CN105734187B - A kind of fragrant leather care products and its preparation method and application - Google Patents
A kind of fragrant leather care products and its preparation method and application Download PDFInfo
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- CN105734187B CN105734187B CN201610110763.0A CN201610110763A CN105734187B CN 105734187 B CN105734187 B CN 105734187B CN 201610110763 A CN201610110763 A CN 201610110763A CN 105734187 B CN105734187 B CN 105734187B
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- C—CHEMISTRY; METALLURGY
- C14—SKINS; HIDES; PELTS; LEATHER
- C14C—CHEMICAL TREATMENT OF HIDES, SKINS OR LEATHER, e.g. TANNING, IMPREGNATING, FINISHING; APPARATUS THEREFOR; COMPOSITIONS FOR TANNING
- C14C11/00—Surface finishing of leather
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Abstract
The invention discloses a kind of fragrant leather care products, calculate, be made up of 1.25 4.90 parts of methyl hydroxybenzoate, 0.90 2.08 parts of monoglyceride, 5.30 6.83 parts of white oil, 3.90 4.90 parts of stearic acid, 3.60 6.42 parts of lanolin, 4.90 5.95 parts of dimethicone, 5.66 8.88 parts of sulfated castor oil, 48 parts of thyme essential oil, 15 parts of nano silver colloidal sol and 50.27 67.97 parts of deionized water by weight.Purposes present invention also offers the preparation method of above-mentioned fragrant leather care products and in nursing corium fabricated product.The present invention is compounded using different greases, and adds thyme essential oil and nano silver colloidal sol, finally prepares the aqueous leather care products of fragrant antimicrobial.Fragrant leather care products prepared by the present invention can make leather surface smooth soft bright, assign fragrance, improve antibiotic property.
Description
Technical field
The invention belongs to chemical field, be related to a kind of leather care products, specifically a kind of fragrant leather care products and
Its preparation method and application.
Background technology
Appeared in as the improvement of people's living standards, corium fabricated product is more and more in life, the nursing to leather
Maintenance also turns into required.Corium fabricated product as natural polymer converted products, rich in collagenic protein and fat
Fat, Long Term Contact air, the easy rough wear in surface, smoothness declines, it is necessary to periodically nursing.Contact mould because it is exposed in air
Bacterium spore, easily produces mould, mildew occurs；And grease easily occurs oxidation and produces peculiar smell.All it is in existing leather nursing product
Add a large amount of greases and moisten leather surface, increase brightness.To go to eliminate the unusual smell, in bating agent, environment-friendly type care agent and skin
Remove from office and the oil-control smells such as lemon, clove oil are added in preservative, assign leather fragrance.But the fragrance essence of existing report
Oil does not have antibiotic property, it is impossible to leather is carried out antibacterial.Nano silver colloidal sol is the argent simple substance that particle diameter is less than 100nm, right
About 650 various bacterias have spectrum bactericidal action.At present the packaging nanometer of molecule is prepared using chitosan and silver nitrate as raw material
Silver-colored leather fungicide, obtains certain fungistatic effect, but manufacture craft is cumbersome, takes 10-20h, and price is costly.With this
Meanwhile, leather itself still suffers from grease smell.
The content of the invention
For above-mentioned technical problem of the prior art, the invention provides a kind of fragrant leather care products and its preparation side
Method and application, described this fragrant leather care products and its preparation method and application will solve leather nursing of the prior art
The technical problem that agent complex manufacturing technology, antibacterial effect be not good and leather itself grease gas is heavier.
The invention provides a kind of fragrant leather care products, calculate by weight, it is constituted and content is as follows：
1.25-4.90 parts of methyl hydroxybenzoate；
0.90-2.08 parts of monoglyceride；
5.30-6.83 parts of white oil；
3.90-4.90 parts of stearic acid；
3.60-6.42 parts of lanolin；
4.90-5.95 parts of dimethicone；
5.66-8.88 parts of sulfated castor oil；
4.00-8.00 parts of thyme essential oil；
1.00-5.00 parts of Nano Silver；
50.27-67.97 parts of deionized water.
