing process, in Pericarpium Citri Reticulatae, the chemical composition generation autoxidation such as flavonoid, aminoacid, saccharide, causes the formation of brown material and the generation of CHENXIANG characteristic odor.
The quality of Pericarpium Citri Reticulatae and aging condition have close relationship, tradition Pericarpium Citri Reticulatae ageing is under field conditions (factors), keep dry and comfortable ventilation, product storage (refers generally to sufficiently large batch sample preserve) in the packing container (referring generally to gunnysack) of good air permeability, change over time, the growth and decline change under ferment effect of its effective inclusions of dry Citrus chachiensis Hort. C. Suavissima Tanaka and cause the process of its color and composition transfer.The Citrus chachiensis Hort. C. Suavissima Tanaka of ageing 3 years and above time just can be referred to as Pericarpium Citri Reticulatae, and one to carry out aging period oversize, is unfavorable for improving yield, and two natural environmental conditions carrying out ageing are difficult to control to, and are entirely operated with artificial experience, it is easy to causes and goes mouldy rotten, affects product quality.
Application number be 201410147656.6 patent of invention disclose the method for rapidly aging of a kind of Pericarpium Citri Reticulatae, it is specially in fresh Citrus chachiensis Hort. C. Suavissima Tanaka is put in drying cabinet, it is dried at 100 ~ 120 DEG C of temperature, until Citrus chachiensis Hort. C. Suavissima Tanaka water content is 20 ~ 30%, cooling, the Citrus chachiensis Hort. C. Suavissima Tanaka of dried cooling is put in airtight container, and oxygen or pure air is passed into constantly from one end of container, gas is discharged from the other end of container, and, make the 0.2 ~ 0.3MPa higher than atmospheric pressure of the air pressure in container, it is 30 ~ 60 minutes that gas in container all changes the time once, the Citrus chachiensis Hort. C. Suavissima Tanaka process time in container is 10 ~ 12 months, thus obtaining the measured Pericarpium Citri Reticulatae of ageing matter.Although the ageing of Pericarpium Citri Reticulatae is achieved good effect by this invention, but its equipment requirements is higher, troublesome poeration, be not easy to promote.
Summary of the invention
In view of this, it is an object of the invention to overcome the deficiencies in the prior art, it is provided that the quick Pericarpium Citri Reticulatae aging method that a kind of ageing process cycle is short, easy to operate, constant product quality is high.
In order to solve above-mentioned technical problem, the present invention adopts following scheme to realize:
A kind of method accelerating Pericarpium Citri Reticulatae ageing, the Citrus chachiensis Hort. C. Suavissima Tanaka cleaned up is dried to it and contains a small amount of moisture, dried Citrus chachiensis Hort. C. Suavissima Tanaka is placed under hot and humid environment process a period of time, being placed in by Citrus chachiensis Hort. C. Suavissima Tanaka under low temperature and low humidity environment again process a period of time, hot and humid process processes with low temperature and low humidity and alternately repeatedly carries out.
Citrus chachiensis Hort. C. Suavissima Tanaka is dried to containing a small amount of moisture, coordinates follow-up hot and humid process alternately to process with low temperature and low humidity, accelerate the formation of brown material in Pericarpium Citri Reticulatae.The present invention have employed the hot and humid process of uniqueness hocket with low temperature and low humidity process, the effective inclusions in Citrus chachiensis Hort. C. Suavissima Tanaka is made to be subject to repetitious stimulation under ferment effect, thus the active substance fast reaction realized in Citrus chachiensis Hort. C. Suavissima Tanaka, the nature ageing effect of 3 ~ 5 years can be reached at short notice.
The Citrus chachiensis Hort. C. Suavissima Tanaka cleaned up is dried in temperature 40 ~ 50 DEG C when.
It is 10 ~ 30% that Citrus chachiensis Hort. C. Suavissima Tanaka is dried to water content.Dried Citrus chachiensis Hort. C. Suavissima Tanaka water content can not be too many, and water content can cause subsequent high temperature high humidity treatment and low temperature and low humidity to process the increase of time too much, and easily goes mouldy；Water content can not be very little, water content very little makes Citrus chachiensis Hort. C. Suavissima Tanaka close to drying completely, Citrus chachiensis Hort. C. Suavissima Tanaka now due on epidermal structure with very different during rich in water, in follow-up hot and humid process and low temperature and low humidity process, the effective inclusions in Citrus chachiensis Hort. C. Suavissima Tanaka can be suppressed on the contrary to react.
