CN105725161B - A kind of allotment type flavoring apple essence and preparation method thereof - Google Patents
A kind of allotment type flavoring apple essence and preparation method thereof Download PDFInfo
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- CN105725161B CN105725161B CN201610089090.5A CN201610089090A CN105725161B CN 105725161 B CN105725161 B CN 105725161B CN 201610089090 A CN201610089090 A CN 201610089090A CN 105725161 B CN105725161 B CN 105725161B
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- XINCECQTMHSORG-UHFFFAOYSA-N Isoamyl isovalerate Chemical compound CC(C)CCOC(=O)CC(C)C XINCECQTMHSORG-UHFFFAOYSA-N 0.000 title claims abstract description 28
- 238000002360 preparation method Methods 0.000 title claims abstract description 14
- QTBSBXVTEAMEQO-UHFFFAOYSA-N Acetic acid Chemical compound CC(O)=O QTBSBXVTEAMEQO-UHFFFAOYSA-N 0.000 claims abstract description 33
- DNIAPMSPPWPWGF-UHFFFAOYSA-N Propylene glycol Chemical compound CC(O)CO DNIAPMSPPWPWGF-UHFFFAOYSA-N 0.000 claims abstract description 33
- LRHPLDYGYMQRHN-UHFFFAOYSA-N N-Butanol Chemical compound CCCCO LRHPLDYGYMQRHN-UHFFFAOYSA-N 0.000 claims abstract description 18
- HCRBXQFHJMCTLF-ZCFIWIBFSA-N ethyl (2r)-2-methylbutanoate Chemical compound CCOC(=O)[C@H](C)CC HCRBXQFHJMCTLF-ZCFIWIBFSA-N 0.000 claims abstract description 18
- ZSIAUFGUXNUGDI-UHFFFAOYSA-N hexan-1-ol Chemical compound CCCCCCO ZSIAUFGUXNUGDI-UHFFFAOYSA-N 0.000 claims abstract description 18
- JARKCYVAAOWBJS-UHFFFAOYSA-N hexanal Chemical compound CCCCCC=O JARKCYVAAOWBJS-UHFFFAOYSA-N 0.000 claims abstract description 18
- AOGQPLXWSUTHQB-UHFFFAOYSA-N hexyl acetate Chemical compound CCCCCCOC(C)=O AOGQPLXWSUTHQB-UHFFFAOYSA-N 0.000 claims abstract description 18
- MLFHJEHSLIIPHL-UHFFFAOYSA-N isoamyl acetate Chemical compound CC(C)CCOC(C)=O MLFHJEHSLIIPHL-UHFFFAOYSA-N 0.000 claims abstract description 18
- ZCHHRLHTBGRGOT-SNAWJCMRSA-N (E)-hex-2-en-1-ol Chemical compound CCC\C=C\CO ZCHHRLHTBGRGOT-SNAWJCMRSA-N 0.000 claims abstract description 17
- UFLHIIWVXFIJGU-ARJAWSKDSA-N (Z)-hex-3-en-1-ol Chemical compound CC\C=C/CCO UFLHIIWVXFIJGU-ARJAWSKDSA-N 0.000 claims abstract description 11
- WLAMNBDJUVNPJU-UHFFFAOYSA-N 2-methylbutyric acid Chemical compound CCC(C)C(O)=O WLAMNBDJUVNPJU-UHFFFAOYSA-N 0.000 claims abstract description 11
- UAXOELSVPTZZQG-UHFFFAOYSA-N tiglic acid Natural products CC(C)=C(C)C(O)=O UAXOELSVPTZZQG-UHFFFAOYSA-N 0.000 claims abstract description 11
- PPXUHEORWJQRHJ-UHFFFAOYSA-N ethyl isovalerate Chemical compound CCOC(=O)CC(C)C PPXUHEORWJQRHJ-UHFFFAOYSA-N 0.000 claims abstract description 10
- 239000002904 solvent Substances 0.000 claims abstract description 10
- HNAGHMKIPMKKBB-UHFFFAOYSA-N 1-benzylpyrrolidine-3-carboxamide Chemical compound C1C(C(=O)N)CCN1CC1=CC=CC=C1 HNAGHMKIPMKKBB-UHFFFAOYSA-N 0.000 claims abstract description 9
- 150000001299 aldehydes Chemical class 0.000 claims abstract description 9
- OBNCKNCVKJNDBV-UHFFFAOYSA-N butanoic acid ethyl ester Natural products CCCC(=O)OCC OBNCKNCVKJNDBV-UHFFFAOYSA-N 0.000 claims abstract description 9
- 239000001813 ethyl (2R)-2-methylbutanoate Substances 0.000 claims abstract description 9
- 229940090910 ethyl 2-methylbutyrate Drugs 0.000 claims abstract description 9
- 229940117955 isoamyl acetate Drugs 0.000 claims abstract description 9
- 125000001972 isopentyl group Chemical group [H]C([H])([H])C([H])(C([H])([H])[H])C([H])([H])C([H])([H])* 0.000 claims abstract description 7
- 239000000203 mixture Substances 0.000 claims description 10
- 239000003205 fragrance Substances 0.000 abstract description 7