Further, a kind of above-mentioned fragrant leather care products, are calculated by weight, and it is constituted and content is as follows：
1.25 parts of methyl hydroxybenzoate；
0.90 part of monoglyceride；
5.58 parts of white oil；
3.90 parts of stearic acid；
3.60 parts of lanolin；
4.90 parts of dimethicone；
6.90 parts of sulfated castor oil；
4.00 parts of thyme essential oil；
1.00 parts of Nano Silver；
67.97 parts of deionized water.
Further, a kind of above-mentioned fragrant leather care products, are calculated by weight, and it is constituted and content is as follows：
4.90 parts of methyl hydroxybenzoate；
1.65 parts of monoglyceride；
6.83 parts of white oil；
4.90 parts of stearic acid；
4.25 parts of lanolin；
5.32 parts of dimethicone；
8.88 parts of sulfated castor oil；
8.00 parts of thyme essential oil；
5.00 parts of Nano Silver；
50.27 parts of deionized water.
Further, a kind of above-mentioned fragrant leather care products, are calculated by weight, and it is constituted and content is as follows：
4.02 parts of methyl hydroxybenzoate；
2.08 parts of monoglyceride；
5.30 parts of white oil；
4.20 parts of stearic acid；
6.42 parts of lanolin；
5.32 parts of dimethicone；
5.66 parts of sulfated castor oil；
5.00 parts of thyme essential oil；
2.50 parts of Nano Silver；
59.50 parts of deionized water.
Further, a kind of above-mentioned fragrant leather care products, are calculated by weight, and it is constituted and content is as follows：
2.45 parts of methyl hydroxybenzoate；
1.49 parts of monoglyceride；
6.83 parts of white oil；
4.08 parts of stearic acid；
4.15 parts of lanolin；
5.95 parts of dimethicone；
8.55 parts of sulfated castor oil；
6.00 parts of thyme essential oil；
3.00 parts of Nano Silver；
57.50 parts of deionized water.
Further, a kind of above-mentioned fragrant leather care products, are calculated by weight, and it is constituted and content is as follows：
3.70 parts of methyl hydroxybenzoate；
0.90 part of monoglyceride；
5.88 parts of white oil；
4.36 parts of stearic acid；
3.72 parts of lanolin；
5.14 parts of dimethicone；
8.86 parts of sulfated castor oil；
7.00 parts of thyme essential oil；
4.00 parts of Nano Silver；
56.44 parts of deionized water.
Present invention also offers a kind of preparation method of above-mentioned fragrant leather care products, comprise the following steps：
1）Methyl hydroxybenzoate, monoglyceride, white oil, stearic acid, lanolin, dimethicone, sulphur are weighed according to parts by weight
It is acidified castor oil, thyme essential oil, Nano Silver and deionized water；
2）Methyl hydroxybenzoate, monoglyceride, white oil, stearic acid, lanolin, dimethicone, sulfated castor oil are mixed
And heated, 70-85 DEG C is warming up to, liquid fat mixture is obtained；
3）Deionized water is heated to 70-85 DEG C, in rotating speed under 400-450r/min stirring condition, addition is walked
Rapid 2）In obtained liquid fat mixture, lasting stirring；
4）By step 3）When the mixed liquor of acquisition is down to 25-30 DEG C with whipping process natural cooling, temperature, add respectively successively
Enter thyme essential oil and Nano Silver, persistently stir 40-60min, obtain fragrant leather care products.
Present invention also offers purposes of the above-mentioned fragrant leather care products in nursing corium fabricated product.
Further, described corium fabricated product is fur clothing, leather shoes, suitcase or corium sofa.
The present invention is compounded using different greases, and adds thyme essential oil and nano silver colloidal sol, utilizes thyme
The characteristics of essential oil takes into account armaticity and antibiotic property as pungent note essential oil, finally prepares the aqueous leather care products of fragrant antimicrobial.
Fragrant leather care products prepared by the present invention can make leather surface smooth soft bright, assign fragrance, improve antibiotic property.The present invention will
Fragrant leather care products are applied to leather surface and being allowed to penetrate into leather nexine, grease can make leather surface smooth soft bright, and
Nano silver colloidal sol and thyme essential oil play its synergy and play antibacterial action jointly.
