CN102517896A - Washing-resistant and spill-resistant fabric and preparation method thereof - Google Patents
Washing-resistant and spill-resistant fabric and preparation method thereof Download PDFInfo
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- CN102517896A CN102517896A CN2011103860608A CN201110386060A CN102517896A CN 102517896 A CN102517896 A CN 102517896A CN 2011103860608 A CN2011103860608 A CN 2011103860608A CN 201110386060 A CN201110386060 A CN 201110386060A CN 102517896 A CN102517896 A CN 102517896A
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Abstract
The invention provides a washing-resistant and spill-resistant fabric and a preparation method thereof. The fabric comprises a base fabric and a spill-resistant coating layer combined on one face of the base fabric, wherein a spill-resistant coating layer is obtained by coating a spill-resistant coating agent on a base fabric. The spill-resistant coating agent consists of the following components in part by weight: 1 to 10 parts of organic fluorine waterproofing agent, 0.4 to 3 parts of silane coupling agent, 0.1 to 4 parts of penetration leveling agent, 1 to 6 parts of thickening agent, 0.5 to 3 parts of cross-linking agent and 74 to 94 parts of water. The surface moisture resistance of the washing-resistant and spill-resistant fabric after washing for multiple times and being normally aired can be kept to be at least the third level. When being applied to various outdoor articles, the fabric has an obvious protection effect.
Description
Technical field
The present invention relates to a kind of washable anti-water-sprinkling fabric and preparation method thereof, be specifically related to a kind ofly can keep washable anti-water-sprinkling fabric of excellent waterproof effect and preparation method thereof after drying through washing normal temperature.
Background technology
The anti-water-sprinkling of existing fabric is handled general the employing and is padded method, prevents the water-sprinkling processing simultaneously at the fabric positive and negative, can't reach the purpose of single waterproof.And the anti-water-sprinkling property of envers can reduce following coating add man-hour fabric with gluing combine powerfully, the adhesion fastness of the polymeric coating layer glue when realizing higher hydraulic pressure coating is affected, cause hydraulic pressure or peel strength to descend.
In addition; Anti-water-sprinkling is handled after washing normal temperature dries, and waterproof effect can obviously descend, and must could keep waterproof effect through oven dry after the washing; This problem is the major defect that exists during present fabric waterproof is handled; Increased inconvenience to the user, therefore, this problem also is the technical problem that needs to be resolved hurrily in this area.
Summary of the invention
In order to address the above problem, the object of the present invention is to provide washable anti-water-sprinkling fabric of a kind of anti-water-sprinkling property that realizes after repeatedly washing normal temperature and drying, keeping higher and preparation method thereof.
Inventor of the present invention finds in the washable anti-water-sprinkling fabric process of preparation through further investigation repeatedly, applies agent through the anti-water-sprinkling that uses specific composition and forms anti-water-sprinkling coating at fabric face, can address the above problem, thereby accomplish the present invention.
The invention provides a kind of washable anti-water-sprinkling fabric; This washable anti-water-sprinkling fabric comprises base cloth and the anti-water-sprinkling coating that is incorporated on the one side of base cloth; Wherein, Said anti-water-sprinkling coating applies agent and obtains through on the one side of base cloth, applying anti-water-sprinkling, and said anti-water-sprinkling applies agent and is made up of the water of thickener, 0.5-3 parts by weight of cross-linking agent and the 74-97 weight portion of the infiltration levelling agent of the silane coupler of the organic fluorine waterproof agent of 1-10 weight portion, 0.4-3 weight portion, 0.1-4 weight portion, 1-6 weight portion.
The present invention also provides a kind of washable anti-water-sprinkling process for making such fabric; This preparation method comprises that applying anti-water-sprinkling on the one side of base cloth applies agent; And carry out dried; Wherein, said anti-water-sprinkling applies agent and is made up of the water of thickener, 0.5-3 parts by weight of cross-linking agent and the 74-97 weight portion of the infiltration levelling agent of the silane coupler of the organic fluorine waterproof agent of 1-10 weight portion, 0.4-3 weight portion, 0.1-4 weight portion, 1-6 weight portion.
