CN105699787B - Coal petrography dielectric constant measurement method based on impedance analyzer - Google Patents

Coal petrography dielectric constant measurement method based on impedance analyzer Download PDF

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CN105699787B
CN105699787B CN201610125775.0A CN201610125775A CN105699787B CN 105699787 B CN105699787 B CN 105699787B CN 201610125775 A CN201610125775 A CN 201610125775A CN 105699787 B CN105699787 B CN 105699787B
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coal petrography
frequency
dielectric constant
permittivity
mixture
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CN105699787A (en
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赵端
程园新
韩楠楠
王习
董飞
丁恩杰
邹翔宇
赵志凯
王昕�
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China University of Mining and Technology CUMT
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    • GPHYSICS
    • G01MEASURING; TESTING
    • G01RMEASURING ELECTRIC VARIABLES; MEASURING MAGNETIC VARIABLES
    • G01R27/00Arrangements for measuring resistance, reactance, impedance, or electric characteristics derived therefrom
    • G01R27/02Measuring real or complex resistance, reactance, impedance, or other two-pole characteristics derived therefrom, e.g. time constant
    • G01R27/26Measuring inductance or capacitance; Measuring quality factor, e.g. by using the resonance method; Measuring loss factor; Measuring dielectric constants ; Measuring impedance or related variables
    • G01R27/2617Measuring dielectric properties, e.g. constants

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  • Investigating Or Analyzing Materials By The Use Of Electric Means (AREA)

Abstract

It is quickly, convenient in view of the deficiencies of the prior art, the present invention provides a kind of coal petrography dielectric constant measurement method based on impedance analyzer, accurately measure the dielectric constant of the coal mixed with rock.The instrument used is simplified, and measuring method is easy to implement, convenient for promoting on a large scale.

