CN105746711A - Milk product for improving sleep and preparation method thereof - Google Patents
Milk product for improving sleep and preparation method thereof Download PDFInfo
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Abstract
The invention provides a milk product for improving sleep; the milk product for improving sleep includes the raw materials: 30 to 99.69 parts by weight of milk, 0.01 to 0.5 part by weight of semen ziziphi spinosae or a semen ziziphi spinosae extract, 0.01 to 0.05 part by weight of vitamin E, and 0.0025 to 0.1 part by weight of sodium ascorbate. The invention also provides a preparation method of the milk product for improving sleep. The semen ziziphi spinosae or the semen ziziphi spinosae extract is added in the milk product for improving sleep, so through storage, no peculiar smell can be produced, and the taste and smell are better.
Description
Technical field
The present invention relates to a kind of milk product, particularly relate to a kind of milk product improving sleep and preparation method thereof.
Background technology
Milk is that a kind of nutritional labeling is complete, ratio of components conveniently, absorption easy to digest, the wholefood that is of high nutritive value.Owing to itself can make people produce tired sleepy biological L-Trp containing a kind of in milk, there is certain sedative-hypnotic effect.In order to make milk have functionalization effect, there is the sedative-hypnotic effect having no side effect, Semen Ziziphi Spinosae extract can be added in milk, in CN102038248A published, but containing fatty oil and flavone compound in Semen Ziziphi Spinosae extract, after storage after a while, easily producing the materials such as butanoic acid, caproic acid, sad and capric acid in milk, these materials can affect mouthfeel and the abnormal smells from the patient of milk product.
Summary of the invention
It is an object of the invention to provide a kind of milk product improving sleep, abnormal flavour, mouthfeel and abnormal smells from the patient will not be produced preferably through storage.
The preparation method that it is a further object of the present invention to provide a kind of milk product improving sleep, the milk product made will not produce abnormal flavour through storage, plays the effect improving sleep.
The invention provides a kind of milk product improving sleep, its raw material includes: milk 30 to 99.69 weight portion, Semen Ziziphi Spinosae or Semen Ziziphi Spinosae extract 0.01 to 0.5 weight portion, vitamin E 0.005 to 0.02 weight portion, sodium ascorbate 0.025 to 0.01 weight portion.Described Semen Ziziphi Spinosae or Semen Ziziphi Spinosae extract are preferably 0.01 to 0.3 weight portion.
In the exemplary embodiment of a kind of milk product improving sleep, described raw material farther includes γ-aminobutyric acid 0.01 to 0.25 weight portion.Described γ-aminobutyric acid is preferably 0.02 to 0.05 weight portion.
In another exemplary embodiment of a kind of milk product improving sleep, described raw material farther includes alpha-lactalbumin 0.005 to 0.03 weight portion.
In another exemplary embodiment of a kind of milk product improving sleep, described raw material farther includes emulsifying agent 0.05 to 0.3 weight portion, and described emulsifying agent is one or more combination single in sucrose fatty acid ester, glyceryl monostearate fat acid esters, diglycerine fatty acid ester, phospholipid and polyglyceryl fatty acid ester.
In another exemplary embodiment of a kind of milk product improving sleep, described raw material farther includes stabilizer 0.01 to 0.2 weight portion, and described stabilizer is from the combination of one or more in phosphoric acid, Sodium Acid Pyrophosphate, sodium pyrophosphate, dalcium biphosphate, potassium dihydrogen phosphate, diammonium phosphate, dipotassium hydrogen phosphate, calcium hydrogen phosphate, tricalcium phosphate, tripotassium phosphate, tertiary sodium phosphate, sodium hexameta phosphate, sodium tripolyphosphate, sodium dihydrogen phosphate, disodium hydrogen phosphate.
The milk product improving sleep provided by the invention, wherein with the addition of Semen Ziziphi Spinosae extract, and will not produce abnormal flavour, mouthfeel and abnormal smells from the patient preferably through storage.