Washable anti-water-sprinkling fabric of the present invention can reach the 4-5 level according to the initial surface moisture resistance of the standard testing of GB/T4745, can keep the excellent waterproof effect through washing normal temperature after drying, and presses among the GB/T8629-2001 washing procedure 4A continuous washing 5 times; Normal temperature dries; The surface moisture resistance can reach more than 3 grades, and the single face waterproof controllable intensity system of washable anti-water-sprinkling fabric, can realize as required back side water pressure resistance coating or overlay film than high-peeling strength; In addition; Add silane coupler when improving the single face waterproof effect, also can improve anti-water-sprinkling scoring that normal temperature dries, improve feel, avoid folding line, and can not reduce back side overlay film fastness.
The specific embodiment
According to washable anti-water-sprinkling fabric of the present invention; This washable anti-water-sprinkling fabric comprises base cloth and the anti-water-sprinkling coating that is incorporated on the one side of base cloth; Wherein, Said anti-water-sprinkling coating applies agent and obtains through on the one side of base cloth, applying anti-water-sprinkling, and said anti-water-sprinkling applies agent and is made up of the water of thickener, 0.5-3 parts by weight of cross-linking agent and the 74-97 weight portion of the infiltration levelling agent of the silane coupler of the organic fluorine waterproof agent of 1-10 weight portion, 0.4-3 weight portion, 0.1-4 weight portion, 1-6 weight portion.
In order further to improve the waterproof effect of washable anti-water-sprinkling fabric of the present invention after washing normal temperature dries; Under preferred situation, said anti-water-sprinkling applies agent and is made up of the water of thickener, 1-2 parts by weight of cross-linking agent and the 82.7-91.2 weight portion of the infiltration levelling agent of the silane coupler of the organic fluorine waterproof agent of 4-6 weight portion, 0.8-1.3 weight portion, 2-4 weight portion, 1-4 weight portion.
According to washable anti-water-sprinkling fabric of the present invention, under preferred situation, said anti-water-sprinkling applies in the agent, and the organic fluorine waterproof agent is perfluoroalkyl acrylate emulsion and/or fluorocarbon.Said perfluoroalkyl acrylate for example can be AG-E710C (Japan AGC company).Said fluorocarbon for example can be OLEOPHOBOL CP-SLA (du pont company).
According to washable anti-water-sprinkling fabric of the present invention; Under preferred situation; Said anti-water-sprinkling applies in the agent; Said silane coupler is for being selected from least a in N-cyclohexyl-γ-aminopropyl methyl dimethoxysilane, γ-glycidoxypropyltrietandysilane andysilane, γ-glycidyl ether oxygen propyl trimethoxy silicane and γ-(2,3-epoxy third oxygen) propyl trimethoxy silicane.
According to washable anti-water-sprinkling fabric of the present invention; Under preferred situation; Said anti-water-sprinkling applies in the agent, and said infiltration levelling agent is to be selected from contract at least a in oxirane infiltration levelling agent, the two carbon fluorine infiltration of nonionic levelling agent, isopropyl alcohol and the emulsified mineral oil of organosilicon fatty alcohol.
According to washable anti-water-sprinkling fabric of the present invention; Under preferred situation; Said anti-water-sprinkling applies in the agent, and said thickener is to be selected from least a in association type acrylic acid ester thickener, polyurethane thickener, modified fibre ether thickener and the mineral oil emulsifing thickener.
According to washable anti-water-sprinkling fabric of the present invention, under preferred situation, said anti-water-sprinkling applies in the agent, and said crosslinking agent is to be selected from least a in aziridine crosslinker, isocyanate crosslinking and the organosilicon cross-linking agent.
According to washable anti-water-sprinkling fabric of the present invention, said base cloth can be the dry goods of various routines in this area, for example can be terylene, polyamide fibre or their BLENDED FABRIC etc.