Description

Coal petrography dielectric constant measurement method based on impedance analyzer
Technical field
The present invention relates to coal petrography dielectric constant measurement technology more particularly to a kind of medium Jie based on precise impedance analyzer Electric constant measuring method.
Background technology
Dielectric constant is a significant data for characterizing dielectric or insulating materials electrical property, and can be called relatively electric Capacity rate or capacitivity.In EM theory, the interaction of medium and electromagnetic wave and field variation are mainly normal by studying dielectric Number, so as to what is analyzed.The capacitance that dielectric constant refers in same capacitor with same substance when being dielectric and vacuum Ratio, represent that dielectric stores the relative ability of electrostatic energy in the electric field, the smaller insulating properties of relative dielectric constant is better.It is different The complex dielectric permittivity of substance is essentially different, and dielectric constant characterizes the interaction between medium and electromagnetic field.
With the development of microwave technology, microwave detection obtains increasingly in the researchs such as industrial agricultural production, national defense construction It is widely applied.Microwave detection usually using the variation of medium dielectric property at microwave frequencies, as microwave by after medium its The variation of attenuation or phase shift detects various non-electrical physical quantitys.
When mining excavation is carried out in underground, the rock of certain content is had among the coal that coalcutter excavates.Coal The higher the better for content, and the quality of coal is softer, and the lower the content of rock the better, and quality is harder, when mining, due to rock It is harder, the knife face of coalcutter can be damaged.Therefore, the content of the coal of coalcutter excavation regions is reasonably controlled during coal mining It is particularly significant, while coal content is ensured, rock content is reduced as possible.Based on this, in exploitation, can be contained by measuring coal It measures to determine whether to carry out current region exploitation.Coal content measurement can be realized by measuring its dielectric constant.Therefore, dielectric Constant has important application value in the measurement of coal content.
At present, the measuring method of dielectric constant has following several classes:Frequency-domain transmission method, time domain transmission, noise correlation method are humorous The methods of cell method of shaking.Frequency-domain transmission method is to measure the most ripe method of material dielectric constant.Low-frequency range using vector impedance method and Bridge method;Microwave frequency band uses standing wave method, Network Analyzer method and Six―port technique.With the development of tunable laser, sub- milli Metric wave, it is infrared, it is seen that the frequency ranges such as light or X ray can use frequency-domain transmission technology.Time domain method can be divided into fast-response and slow sound Should, slow-response is mainly by measuring the charging and discharging curve of capacitance, the relaxation behavior under inverting material very low frequency.Fast-response can by when The data that domain measures are transformed into frequency domain.At this point, frequency-domain transmission method and time domain method Dual Method each other.Noise correlation method be it is infrared with Super band measures the effective ways of material dielectric constant, in recent years the trend of oriented low-frequency range development.Resonant-cavity Method is microwave frequency band The method of Measuring Dielectric Constant needs that material size, influence of the wall size to measurement result are discussed.
The device of above-mentioned dielectric constant measurement method it is more complicated, promote the use of on a large scale be difficult.
Invention content
The purpose of the present invention is being directed to the deficiency of above-mentioned technology, a kind of coal petrography dielectric constant based on impedance analyzer is provided Measuring method, it is quickly, convenient, accurately measure the dielectric constant of the coal mixed with rock.The instrument used is simplified, and measuring method is held It easily realizes, convenient for promoting on a large scale.
A kind of coal petrography dielectric constant measurement method based on impedance analyzer is claimed in the application, includes the following steps:
S101, on-resistance analyzer determine to test the stable frequency section of dielectric constant;
Wherein, impedance analyzer, including alternating current source, resistance, balance system, external-connected port, plane-parallel capacitor;
Measure plane-parallel capacitor blank state resonant frequency, and obtain capacitance can stable frequency section, The capacitance of different material is measured for the later stage and resonant frequency establishes data basis;
S102 for the coal petrography mixture of various ratios, establishes resonant frequency f and the mathematical model a of permittivity ε;
After the coal petrography mixture of known various ratios is filled into plane-parallel capacitor, basis after impedance analyzer operation Internal measuring state, for meeting automatic stabilisation in a frequency, this frequency is resonant frequency f;
Under resonant frequency f, measurement obtains capacitance C, public by the measurement of following plane-parallel capacitor dielectric constant Formula, and then obtain the permittivity ε of substance;
Wherein, ε is the dielectric constant of medium between capacitor plate;D represents two parallel plate distances;S represents two parallel poles Plate relative area;
So far, the resonant frequency f of the coal petrography mixture of various ratios and the mathematical model a of permittivity ε are obtained.
S103 for the coal petrography mixture of various ratios, for a certain coal petrography mixture, is adjusted inside impedance analyzer Detection frequency f ', test the capacitances under different detection frequencies, and pass through the measure equation of plane-parallel capacitor dielectric constant Be calculated different permittivity εs ', and then obtain permittivity ε ' with detection frequency f ' change trend curve, establish close It is model b;