The preparation method that present invention also offers the milk product of above-mentioned improvement sleep, including: take vitamin E, take the part milk of vitamin E weight 30 to 50 times, by part Milk During Heating to 70-75 DEG C, form the first feed liquid with the part milk dissolving vitamin E after heating；Taking remaining milk, stirring is also slowly warmed up to 40-45 DEG C, is added by other raw material, and mix and blend forms the second feed liquid, then the second feed liquid is warmed up to 70-75 DEG C；First feed liquid and the second feed liquid are mixed to form the 3rd feed liquid keep 10-20 minute at 70-75 DEG C, fully dissolve；Blending tank is squeezed into after 3rd feed liquid is cooled to 0-20 DEG C.The method can more effectively retain the effective ingredient in milk product, and milk product will not produce abnormal flavour through storage so that it is plays the effect improving sleep.
Detailed description of the invention
In the present invention, in order to suppress protein precipitation and fat floating better, improve the mouthfeel of product, the thickening agent of 0.003 to 0.03 weight portion can be increased in the feed, the thickening agent combination of one or more in sodium carboxymethyl cellulose, carrageenan, gelatin, microcrystalline Cellulose, gellan gum, xanthan gum, propylene glycol alginate, Konjac glucomannan, agar, locust bean gum, guar gum and pectin.
In the present invention, in order to improve the mouthfeel of product, can also increasing acidity regulator, white sugar or Mel in the feed, acidity regulator therein can be selected from the combination of one or more in sodium citrate, sodium pyrophosphate, sodium dihydrogen phosphate, disodium hydrogen phosphate, sodium tripolyphosphate, sodium hexameta phosphate, potassium dihydrogen phosphate, dalcium biphosphate, tertiary sodium phosphate.
nullIn the present invention，In order to increase the nutrition of product，Nutrient can also be added in the feed，Nutrient can be selected from vitamin A、Vitamin B complex、Vitamin D、Vitamin C、Vitamin E、Calcium lactate、Taurine、Folic acid、Nicotinic acid、Choline、Ferrous sulfate、Ferric citrate、Zinc sulfate、Zinc gluconate、Sodium selenite、Magnesium sulfate、Magnesium gluconate、L-carnitine、Lactoferrin、Immunoglobulin、Breast mineral salt、Ferrous sulfate、Sodium iron ethylenediaminetetraacetate、Ferric phrophosphate、Calcium carbonate、Calcium gluconate、L-calcium lactate、Calcium hydrogen phosphate、Zinc citrate、Zinc acetate、Zinc carbonate、Sodium selenite、Yeast rich in selenium、Selenium protein、Selenocarrageenan、Magnesium sulfate、Magnesium carbonate、Arachidonic acid、Docosahexenoic acid、Phosphopeptide caseinates etc. are to the combination of one or more in the useful trace element of human body.
Vitamin E in the present invention includes natural Vitamin E and synthesising complex E.
Embodiment 1.
Raw material:
Milk 996.6kg, Semen Ziziphi Spinosae extract 1kg, natural Vitamin E 0.05kg, sodium ascorbate 0.25Kg；
Emulsifying agent is 2kg altogether, wherein sucrose fatty acid ester: glyceryl monostearate fat acid esters=1:1；
Stabilizer: sodium hexameta phosphate is 0.1kg altogether.
Preparation method:
Take vitamin E, then take the part milk of vitamin E weight 30 times, by this part Milk During Heating to 75 DEG C, form the first feed liquid with vitamin E described in the part milk dissolving after heating；
Taking remaining milk, stirring is also slowly warmed up to 45 DEG C, is added by other raw material, and mix and blend forms the second feed liquid, then the second feed liquid is warmed up to 75 DEG C；
First feed liquid and the second feed liquid are mixed to form the 3rd feed liquid keep 15 minutes at 75 DEG C, fully dissolve；
Blending tank is squeezed into after 3rd feed liquid is cooled to 7 DEG C.
Embodiment 2.
Raw material:
Milk 996.1kg, Semen Ziziphi Spinosae 1kg, natural Vitamin E 0.2kg, sodium ascorbate 0.1kg, γ-aminobutyric acid 0.5kg, alpha-lactalbumin 0.1kg；
Emulsifying agent is 1.8kg altogether, wherein sucrose fatty acid ester: glyceryl monostearate fat acid esters=1:0.8；
Mel 0.1kg.
Thickening agent: carrageenan 0.1kg.