- 238000000034 method Methods 0.000 description 8
- 239000000686 essence Substances 0.000 description 5
- XYHKNCXZYYTLRG-UHFFFAOYSA-N 1h-imidazole-2-carbaldehyde Chemical compound O=CC1=NC=CN1 XYHKNCXZYYTLRG-UHFFFAOYSA-N 0.000 description 4
- GWYFCOCPABKNJV-UHFFFAOYSA-M 3-Methylbutanoic acid Natural products CC(C)CC([O-])=O GWYFCOCPABKNJV-UHFFFAOYSA-M 0.000 description 4
- GWYFCOCPABKNJV-UHFFFAOYSA-N beta-methyl-butyric acid Natural products CC(C)CC(O)=O GWYFCOCPABKNJV-UHFFFAOYSA-N 0.000 description 4
- 150000002148 esters Chemical class 0.000 description 4
- 239000007788 liquid Substances 0.000 description 4
- 239000002304 perfume Substances 0.000 description 4
- 235000016709 nutrition Nutrition 0.000 description 3
- 239000000126 substance Substances 0.000 description 3
- HVYWMOMLDIMFJA-DPAQBDIFSA-N cholesterol Chemical compound C1C=C2C[C@@H](O)CC[C@]2(C)[C@@H]2[C@@H]1[C@@H]1CC[C@H]([C@H](C)CCCC(C)C)[C@@]1(C)CC2 HVYWMOMLDIMFJA-DPAQBDIFSA-N 0.000 description 2
- 230000000694 effects Effects 0.000 description 2
- 235000020052 applejack Nutrition 0.000 description 1
- 235000013361 beverage Nutrition 0.000 description 1
- 210000004720 cerebrum Anatomy 0.000 description 1
- 239000003795 chemical substances by application Substances 0.000 description 1
- 235000012000 cholesterol Nutrition 0.000 description 1
- 235000013399 edible fruits Nutrition 0.000 description 1
- 230000002526 effect on cardiovascular system Effects 0.000 description 1
- 239000000796 flavoring agent Substances 0.000 description 1
- 235000019634 flavors Nutrition 0.000 description 1
- 235000013305 food Nutrition 0.000 description 1
- 239000004615 ingredient Substances 0.000 description 1
- 238000004519 manufacturing process Methods 0.000 description 1
- 230000035764 nutrition Effects 0.000 description 1
- 239000002994 raw material Substances 0.000 description 1
- 230000033764 rhythmic process Effects 0.000 description 1
- 230000002557 soporific effect Effects 0.000 description 1
- 230000009466 transformation Effects 0.000 description 1
- 239000000052 vinegar Substances 0.000 description 1
- 235000021419 vinegar Nutrition 0.000 description 1
- 239000011782 vitamin Substances 0.000 description 1
- 229940088594 vitamin Drugs 0.000 description 1
- 229930003231 vitamin Natural products 0.000 description 1
- 235000013343 vitamin Nutrition 0.000 description 1
- 150000003722 vitamin derivatives Chemical class 0.000 description 1
Classifications
-
- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23V—INDEXING SCHEME RELATING TO FOODS, FOODSTUFFS OR NON-ALCOHOLIC BEVERAGES AND LACTIC OR PROPIONIC ACID BACTERIA USED IN FOODSTUFFS OR FOOD PREPARATION
- A23V2002/00—Food compositions, function of food ingredients or processes for food or foodstuffs
Landscapes
- Fats And Perfumes (AREA)
- Seasonings (AREA)
Abstract
The invention discloses a kind of allotment type flavoring apple essence, the acetic acid solution and solvent propylene glycol that 2-Methyl Butyric Acid solution that the leaf-alcohol solution for being 10% by hexanal, trans- 2- hexenoic aldehyde, ethyl butyrate, ethyl 2-methylbutyrate, ethyl isovalerate, isoamyl acetate, iso-amyl iso-valeriate, hexyl acetate, butanol, hexanol, mass percent concentration, trans- 2- hexenol, mass percent concentration are 10%, mass percent concentration are 10% are formed.The present invention also provides the preparation method of above-mentioned allotment type flavoring apple essence, the present invention deploy according to naturally apple-flavored, and obtained flavoring apple essence gives off a strong fragrance, is natural true to nature.