The present invention is compared with prior art, and its technological progress is significant.A kind of fragrant leather care products of the present invention, by
In rich in grease, its brightness can be increased after leather surface is smeared；Thyme essential oil has medicinal herbs fragrance, and fragrance makes one pleased
It is happy, and the antibiotic property of itself can effectively suppress the growth of leather surface mould with nano silver colloidal sol synergy, extension leather
Service life.
Embodiment
The present invention is described in further detail below by embodiment, but is not intended to limit the present invention：
Embodiment 1
A kind of fragrant leather care products, are calculated by weight, and it is constituted and content is as follows：
1.25 parts of methyl hydroxybenzoate；
0.90 part of monoglyceride；
5.58 parts of white oil；
3.90 parts of stearic acid；
3.60 parts of lanolin；
4.90 parts of dimethicone；
6.90 parts of sulfated castor oil；
4.00 parts of thyme essential oil；
1.00 parts of Nano Silver；
67.97 parts of deionized water.
The preparation method of above-mentioned fragrant leather care products, specifically includes following steps：
（1）By 1.25 parts of methyl hydroxybenzoates, 0.90 part of monoglyceride, 5.58 parts of white oils, 3.90 parts of stearic acid, 3.60 parts of wools
Fat, 4.90 parts of dimethicones, 6.90 parts of sulfated castor oils are mixed and heated, and are warming up to 80 DEG C and are obtained liquid fat mixing
Thing.
（2）67.97 parts of deionized waters are heated to 80 DEG C, magneton is added and is placed on magnetic stirring apparatus, be in rotating speed
Under conditions of 400r/min, it is rapidly added（1）In obtained liquid fat mixture, lasting stirring.
（3）When liquid to be mixed is down to 25 DEG C with whipping process natural cooling, temperature, with 3mL/min rate of addition successively
4.00 parts of thyme essential oils and 1.00 parts of Nano Silvers are separately added into, 40min is persistently stirred, fragrant leather care products are obtained.
Above-mentioned fragrant leather care products are nursed to leather and antibiotic property test is carried out, compare inhibition zone to judge
Fragrant leather care products are strong and weak to the antibiotic effect of leather.
Above-mentioned fragrant leather care products are used for the processing of leather, comprised the following steps that：
Under the conditions of 25 DEG C, using ammoniacal liquor washleather surface, after drying naturally, the fragrant leather care products of 0.05g are taken to apply
In a diameter of 25mm leather surface, that is, obtain with the treated leather of fragrant leather care products.
The above-mentioned leather treated through fragrant leather care products is carried out below fragrant antimicrobial measure of merit, step：
（1）Take concentration containing strain be 107~108CFU/ml production aspergillus flavus, Penicillium citreo-viride, aspergillus niger, Escherichia coli and
The bacteria suspension 0.5ml of staphylococcus aureus is uniformly coated on the solid medium of beef extract-peptone, and flat board containing bacterium is made；
（2）By step（1）It is middle handled through fragrant care agent after leather, take a diameter of 25mm untreated leather conduct
Reference, takes three groups of Duplicate Samples respectively, and all leather samples are carried out into ultraviolet irradiation in biological aseptic operating platform, and sterilize 30min；
（3）By step（2）In sterilized fragrant leather and common leather be respectively placed in step（1）In flat board containing bacterium on
Cultivated in 28 DEG C of constant incubators；
（4）It is put into incubator to rise every 24h observations once, the antibacterial circle diameter for recording and producing fragrant leather subtracts general
The antibacterial circle diameter that logical leather is produced, parallel determination three times is averaged as the antibacterial effect data of the fragrant leather.
Test result is shown：Common leather sample covers with mould after placing 8 days；The skin treated through fragrant leather care products
Leather antibacterial circle diameter under production aspergillus flavus environment reaches antibacterial circle diameter under 3mm, Penicillium citreo-viride environment and reached under 10mm, aspergillus niger environment
Antibacterial circle diameter reaches antibacterial circle diameter under 3mm, Escherichia coli environment and reaches antibacterial circle diameter under 6mm, staphylococcus aureus environment
Up to 16mm.