Preparation method:
Take vitamin E, then take the part milk of vitamin E weight 30 times, by this part Milk During Heating to 75 DEG C, form the first feed liquid with vitamin E described in the part milk dissolving after heating；
Taking remaining milk, stirring is also slowly warmed up to 45 DEG C, is added by other raw material, and mix and blend forms the second feed liquid, then the second feed liquid is warmed up to 75 DEG C；
First feed liquid and the second feed liquid are mixed to form the 3rd feed liquid keep 15 minutes at 75 DEG C, fully dissolve；
Blending tank is squeezed into after 3rd feed liquid is cooled to 7 DEG C.
Embodiment 3.
Raw material:
Milk 988.42kg, Semen Ziziphi Spinosae 5kg, natural Vitamin E 0.1kg, sodium ascorbate 0.2kg, γ-aminobutyric acid 0.2kg, alpha-lactalbumin 0.05kg；
Emulsifying agent is 3kg altogether, wherein glyceryl monostearate fat acid esters: phospholipid=1:1；
Mel 3kg.
Thickening agent: gellan gum 0.03kg.
Preparation method:
Take vitamin E, then take the part milk of vitamin E weight 30 times, by this part Milk During Heating to 75 DEG C, form the first feed liquid with vitamin E described in the part milk dissolving after heating；
Taking remaining milk, stirring is also slowly warmed up to 45 DEG C, is added by other raw material, and mix and blend forms the second feed liquid, then the second feed liquid is warmed up to 75 DEG C；
First feed liquid and the second feed liquid are mixed to form the 3rd feed liquid keep 15 minutes at 75 DEG C, fully dissolve；
Blending tank is squeezed into after 3rd feed liquid is cooled to 7 DEG C.
Embodiment 4.
Raw material:
Milk 993.1kg, Semen Ziziphi Spinosae extract 2kg, natural Vitamin E 0.05kg, sodium ascorbate 0.25kg, γ-aminobutyric acid 0.5kg, alpha-lactalbumin 0.3kg；
Emulsifying agent is 0.5kg altogether, wherein glyceryl monostearate fat acid esters: phospholipid=1:2；
Stabilizer: sodium tripolyphosphate 1kg
Mel 0.5kg.
Thickening agent: sodium carboxymethyl cellulose: microcrystalline Cellulose=1:1, altogether 0.3kg.
Preparation method:
Take vitamin E, then take the part milk of vitamin E weight 30 times, by this part Milk During Heating to 75 DEG C, form the first feed liquid with vitamin E described in the part milk dissolving after heating；
Taking remaining milk, stirring is also slowly warmed up to 45 DEG C, is added by other raw material, and mix and blend forms the second feed liquid, then the second feed liquid is warmed up to 75 DEG C；
First feed liquid and the second feed liquid are mixed to form the 3rd feed liquid keep 15 minutes at 75 DEG C, fully dissolve；
Blending tank is squeezed into after 3rd feed liquid is cooled to 10 DEG C.
Embodiment 5.
Raw material:
Milk 300kg, Semen Ziziphi Spinosae extract 0.1kg, natural Vitamin E 0.15kg, sodium ascorbate 0.75kg, γ-aminobutyric acid 2.5kg, alpha-lactalbumin 0.5kg；
Emulsifying agent is 3kg altogether, wherein sucrose fatty acid ester: glyceryl monostearate fat acid esters=1:1；
Stabilizer: sodium hexameta phosphate 2kg；
Mel: 2kg；
Acidity regulator is 1kg altogether, wherein citric acid: lactic acid=2:2.5；
White sugar 30kg；
1000kg is supplied with pure water.
Preparation method:
Take vitamin E, then take the part milk of vitamin E weight 40 times, by this part Milk During Heating to 72 DEG C, form the first feed liquid with vitamin E described in the part milk dissolving after heating；
Taking remaining milk, stirring is also slowly warmed up to 42 DEG C, is added by other raw material, and mix and blend forms the second feed liquid, then the second feed liquid is warmed up to 72 DEG C；
First feed liquid and the second feed liquid are mixed to form the 3rd feed liquid keep 10 minutes at 70 DEG C, fully dissolve；
Blending tank is squeezed into after 3rd feed liquid is cooled to 0 DEG C.
Embodiment 6.