Description
Technical field
The invention belongs to flavour of food products fields, are related to a kind of essence more particularly to a kind of fumet or fruity agent, specific next
Say it is a kind of allotment type flavoring apple essence and preparation method thereof.
Background technique
Apple is one of highest healthy fruit of generally acknowledged nutritional profile, and full of nutrition, pleasant aroma contains lot of trace
The nutritional ingredient of a variety of needed by human body such as element and vitamin can reduce cholesterol, and protection is cardiovascular, has cerebrum tonifying blood-nourishing, allays excitement
Soporific function.Fragrance specific to apple is quite liked by people, therefore prepares allotment type flavoring apple essence, simulates the natural perfume of apple
Gas has very important significance, it may be used on apple beverage, in the production process of applejack and apple vinegar, can have
Effect improves the fragrance and mouthfeel of product, promotes value-added content of product.
Summary of the invention
For above-mentioned technology in the prior art, the present invention provides a kind of allotment type flavoring apple essence and preparation method thereof,
Described this allotment type flavoring apple essence and preparation method thereof solves that fragrance in the prior art is uncoordinated, unlifelike technology
Problem.
The present invention provides a kind of allotment type flavoring apple essences, and count by weight percentage, composition and content are as follows:
Wherein, the 2-Methyl Butyric Acid that mass percent concentration is 10% leaf-alcohol solution, mass percent concentration are 10%
Solution, mass percent concentration are that the solvent in 10% acetic acid solution is propylene glycol.
The present invention also provides a kind of preparation methods of above-mentioned allotment type flavoring apple essence, include the following steps:
1) hexanal, trans- 2- hexenoic aldehyde, ethyl butyrate, ethyl 2-methylbutyrate, isovaleric acid second are weighed according to mass percent
Ester, isoamyl acetate, iso-amyl iso-valeriate, hexyl acetate, butanol, hexanol, mass percent concentration be 10% leaf-alcohol solution,
The acetic acid that 2-Methyl Butyric Acid solution that trans- 2- hexenol, mass percent concentration are 10%, mass percent concentration are 10% is molten
Liquid and solvent propylene glycol；
2) by hexanal, trans- 2- hexenoic aldehyde, ethyl butyrate, ethyl 2-methylbutyrate, ethyl isovalerate, isoamyl acetate, different
Isoamyl isovalerate, hexyl acetate, butanol, hexanol, the leaf-alcohol solution that mass percent concentration is 10%, trans- 2- hexenol, quality
The acetic acid solution and solvent propylene glycol that 2-Methyl Butyric Acid solution that percent concentration is 10%, mass percent concentration are 10% are equal
It is even to mix to get flavoring apple essence is arrived.
The present invention chooses suitable raw material according to the odor characteristic of natural apple and note structure, modulate give off a strong fragrance,
Fine and smooth, natural flavoring apple essence true to nature.
The present invention is compared with prior art, and technological progress is significant.Flavoring apple essence of the invention is according to natural apple
Made of fruity rhythm is deployed, there is the features such as fidelity is high, good application effect.