According to washable anti-water-sprinkling process for making such fabric of the present invention; This preparation method is included in and applies anti-water-sprinkling on the one side of base cloth and apply agent; And carry out dried; Wherein, said anti-water-sprinkling applies agent and is made up of the water of thickener, 0.5-3 parts by weight of cross-linking agent and the 74-97 weight portion of the infiltration levelling agent of the silane coupler of the organic fluorine waterproof agent of 1-10 weight portion, 0.4-3 weight portion, 0.1-4 weight portion, 1-6 weight portion.
According to washable anti-water-sprinkling process for making such fabric of the present invention; Under preferred situation, in order to realize infiltrative controllability, it is inner to reach the capillary that both is penetrated into fiber; Non-leakage again effect to envers; Also promptly reach in 5 grades at the surperficial moisture resistance of one side (face of drenching with rain) that applies anti-water-sprinkling coating agent, the one side that uncoated anti-water-sprinkling applies agent can keep not having water proofing property or more rudimentary scoring, is not more than in the base cloth grammes per square metre under the situation of 120gsm; With respect to the area of base cloth, the consumption that anti-water-sprinkling applies agent is 0.066-0.074kg/m
2Under the situation of base cloth grammes per square metre greater than 120gsm, with respect to the area of base cloth, the consumption that anti-water-sprinkling applies agent is 0.080-0.112kg/m
2Gsm (also being expressed as g/sm) is meant every square metre of gram, just every Gram Mass.Said consumption can adopt this area conventional method to measure and obtain, and for example will prevent that water-sprinkling applies after agent evenly is coated on the base cloth of certain area, calculates the use amount that anti-water-sprinkling applies agent, is converted into the coated weight of unit are again.
According to washable anti-water-sprinkling process for making such fabric of the present invention; In order further to improve the waterproof effect of washable anti-water-sprinkling fabric of the present invention after washing normal temperature dries; Under preferred situation, the condition of said dried comprises: baking temperature is 125-175 ℃, and be 50s-120s drying time.Said drying mode can be dry for gradient increased temperature.Preferably in said baking temperature scope, carry out drying with 1-30 ℃ gradient.
Below in conjunction with embodiment the present invention is further specified.
Embodiment 1:
Present embodiment is used to explain washable anti-water-sprinkling fabric of the present invention and preparation method thereof.
(1) component with following weight portion is mixed into anti-water-sprinkling coating agent
Organic fluorine waterproof agent: Asahi Glass 7600 (Japan AGC company, AG-7600) 1
Silane coupler:
A-187 Silane (U.S. steps figure (Momentive) new high-tech material group) 0.4
Infiltration levelling agent: isopropyl alcohol/fluorinated acrylate (Dandong Fixed Star Fine Chemical Co., Ltd, FS-TM) 0.1
Thickener: TF (Dandong Fixed Star Fine Chemical Co., Ltd/association type polyurethane) 1
Crosslinking agent: FS_417 (Dandong Fixed Star Fine Chemical Co., Ltd/active isocyanate) 0.5
Water 97
(2) base cloth uses 200D polyamide fibre drillipg (grammes per square metre 90gsm)
(3) coating equipment uses one segmentation gluing to apply stenter H-10000 (closing Xing company on the Taiwan)
(4) the anti-water-sprinkling that will process applies agent and evenly is coated on the one side of base cloth and carries out dried.Anti-water-sprinkling applies the agent consumption: 0.0685kg/m
2The dry baking oven that uses carries out, and successively oven temperature is set at 130 ℃, 150 ℃, 160 ℃, 170 ℃, and the dry identical time under each temperature spot, be 58 seconds total drying time.
Obtain washable anti-water-sprinkling fabric A1.The surperficial moisture resistance of the washable anti-water-sprinkling fabric A1 of gained and feel as shown in table 1.
Table 1
Method of testing and standard
(1) washing standard adopts washing procedure 4A among the GB/T 8629-2001
(2) surperficial moisture resistance is according to the standard testing of GB/T4745
(3) surperficial moisture resistance data record data for product normal temperature after drying after the washing 5 times
(4) feel is appraised through comparison by rule of thumb
Embodiment 2
Present embodiment is used to explain washable anti-water-sprinkling fabric of the present invention and preparation method thereof.