Embodiment 2：
A kind of fragrant leather care products, are calculated by weight, and it is constituted and content is as follows：
4.90 parts of methyl hydroxybenzoate；
1.65 parts of monoglyceride；
6.83 parts of white oil；
4.90 parts of stearic acid；
4.25 parts of lanolin；
5.32 parts of dimethicone；
8.88 parts of sulfated castor oil；
8.00 parts of thyme essential oil；
5.00 parts of Nano Silver；
50.27 parts of deionized water.
（1）By 4.90 parts of methyl hydroxybenzoates, 1.65 parts of monoglycerides, 6.83 parts of white oils, 4.90 parts of stearic acid, 4.25 parts of wools
Fat, 5.32 parts of dimethicones, 8.88 parts of sulfated castor oils are mixed and heated, and are warming up to 80 DEG C and are obtained liquid fat mixing
Thing.
（2）50.27 parts of deionized waters are heated to 80 DEG C, magneton is added and is placed on magnetic stirring apparatus, be in rotating speed
Under conditions of 400r/min, it is rapidly added（1）In obtained liquid fat mixture, lasting stirring.
（3）When liquid to be mixed is down to 25 DEG C with whipping process natural cooling, temperature, with 3mL/min rate of addition successively
8.00 parts of thyme essential oils and 5.00 parts of Nano Silvers are separately added into, 40min is persistently stirred, fragrant leather care products are obtained.
Above-mentioned fragrant leather care products are nursed to leather and antibiotic property test is carried out, compare inhibition zone to judge
Fragrant leather care products are strong and weak to the antibiotic effect of leather.
Test result is shown：Common leather sample covers with mould after placing 8 days；The skin treated through fragrant leather care products
Leather antibacterial circle diameter under production aspergillus flavus environment reaches antibacterial circle diameter under 5mm, Penicillium citreo-viride environment and reached under 14mm, aspergillus niger environment
Antibacterial circle diameter reaches 12mm, and to reach inhibition zone under 12mm, staphylococcus aureus environment straight for antibacterial circle diameter under Escherichia coli environment
Footpath reaches 29mm.
Embodiment 3：
A kind of fragrant leather care products, are calculated by weight, and it is constituted and content is as follows：
4.02 parts of methyl hydroxybenzoate；
2.08 parts of monoglyceride；
5.30 parts of white oil；
4.20 parts of stearic acid；
6.42 parts of lanolin；
5.32 parts of dimethicone；
5.66 parts of sulfated castor oil；
5.00 parts of thyme essential oil；
2.50 parts of Nano Silver；
59.50 parts of deionized water.
（1）By 4.02 parts of methyl hydroxybenzoates, 2.08 parts of monoglycerides, 5.30 parts of white oils, 4.20 parts of stearic acid, 6.42 parts of wools
Fat, 5.32 parts of dimethicones, 5.66 parts of sulfated castor oils are mixed and heated, and are warming up to 80 DEG C and are obtained liquid fat mixing
Thing.
（2）59.50 parts of deionized waters are heated to 80 DEG C, magneton is added and is placed on magnetic stirring apparatus, be in rotating speed
Under conditions of 400r/min, it is rapidly added（1）In obtained liquid fat mixture, lasting stirring.
（3）When liquid to be mixed is down to 25 DEG C with whipping process natural cooling, temperature, with 3mL/min rate of addition successively
5.00 parts of thyme essential oils and 2.50 parts of Nano Silvers are separately added into, 40min is persistently stirred, fragrant leather care products are obtained.
Corium fabricated product is nursed using the fragrant leather nursing frost of above-mentioned gained, corium fabricated product includes：
Leather shoes, suitcase and corium sofa etc..
Above-mentioned fragrant leather care products are nursed to leather and antibiotic property test is carried out, compare inhibition zone to judge
Fragrant leather care products are strong and weak to the antibiotic effect of leather.
Test result is shown：Common leather sample covers with mould after placing 8 days；The skin treated through fragrant leather care products
Leather antibacterial circle diameter under production aspergillus flavus environment reaches antibacterial circle diameter under 3mm, Penicillium citreo-viride environment and reached under 20mm, aspergillus niger environment
Antibacterial circle diameter reaches 10mm, and to reach inhibition zone under 10mm, staphylococcus aureus environment straight for antibacterial circle diameter under Escherichia coli environment
Footpath reaches 37mm.