Specific embodiment
Embodiment 1
A kind of allotment type flavoring apple essence, count by weight percentage, composition and content are as follows:
Method preparation is prepared by the following procedure in above-mentioned flavoring apple essence, and specific step is as follows for preparation process:
Hexanal, trans- 2- hexenoic aldehyde, ethyl butyrate, ethyl 2-methylbutyrate, isovaleric acid second are weighed according to mass percent
Ester, isoamyl acetate, iso-amyl iso-valeriate, hexyl acetate, butanol, hexanol, mass percent concentration be 10% leaf-alcohol solution,
The acetic acid that 2-Methyl Butyric Acid solution that trans- 2- hexenol, mass percent concentration are 10%, mass percent concentration are 10% is molten
Liquid and solvent propylene glycol uniformly mix, and then uniformly mix above-mentioned substance to get flavoring apple essence is arrived.Obtained essence fragrance fragrance
Strongly fragrant, the characteristic perfume with apple, natural sense is by force.
Embodiment 2
A kind of allotment type flavoring apple essence, count by weight percentage, composition and content are as follows:
Method preparation is prepared by the following procedure in above-mentioned flavoring apple essence, and specific step is as follows for preparation process:
Hexanal, trans- 2- hexenoic aldehyde, ethyl butyrate, ethyl 2-methylbutyrate, isovaleric acid second are weighed according to mass percent
Ester, isoamyl acetate, iso-amyl iso-valeriate, hexyl acetate, butanol, hexanol, mass percent concentration be 10% leaf-alcohol solution,
The acetic acid that 2-Methyl Butyric Acid solution that trans- 2- hexenol, mass percent concentration are 10%, mass percent concentration are 10% is molten
Then liquid and solvent propylene glycol uniformly mix above-mentioned substance to get flavoring apple essence is arrived.Obtained essence fragrant aroma, has
The characteristic perfume of apple, natural sense are strong.
Embodiment 3
A kind of allotment type flavoring apple essence, count by weight percentage, composition and content are as follows:
Method preparation is prepared by the following procedure in above-mentioned flavoring apple essence, and specific step is as follows for preparation process:
Hexanal, trans- 2- hexenoic aldehyde, ethyl butyrate, ethyl 2-methylbutyrate, isovaleric acid second are weighed according to mass percent
Ester, isoamyl acetate, iso-amyl iso-valeriate, hexyl acetate, butanol, hexanol, mass percent concentration be 10% leaf-alcohol solution,
The acetic acid that 2-Methyl Butyric Acid solution that trans- 2- hexenol, mass percent concentration are 10%, mass percent concentration are 10% is molten
Then liquid and solvent propylene glycol uniformly mix above-mentioned substance to get flavoring apple essence is arrived.Obtained essence fragrant aroma, has
The characteristic perfume of apple, natural sense are strong.
Content belonging to above is only the basic explanation under present inventive concept, and that is done according to the technique and scheme of the present invention appoints
What equivalent transformation, belongs to the scope of protection of the invention.
Claims (2)
1. a kind of allotment type flavoring apple essence, it is characterised in that count by weight percentage, composition and content are as follows:
Hexanal 0.05%-0.2%,
Trans- 2- hexenoic aldehyde 0.05%-0.5%,
Ethyl butyrate 1%-10%,
Ethyl 2-methylbutyrate 0.1%-1%,
Ethyl isovalerate 0.2%-2%,
Isoamyl acetate 0.5%-5%,
Iso-amyl iso-valeriate 0.2%-2%,
Hexyl acetate 0.05%-0.5%,
Butanol 0.1%-1%,
Hexanol 0.1%-0.5%,
The leaf-alcohol solution 0.05%-0.2% that mass percent concentration is 10%,
Trans- 2- hexenol 0.1%-1%,
The 2-Methyl Butyric Acid solution 0.15%-1.5% that mass percent concentration is 10%,
Mass percent concentration is 10% acetic acid solution 0.02%-0.2%,
Propylene glycol surplus；
Wherein, 2-Methyl Butyric Acid solution that mass percent concentration is 10% leaf-alcohol solution, mass percent concentration are 10%, matter
It is propylene glycol that percent concentration, which is measured, as the solvent in 10% acetic acid solution.
