CN106637950A - Finishing agent having function of reinforcing air permeability of textiles and preparation method of finishing agent - Google Patents
Finishing agent having function of reinforcing air permeability of textiles and preparation method of finishing agent Download PDFInfo
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- CN106637950A CN106637950A CN201611159826.8A CN201611159826A CN106637950A CN 106637950 A CN106637950 A CN 106637950A CN 201611159826 A CN201611159826 A CN 201611159826A CN 106637950 A CN106637950 A CN 106637950A
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- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06M—TREATMENT, NOT PROVIDED FOR ELSEWHERE IN CLASS D06, OF FIBRES, THREADS, YARNS, FABRICS, FEATHERS OR FIBROUS GOODS MADE FROM SUCH MATERIALS
- D06M13/00—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with non-macromolecular organic compounds; Such treatment combined with mechanical treatment
- D06M13/10—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with non-macromolecular organic compounds; Such treatment combined with mechanical treatment with compounds containing oxygen
- D06M13/224—Esters of carboxylic acids; Esters of carbonic acid
- D06M13/2246—Esters of unsaturated carboxylic acids
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- D06M11/00—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with inorganic substances or complexes thereof; Such treatment combined with mechanical treatment, e.g. mercerising
- D06M11/51—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with inorganic substances or complexes thereof; Such treatment combined with mechanical treatment, e.g. mercerising with sulfur, selenium, tellurium, polonium or compounds thereof
- D06M11/55—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with inorganic substances or complexes thereof; Such treatment combined with mechanical treatment, e.g. mercerising with sulfur, selenium, tellurium, polonium or compounds thereof with sulfur trioxide; with sulfuric acid or thiosulfuric acid or their salts
- D06M11/56—Sulfates or thiosulfates other than of elements of Groups 3 or 13 of the Periodic System
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- D06M11/00—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with inorganic substances or complexes thereof; Such treatment combined with mechanical treatment, e.g. mercerising
- D06M11/77—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with inorganic substances or complexes thereof; Such treatment combined with mechanical treatment, e.g. mercerising with silicon or compounds thereof
- D06M11/79—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with inorganic substances or complexes thereof; Such treatment combined with mechanical treatment, e.g. mercerising with silicon or compounds thereof with silicon dioxide, silicic acids or their salts
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- D06M13/00—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with non-macromolecular organic compounds; Such treatment combined with mechanical treatment
- D06M13/10—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with non-macromolecular organic compounds; Such treatment combined with mechanical treatment with compounds containing oxygen
- D06M13/224—Esters of carboxylic acids; Esters of carbonic acid
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- D06M13/00—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with non-macromolecular organic compounds; Such treatment combined with mechanical treatment
- D06M13/10—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with non-macromolecular organic compounds; Such treatment combined with mechanical treatment with compounds containing oxygen
- D06M13/224—Esters of carboxylic acids; Esters of carbonic acid
- D06M13/236—Esters of carboxylic acids; Esters of carbonic acid containing halogen atoms
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- D06M15/00—Treating fibres, threads, yarns, fabrics, or fibrous goods made from such materials, with macromolecular compounds; Such treatment combined with mechanical treatment
- D06M15/01—Treating fibres, threads, yarns, fabrics, or fibrous goods made from such materials, with macromolecular compounds; Such treatment combined with mechanical treatment with natural macromolecular compounds or derivatives thereof
- D06M15/03—Polysaccharides or derivatives thereof
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- D06M15/00—Treating fibres, threads, yarns, fabrics, or fibrous goods made from such materials, with macromolecular compounds; Such treatment combined with mechanical treatment
- D06M15/01—Treating fibres, threads, yarns, fabrics, or fibrous goods made from such materials, with macromolecular compounds; Such treatment combined with mechanical treatment with natural macromolecular compounds or derivatives thereof
- D06M15/03—Polysaccharides or derivatives thereof
- D06M15/05—Cellulose or derivatives thereof
- D06M15/09—Cellulose ethers
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- D06M15/00—Treating fibres, threads, yarns, fabrics, or fibrous goods made from such materials, with macromolecular compounds; Such treatment combined with mechanical treatment
- D06M15/19—Treating fibres, threads, yarns, fabrics, or fibrous goods made from such materials, with macromolecular compounds; Such treatment combined with mechanical treatment with synthetic macromolecular compounds
- D06M15/37—Macromolecular compounds obtained otherwise than by reactions only involving carbon-to-carbon unsaturated bonds
- D06M15/507—Polyesters
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- D06M15/00—Treating fibres, threads, yarns, fabrics, or fibrous goods made from such materials, with macromolecular compounds; Such treatment combined with mechanical treatment
