CN105696332A - Mildew-resistant finishing method of silk fabric - Google Patents

Mildew-resistant finishing method of silk fabric Download PDF

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Publication number
CN105696332A
CN105696332A CN201610141583.9A CN201610141583A CN105696332A CN 105696332 A CN105696332 A CN 105696332A CN 201610141583 A CN201610141583 A CN 201610141583A CN 105696332 A CN105696332 A CN 105696332A
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China
Prior art keywords
parts
aqueous solution
silk fabric
silk
fabric
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Withdrawn
Application number
CN201610141583.9A
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Chinese (zh)
Inventor
董根琴
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HUZHOU HONGXIN SILK FACTORY
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HUZHOU HONGXIN SILK FACTORY
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Priority to CN201610141583.9A priority Critical patent/CN105696332A/en
Publication of CN105696332A publication Critical patent/CN105696332A/en
Withdrawn legal-status Critical Current

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    • D—TEXTILES; PAPER
    • D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
    • D06M—TREATMENT, NOT PROVIDED FOR ELSEWHERE IN CLASS D06, OF FIBRES, THREADS, YARNS, FABRICS, FEATHERS OR FIBROUS GOODS MADE FROM SUCH MATERIALS
    • D06M15/00—Treating fibres, threads, yarns, fabrics, or fibrous goods made from such materials, with macromolecular compounds; Such treatment combined with mechanical treatment
    • D06M15/01—Treating fibres, threads, yarns, fabrics, or fibrous goods made from such materials, with macromolecular compounds; Such treatment combined with mechanical treatment with natural macromolecular compounds or derivatives thereof
    • D06M15/03—Polysaccharides or derivatives thereof
    • D—TEXTILES; PAPER
    • D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
    • D06M—TREATMENT, NOT PROVIDED FOR ELSEWHERE IN CLASS D06, OF FIBRES, THREADS, YARNS, FABRICS, FEATHERS OR FIBROUS GOODS MADE FROM SUCH MATERIALS
    • D06M11/00—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with inorganic substances or complexes thereof; Such treatment combined with mechanical treatment, e.g. mercerising
    • D06M11/07—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with inorganic substances or complexes thereof; Such treatment combined with mechanical treatment, e.g. mercerising with halogens; with halogen acids or salts thereof; with oxides or oxyacids of halogens or salts thereof
    • D06M11/11—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with inorganic substances or complexes thereof; Such treatment combined with mechanical treatment, e.g. mercerising with halogens; with halogen acids or salts thereof; with oxides or oxyacids of halogens or salts thereof with halogen acids or salts thereof
    • D06M11/155—Halides of elements of Groups 2 or 12 of the Periodic Table
    • D—TEXTILES; PAPER
    • D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
    • D06M—TREATMENT, NOT PROVIDED FOR ELSEWHERE IN CLASS D06, OF FIBRES, THREADS, YARNS, FABRICS, FEATHERS OR FIBROUS GOODS MADE FROM SUCH MATERIALS
    • D06M11/00—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with inorganic substances or complexes thereof; Such treatment combined with mechanical treatment, e.g. mercerising
    • D06M11/51—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with inorganic substances or complexes thereof; Such treatment combined with mechanical treatment, e.g. mercerising with sulfur, selenium, tellurium, polonium or compounds thereof
    • D06M11/55—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with inorganic substances or complexes thereof; Such treatment combined with mechanical treatment, e.g. mercerising with sulfur, selenium, tellurium, polonium or compounds thereof with sulfur trioxide; with sulfuric acid or thiosulfuric acid or their salts
    • D06M11/56—Sulfates or thiosulfates other than of elements of Groups 3 or 13 of the Periodic Table
    • D—TEXTILES; PAPER
    • D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
    • D06M—TREATMENT, NOT PROVIDED FOR ELSEWHERE IN CLASS D06, OF FIBRES, THREADS, YARNS, FABRICS, FEATHERS OR FIBROUS GOODS MADE FROM SUCH MATERIALS
    • D06M11/00—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with inorganic substances or complexes thereof; Such treatment combined with mechanical treatment, e.g. mercerising
    • D06M11/77—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with inorganic substances or complexes thereof; Such treatment combined with mechanical treatment, e.g. mercerising with silicon or compounds thereof
    • D06M11/78—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with inorganic substances or complexes thereof; Such treatment combined with mechanical treatment, e.g. mercerising with silicon or compounds thereof with silicon; with halides or oxyhalides of silicon; with fluorosilicates
    • D—TEXTILES; PAPER
    • D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
    • D06M—TREATMENT, NOT PROVIDED FOR ELSEWHERE IN CLASS D06, OF FIBRES, THREADS, YARNS, FABRICS, FEATHERS OR FIBROUS GOODS MADE FROM SUCH MATERIALS
    • D06M13/00—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with non-macromolecular organic compounds; Such treatment combined with mechanical treatment
    • D06M13/322—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with non-macromolecular organic compounds; Such treatment combined with mechanical treatment with compounds containing nitrogen
    • D06M13/35—Heterocyclic compounds
    • D06M13/352—Heterocyclic compounds having five-membered heterocyclic rings
    • D—TEXTILES; PAPER
    • D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
    • D06M—TREATMENT, NOT PROVIDED FOR ELSEWHERE IN CLASS D06, OF FIBRES, THREADS, YARNS, FABRICS, FEATHERS OR FIBROUS GOODS MADE FROM SUCH MATERIALS
    • D06M13/00—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with non-macromolecular organic compounds; Such treatment combined with mechanical treatment
    • D06M13/50—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with non-macromolecular organic compounds; Such treatment combined with mechanical treatment with organometallic compounds; with organic compounds containing boron, silicon, selenium or tellurium atoms
    • D06M13/51—Compounds with at least one carbon-metal or carbon-boron, carbon-silicon, carbon-selenium, or carbon-tellurium bond
    • D06M13/513—Compounds with at least one carbon-metal or carbon-boron, carbon-silicon, carbon-selenium, or carbon-tellurium bond with at least one carbon-silicon bond
    • D—TEXTILES; PAPER
    • D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
    • D06M—TREATMENT, NOT PROVIDED FOR ELSEWHERE IN CLASS D06, OF FIBRES, THREADS, YARNS, FABRICS, FEATHERS OR FIBROUS GOODS MADE FROM SUCH MATERIALS
    • D06M15/00—Treating fibres, threads, yarns, fabrics, or fibrous goods made from such materials, with macromolecular compounds; Such treatment combined with mechanical treatment
    • D06M15/19—Treating fibres, threads, yarns, fabrics, or fibrous goods made from such materials, with macromolecular compounds; Such treatment combined with mechanical treatment with synthetic macromolecular compounds
    • D06M15/21—Macromolecular compounds obtained by reactions only involving carbon-to-carbon unsaturated bonds
    • D06M15/327—Macromolecular compounds obtained by reactions only involving carbon-to-carbon unsaturated bonds of unsaturated alcohols or esters thereof
    • D06M15/333—Macromolecular compounds obtained by reactions only involving carbon-to-carbon unsaturated bonds of unsaturated alcohols or esters thereof of vinyl acetate; Polyvinylalcohol
    • D—TEXTILES; PAPER
    • D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
    • D06M—TREATMENT, NOT PROVIDED FOR ELSEWHERE IN CLASS D06, OF FIBRES, THREADS, YARNS, FABRICS, FEATHERS OR FIBROUS GOODS MADE FROM SUCH MATERIALS
    • D06M2101/00—Chemical constitution of the fibres, threads, yarns, fabrics or fibrous goods made from such materials, to be treated
    • D06M2101/02—Natural fibres, other than mineral fibres
    • D06M2101/10—Animal fibres
    • D—TEXTILES; PAPER
    • D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
    • D06M—TREATMENT, NOT PROVIDED FOR ELSEWHERE IN CLASS D06, OF FIBRES, THREADS, YARNS, FABRICS, FEATHERS OR FIBROUS GOODS MADE FROM SUCH MATERIALS
    • D06M2200/00—Functionality of the treatment composition and/or properties imparted to the textile material
    • D06M2200/50—Modified hand or grip properties; Softening compositions