The condition of described hot and humid process is temperature 30 ~ 50 DEG C, humidity 70 ~ 90%, processes 30 ~ 50 days time.
Pass into outside air during hot and humid process to ensure that Citrus chachiensis Hort. C. Suavissima Tanaka fully contacts with oxygen, and to keep Citrus chachiensis Hort. C. Suavissima Tanaka water content be 20 ~ 30%.Outside air herein is the environment of relatively-high temperature high humidity treatment, it is therefore intended that makes Pericarpium Citri Reticulatae and oxygen be fully contacted, and regulates the water content of Citrus chachiensis Hort. C. Suavissima Tanaka, may advantageously facilitate the generation of oxidation reaction in Pericarpium Citri Reticulatae.As being placed in temperature and humidity control incubator by Citrus chachiensis Hort. C. Suavissima Tanaka, opening chamber door and can realize passing into of outside air, this mode is also most convenient, and cost is minimum.By ensureing that Citrus chachiensis Hort. C. Suavissima Tanaka and oxygen are fully contacted, and keep the water content of Citrus chachiensis Hort. C. Suavissima Tanaka, coordinate with the change of moisture content of Citrus chachiensis Hort. C. Suavissima Tanaka during low temperature and low humidity so that Citrus chachiensis Hort. C. Suavissima Tanaka repeatedly receives stimulation under two states, and its internal structure changes repeatedly, can greatly promote the reaction of effective inclusions.
The condition that described low temperature and low humidity processes is temperature 20 ~ 30 DEG C, and humidity 50 ~ 60%, the process time is 10 ~ 20 days.
Low temperature and low humidity passes into outside air to ensure that Citrus chachiensis Hort. C. Suavissima Tanaka fully contacts with oxygen during processing, and to keep Citrus chachiensis Hort. C. Suavissima Tanaka water content be 5 ~ 15%.
It is 3 ~ 5 times that hot and humid process and low temperature and low humidity process alternate frequency.Number of processes is not The more the better, if the effective inclusions worked as in Citrus chachiensis Hort. C. Suavissima Tanaka is after completion of the reaction, if proceeding hot and humid process and low temperature and low humidity process, Citrus chachiensis Hort. C. Suavissima Tanaka system now can be made to be damaged, cause that going mouldy easily occurs in follow-up Citrus chachiensis Hort. C. Suavissima Tanaka.
Preferably, a kind of method accelerating Pericarpium Citri Reticulatae ageing, it is 10 ~ 30% that the Citrus chachiensis Hort. C. Suavissima Tanaka cleaned up is dried to Citrus chachiensis Hort. C. Suavissima Tanaka water content at 40 ~ 50 DEG C, dried Citrus chachiensis Hort. C. Suavissima Tanaka is placed under the hot and humid condition of temperature 40～50 DEG C, humidity 80～90% and processes 30 ~ 50 days, process 10 ~ 20 days when Citrus chachiensis Hort. C. Suavissima Tanaka is placed in the low temperature and low humidity of temperature 20～25 DEG C, humidity 50～60% again, hot and humid process and low temperature and low humidity alternate treatment 3 ~ 5 times.
Passing into outside air during hot and humid process to ensure that Citrus chachiensis Hort. C. Suavissima Tanaka fully contacts with oxygen, and to keep Citrus chachiensis Hort. C. Suavissima Tanaka water content be 20 ~ 25%, low temperature and low humidity passes into outside air to ensure that Citrus chachiensis Hort. C. Suavissima Tanaka fully contacts with oxygen during processing, and to keep Citrus chachiensis Hort. C. Suavissima Tanaka water content be 5 ~ 10%.