- D06M15/19—Treating fibres, threads, yarns, fabrics, or fibrous goods made from such materials, with macromolecular compounds; Such treatment combined with mechanical treatment with synthetic macromolecular compounds
- D06M15/37—Macromolecular compounds obtained otherwise than by reactions only involving carbon-to-carbon unsaturated bonds
- D06M15/53—Polyethers
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- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
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- D06M15/00—Treating fibres, threads, yarns, fabrics, or fibrous goods made from such materials, with macromolecular compounds; Such treatment combined with mechanical treatment
- D06M15/19—Treating fibres, threads, yarns, fabrics, or fibrous goods made from such materials, with macromolecular compounds; Such treatment combined with mechanical treatment with synthetic macromolecular compounds
- D06M15/37—Macromolecular compounds obtained otherwise than by reactions only involving carbon-to-carbon unsaturated bonds
- D06M15/564—Polyureas, polyurethanes or other polymers having ureide or urethane links; Precondensation products forming them
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- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06M—TREATMENT, NOT PROVIDED FOR ELSEWHERE IN CLASS D06, OF FIBRES, THREADS, YARNS, FABRICS, FEATHERS OR FIBROUS GOODS MADE FROM SUCH MATERIALS
- D06M15/00—Treating fibres, threads, yarns, fabrics, or fibrous goods made from such materials, with macromolecular compounds; Such treatment combined with mechanical treatment
- D06M15/19—Treating fibres, threads, yarns, fabrics, or fibrous goods made from such materials, with macromolecular compounds; Such treatment combined with mechanical treatment with synthetic macromolecular compounds
- D06M15/37—Macromolecular compounds obtained otherwise than by reactions only involving carbon-to-carbon unsaturated bonds
- D06M15/643—Macromolecular compounds obtained otherwise than by reactions only involving carbon-to-carbon unsaturated bonds containing silicon in the main chain
- D06M15/6433—Macromolecular compounds obtained otherwise than by reactions only involving carbon-to-carbon unsaturated bonds containing silicon in the main chain containing carboxylic groups
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- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06M—TREATMENT, NOT PROVIDED FOR ELSEWHERE IN CLASS D06, OF FIBRES, THREADS, YARNS, FABRICS, FEATHERS OR FIBROUS GOODS MADE FROM SUCH MATERIALS
- D06M15/00—Treating fibres, threads, yarns, fabrics, or fibrous goods made from such materials, with macromolecular compounds; Such treatment combined with mechanical treatment
- D06M15/19—Treating fibres, threads, yarns, fabrics, or fibrous goods made from such materials, with macromolecular compounds; Such treatment combined with mechanical treatment with synthetic macromolecular compounds
- D06M15/37—Macromolecular compounds obtained otherwise than by reactions only involving carbon-to-carbon unsaturated bonds
- D06M15/643—Macromolecular compounds obtained otherwise than by reactions only involving carbon-to-carbon unsaturated bonds containing silicon in the main chain
- D06M15/6436—Macromolecular compounds obtained otherwise than by reactions only involving carbon-to-carbon unsaturated bonds containing silicon in the main chain containing amino groups
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- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06M—TREATMENT, NOT PROVIDED FOR ELSEWHERE IN CLASS D06, OF FIBRES, THREADS, YARNS, FABRICS, FEATHERS OR FIBROUS GOODS MADE FROM SUCH MATERIALS
- D06M2200/00—Functionality of the treatment composition and/or properties imparted to the textile material
- D06M2200/10—Repellency against liquids
- D06M2200/11—Oleophobic properties
Abstract
The invention discloses a finishing agent having a function of reinforcing the air permeability of textiles and a preparation method of the finishing agent. The finishing agent adopts methyl oleate, isophthalic acid diphenyl ester, dimethiconol stearate and aqueous polyurethane as main components. According to the finishing agent disclosed by the invention, a naphthalene sulfonate-formaldehyde condensation compound, aluminum tartrate, phthalic acid ester, polyglycerol monostearate, 2-fluorine-5-nitrobenzoate, sodium persulfate, sodium laureth ulfate, amino silicone oil, 6-hydroxyflavone, nanometer jade particles, a surfactant, a thickening agent and deionized water are added, and technologies including heating, stirring, ultrasonic dispersion, ball milling, reaction under nitrogen environment and the like are used for assisting, so that after the finishing agent prepared by the preparation method disclosed by the invention is used, the textiles have favorable air permeability, the evaporating speed of water is high, the oil resistance is high, requirements of the industry can be met, and the textiles have good application prospects.
Description
Technical field
The present invention relates to textile dyeing and finishing technical field, more particularly to a kind of finishing agent and its system for strengthening yarn fabric gas permeability
Preparation Method.
Background technology
The finishing functions of textile are that to give yarn fabric to meet some Special use requirements of textile excellent
Using the Special Finishing processing method of the, performance such as safety, outward appearance.The functional finish of textile is then with chemistry, biological doctor
The development of the multidisciplinary technology such as, polymer composite, photochemistry, thermodynamics, electricity, ecology get up one
Class product.Due to textile finishing functions for textile some specific performances, thus purpose is strong, and effect is good,
Value-added content of product is also high.Textile is Jing after functional treatment, and its application target and scope are clearly, also very popular.