Embodiment 4：
A kind of fragrant leather care products, are calculated by weight, and it is constituted and content is as follows：
2.45 parts of methyl hydroxybenzoate；
1.49 parts of monoglyceride；
6.83 parts of white oil；
4.08 parts of stearic acid；
4.15 parts of lanolin；
5.95 parts of dimethicone；
8.55 parts of sulfated castor oil；
6.00 parts of thyme essential oil；
3.00 parts of Nano Silver；
57.50 parts of deionized water.
（1）By 2.45 parts of methyl hydroxybenzoates, 1.49 portions of monoglycerides, 6.83 portions of white oils, 4. 08 portions of stearic acid, 4.15 portions of sheep
Hair fat, 5.95 parts of dimethicones, 8.55 parts of sulfated castor oils mixs and heated, be warming up to 80 DEG C liquid fat is mixed
Compound.
（2）57.50 parts of deionized waters are heated to 80 DEG C, magneton is added and is placed on magnetic stirring apparatus, be in rotating speed
Under conditions of 400r/min, it is rapidly added（1）In obtained liquid fat mixture, lasting stirring.
（3）When liquid to be mixed is down to 25 DEG C with whipping process natural cooling, temperature, with 3mL/min rate of addition successively
6.00 parts of thyme essential oils and 3.00 parts of Nano Silvers are separately added into, 40min is persistently stirred, fragrant leather care products are obtained.
Above-mentioned fragrant leather care products are nursed to leather and antibiotic property test is carried out, compare inhibition zone to judge
Fragrant leather care products are strong and weak to the antibiotic effect of leather.
Test result is shown：Common leather sample covers with mould after placing 8 days；The skin treated through fragrant leather care products
Leather antibacterial circle diameter under production aspergillus flavus environment reaches antibacterial circle diameter under 4mm, Penicillium citreo-viride environment and reached under 36mm, aspergillus niger environment
Antibacterial circle diameter reaches antibacterial circle diameter under 8mm, Escherichia coli environment and reaches antibacterial circle diameter under 12mm, staphylococcus aureus environment
Up to 58mm.
Embodiment 5：
A kind of fragrant leather care products, are calculated by weight, and it is constituted and content is as follows：
3.70 parts of methyl hydroxybenzoate；
0.90 part of monoglyceride；
5.88 parts of white oil；
4.36 parts of stearic acid；
3.72 parts of lanolin；
5.14 parts of dimethicone；
8.86 parts of sulfated castor oil；
7.00 parts of thyme essential oil；
4.00 parts of Nano Silver；
56.44 parts of deionized water.
1）By 3.70 parts of methyl hydroxybenzoates, 0.90 part of monoglyceride, 5.88 parts of white oils, 4.36 parts of stearic acid, 3.72 parts of wools
Fat, 5.14 parts of dimethicones, 8.86 parts of sulfated castor oils are mixed and heated, and are warming up to 80 DEG C and are obtained liquid fat mixing
Thing.
（2）56.44 parts of deionized waters are heated to 80 DEG C, magneton is added and is placed on magnetic stirring apparatus, be in rotating speed
Under conditions of 400r/min, it is rapidly added（1）In obtained liquid fat mixture, lasting stirring.
（3）When liquid to be mixed is down to 25 DEG C with whipping process natural cooling, temperature, with 3mL/min rate of addition successively
7.00 parts of thyme essential oils and 4.00 parts of Nano Silvers are separately added into, 40min is persistently stirred, fragrant leather care products are obtained.
Above-mentioned fragrant leather care products are nursed to leather and antibiotic property test is carried out, compare inhibition zone to judge
Fragrant leather care products are strong and weak to the antibiotic effect of leather.
Test result is shown：Common leather sample covers with mould after placing 8 days；The skin treated through fragrant leather care products
Leather antibacterial circle diameter under production aspergillus flavus environment reaches antibacterial circle diameter under 2mm, Penicillium citreo-viride environment and reached under 10mm, aspergillus niger environment
Antibacterial circle diameter reaches antibacterial circle diameter under 9mm, Escherichia coli environment and reaches antibacterial circle diameter under 8mm, staphylococcus aureus environment
Up to 12mm.