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  • Engineering & Computer Science (AREA)
  • Textile Engineering (AREA)
  • Chemical & Material Sciences (AREA)
  • Inorganic Chemistry (AREA)
  • Organic Chemistry (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Treatments For Attaching Organic Compounds To Fibrous Goods (AREA)
  • Chemical Or Physical Treatment Of Fibers (AREA)

Abstract

The invention discloses a mildew-resistant finishing method of silk fabric. The method comprises steps as follows: water is added to a finishing agent, an aqueous solution is prepared, then the aqueous solution is sprayed on the surface of the fabric with a high-pressure spraying technology, and then the fabric is dried, wherein the finishing agent is prepared from components in parts by weight as follows: 40-48 parts of deionized water, 3-10 parts of ethylene glycol monobutyl ether acetate, 3-6 parts of sodium fluosilicate, 3-6 parts of chitosan, 15-20 parts of 2-methyl-4-isothiazoline-3-ketone, 11-14 parts of garlic juice, 4-12 parts of barium sulfate, 2-6 parts of sodium xylene sulfonate, 4-8 parts of methyl cyclosiloxane, 2-9 parts of polyvinyl alcohol, 1-7 parts of calcium chloride and 5-10 parts of ammonium polyphosphate. The mildew-resistant finishing method of the silk fabric is safe and effective, and the silk fabric finished with the method is good in mildew resistance, high in washability and safe and non-irritating after being contacted with skin surface for a long time and touches soft.