According to statistics, the demand of world's function textile is more than 50,000,000,000 meters, and the demand of China's function textile is nearly 5,000,000,000 meters.Weaving
The world demand amount of processing and arrangement chemicals increases every year 4.2%, and annual sales amount has reached tens billion of dollars.Feature is spun
The range of application of fabric is relatively broad, is such as used as biomedical tissue and organ；For the antibacterial diseases prevention of preventive medicine, health care
The physiotherapy body shaping of beauty；Fire-retardant, the antistatic of special trade, high/low temperature protection；Domestic environment improves, dust suction noise control, Fu Yousheng
Reason health, mite killing is antifouling, refuses oily water repellent, all kinds of radiation protections etc..Also, from the point of view of development, the arrangement of functional textile
Content and range of application are also during constantly expand, just gradually penetrating into the production of mill run and arranging.
Correspondingly, textile finish also mainly has following species：（1）Antistatic finishing agent：Textile band is quiet
Dust suction and the easy mutual adsorption phenomena for staiing phenomenon, clothes and clothes, clothes and human body after electricity, gently then produces picotement, electricity
Spark, it is heavy then using closing fire and explosion accident beyond fine fabric can cause.Anti-static fabric mainly has embedding knits conductive wire
Arrange with fabric face, the latter is that fabric Jing antistatic additive cover arrangement, can neutralize electrostatic load, reduces sheet resistance, is reduced
Static focus, strengthens fabric moisture so as to reach the effect for eliminating electrostatic.（2）Heat-resistant fireproof finishing agent：Using carbon fiber
High temperature resistant, radiation hardness, corrosion resistant feature performance, are largely used to air material, architectural engineering；Using high temperature resistant, fire-retardant and height
The aramid fiber of toughness makes protective garment, fire-entry suit and ballistic protective clothing.Phosphorous-containing polyester makees flame retardant textiles, for hospital, healthcare industry
And decoration industry；It is used as curtain, wall paper decoration added with the polypropylene fibre of fire retardant；Melamine fiber high temperature resistant, pliability very well, has
There is certain flame retardant efficiency, for fire-fighting domain.（3）Antibacterial finishing agent：Under ideal climate between fabric, bacterium can not
Interrupted ground amount reproduction, causes skin infection, causes sanitary condition deterioration and transmission of disease and spreads.Austrian Meng Daier
Cellulosic fabric is using capsule of nano antibacterial and deodouring technology to bacteriostasis rates such as staphylococcus aureus, gonococcus, Escherichia coli
Up to more than 99%, skin delay skin aging is protected.There is good antimicrobial effect using extensive organosilicone quaternary ammonium salt
With, can effectively suppress and killing cause infection or pathogenicity Gram-negative, positive bacteria, staphylococcus aureus, Candida albicans
The virus such as bacterium and Escherichia coli.It is used for the antibiotic finish of underwear, towel, sheet, shoes store, carpet and medical textile.（4）It is anti-
Moth finishing agent：Wool, silk, eider down, fur etc. are damaged by worms and invade food the rate of complaints up to 7.7%, are only second to change colour, are faded, stain, shrinking,
The 5th is arranged, mothproofing agent once used naphthalene, paracide and camphor, was typically now processed with pyrethroid.（5）Ultraviolet protection is whole
Reason agent：The ultraviolet radioactive for most having harm is at 300 ~ 310 UV-B peaks.The ultraviolet radioactive of fabric is penetrated by two kinds of wave components：One
Kind meeting is immovable through fabric, and another kind of dispersive wave can react with fabric.Ultraviolet protection is arranged ultraviolet radiation absorption
With the class of ultraviolet screener two.（6）PH adjusts finishing agent：There are 40 many kinds of substance in sweat:Sodium chloride, urea, lactic acid and amino acid,
Skin surface general pH=6, the initial stage pH that perspires drops to 4.4, and perspire in a large number pH=7, and time length, urea decomposites NH3, and pH reaches
To 8.0.The pH value of acid rain is less than 5.6.PH finishing agents are combined using nanoceramic particles with fiber, can adjust pH value, and simultaneous
There are sterilized smelly eliminating, ultraviolet screener effect.（7）Heat storing heat preserving finishing agent：Fabric heat-insulation conventional method has：Add carbon in spinning solution
Change zircon ceramic powder, absorb light and release heat, the far infrared of reflection human-body emitting so as to thermal isolation and heat storage；Doughnut is incubated
With automatic heat preserving arrange etc..It is to make iso-butane and propane mixture using catalyst to have studied successful automatic heat preserving cardinal principle
Flameless combustion, each heater block weighs about 495g.
Although having there is the finishing agent of above-mentioned different characteristics at present, specific to each class, what it had uses effect
Fruit need further raising.Therefore, corresponding textile finish is developed for the different qualities required for textile with
Phase greatly improves the performance of textile and just seems particularly necessary.