Raw material:
Milk 800kg, Semen Ziziphi Spinosae extract 3kg, natural Vitamin E 0.15kg, sodium ascorbate 1kg, γ-aminobutyric acid 0.1kg, alpha-lactalbumin 0.5kg；
Emulsifying agent is 3kg altogether, wherein sucrose fatty acid ester: glyceryl monostearate fat acid esters=1:2；
Stabilizer: sodium hexameta phosphate 2kg；
Mel: 2kg；
Vitamin D: 1kg；
1000kg is supplied with pure water.
Preparation method:
Take vitamin E, then take the part milk of vitamin E weight 50 times, by this part Milk During Heating to 70 DEG C, form the first feed liquid with vitamin E described in the part milk dissolving after heating；
Taking remaining milk, stirring is also slowly warmed up to 40 DEG C, is added by other raw material, and mix and blend forms the second feed liquid, then the second feed liquid is warmed up to 70 DEG C；
First feed liquid and the second feed liquid are mixed to form the 3rd feed liquid keep 15 minutes at 70 DEG C, fully dissolve；
Blending tank is squeezed into after 3rd feed liquid is cooled to 20 DEG C.
Embodiment 7.
The raw material that embodiment 7 uses is identical with embodiment 1, and wherein vitamin E is synthesising complex E.Preparation method is also identical with embodiment 1.
Reference examples 1(only adds vitamin E).
Milk 996.85kg, Semen Ziziphi Spinosae extract 1kg, natural Vitamin E 0.05kg；
Emulsifying agent is 2kg altogether, wherein sucrose fatty acid ester: glyceryl monostearate fat acid esters=1:1；
Stabilizer: sodium hexameta phosphate is 0.1kg altogether.
Preparation method:
Take vitamin E, then take the part milk of vitamin E weight 30 times, by this part Milk During Heating to 75 DEG C, form the first feed liquid with vitamin E described in the part milk dissolving after heating；
Taking remaining milk, stirring is also slowly warmed up to 45 DEG C, is added by other raw material, and mix and blend forms the second feed liquid, then the second feed liquid is warmed up to 75 DEG C；
First feed liquid and the second feed liquid are mixed to form the 3rd feed liquid keep 15 minutes at 75 DEG C, fully dissolve；
Blending tank is squeezed into after 3rd feed liquid is cooled to 7 DEG C.
Reference examples 2(only adds ascorbic acid and receives).
Milk 996.65kg, Semen Ziziphi Spinosae extract 1kg, sodium ascorbate 0.25Kg；
Emulsifying agent is 2kg altogether, wherein sucrose fatty acid ester: glyceryl monostearate fat acid esters=1:1；
Stabilizer: sodium hexameta phosphate is 0.1kg altogether.
Preparation method:
Take vitamin E, then take the part milk of vitamin E weight 30 times, by this part Milk During Heating to 75 DEG C, form the first feed liquid with vitamin E described in the part milk dissolving after heating；
Taking remaining milk, stirring is also slowly warmed up to 45 DEG C, is added by other raw material, and mix and blend forms the second feed liquid, then the second feed liquid is warmed up to 75 DEG C；
First feed liquid and the second feed liquid are mixed to form the 3rd feed liquid keep 15 minutes at 75 DEG C, fully dissolve；
Blending tank is squeezed into after 3rd feed liquid is cooled to 7 DEG C.
Reference examples 3(is without antioxidant).
Milk 996.9kg, Semen Ziziphi Spinosae extract 1kg；
Emulsifying agent is 2kg altogether, wherein sucrose fatty acid ester: glyceryl monostearate fat acid esters=1:1；
Stabilizer: sodium hexameta phosphate is 0.1kg altogether.
Preparation method:
Take vitamin E, then take the part milk of vitamin E weight 30 times, by this part Milk During Heating to 75 DEG C, form the first feed liquid with vitamin E described in the part milk dissolving after heating；
Taking remaining milk, stirring is also slowly warmed up to 45 DEG C, is added by other raw material, and mix and blend forms the second feed liquid, then the second feed liquid is warmed up to 75 DEG C；
First feed liquid and the second feed liquid are mixed to form the 3rd feed liquid keep 15 minutes at 75 DEG C, fully dissolve；
Blending tank is squeezed into after 3rd feed liquid is cooled to 7 DEG C.