2. a kind of preparation method of allotment type flavoring apple essence described in claim 1, it is characterised in that include the following steps:
1) according to mass percent weigh hexanal, trans- 2- hexenoic aldehyde, ethyl butyrate, ethyl 2-methylbutyrate, ethyl isovalerate,
Isoamyl acetate, iso-amyl iso-valeriate, hexyl acetate, butanol, hexanol, the leaf-alcohol solution, trans- that mass percent concentration is 10%
Acetic acid solution that 2-Methyl Butyric Acid solution that 2- hexenol, mass percent concentration are 10%, mass percent concentration are 10% and
Solvent propylene glycol；
2) by hexanal, trans- 2- hexenoic aldehyde, ethyl butyrate, ethyl 2-methylbutyrate, ethyl isovalerate, isoamyl acetate, isovaleric acid
Isopentyl ester, hexyl acetate, butanol, hexanol, the leaf-alcohol solution that mass percent concentration is 10%, trans- 2- hexenol, quality percentage
The acetic acid solution and solvent propylene glycol that 2-Methyl Butyric Acid solution that specific concentration is 10%, mass percent concentration are 10% uniformly mix
It closes to get flavoring apple essence is arrived.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201610089090.5A CN105725161B (en) | 2016-02-17 | 2016-02-17 | A kind of allotment type flavoring apple essence and preparation method thereof |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201610089090.5A CN105725161B (en) | 2016-02-17 | 2016-02-17 | A kind of allotment type flavoring apple essence and preparation method thereof |
Publications (2)
| Publication Number | Publication Date |
|---|---|
| CN105725161A CN105725161A (en) | 2016-07-06 |
| CN105725161B true CN105725161B (en) | 2018-12-14 |
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| Application Number | Title | Priority Date | Filing Date |
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| CN201610089090.5A Active CN105725161B (en) | 2016-02-17 | 2016-02-17 | A kind of allotment type flavoring apple essence and preparation method thereof |
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Families Citing this family (7)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN106520489A (en) * | 2016-11-08 | 2017-03-22 | 上海应用技术大学 | Apple-rose mixed fruit type premade cocktail and preparation method thereof |
| CN107345175A (en) * | 2016-11-30 | 2017-11-14 | 湖北中烟工业有限责任公司 | Apple fragrance type flavouring essence for tobacco and preparation method thereof |
| CN108125204B (en) * | 2017-10-31 | 2021-05-11 | 浙江杭曼食品科技有限公司 | Apple-flavored essence and preparation method thereof |
| CN109674017A (en) * | 2018-12-07 | 2019-04-26 | 沈昌亮 | A kind of flavoring apple essence group and preparation method thereof |
| CN110050982A (en) * | 2019-04-01 | 2019-07-26 | 苏州禾田香料有限公司 | A kind of green apple type edible essence containing the third two acetal of trans- 2- hexenoic aldehyde |
| CN110558603A (en) * | 2019-09-12 | 2019-12-13 | 深圳雾芯科技有限公司 | Flavor composition and electronic cigarette liquid containing same |
| CN114680086B (en) * | 2020-12-25 | 2023-07-04 | 广州百花香料股份有限公司 | Essence for bait |
Citations (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN101779784A (en) * | 2010-01-29 | 2010-07-21 | 上海百润香精香料股份有限公司 | Apple essence formula |
| CN102499360A (en) * | 2011-11-17 | 2012-06-20 | 湖北中烟工业有限责任公司 | Natural apple essence and preparation method thereof |
| CN103320225A (en) * | 2013-06-03 | 2013-09-25 | 吴江市利达上光制品有限公司 | Water-soluble apple essence |
| CN104643003A (en) * | 2015-03-17 | 2015-05-27 | 王婧婧 | Apple essence formula for dairy product |
-
2016
- 2016-02-17 CN CN201610089090.5A patent/CN105725161B/en active Active
Patent Citations (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN101779784A (en) * | 2010-01-29 | 2010-07-21 | 上海百润香精香料股份有限公司 | Apple essence formula |
| CN102499360A (en) * | 2011-11-17 | 2012-06-20 | 湖北中烟工业有限责任公司 | Natural apple essence and preparation method thereof |
| CN103320225A (en) * | 2013-06-03 | 2013-09-25 | 吴江市利达上光制品有限公司 | Water-soluble apple essence |
| CN104643003A (en) * | 2015-03-17 | 2015-05-27 | 王婧婧 | Apple essence formula for dairy product |
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| Publication number | Publication date |
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| CN105725161A (en) | 2016-07-06 |
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