The content of the invention
To solve above-mentioned technical problem, the present invention provides a kind of finishing agent for strengthening yarn fabric gas permeability, by using special
Fixed raw material is combined, and coordinates specific production technology so that it is good that the finishing agent being prepared from using after has yarn fabric
Good gas permeability, and moisture evaporation speed is high, and oil repellency is strong, disclosure satisfy that the requirement of industry, with preferably using front
Scape.
The purpose of the present invention can be achieved through the following technical solutions：
A kind of finishing agent for strengthening yarn fabric gas permeability, is prepared by the raw materials in：Methyl oleate 35-45 parts, isophthalic
Diformazan diphenyl phthalate 30-40 parts, dimethiconol stearate 25-35 parts, aqueous polyurethane 20-30 parts, naphthalene sulfonic acids
Salt formaldehyde condensation products 12-18 parts, tartaric acid aluminium 10-16 part, phthalic acid ester 8-12 parts, polyglycerol monostearate 8-10 part,
2- fluorine-5-nitro benzoic acid methyl esters 6-10 parts, sodium peroxydisulfate 6-8 parts, sodium laureth sulfate 4-6 parts, amido silicon oil 3-5 parts,
6- flavonol 2-4 parts, nanometer jade particulate 1-3 parts, surfactant 3-5 parts, thickener 3-5 parts, 300 parts of deionized water.
Preferably, the surfactant is in AEO, alhpa olefin sulfonate, isethionate
Any one.
Preferably, any one of the thickener in carboxymethylcellulose calcium, carragheen, aerosil.
The preparation method of the finishing agent of described enhancing yarn fabric gas permeability, comprises the following steps：
（1）Each raw material is accurately weighed by the weight portion；
（2）100 parts of ionized water is removed, naphthalenesulfonate formaldehyde condensation compound, tartaric acid aluminium, phthalic acid ester, poly- sweet is added thereto to
Oily monostearate, 2- fluorine-5-nitro benzoic acid methyl esters, sodium peroxydisulfate, sodium laureth sulfate, are heated to 55 DEG C, and temperature is steady
Magnetic agitation is carried out after fixed, magnetic agitation rotating speed is 200 rpm, is stirred until homogeneous, and obtains mixed liquor A；
（3）By deionized water, 200 parts mix with methyl oleate, diphenyl iso-phthalate, are warming up to 90-110 DEG C, add amino
Silicone oil, 6- flavonols, nanometer jade particulate, ultrasonic disperse 0.5-1.5 hours, are mixed under the power of 250-350W
Liquid B；
（4）Mixed liquor A and mixed liquid B are merged, ball mill is sent into, ball milling 1.5-2.5 hours make each component in mixed liquor complete
It is dispersed, dimethiconol stearate, aqueous polyurethane are subsequently added, nitrogen is passed through, the magnetic at 90 DEG C of temperature
Power stirring reaction 3 hours；
（5）After reaction terminates, when being cooled to 60 DEG C, surfactant, thickener are added in reactant liquor, subsequently carry out magnetic
Power is stirred, until all of composition is well mixed, obtains finished product.
Preferably, the step（3）In, the power of ultrasonic disperse is 300W, and ultrasonic time is 1 hour.
Preferably, the step（4）In, the speed of magnetic agitation is 150-250 r/min.
Compared with prior art, its advantage is the present invention：
（1）The finishing agent of the enhancing yarn fabric gas permeability of the present invention is with methyl oleate, diphenyl iso-phthalate, poly dimethyl silicon
Oxygen alkanol stearate, aqueous polyurethane are main component, by adding naphthalenesulfonate formaldehyde condensation compound, tartaric acid aluminium, benzene two
Formic acid esters, polyglycerol monostearate, 2- fluorine-5-nitro benzoic acid methyl esters, sodium peroxydisulfate, sodium laureth sulfate, amino silicone
Oil, 6- flavonols, nanometer jade particulate, surfactant, thickener, deionized water, are aided with heating, stirring, ultrasound point
The technique such as reaction under scattered, ball milling, nitrogen environment so that the finishing agent being prepared from makes yarn fabric have good breathing freely using after
Property, and moisture evaporation speed is high, and oil repellency is strong, the requirement of industry is disclosure satisfy that, with preferable application prospect.
（2）The finishing agent raw material for strengthening yarn fabric gas permeability of the invention is cheap, process is simple, is suitable to heavy industrialization
With practical.
Specific embodiment
The technical scheme invented is described in detail with reference to specific embodiment.