Description

A kind of silk fabric mildew resistant finish method
Technical field
The invention belongs to textile technology field, be specifically related to a kind of silk fabric mildew resistant finish method。
Technical background
Silk fabric is to be made into silkworm silk or synthetic fibers, staple fibre, short silk etc.；General name with the pure fabric knitted or be interwoven of silkworm silk or artificial silk。Through effort for many years, China strives again the leading position on silk market, the world, and silk industry becomes the pillar industry of earning foreign exchange of country, builds up more complete silk industry system, and silk product has been on sale throughout countries and regions, more than 100, the whole world。
Silk broadcloth is made up of azelon, has fabulous biocompatibility with human body, in addition smooth surface, and the friction of human body is stimulated coefficient to be minimum in each fibrid by it, is only 7.4%。Moisture adsorption and releasing are good。Fibroin fiber is enriched the hydrophilic radicals such as many amidos (-CONH), amino (-NH2), again due to its porous, it is easy to water diffusion, so it can absorb moisture in atmosphere or distribute moisture, and keeps certain moisture。Under normal temperature, it can help skin to possess certain moisture, does not make skin excessively dry；Wear in summer, sweat and the heat that human body is discharged can be distributed rapidly again, make people feel nice and cool incomparable。Silk not only has good heat dispersion, also has good warmth retention property。Its heat insulating ability has benefited from its multi-void fiber structure。In a silk fiber, there are many superfine little fibers, and these tiny fibers are made up of more tiny fiber。Therefore, the silkworm silk seeming solid actually has 38% to be above hollow, there is substantial amounts of air in these spaces, and these air prevent distributing of heat, make silk have good warmth retention property。Sound-absorbing, dust suction, fire-retardant。Real silk fabric has higher voidage, thus has good sound absorption properties with inspiratory, thus except making clothing, it may also be used for interior decoration, such as real silk carpet, tapestry, curtain, wall paper etc.。Owing to silkworm silk has moisture absorption, moisture releasing performance and moisture retention, inspiratory and porous, can also adjust indoor temperature and humidity, and harmful gas, dust, microorganism can be sopped up。It addition, the thermal denaturation of cocoon fiber is little, relatively heat-resisting。It is when being heated to 100 DEG C, and only about 5～8% is brittle, and the hot variation of most of synthetic fibers than real silk big 4～5 times。The ignition temperature of silkworm silk, at 300～400 DEG C, belongs to flame retardant fibre, and the ignition temperature of synthetic fibers is at 200～260 DEG C, namely inflammable, meltable。Therefore, adopt silk fiber as the raw material of interior decoration, not only can play sound-absorbing, dust suction, insulation effect, also have and play anti-flaming function。The health care of cocoon fiber is irreplaceable, wherein contains 18 seed amino acid necessary to human body, very nearly the same with the aminoacid contained by human body skin, therefore has again the laudatory title of " Second Skin " of the mankind。Wear real silk clothes, not only can prevent ultraviolet radiation, defence harmful gas from invading and also can also the vigor of reinforcement table Skin Cell, promote the metabolism of Skin Cell, some dermatosis had good auxiliary therapeutic action simultaneously。
But the various textiles used the mankind and human skin are likely to parasitic various bacteria or microorganism, they utilize the metabolism product nutrient substance of human body to carry out growing and breeding, not only stimulate human body skin, cause discomfort, even result in pathological changes, but also fabric can be made to produce to go mouldy, it is detrimental to health。For that purpose it is necessary to use antibacterial and mouldproof finishing agent to arrange。But sealing compound Performance comparision in the market is single, and anti-mold effect is not good。Therefore how overcoming the deficiencies in the prior art is the problem that current textile technology field needs solution badly。
Summary of the invention
To achieve these goals, the invention provides a kind of silk fabric mildew resistant finish method。
It is an object of the invention to be achieved through the following technical solutions:
A kind of silk fabric mildew resistant finish method, the method has following steps: first being added water by finishing agent is configured to aqueous solution, then adopts the technique of high pressure painting that aqueous solution is sprayed on fabric face, finally dries；Described finishing agent is made up of the component of following parts by weight: deionized water 40-48 part, ethylene glycol monomethyl ether acetate 3-10 part, prodan 3-6 part, chitosan 3-6 part, MIT 15-20 part, Bulbus Allii juice 11-14 part, barium sulfate 4-12 part, sodium xylene sulfonate 2-6 part, methyl cyclosiloxane 4-8 part, polyvinyl alcohol 2-9 part, calcium chloride 1-7 part, APP 5-10 part。
The preparation technology of finishing agent is common process, and those of ordinary skill in the art can skillfully grasp。
In described spraying process, the temperature of aqueous solution is 70-80 DEG C, and spray time is 5-10min。
Described drying temperature is 80-90 DEG C, and the time is 30s。
The concentration of described aqueous solution is 800-1000ppm。
The method have the advantages that silk fabric mildew resistant finish method of the present invention, safety and effectively, use the inventive method to arrange the silk fabric prepared, fungicidal properties is good, and washability is strong, soft, fabric and skin surface Long Term Contact, safe and non-stimulating。
Detailed description of the invention
The following stated is only the preferred embodiments of the present invention, it is not limited to the present invention, although the present invention being described in detail with reference to previous embodiment, for a person skilled in the art, technical scheme described in foregoing embodiments still can be modified by it, or wherein portion of techniques feature carries out equivalent replacement。All within the spirit and principles in the present invention, any amendment of making, equivalent replacement, improvement etc., should be included within protection scope of the present invention。
Embodiment 1
A kind of silk fabric mildew resistant finish method, it has following steps: first being added water by finishing agent is configured to aqueous solution, then adopts the technique of high pressure painting that aqueous solution is sprayed on fabric face, finally dries；Described finishing agent is made up of the component of following parts by weight: deionized water 40 parts, ethylene glycol monomethyl ether acetate 3 parts, prodan 3 parts, chitosan 3 parts, MIT 15 parts, Bulbus Allii juice 11 parts, 4 parts of barium sulfate, sodium xylene sulfonate 2 parts, methyl cyclosiloxane 4 parts, polyvinyl alcohol 2 parts, 1 part of calcium chloride, APP 5 parts。
In described spraying process, the temperature of aqueous solution is 70-80 DEG C, and spray time is 5-10min。
Described drying temperature is 80-90 DEG C, and the time is 30s。
The concentration of described aqueous solution is 800-1000ppm。
Embodiment 2
A kind of silk fabric mildew resistant finish method, it has following steps: first being added water by finishing agent is configured to aqueous solution, then adopts the technique of high pressure painting that aqueous solution is sprayed on fabric face, finally dries；Described finishing agent is made up of the component of following parts by weight: deionized water 48 parts, ethylene glycol monomethyl ether acetate 10 parts, prodan 6 parts, chitosan 6 parts, MIT 20 parts, Bulbus Allii juice 14 parts, 12 parts of barium sulfate, sodium xylene sulfonate 6 parts, methyl cyclosiloxane 8 parts, polyvinyl alcohol 9 parts, 7 parts of calcium chloride, APP 10 parts。
In described spraying process, the temperature of aqueous solution is 70-80 DEG C, and spray time is 5-10min。
Described drying temperature is 80-90 DEG C, and the time is 30s。
The concentration of described aqueous solution is 800-1000ppm。
Embodiment 3
A kind of silk fabric mildew resistant finish method, it has following steps: first being added water by finishing agent is configured to aqueous solution, then adopts the technique of high pressure painting that aqueous solution is sprayed on fabric face, finally dries；Described finishing agent is made up of the component of following parts by weight: deionized water 44 parts, ethylene glycol monomethyl ether acetate 6 parts, prodan 5 parts, chitosan 5 parts, MIT 17 parts, Bulbus Allii juice 13 parts, 7 parts of barium sulfate, sodium xylene sulfonate 4 parts, methyl cyclosiloxane 6 parts, polyvinyl alcohol 6 parts, 4 parts of calcium chloride, APP 7 parts。
In described spraying process, the temperature of aqueous solution is 70-80 DEG C, and spray time is 5-10min。
Described drying temperature is 80-90 DEG C, and the time is 30s。
The concentration of described aqueous solution is 800-1000ppm。