Effect test.
Milk product containing Semen Ziziphi Spinosae and Semen Ziziphi Spinosae extract is in storage process, and milk therein can produce butanoic acid, caproic acid, sad and capric acid, and these materials can affect mouthfeel and the abnormal smells from the patient of milk product.
This effect test uses following methods detection butanoic acid, caproic acid, sad and capric acid.
Weigh and take 1 μ L after the methanol solution first of the above-mentioned each product boron trifluoride of about 0.2g acetifies and carry out makings analysis；
SPM-GC-MS condition: capillary column adopts PEG20M fused-silica capillary column (L.D is 30m*0.25mm, and thickness of liquid film is 0.25 μm), and carrier gas is He, and flow velocity is 0.8mL/min.The initial column temperature of chromatographic column is 40 DEG C and keeps 4min, is raised to 60 DEG C with 3 DEG C/min, is then raised to 120 DEG C with 6 DEG C/min, is finally raised to 230 DEG C with 10 DEG C/min and keeps 5min.Injector temperature 230 DEG C, Splitless injecting-Sample, detector temperature 280 DEG C.
Mass Spectrometry Conditions: ionization mode is EI, ionization voltage 70eV, filament emission current is 200 μ A, ion source temperature 20 DEG C, and interface temperature is 250 DEG C.
Use areas of peak normalization method to calculate mass fractions relative and represent the primary quantity such as table 1 below of butanoic acid in the product of embodiment 1, reference examples 1, reference examples 2 and reference examples 3, caproic acid, sad and capric acid:
Table 1: butanoic acid in the product of embodiment 1, reference examples 1, reference examples 2 and reference examples 3, caproic acid, sad and capric acid primary quantity
| Embodiment | Butanoic acid | Caproic acid | Sad | Capric acid |
| Embodiment 1 | 0% | 0.35% | 0.42% | 0.45% |
| Reference examples 1 | 0.03% | 0.32% | 0.40% | 0.38% |
| Reference examples 2 | 0% | 0.37% | 0.29% | 0.55% |
| Reference examples 3 | 0.05% | 0.28% | 0.34% | 0.35% |
By in the product of embodiment 1, reference examples 1, reference examples 2 and reference examples 3 temperature be 15-25 DEG C, humidity places 30 days when being 40-60%, then detects in aforementioned manners.Use areas of peak normalization method to calculate mass fractions relative and represent the surplus such as table 2 below of butanoic acid, caproic acid, sad and capric acid:
Table 2: butanoic acid in the product of embodiment 1, reference examples 1, reference examples 2 and reference examples 3, caproic acid, sad and capric acid surplus
| Embodiment | Butanoic acid | Caproic acid | Sad | Capric acid |
| Embodiment 1 | 1.55% | 1.43% | 1.32% | 1.25% |
| Reference examples 1 | 10.23% | 10.11% | 10.10% | 9.89% |
| Reference examples 2 | 13.45% | 12.56% | 12.36% | 12.22% |
| Reference examples 3 | 22.45% | 21.34% | 20.43% | 19.86% |
The numerical value of table 2 is individually subtracted the numerical value of table 1 and obtains the increase amount such as table 3 below of butanoic acid in storing process, caproic acid, sad and capric acid:
Table 3: the product of embodiment 1, reference examples 1, reference examples 2 and reference examples 3 is the increase amount of butanoic acid, caproic acid, sad and capric acid in storing process
| Embodiment | Butanoic acid | Caproic acid | Sad | Capric acid |
| Embodiment 1 | 1.55% | 1.08% | 0.90% | 0.80% |
| Reference examples 1 | 10.20% | 9.79% | 9.70% | 9.51% |
| Reference examples 2 | 13.45% | 12.19% | 12.07% | 11.67% |
| Reference examples 3 | 22.40% | 21.06% | 20.09% | 19.51% |
Embodiment 1 butanoic acid, caproic acid, sad and capric acid increase amount in storing process is less as can be seen from Table 3.Illustrate embodiment 1 in storage process compared with reference examples 1 and 2 produce butanoic acid, caproic acid, sad and capric acid is less.