Compared with prior art, there is advantages that the Pericarpium Citri Reticulatae ageing process of the present invention utilizes physical method to promote the chemical reaction of active substance in Citrus chachiensis Hort. C. Suavissima Tanaka, can quickly realize the Pericarpium Citri Reticulatae nature ageing ageing quality of 3～5 years, this technique can effectively prevent Pericarpium Citri Reticulatae from going mouldy in ageing process, control the quality of Pericarpium Citri Reticulatae preferably, easy and simple to handle, it is simple to promote, and without any additive, Quality of Pericarpium is safe and reliable.
Detailed description of the invention
In order to allow those skilled in the art be more fully understood that technical scheme, below the present invention is further elaborated.
Embodiment 1
A kind of method accelerating Pericarpium Citri Reticulatae ageing, the fresh Citrus chachiensis Hort. C. Suavissima Tanaka cleaned up is placed in heat pump drying case and is dried at 40 DEG C, until Citrus chachiensis Hort. C. Suavissima Tanaka water content is 10%, dried Citrus chachiensis Hort. C. Suavissima Tanaka is placed in temperature and humidity control incubator, in temperature 30 DEG C, hot and humid process 30 days is carried out when humidity 70%, and every two days of period opened chamber door and makes Citrus chachiensis Hort. C. Suavissima Tanaka fully contact with oxygen with supplementary outside air, and keep water content 20%, hot and humid be disposed after, regulating temperature is 20 DEG C, humidity 50%, carry out low temperature and low humidity to process 10 days, every two days of period opened chamber door and with supplementary outside air, Citrus chachiensis Hort. C. Suavissima Tanaka is fully contacted with oxygen, and keep water content 5%, hot and humid process processes with low temperature and low humidity and hockets 3 times.Opening the frequency of chamber door, number of times and time can adjust according to actual humiture, it is therefore intended that keep the water content of Citrus chachiensis Hort. C. Suavissima Tanaka.Through Pericarpium Citri Reticulatae expert testimony, product has reached the nature ageing ageing quality of about 5 years.
Embodiment 2
A kind of method accelerating Pericarpium Citri Reticulatae ageing, the fresh Citrus chachiensis Hort. C. Suavissima Tanaka cleaned up is placed in heat pump drying case and is dried at 50 DEG C, until Citrus chachiensis Hort. C. Suavissima Tanaka water content is 30%, dried Citrus chachiensis Hort. C. Suavissima Tanaka is placed in temperature and humidity control incubator, in temperature 50 C, hot and humid process 50 days is carried out when humidity 90%, and every two days of period opened chamber door and makes Citrus chachiensis Hort. C. Suavissima Tanaka fully contact with oxygen with supplementary outside air, and keep water content 30%, hot and humid be disposed after, regulating temperature is 30 DEG C, humidity 60%, carry out low temperature and low humidity to process 20 days, every two days of period opened chamber door and with supplementary outside air, Citrus chachiensis Hort. C. Suavissima Tanaka is fully contacted with oxygen, and keep water content 15%, hot and humid process processes with low temperature and low humidity and hockets 4 times.Through Pericarpium Citri Reticulatae expert testimony, product has reached the nature ageing ageing quality of about 4.5 years.
Embodiment 3
A kind of method accelerating Pericarpium Citri Reticulatae ageing, be placed in heat pump drying case by the fresh Citrus chachiensis Hort. C. Suavissima Tanaka cleaned up being dried to Citrus chachiensis Hort. C. Suavissima Tanaka water content under 45 DEG C of conditions is 20%, dried Citrus chachiensis Hort. C. Suavissima Tanaka is placed in temperature and humidity control incubator, in temperature 40 DEG C, hot and humid process 40 days is carried out when humidity 80%, and every 2 days of period opened chamber door and makes Citrus chachiensis Hort. C. Suavissima Tanaka fully contact with oxygen with supplementary outside air, and keep water content 25%, hot and humid be disposed after, regulating temperature is 25 DEG C, humidity 55%, carry out low temperature and low humidity to process 15 days, every two days of period opened chamber door and with supplementary outside air, Citrus chachiensis Hort. C. Suavissima Tanaka is fully contacted with oxygen, and keep water content 10%, hot and humid process processes with low temperature and low humidity and hockets 5 times.Through Pericarpium Citri Reticulatae expert testimony, product has reached the nature ageing ageing quality of about 6 years.