Corium fabricated product leather leather surface after the present invention is smeared substantially becomes smooth soft bright, soft；Leather
Give out the peculiar fragrance of thyme essential oil.The present invention is directed to Escherichia coli, staphylococcus aureus, yellowish green aspergillus, production respectively
Aspergillus flavus and aspergillus niger carry out antibiotic property experiment, and experiment leather produces inhibition zone and shows that the present invention has well to above mould
Antibiotic property, especially to staphylococcus aureus and yellowish green aspergillus.
Claims (2)
1. a kind of fragrant leather care products, it is characterised in that calculate by weight, it is constituted and content is as follows：
1.25-4.90 parts of methyl hydroxybenzoate；
0.90-2.08 parts of monoglyceride；
5.30-6.83 parts of white oil；
3.90-4.90 parts of stearic acid；
3.60-6.42 parts of lanolin；
4.90-5.95 parts of dimethicone；
5.66-8.88 parts of sulfated castor oil；
4.00-8.00 parts of thyme essential oil；
1.00-5.00 parts of Nano Silver；
50.27-67.97 parts of deionized water；
A kind of preparation method of above-mentioned fragrant leather care products, comprises the following steps：
1）Methyl hydroxybenzoate, monoglyceride, white oil, stearic acid, lanolin, dimethicone, sulphation are weighed according to parts by weight
Castor oil, thyme essential oil, Nano Silver and deionized water；
2）Methyl hydroxybenzoate, monoglyceride, white oil, stearic acid, lanolin, dimethicone, sulfated castor oil are mixed and gone forward side by side
Row heating, is warming up to 70-85 DEG C and obtains liquid fat mixture；
3）Deionized water is heated to 70-85 DEG C, in the case where rotating speed is 400-450r/min stirring condition, step 2 is added）
In obtained liquid fat mixture, lasting stirring；
4）By step 3）When the mixed liquor of acquisition is down to 25-30 DEG C with whipping process natural cooling, temperature, hundred are separately added into successively
In essential oil and Nano Silver, persistently stir 40-60min, obtain fragrant leather care products.
2. purposes of the fragrant leather care products in nursing corium fabricated product described in claim 1, described corium processing
Product is fur clothing, leather shoes, suitcase or corium sofa.
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Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN108379211A (en) * | 2018-05-24 | 2018-08-10 | 长沙小如信息科技有限公司 | A kind of dental care liquid and preparation method thereof |
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| Publication number | Priority date | Publication date | Assignee | Title |
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| CN108396083A (en) * | 2018-02-26 | 2018-08-14 | 合肥远科服装设计有限公司 | A kind of environmental-friendly leather care agent and preparation method thereof |
| CN108456756A (en) * | 2018-03-14 | 2018-08-28 | 合肥远科服装设计有限公司 | A kind of wrinkle resistant antibacterial fragrant care agent of fur clothing |
| CN108265136B (en) * | 2018-03-23 | 2021-01-26 | 长沙小新新能源科技有限公司 | Leather care agent and preparation method thereof |
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| Publication number | Priority date | Publication date | Assignee | Title |
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| JPH0768560B2 (en) * | 1991-05-13 | 1995-07-26 | 寛純 角 | How to make leather waterproof and water repellent |
| CN1131321C (en) * | 1999-09-03 | 2003-12-17 | 刘京刚 | Leather beautifying cream |
| CA2650596A1 (en) * | 2006-04-28 | 2007-11-08 | Buckman Laboratories International, Inc. | Fungicidal compositions and methods of using the same |
| CN101403019A (en) * | 2008-10-31 | 2009-04-08 | 刘庆刚 | Leather maintaining cosmetic |
| CN102994665A (en) * | 2012-12-05 | 2013-03-27 | 袁辉 | Environment-friendly leather caring agent |
| CN103691967B (en) * | 2014-01-09 | 2016-01-27 | 三河市京纳环保技术有限公司 | A kind of simple method for preparing of novel extensive nano-silver hydrosol |
| CN104878136A (en) * | 2015-05-20 | 2015-09-02 | 周淑华 | Leather maintenance agent and preparation method thereof |
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| CN108379211A (en) * | 2018-05-24 | 2018-08-10 | 长沙小如信息科技有限公司 | A kind of dental care liquid and preparation method thereof |
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