Embodiment 1
（1）35 parts of methyl oleate, 30 parts of diphenyl iso-phthalate, dimethiconol are accurately weighed by the weight portion
25 parts of stearate, 20 parts of aqueous polyurethane, 12 parts of naphthalenesulfonate formaldehyde condensation compound, 10 parts of tartaric acid aluminium, phthalic acid ester 8
Part, 8 parts of polyglycerol monostearate, 6 parts of 2- fluorine-5-nitro benzoic acids methyl esters, 6 parts of sodium peroxydisulfate, sodium laureth sulfate 4
Part, 3 parts of amido silicon oil, 1 part of part, nanometer jade particulate of 6- flavonols 2,3 parts of AEO, carboxymethyl cellulose
Plain 3 parts, 300 parts of deionized water；
（2）100 parts of ionized water is removed, naphthalenesulfonate formaldehyde condensation compound, tartaric acid aluminium, phthalic acid ester, poly- sweet is added thereto to
Oily monostearate, 2- fluorine-5-nitro benzoic acid methyl esters, sodium peroxydisulfate, sodium laureth sulfate, are heated to 55 DEG C, and temperature is steady
Magnetic agitation is carried out after fixed, magnetic agitation rotating speed is 200 rpm, is stirred until homogeneous, and obtains mixed liquor A；
（3）By deionized water, 200 parts mix with methyl oleate, diphenyl iso-phthalate, are warming up to 90 DEG C, add amino silicone
Oil, 6- flavonols, nanometer jade particulate, ultrasonic disperse 1 hour, obtains mixed liquid B under the power of 300W；
（4）Mixed liquor A and mixed liquid B are merged, ball mill is sent into, ball milling 1.5 hours makes each component substantially uniformity in mixed liquor
Dispersion, is subsequently added dimethiconol stearate, aqueous polyurethane, is passed through nitrogen, with 150 at 90 DEG C of temperature
The speed magnetic agitation of r/min is reacted 3 hours；
（5）After reaction terminates, when being cooled to 60 DEG C, AEO, carboxymethyl cellulose are added in reactant liquor
Element, subsequently carries out magnetic agitation, until all of composition is well mixed, obtains finished product.
The performance test results of the obtained finishing agent for strengthening yarn fabric gas permeability are as shown in table 1.
Embodiment 2
（1）40 parts of methyl oleate, 35 parts of diphenyl iso-phthalate, dimethiconol are accurately weighed by the weight portion
30 parts of stearate, 25 parts of aqueous polyurethane, 15 parts of naphthalenesulfonate formaldehyde condensation compound, 13 parts of tartaric acid aluminium, phthalic acid ester 10
Part, 9 parts of polyglycerol monostearate, 8 parts of 2- fluorine-5-nitro benzoic acids methyl esters, 7 parts of sodium peroxydisulfate, sodium laureth sulfate 5
Part, 4 parts of amido silicon oil, 2 parts of part, nanometer jade particulate of 6- flavonols 3,4 parts of alhpa olefin sulfonate, 4 parts of carragheen, deionization
300 parts of water；
（2）100 parts of ionized water is removed, naphthalenesulfonate formaldehyde condensation compound, tartaric acid aluminium, phthalic acid ester, poly- sweet is added thereto to
Oily monostearate, 2- fluorine-5-nitro benzoic acid methyl esters, sodium peroxydisulfate, sodium laureth sulfate, are heated to 55 DEG C, and temperature is steady
Magnetic agitation is carried out after fixed, magnetic agitation rotating speed is 200 rpm, is stirred until homogeneous, and obtains mixed liquor A；
（3）By deionized water, 200 parts mix with methyl oleate, diphenyl iso-phthalate, are warming up to 100 DEG C, add amino silicone
Oil, 6- flavonols, nanometer jade particulate, ultrasonic disperse 1 hour, obtains mixed liquid B under the power of 300W；
（4）Mixed liquor A and mixed liquid B are merged, ball mill is sent into, ball milling 2 hours makes each component substantially uniformity point in mixed liquor
Dissipate, be subsequently added dimethiconol stearate, aqueous polyurethane, be passed through nitrogen, with 200 r/ at 90 DEG C of temperature
The speed magnetic agitation of min is reacted 3 hours；
（5）After reaction terminates, when being cooled to 60 DEG C, alhpa olefin sulfonate, carragheen are added in reactant liquor, subsequently carried out
Magnetic agitation, until all of composition is well mixed, obtains finished product.
The performance test results of the obtained finishing agent for strengthening yarn fabric gas permeability are as shown in table 1.