In natural ageing process, in Pericarpium Citri Reticulatae, main component content of hesperidin is gradually reduced, and polymethoxyflavone (Nobiletin and Pericarpium Citri tangerinae element) content constantly rises.Color is dimmed gradually, and fresh fruit abnormal smells from the patient is gradually lowered, and aged aroma appears gradually.
Compare by the Hesperidin in Pericarpium Citri Reticulatae, Nobiletin and Pericarpium Citri tangerinae cellulose content are carried out detection, the present embodiment is more unprocessed allow its natural ageing Pericarpium Citri Reticulatae and through hot and humid and low temperature and low humidity alternate treatment accelerated ageing Pericarpium Citri Reticulatae sample, to the change of Hesperidin, Nobiletin and Pericarpium Citri tangerinae cellulose content in their ageing process, the effect that the artificial method for rapidly aging of the present invention is described directly perceived.
Hesperidin, Nobiletin and Pericarpium Citri tangerinae cellulose content are all pass through high-performance liquid chromatography method.Concrete grammar is as follows:
One, high-efficient liquid phase chromatogram condition
Mobile phase: eluent A is acetonitrile solution, eluent B is water
Detection wavelength: 280nm and 330nm
Column temperature: 25 DEG C
Condition of gradient elution:
0-5min, the percent by volume of eluent A is 25%, and the percent by volume of eluent B is 75%；
5-15min, the percent by volume of eluent A at the uniform velocity rises to 50% from 25%, and the percent by volume of eluent B is at the uniform velocity down to 50% from 75%；
15-35min, the percent by volume of eluent A at the uniform velocity rises to 60% from 50%, and the percent by volume of eluent B is at the uniform velocity down to 40% from 50%；
35-40min, the percent by volume of eluent A at the uniform velocity rises to 85% from 60%, and the percent by volume of eluent B at the uniform velocity rises to 15% from 40%；
40-45min, the percent by volume of eluent A is at the uniform velocity down to 25% from 85%, and the percent by volume of eluent B at the uniform velocity rises to 75% from 15%.
Two, the preparation of need testing solution
Weighing drying sample powder 2.00g, with 100ml methanol ultrasonic extraction 20min, sucking filtration, filtering residue again with 50ml methanol extraction once, repeats above operation.Be settled to 50ml after the concentration of united extraction liquid, shake up, with 0.45 μm of membrane filtration, gained filtrate as need testing solution, put 4 DEG C standby.
Three, the preparation of reference substance solution
Precision weighs Hesperidin 0.0022g, Nobiletin 0.0014g and Pericarpium Citri tangerinae element 0.0024g, dissolves with methanol respectively, by methanol constant volume to 10ml after mixing.
Four, the drafting of standard curve
Take Hesperidin (0.22mg/ml), Nobiletin (0.14mg/ml), Pericarpium Citri tangerinae element (0.24mg/ml) reference substance, peak area is measured according to chromatographic condition, and with peak area (y), different reference substance concentration (x, mg/ml) are carried out linear regression, regression equation is:
y=a·x+b
In formula:
Y is the peak area of reference substance solution；
X is the concentration (mg/ml) of reference substance solution；
A, b are constant.
The result of the equation of linear regression of three kinds of test substances is as follows.
Five, need testing solution is measured
Accurate absorption 10 μ l need testing solutions, according to chromatographic condition, measure peak area under 280nm and 330nm.The composition of different retention times is carried out cubage.
In the ageing process that the present embodiment detects, in Pericarpium Citri Reticulatae, the changes of contents of Hesperidin, Nobiletin and Pericarpium Citri tangerinae element is as shown in table 1 below.
The untreated sample of table 1 from process after Pericarpium Citri Reticulatae sample different ageing stage Substances variations (mg/ml)
From table 1 it follows that at 0 day, compared with the Hesperidin of undressed Pericarpium Citri Reticulatae sample, hot and humid with low temperature and low humidity alternate treatment after 1 time the Hesperidin rate of descent of Pericarpium Citri Reticulatae be 3.39%.After alternate treatment 3 times, processing ageing Pericarpium Citri Reticulatae sample compared with unprocessed ageing Pericarpium Citri Reticulatae sample, content of hesperidin range of decrease rate reaches 19.70%, and the rate of increase of Nobiletin content is 15.79%, and the rate of increase of Pericarpium Citri tangerinae cellulose content reaches 36.36%.