For the coal petrography mixture that dielectric constant is unknown, the coal petrography mixture is obtained with impedance analyzer measurement by S104 Resonant frequency F, and pass through resonant frequency f and the mathematical model a of permittivity ε, the dielectric constant of the coal petrography mixture is obtained, together When the specific coal petrography ratio of the coal petrography mixture can be also known by mathematical model a.
S105 according to the coal petrography mixture of the obtained special ratios of step S104, is extracted from step S103 and is corresponded to The permittivity ε of the coal petrography mixture ' and with the relational model b of detection frequency f ' variations, so as to learn:As detection frequency f ' When changing, permittivity ε ' variation.
Further, in the S103, range desirable the detection frequency f ' between 10Hz to 120MHz, every 10MHz generates a detection signal.
Further, for the coal petrography mixture of ratio in common 11, the mathematical model a is as shown in the table:
Compared with prior art, the method provided by the present invention utilizes precise impedance analyzer, easy to operate, highly practical.
Description of the drawings
Fig. 1 is the circuit diagram implemented using precise impedance analyzer.
Specific embodiment
Below by specific embodiment, the invention will be further described, and following embodiment is descriptive, is not limit Qualitatively, it is impossible to which protection scope of the present invention is limited with this.
Technical principle:The calculation formula of plane-parallel capacitor capacitance is
Wherein, ε is the dielectric constant of medium between capacitor plate;D represents two parallel plate distances;S represents two parallel poles Plate relative area.
From formula as can be seen that the output capacitance of plane-parallel capacitor is inversely proportional with pole plate spacing, the right opposite between pole plate Product is directly proportional,
It follows that there are certain relationships between permittivity ε and capacitance C.Can by measuring the capacitances of unknown materials, Obtain dielectric constant.
The claimed coal petrography dielectric constant measurement method based on impedance analyzer of the application, includes the following steps:
S101, on-resistance analyzer determine to test the stable frequency section of dielectric constant;
In embodiments of the present invention, the precise impedance analyzer is Shanghai Ke Erweien electronics corporations, model 6500B.Wherein, as shown in Figure 1, including alternating current source, resistance, balance system is external for the circuit structure inside impedance analyzer The parts such as port, plate condenser.
Measure plane-parallel capacitor blank state resonant frequency, and obtain capacitance C can stable frequency section, The capacitance C of different material is measured for the later stage and resonant frequency establishes data basis.
S102 for the coal petrography mixture of various ratios, establishes resonant frequency f and the mathematical model a of permittivity ε;
After the coal petrography mixture of known various ratios is filled into plane-parallel capacitor, basis after impedance analyzer operation Internal measuring state, for meeting automatic stabilisation in a frequency, this frequency is resonant frequency f;
Under resonant frequency f, measurement obtains capacitance C, public by the measurement of following plane-parallel capacitor dielectric constant Formula, and then obtain the permittivity ε of substance.
Wherein, ε is the dielectric constant of medium between capacitor plate;D represents two parallel plate distances;S represents two parallel poles Plate relative area.
So far, the resonant frequency f of the coal petrography mixture of various ratios and the mathematical model a of permittivity ε are obtained.
In embodiments of the present invention, the known media is 11 kinds, measures its dielectric constant at the resonant frequency fx, obtains 11 groups of basic datas, as the basis for establishing the mathematical model between resonant frequency f and permittivity ε.
The known media is 11 kinds, measures its dielectric constant at the resonant frequency fx.It is as shown in the table:
S103 for the coal petrography mixture of various ratios, for a certain coal petrography mixture, is adjusted inside impedance analyzer Detection frequency f ', test the capacitances under different detection frequencies, and pass through the measure equation of plane-parallel capacitor dielectric constant Be calculated different permittivity εs ', and then obtain permittivity ε ' with detection frequency f ' change trend curve, establish close It is model b;
A kind of substance can obtain fixed dielectric constant, but work as measuring environment in the case where determining detection frequency and measuring environment It changes, dielectric constant can also change.Frequency can lead to the variation of substance internal structure, in general, dielectric constant It can reduce with the raising of detection frequency.
In present example, the desirable ranges of frequency f ' of signal are detected between 10Hz to 120MHz, it can be every 10MHz generates a detection signal.
For the coal petrography mixture that dielectric constant is unknown, the coal petrography mixture is obtained with impedance analyzer measurement by S104 Resonant frequency F, and pass through resonant frequency f and the mathematical model a of permittivity ε, the dielectric constant of the coal petrography mixture is obtained, together When the specific coal petrography ratio of the coal petrography mixture can be also known by mathematical model a.
For example, certain coal petrography mixture, obtains resonant frequency F=50MHz using impedance analyzer measurement, can obtain the coal The dielectric constant of rock mixture is 3.57, and coal petrography ratio is 1:1.
S105 according to the coal petrography mixture of the obtained special ratios of step S104, is extracted from step S103 and is corresponded to The permittivity ε of the coal petrography mixture ' and with the relational model b of detection frequency f ' variations, so as to learn:As detection frequency f ' When changing, permittivity ε ' variation.
Data basis is established, and then more effectively distinguish the ore deposit underground coal and rock for the processing in later stage purification as a result, carried The high coefficient of mining of coal reduces the content of solid rock, can better ensure that the quality of coal.
It should be understood that the application of the present invention is not limited to the above, it for those of ordinary skills, can To be improved or converted according to the above description, all these modifications and variations should all belong to the guarantor of appended claims of the present invention Protect range.