Embodiment 3
（1）45 parts of methyl oleate, 40 parts of diphenyl iso-phthalate, dimethiconol are accurately weighed by the weight portion
35 parts of stearate, 30 parts of aqueous polyurethane, 18 parts of naphthalenesulfonate formaldehyde condensation compound, 16 parts of tartaric acid aluminium, phthalic acid ester 12
Part, 10 parts of polyglycerol monostearate, 10 parts of 2- fluorine-5-nitro benzoic acids methyl esters, 8 parts of sodium peroxydisulfate, sodium laureth sulfate 6
Part, 5 parts of amido silicon oil, 3 parts of part, nanometer jade particulate of 6- flavonols 4,5 parts of isethionate, aerosil 5
Part, 300 parts of deionized water；
（2）100 parts of ionized water is removed, naphthalenesulfonate formaldehyde condensation compound, tartaric acid aluminium, phthalic acid ester, poly- sweet is added thereto to
Oily monostearate, 2- fluorine-5-nitro benzoic acid methyl esters, sodium peroxydisulfate, sodium laureth sulfate, are heated to 55 DEG C, and temperature is steady
Magnetic agitation is carried out after fixed, magnetic agitation rotating speed is 200 rpm, is stirred until homogeneous, and obtains mixed liquor A；
（3）By deionized water, 200 parts mix with methyl oleate, diphenyl iso-phthalate, are warming up to 110 DEG C, add amino silicone
Oil, 6- flavonols, nanometer jade particulate, ultrasonic disperse 1 hour, obtains mixed liquid B under the power of 300W；
（4）Mixed liquor A and mixed liquid B are merged, ball mill is sent into, ball milling 2.5 hours makes each component substantially uniformity in mixed liquor
Dispersion, is subsequently added dimethiconol stearate, aqueous polyurethane, is passed through nitrogen, with 250 at 90 DEG C of temperature
The speed magnetic agitation of r/min is reacted 3 hours；
（5）After reaction terminates, when being cooled to 60 DEG C, isethionate, aerosil are added in reactant liquor, with
After carry out magnetic agitation, until all of composition is well mixed, obtain finished product.
The performance test results of the obtained finishing agent for strengthening yarn fabric gas permeability are as shown in table 1.
Embodiment 4
（1）45 parts of methyl oleate, 30 parts of diphenyl iso-phthalate, dimethiconol are accurately weighed by the weight portion
35 parts of stearate, 20 parts of aqueous polyurethane, 18 parts of naphthalenesulfonate formaldehyde condensation compound, 10 parts of tartaric acid aluminium, phthalic acid ester 12
Part, 8 parts of polyglycerol monostearate, 10 parts of 2- fluorine-5-nitro benzoic acids methyl esters, 6 parts of sodium peroxydisulfate, sodium laureth sulfate 6
Part, 3 parts of amido silicon oil, 1 part of part, nanometer jade particulate of 6- flavonols 4,5 parts of AEO, 3 parts of carragheen,
300 parts of deionized water；
（2）100 parts of ionized water is removed, naphthalenesulfonate formaldehyde condensation compound, tartaric acid aluminium, phthalic acid ester, poly- sweet is added thereto to
Oily monostearate, 2- fluorine-5-nitro benzoic acid methyl esters, sodium peroxydisulfate, sodium laureth sulfate, are heated to 55 DEG C, and temperature is steady
Magnetic agitation is carried out after fixed, magnetic agitation rotating speed is 200 rpm, is stirred until homogeneous, and obtains mixed liquor A；
（3）By deionized water, 200 parts mix with methyl oleate, diphenyl iso-phthalate, are warming up to 110 DEG C, add amino silicone
Oil, 6- flavonols, nanometer jade particulate, ultrasonic disperse 1 hour, obtains mixed liquid B under the power of 300W；
（4）Mixed liquor A and mixed liquid B are merged, ball mill is sent into, ball milling 1.5 hours makes each component substantially uniformity in mixed liquor
Dispersion, is subsequently added dimethiconol stearate, aqueous polyurethane, is passed through nitrogen, with 250 at 90 DEG C of temperature
The speed magnetic agitation of r/min is reacted 3 hours；
（5）After reaction terminates, when being cooled to 60 DEG C, AEO, carragheen are added in reactant liquor, subsequently
Magnetic agitation is carried out, until all of composition is well mixed, finished product is obtained.
The performance test results of the obtained finishing agent for strengthening yarn fabric gas permeability are as shown in table 1.
Comparative example 1
（1）40 parts of methyl oleate, 35 parts of diphenyl iso-phthalate, dimethiconol are accurately weighed by the weight portion
30 parts of stearate, 25 parts of aqueous polyurethane, 15 parts of naphthalenesulfonate formaldehyde condensation compound, 13 parts of tartaric acid aluminium, phthalic acid ester 10
Part, 9 parts of polyglycerol monostearate, 8 parts of 2- fluorine-5-nitro benzoic acids methyl esters, 5 parts of sodium laureth sulfate, amido silicon oil 4
Part, 2 parts of nanometer jade particulate, 4 parts of alhpa olefin sulfonate, 4 parts of carragheen, 300 parts of deionized water；
（2）100 parts of ionized water is removed, naphthalenesulfonate formaldehyde condensation compound, tartaric acid aluminium, phthalic acid ester, poly- sweet is added thereto to
Oily monostearate, 2- fluorine-5-nitro benzoic acid methyl esters, sodium laureth sulfate, are heated to 55 DEG C, and magnetic is carried out after temperature stabilization
Power is stirred, and magnetic agitation rotating speed is 200 rpm, is stirred until homogeneous, and obtains mixed liquor A；
（3）By deionized water, 200 parts mix with methyl oleate, diphenyl iso-phthalate, are warming up to 100 DEG C, add amino silicone
Oil, nanometer jade particulate, ultrasonic disperse 1 hour, obtains mixed liquid B under the power of 300W；
（4）Mixed liquor A and mixed liquid B are merged, ball mill is sent into, ball milling 2 hours makes each component substantially uniformity point in mixed liquor
Dissipate, be subsequently added dimethiconol stearate, aqueous polyurethane, be passed through nitrogen, with 200 r/ at 90 DEG C of temperature
The speed magnetic agitation of min is reacted 3 hours；
（5）After reaction terminates, when being cooled to 60 DEG C, alhpa olefin sulfonate, carragheen are added in reactant liquor, subsequently carried out
Magnetic agitation, until all of composition is well mixed, obtains finished product.