Comparative example 1
This comparative example is similar to Example 1, is distinctive in that, hot and humid process 120 days and cancellation low temperature and low humidity process.Through Pericarpium Citri Reticulatae expert testimony, product ageing quality is worse than the nature ageing Pericarpium Citri Reticulatae of 1 year.
Comparative example 2
This comparative example is similar to Example 1, is distinctive in that, low temperature and low humidity processes 120 days and cancels hot and humid process.Through Pericarpium Citri Reticulatae expert testimony, product ageing quality is worse than the nature ageing Pericarpium Citri Reticulatae of 1 year.
Comparative example 3
This comparative example is similar to Example 2, is distinctive in that, it is 1 time that hot and humid process and low temperature and low humidity process alternate frequency.Through Pericarpium Citri Reticulatae expert testimony, product reaches the nature ageing ageing quality of about 1 year.
Comparative example 4
This comparative example is similar to Example 2, is distinctive in that, it is 8 times that hot and humid process and low temperature and low humidity process alternate frequency.Through Pericarpium Citri Reticulatae expert testimony, product reaches the nature ageing ageing quality of about 2 years, easily goes mouldy in subsequent storage process.
Comparative example 5
This comparative example is similar to Example 3, is distinctive in that, the condition of hot and humid process is 60 DEG C, humidity 95%.Through Pericarpium Citri Reticulatae expert testimony, product reaches the nature ageing ageing quality of about 2 years.
Comparative example 6
This comparative example is similar to Example 3, is distinctive in that, the condition that low temperature and low humidity processes is 15 DEG C, humidity 40%.Through Pericarpium Citri Reticulatae expert testimony, product reaches the nature ageing ageing quality of about 1.5 years.
In conjunction with the embodiments 1 ~ 3 and comparative example 1 ~ 6 can be seen that, the present invention is processed by hot and humid process and low temperature and low humidity and hockets, and can effectively accelerate the ageing effect of Pericarpium Citri Reticulatae；As comparative example 1 ~ 3, hot and humid process and low temperature and low humidity process, if lacking one of them condition, all ageing effect can be had a negative impact；Inventors performed substantial amounts of test, if having drawn there is trickle change in the interval each condition of condition of optimum, all can ageing effect be had a negative impact.
Above-described embodiment is only the wherein specific implementation of the present invention, and it describes comparatively concrete and detailed, but therefore can not be interpreted as the restriction to the scope of the claims of the present invention.It should be pointed out that, for the person of ordinary skill of the art, without departing from the inventive concept of the premise, it is also possible to make some deformation and improvement, these apparent alternative forms belong to protection scope of the present invention.
Claims (10)
1. the method accelerating Pericarpium Citri Reticulatae ageing, it is characterized in that, the Citrus chachiensis Hort. C. Suavissima Tanaka cleaned up is dried to it and contains a small amount of moisture, dried Citrus chachiensis Hort. C. Suavissima Tanaka is placed under hot and humid environment process a period of time, being placed in by Citrus chachiensis Hort. C. Suavissima Tanaka under low temperature and low humidity environment again process a period of time, hot and humid process processes with low temperature and low humidity and alternately repeatedly carries out.
2. the method for acceleration Pericarpium Citri Reticulatae ageing according to claim 1, it is characterised in that the Citrus chachiensis Hort. C. Suavissima Tanaka cleaned up is dried in temperature 40 ~ 50 DEG C when.
3. the method for acceleration Pericarpium Citri Reticulatae ageing according to claim 2, it is characterised in that it is 10 ~ 30% that Citrus chachiensis Hort. C. Suavissima Tanaka is dried to water content.
4. the method accelerating Pericarpium Citri Reticulatae ageing according to any one of claim 1 ~ 3, it is characterised in that the condition of described hot and humid process is temperature 30 ~ 50 DEG C, humidity 70 ~ 90%, processes 30 ~ 50 days time.
5. the method for acceleration Pericarpium Citri Reticulatae ageing according to claim 4, it is characterised in that pass into outside air during hot and humid process, and to keep Citrus chachiensis Hort. C. Suavissima Tanaka water content be 20 ~ 30%.