Claims (3)

1. a kind of coal petrography dielectric constant measurement method based on impedance analyzer, includes the following steps:
S101, on-resistance analyzer determine to test the stable frequency section of dielectric constant;
Wherein, impedance analyzer, including alternating current source, resistance, balance system, external-connected port, plane-parallel capacitor;
Measure plane-parallel capacitor blank state resonant frequency, and obtain capacitance can stable frequency section, after being Phase measures the capacitance of different material and resonant frequency establishes data basis;
S102 for the coal petrography mixture of various ratios, establishes resonant frequency f and the mathematical model a of permittivity ε;
After the coal petrography mixture of known various ratios is filled into plane-parallel capacitor, according to inside after impedance analyzer operation Measuring state, can automatic stabilisation in a frequency, this frequency be resonant frequency f;
Under resonant frequency f, measurement obtains capacitance C, by the measure equation of following plane-parallel capacitor dielectric constant, into And obtain the permittivity ε of substance;
Wherein, ε is the dielectric constant of medium between capacitor plate;D represents two parallel plate distances;S represents two parallel plate electrode phases To area;
So far, the resonant frequency f of the coal petrography mixture of various ratios and the mathematical model a of permittivity ε are obtained;
S103 for the coal petrography mixture of various ratios, for a certain coal petrography mixture, adjusts the inspection inside impedance analyzer Measured frequency f ' tests the capacitance under different detection frequencies, and the measure equation for passing through plane-parallel capacitor dielectric constant calculates Obtain different permittivity εs ', and then obtain permittivity ε ' with detection frequency f ' change trend curve, opening relationships mould Type b;
For the coal petrography mixture that dielectric constant is unknown, the resonance of the coal petrography mixture is obtained with impedance analyzer measurement by S104 Frequency f, and pass through resonant frequency f and the mathematical model a of permittivity ε, the dielectric constant of the coal petrography mixture is obtained, while The specific coal petrography ratio of the coal petrography mixture can be known by mathematical model a;
S105 according to the coal petrography mixture of the obtained special ratios of step S104, is extracted from step S103 corresponding to the coal The permittivity ε of rock mixture ' and with the relational model b of detection frequency f ' variations, so as to learn:When detection frequency f ' generations During variation, permittivity ε ' variation.
2. the method as described in claim 1, in the S103, range desirable the detection frequency f ' is arrived in 10Hz Between 120MHz, a detection signal is generated every 10MHz.
3. the method as described in claim 1, for the coal petrography mixture of ratio in common 11, the mathematical model a is as follows Shown in table:
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CN106199206B (en) * 2016-07-08 2019-02-01 中国石油大学(北京) The measuring device and its measurement method of core vertically and horizontally dielectric parameter
CN106932651A (en) * 2017-03-23 2017-07-07 武汉理工大学 Irregular shape is gathered materials the detection method of dielectric constant
CN110726880A (en) * 2019-10-24 2020-01-24 国网重庆市电力公司电力科学研究院 Method for evaluating aging state of capacitive bushing insulation system based on frequency domain and time domain
CN112730539A (en) * 2020-12-23 2021-04-30 中山艾尚智同信息科技有限公司 Detection equipment for sandstone moisture content based on interdigital capacitor
CN114856708A (en) * 2022-05-27 2022-08-05 中国矿业大学(北京) Coal gangue dynamic identification method and device based on dielectric constant difference