The performance test results of the obtained finishing agent for strengthening yarn fabric gas permeability are as shown in table 1.
Comparative example 2
（1）45 parts of methyl oleate, 30 parts of diphenyl iso-phthalate, dimethiconol are accurately weighed by the weight portion
35 parts of stearate, 20 parts of aqueous polyurethane, 18 parts of naphthalenesulfonate formaldehyde condensation compound, 10 parts of tartaric acid aluminium, phthalic acid ester 12
Part, 8 parts of polyglycerol monostearate, 10 parts of 2- fluorine-5-nitro benzoic acids methyl esters, 6 parts of sodium peroxydisulfate, sodium laureth sulfate 6
Part, 4 parts of 6- flavonols, 5 parts of AEO, 3 parts of carragheen, 300 parts of deionized water；
（2）100 parts of ionized water is removed, naphthalenesulfonate formaldehyde condensation compound, tartaric acid aluminium, phthalic acid ester, poly- sweet is added thereto to
Oily monostearate, 2- fluorine-5-nitro benzoic acid methyl esters, sodium peroxydisulfate, sodium laureth sulfate, are heated to 55 DEG C, and temperature is steady
Magnetic agitation is carried out after fixed, magnetic agitation rotating speed is 200 rpm, is stirred until homogeneous, and obtains mixed liquor A；
（3）By deionized water, 200 parts mix with methyl oleate, diphenyl iso-phthalate, are warming up to 110 DEG C, add 6- hydroxyls
Flavones, ultrasonic disperse 1 hour, obtains mixed liquid B under the power of 300W；
（4）Mixed liquor A and mixed liquid B are merged, ball mill is sent into, ball milling 1.5 hours makes each component substantially uniformity in mixed liquor
Dispersion, is subsequently added dimethiconol stearate, aqueous polyurethane, is passed through nitrogen, with 250 at 90 DEG C of temperature
The speed magnetic agitation of r/min is reacted 3 hours；
（5）After reaction terminates, when being cooled to 60 DEG C, AEO, carragheen are added in reactant liquor, subsequently
Magnetic agitation is carried out, until all of composition is well mixed, finished product is obtained.
The performance test results of the obtained finishing agent for strengthening yarn fabric gas permeability are as shown in table 1.
The finishing agent of embodiment 1-4 and the enhancing yarn fabric gas permeability of comparative example 1-2 is applied to into respectively yarn fabric laggard
Row fabric air-permeability rate, moisture evaporation speed, oil repellency evaluate this several tests.
Table 1
| Air penetrability（mm/s） | Evaporation rate（g/h） | Oil repellency | |
| Embodiment 1 | 52.53 | 0.39 | It is excellent |
| Embodiment 2 | 55.64 | 0.47 | It is excellent |
| Embodiment 3 | 54.81 | 0.35 | It is excellent |
| Embodiment 4 | 53.07 | 0.43 | It is excellent |
| Comparative example 1 | 41.25 | 0.31 | Well |
| Comparative example 2 | 39.73 | 0.29 | Well |
The finishing agent of the enhancing yarn fabric gas permeability of the present invention is with methyl oleate, diphenyl iso-phthalate, polydimethylsiloxanes
Alkanol stearate, aqueous polyurethane are main component, by adding naphthalenesulfonate formaldehyde condensation compound, tartaric acid aluminium, benzene diformazan
Acid esters, polyglycerol monostearate, 2- fluorine-5-nitro benzoic acid methyl esters, sodium peroxydisulfate, sodium laureth sulfate, amido silicon oil,
6- flavonols, nanometer jade particulate, surfactant, thickener, deionized water, are aided with heating, stirring, ultrasonic disperse, ball
The technique such as reaction under mill, nitrogen environment so that the finishing agent being prepared from makes yarn fabric have good gas permeability using after, and
And moisture evaporation speed is high, oil repellency is strong, the requirement of industry is disclosure satisfy that, with preferable application prospect.The increasing of the present invention
The finishing agent raw material of strong yarn fabric gas permeability is cheap, process is simple, is suitable to heavy industrialization utilization, practical.