6. the method for acceleration Pericarpium Citri Reticulatae ageing according to claim 4, it is characterised in that the condition that described low temperature and low humidity processes is temperature 20 ~ 30 DEG C, and humidity 50 ~ 60%, the process time is 10 ~ 20 days.
7. the method for acceleration Pericarpium Citri Reticulatae ageing according to claim 6, it is characterised in that low temperature and low humidity passes into outside air during processing, and to keep Citrus chachiensis Hort. C. Suavissima Tanaka water content be 5 ~ 15%.
8. the method for acceleration Pericarpium Citri Reticulatae ageing according to claim 7, it is 3 ~ 5 times that hot and humid process and low temperature and low humidity process alternate frequency.
9. the method accelerating Pericarpium Citri Reticulatae ageing, it is characterized in that, it is 10 ~ 30% that the Citrus chachiensis Hort. C. Suavissima Tanaka cleaned up is dried to Citrus chachiensis Hort. C. Suavissima Tanaka water content at 40 ~ 50 DEG C, dried Citrus chachiensis Hort. C. Suavissima Tanaka is placed under the hot and humid condition of temperature 40～50 DEG C, humidity 80～90% and processes 30 ~ 50 days, process 10 ~ 20 days when Citrus chachiensis Hort. C. Suavissima Tanaka is placed in the low temperature and low humidity of temperature 20～25 DEG C, humidity 50～60% again, hot and humid process and low temperature and low humidity alternate treatment 3 ~ 5 times.
10. the method for acceleration Pericarpium Citri Reticulatae ageing according to claim 9, it is characterised in that pass into outside air during hot and humid process, and to keep Citrus chachiensis Hort. C. Suavissima Tanaka water content be 20 ~ 25%, low temperature and low humidity passes into outside air during processing, and to keep Citrus chachiensis Hort. C. Suavissima Tanaka water content be 5 ~ 10%.
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| CN111588765A (en) * | 2020-05-28 | 2020-08-28 | 陈美橘 | Preparation method of dried orange peel |
| CN111973673A (en) * | 2020-09-11 | 2020-11-24 | 华南农业大学 | Method for accelerating aging of dried orange peel |
| CN112205648A (en) * | 2020-09-04 | 2021-01-12 | 江门市御广陈皮茶业有限公司 | Dried tangerine peel and dried tangerine peel |
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| CN106619935A (en) * | 2016-12-27 | 2017-05-10 | 中国农业科学院农产品加工研究所 | Preparation method of dried tangerine peels |
| CN106619935B (en) * | 2016-12-27 | 2020-01-24 | 中国农业科学院农产品加工研究所 | Preparation method of dried orange peel |
| CN111588765A (en) * | 2020-05-28 | 2020-08-28 | 陈美橘 | Preparation method of dried orange peel |
| CN112205648A (en) * | 2020-09-04 | 2021-01-12 | 江门市御广陈皮茶业有限公司 | Dried tangerine peel and dried tangerine peel |
| CN111973673A (en) * | 2020-09-11 | 2020-11-24 | 华南农业大学 | Method for accelerating aging of dried orange peel |
| CN111973673B (en) * | 2020-09-11 | 2022-03-11 | 华南农业大学 | Method for accelerating aging of dried orange peel |
| CN113331368A (en) * | 2021-03-12 | 2021-09-03 | 广东省农业科学院蚕业与农产品加工研究所 | Method for accelerating aging of dried orange peel |
| CN113749252A (en) * | 2021-08-25 | 2021-12-07 | 湖北土老憨生态农业科技股份有限公司 | Processing method for improving quality of dried orange peel (orange peel) powder |
| CN113749252B (en) * | 2021-08-25 | 2023-06-30 | 湖北土老憨生态农业科技股份有限公司 | Processing method for improving quality of dried orange peel (orange peel) powder |
| CN114766638A (en) * | 2022-03-01 | 2022-07-22 | 江门丽宫国际食品股份有限公司 | Method for improving quality of dried orange peel |
| CN114814003A (en) * | 2022-04-01 | 2022-07-29 | 广州白云山陈李济药厂有限公司 | Quantitative detection method for aging degree of dried orange peel |
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