Citations (12)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US6014029A (en) * 1997-11-12 2000-01-11 Climonics Ltda Sensor for sensing changes in the permittivity of a medium in which it is disposed
CN1274083A (en) * 2000-05-09 2000-11-22 西安电子科技大学 Method for measuring complex dielectric constant of solid dielectric medium
US6366096B1 (en) * 1999-08-06 2002-04-02 University Of Maryland, College Park Apparatus and method for measuring of absolute values of penetration depth and surface resistance of metals and superconductors
RU2247399C1 (en) * 2004-01-20 2005-02-27 Ульяновский государственный технический университет Device for measurement of high values of complex permittivity of low-impedance materials at microwave frequencies
CN101634672A (en) * 2009-07-10 2010-01-27 中国电子科技集团公司第五十五研究所 Micro-wave on-wafer testing method based on unknown material substrate
WO2013009251A1 (en) * 2011-07-08 2013-01-17 Imego Ab Method to use a probe to monitor interfacial changes of capacitance and resistance
CN103675466A (en) * 2013-12-09 2014-03-26 浙江大学 Complex dielectric constant measuring device and method based on SRR
CN103743956A (en) * 2014-01-08 2014-04-23 中电科技扬州宝军电子有限公司 High-sensitivity liquid substance dielectric constant sensor
CN103913640A (en) * 2014-02-12 2014-07-09 南京信息工程大学 Test system and method for accurately measuring dielectric constants
CN104407232A (en) * 2014-11-26 2015-03-11 电子科技大学 System and method for testing microwave complex permittivity of dielectric material
CN204462256U (en) * 2015-02-11 2015-07-08 嘉兴佳利电子股份有限公司 A kind of test fixture of LTCC material dielectric constant
CN104964639A (en) * 2015-07-01 2015-10-07 中国矿业大学 Device and method for detecting surrounding rock strain based on micro capacitance detection

Family Cites Families (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US6815958B2 (en) * 2003-02-07 2004-11-09 Multimetrixs, Llc Method and apparatus for measuring thickness of thin films with improved accuracy

Patent Citations (12)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US6014029A (en) * 1997-11-12 2000-01-11 Climonics Ltda Sensor for sensing changes in the permittivity of a medium in which it is disposed
US6366096B1 (en) * 1999-08-06 2002-04-02 University Of Maryland, College Park Apparatus and method for measuring of absolute values of penetration depth and surface resistance of metals and superconductors
CN1274083A (en) * 2000-05-09 2000-11-22 西安电子科技大学 Method for measuring complex dielectric constant of solid dielectric medium
RU2247399C1 (en) * 2004-01-20 2005-02-27 Ульяновский государственный технический университет Device for measurement of high values of complex permittivity of low-impedance materials at microwave frequencies
CN101634672A (en) * 2009-07-10 2010-01-27 中国电子科技集团公司第五十五研究所 Micro-wave on-wafer testing method based on unknown material substrate
WO2013009251A1 (en) * 2011-07-08 2013-01-17 Imego Ab Method to use a probe to monitor interfacial changes of capacitance and resistance
CN103675466A (en) * 2013-12-09 2014-03-26 浙江大学 Complex dielectric constant measuring device and method based on SRR
CN103743956A (en) * 2014-01-08 2014-04-23 中电科技扬州宝军电子有限公司 High-sensitivity liquid substance dielectric constant sensor
CN103913640A (en) * 2014-02-12 2014-07-09 南京信息工程大学 Test system and method for accurately measuring dielectric constants
CN104407232A (en) * 2014-11-26 2015-03-11 电子科技大学 System and method for testing microwave complex permittivity of dielectric material
CN204462256U (en) * 2015-02-11 2015-07-08 嘉兴佳利电子股份有限公司 A kind of test fixture of LTCC material dielectric constant
CN104964639A (en) * 2015-07-01 2015-10-07 中国矿业大学 Device and method for detecting surrounding rock strain based on micro capacitance detection

Non-Patent Citations (2)

* Cited by examiner, † Cited by third party
Title
印制板实测阻抗反推介质介电常数的研究;穆敦发等;《绝缘材料》;20140220(第1期);89-92页 *
安捷伦4396B阻抗分析仪在测试吸波材料复相对介电常数上的应用;张晓宁等;《安全与电磁兼容》;20061025;71-73页 *

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