Embodiments of the invention are the foregoing is only, the scope of the claims of the present invention is not thereby limited, it is every using this
Equivalent structure or equivalent flow conversion that bright description is made, or directly or indirectly it is used in other related technology necks
Domain, is included within the scope of the present invention.
Claims (6)
1. it is a kind of strengthen yarn fabric gas permeability finishing agent, it is characterised in that：It is prepared by the raw materials in：Methyl oleate
35-45 parts, diphenyl iso-phthalate 30-40 parts, dimethiconol stearate 25-35 parts, aqueous polyurethane 20-
30 parts, naphthalenesulfonate formaldehyde condensation compound 12-18 parts, tartaric acid aluminium 10-16 part, phthalic acid ester 8-12 parts, polyglycereol list it is stearic
Acid esters 8-10 parts, 2- fluorine-5-nitro benzoic acid methyl esters 6-10 parts, sodium peroxydisulfate 6-8 parts, sodium laureth sulfate 4-6 parts, amino
Silicone oil 3-5 parts, 6- flavonol 2-4 parts, nanometer jade particulate 1-3 parts, surfactant 3-5 parts, thickener 3-5 parts, go from
300 parts of sub- water.
2. it is according to claim 1 strengthen yarn fabric gas permeability finishing agent, it is characterised in that：The surfactant choosing
Any one from AEO, alhpa olefin sulfonate, isethionate.
3. it is according to claim 1 strengthen yarn fabric gas permeability finishing agent, it is characterised in that：The thickener is selected from carboxylic
Any one in methylcellulose, carragheen, aerosil.
4. according to the preparation method of the arbitrary described finishing agent for strengthening yarn fabric gas permeability of claim 1-3, it is characterised in that
Comprise the following steps：
（1）Each raw material is accurately weighed by the weight portion；
（2）100 parts of ionized water is removed, naphthalenesulfonate formaldehyde condensation compound, tartaric acid aluminium, phthalic acid ester, poly- sweet is added thereto to
Oily monostearate, 2- fluorine-5-nitro benzoic acid methyl esters, sodium peroxydisulfate, sodium laureth sulfate, are heated to 55 DEG C, and temperature is steady
Magnetic agitation is carried out after fixed, magnetic agitation rotating speed is 200 rpm, is stirred until homogeneous, and obtains mixed liquor A；
（3）By deionized water, 200 parts mix with methyl oleate, diphenyl iso-phthalate, are warming up to 90-110 DEG C, add amino
Silicone oil, 6- flavonols, nanometer jade particulate, ultrasonic disperse 0.5-1.5 hours, are mixed under the power of 250-350W
Liquid B；
（4）Mixed liquor A and mixed liquid B are merged, ball mill is sent into, ball milling 1.5-2.5 hours make each component in mixed liquor complete
It is dispersed, dimethiconol stearate, aqueous polyurethane are subsequently added, nitrogen is passed through, the magnetic at 90 DEG C of temperature
Power stirring reaction 3 hours；
（5）After reaction terminates, when being cooled to 60 DEG C, surfactant, thickener are added in reactant liquor, subsequently carry out magnetic
Power is stirred, until all of composition is well mixed, obtains finished product.
5. it is according to claim 4 strengthen yarn fabric gas permeability finishing agent preparation method, it is characterised in that the step
Suddenly（3）In, the power of ultrasonic disperse is 300W, and ultrasonic time is 1 hour.
6. it is according to claim 4 strengthen yarn fabric gas permeability finishing agent preparation method, it is characterised in that the step
Suddenly（4）In, the speed of magnetic agitation is 150-250 r/min.
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| Publication number | Priority date | Publication date | Assignee | Title |
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| CN107881781A (en) * | 2017-11-30 | 2018-04-06 | 苏州绣艳天下刺绣工艺有限公司 | A kind of preparation method of embroidery poromeric finishing agent |
| CN109137525A (en) * | 2018-08-01 | 2019-01-04 | 苏州市天翱特种织绣有限公司 | A kind of cotton fabric air-moisture-permeable finishing agent and preparation method thereof |
| CN110195353A (en) * | 2019-06-08 | 2019-09-03 | 苏州迅轩纺织有限公司 | A kind of cotton fabric air-moisture-permeable finishing agent and preparation method thereof |
| CN111088577A (en) * | 2019-12-31 | 2020-05-01 | 石狮市锦祥漂染有限公司 | Preparation method of moisture-absorbing and sweat-releasing fabric |
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| CN110195353A (en) * | 2019-06-08 | 2019-09-03 | 苏州迅轩纺织有限公司 | A kind of cotton fabric air-moisture-permeable finishing agent and preparation method thereof |
| CN111088577A (en) * | 2019-12-31 | 2020-05-01 | 石狮市锦祥漂染有限公司 | Preparation method of moisture-absorbing and sweat-releasing fabric |
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