Claims (4)

1. a silk fabric mildew resistant finish method, it is characterised in that described method has following steps: first being added water by finishing agent is configured to aqueous solution, then adopts the technique of high pressure painting that aqueous solution is sprayed on fabric face, finally dries；Described finishing agent is made up of the component of following parts by weight: deionized water 40-48 part, ethylene glycol monomethyl ether acetate 3-10 part, prodan 3-6 part, chitosan 3-6 part, MIT 15-20 part, Bulbus Allii juice 11-14 part, barium sulfate 4-12 part, sodium xylene sulfonate 2-6 part, methyl cyclosiloxane 4-8 part, polyvinyl alcohol 2-9 part, calcium chloride 1-7 part, APP 5-10 part。
2. a kind of silk fabric mildew resistant finish method according to claim 1, it is characterised in that in described spraying process, the temperature of aqueous solution is 70-80 DEG C, and spray time is 5-10min。
3. a kind of silk fabric mildew resistant finish method according to claim 1, it is characterised in that described drying temperature is 80-90 DEG C, and the time is 30s。
4. a kind of silk fabric mildew resistant finish method according to claim 1, it is characterised in that the concentration of described aqueous solution is 800-1000ppm。
CN201610141583.9A 2016-03-11 2016-03-11 Mildew-resistant finishing method of silk fabric Withdrawn CN105696332A (en)

Priority Applications (1)

Application Number Priority Date Filing Date Title
CN201610141583.9A CN105696332A (en) 2016-03-11 2016-03-11 Mildew-resistant finishing method of silk fabric

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
CN201610141583.9A CN105696332A (en) 2016-03-11 2016-03-11 Mildew-resistant finishing method of silk fabric

Publications (1)

Publication Number Publication Date
CN105696332A true CN105696332A (en) 2016-06-22

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Country Status (1)

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Citations (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN101210143A (en) * 2006-12-31 2008-07-02 北京金源化学集团有限公司 Environment-friendly type long-acting mildew-resisting paint and preparing method thereof
CN103668953A (en) * 2012-09-21 2014-03-26 上海韬鸿化工科技有限公司 Mildew-proof antibacterial finishing agent, mildew-proof antibacterial finishing method and mildew-proof antibacterial fabrics
CN103668975A (en) * 2012-09-21 2014-03-26 青岛道合生物科技有限公司 Rot resistant finishing agent special for textiles

Patent Citations (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN101210143A (en) * 2006-12-31 2008-07-02 北京金源化学集团有限公司 Environment-friendly type long-acting mildew-resisting paint and preparing method thereof
CN103668953A (en) * 2012-09-21 2014-03-26 上海韬鸿化工科技有限公司 Mildew-proof antibacterial finishing agent, mildew-proof antibacterial finishing method and mildew-proof antibacterial fabrics
CN103668975A (en) * 2012-09-21 2014-03-26 青岛道合生物科技有限公司 Rot resistant finishing agent special for textiles

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