In this article, " schematically " expression " serves as example, example or explanation ", should will not be construed to a kind of preferred or more advantage technical scheme described herein as any diagram of " schematically ", embodiment.
Except as otherwise noted, numerical range herein not only includes the gamut in two end points, also includes being contained in some subranges therein.
It is to be understood that, although this specification describes according to each embodiment, but not each embodiment only comprises an independent technical scheme, this narrating mode of description is only for clarity sake, description should be made as a whole by those skilled in the art, technical scheme in each embodiment through appropriately combined, can also form other embodiments that it will be appreciated by those skilled in the art that.
The a series of detailed description of those listed above is only for illustrating of the possible embodiments of the present invention; they also are not used to limit the scope of the invention; all without departing from the spiritual equivalent embodiments made of skill of the present invention or change; such as the combination of feature, segmentation or repetition, should be included within protection scope of the present invention.
Claims (7)
1. the milk product improving sleep, it is characterised in that its raw material includes: milk 30 to 99.69 weight portion, Semen Ziziphi Spinosae or Semen Ziziphi Spinosae extract 0.01 to 0.5 weight portion, vitamin E 0.005 to 0.02 weight portion, sodium ascorbate 0.025 to 0.01 weight portion.
2. a kind of milk product improving sleep as claimed in claim 1, wherein, described raw material farther includes γ-aminobutyric acid 0.01 to 0.25 weight portion.
3. a kind of milk product improving sleep as claimed in claim 1, wherein, described raw material farther includes alpha-lactalbumin 0.005 to 0.03 weight portion.
4. a kind of milk product improving sleep as claimed in claim 1, wherein, described raw material farther includes emulsifying agent 0.05 to 0.3 weight portion, the combination of one or more in sucrose fatty acid ester, glyceryl monostearate fat acid esters, diglycerine fatty acid ester, phospholipid and polyglyceryl fatty acid ester of the described emulsifying agent.
5. a kind of milk product improving sleep as claimed in claim 1, wherein, described raw material farther includes stabilizer 0.01 to 0.2 weight portion, and described stabilizer is from the combination of one or more in phosphoric acid, Sodium Acid Pyrophosphate, sodium pyrophosphate, dalcium biphosphate, potassium dihydrogen phosphate, diammonium phosphate, dipotassium hydrogen phosphate, calcium hydrogen phosphate, tricalcium phosphate, tripotassium phosphate, tertiary sodium phosphate, sodium hexameta phosphate, sodium tripolyphosphate, sodium dihydrogen phosphate, disodium hydrogen phosphate.
6. a kind of milk product improving sleep as claimed in claim 1, wherein, described raw material farther includes thickening agent 0.003 to 0.03 weight portion, and described thickening agent is from the combination of one or more in sodium carboxymethyl cellulose, carrageenan, gelatin, microcrystalline Cellulose, gellan gum, xanthan gum, propylene glycol alginate, Konjac glucomannan, agar, locust bean gum, guar gum and pectin.
7. the preparation method of a kind of milk product improving sleep as claimed in claim 1, it is characterised in that:
Take described vitamin E, take the part milk of vitamin E weight 30 to 50 times, by described part Milk During Heating to 70-75 DEG C, form the first feed liquid with vitamin E described in the part milk dissolving after heating；
Taking remaining milk, stirring is also slowly warmed up to 40-45 DEG C, is added by other raw material, and mix and blend forms the second feed liquid, then described second feed liquid is warmed up to 70-75 DEG C；
Described first feed liquid and the second feed liquid are mixed to form the 3rd feed liquid keep 10-20 minute at 70-75 DEG C, fully dissolve；
Blending tank is squeezed into after described 3rd feed liquid is cooled to 0-20 DEG C.
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| US11554162B2 (en) | 2018-03-14 | 2023-01-17 | Kolfarma S.R.L. | Pharmaceutical or food supplement preparation based on alpha-lactalbumin |
| CN109349645A (en) * | 2018-10-30 | 2019-02-19 | 广州普维君健药业有限公司 | Probiotic composition, health food and its preparation method and application |
| CN112616929A (en) * | 2020-11-24 | 2021-04-09 | 本溪木兰花乳业有限责任公司 | Milk product beneficial to sleep and preparation method thereof |
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