(1) component with following weight portion is mixed into anti-water-sprinkling coating agent
Organic fluorine waterproof agent: the difficult to understand sharp precious CP-SLA of fluorine of Du Pont's Teflon (du pont company, OLEOPHOBOL CP-SLA) 4.5
Silane coupler: KH-560 (Hubei Xiantao Blue Sky Chemical Co., Ltd) 1
Infiltration levelling agent: HB (Dandong Fixed Star Fine Chemical Co., Ltd/emulsified mineral oil) 4.0
Thickener: 200E (Dandong Fixed Star Fine Chemical Co., Ltd/association acrylic acid ester) 1.4
Crosslinking agent;
BL XP 2706 (Bayer A.G, BL XP 2706) 1.2
Water 87.9
(2) base cloth uses 300D terylene OXFORD (grammes per square metre 150gsm)
(3) coating equipment uses one segmentation gluing to apply stenter H-10000 (closing Xing company on the Taiwan)
(4) the anti-water-sprinkling that will process applies agent and evenly is coated on the one side of base cloth and carries out dried.Applying the agent consumption is: 0.088kg/m
2The dry baking oven that uses carries out, and successively oven temperature is set at 125 ℃, 150 ℃, 160 ℃, 170 ℃, and to the dry identical time under the temperature spot, be 80 seconds total drying time respectively.
Obtain washable anti-water-sprinkling fabric A2.The surperficial moisture resistance of the washable anti-water-sprinkling fabric A2 of gained and feel as shown in table 2.
Table 2
Method of testing and standard
(1) washing standard adopts washing procedure 4A among the GB/T 8629-2001
(2) surperficial moisture resistance is according to the standard testing of GB/T4745
(3) surperficial moisture resistance data record data for product normal temperature after drying after the washing 5 times
(4) feel is appraised through comparison by rule of thumb
Embodiment 3
Present embodiment is used to explain washable anti-water-sprinkling fabric of the present invention and preparation method thereof.
(1) component with following weight portion is mixed into anti-water-sprinkling coating agent
Organic fluorine waterproof agent: FS-506C (Dandong Fixed Star Fine Chemical Co., Ltd) 10
Silane coupler: KH-104 (Nanjing longitude and latitude chemical industry) 3
Infiltration levelling agent: FS-JC (Dandong Fixed Star Fine Chemical Co., Ltd) 4
Thickener: FS-U50 (Dandong Fixed Star Fine Chemical Co., Ltd) 6
Crosslinking agent: SAC-100 (the outstanding grace chemical industry in Shanghai) 3
Water 74
(2) base cloth uses 1/2 twill peach face (grammes per square metre 170gsm)
(3) coating equipment uses one segmentation gluing coating stenter H-10000 (closing Xing company on the Taiwan)
(4) the anti-water-sprinkling that will process applies agent and evenly coats on the one side of base cloth and carry out dried.Applying the agent consumption is: 0.115kg/m
2The dry baking oven that uses carries out, and successively oven temperature is set at 125 ℃, 150 ℃, 160 ℃, 175 ℃, and to the dry identical time under the temperature spot, be 120 seconds total drying time respectively.
Obtain washable anti-water-sprinkling fabric A3.The surperficial moisture resistance of the washable anti-water-sprinkling fabric A3 of gained and feel as shown in table 3.
Table 3
Method of testing and standard
(1) washing standard adopts washing procedure 4A among the GB/T 8629-2001
(2) surperficial moisture resistance is according to the standard testing of GB/T4745
(3) surperficial moisture resistance data record data for product normal temperature after drying after the washing 5 times
(4) feel is appraised through comparison by rule of thumb
Washable anti-water-sprinkling fabric of the present invention can reach the 4-5 level according to the initial surface moisture resistance of the standard testing of GB/T4745; Press among the GB/T 8629-2001 washing procedure 4A continuous washing 5 times; Normal temperature dries; The surface moisture resistance can reach more than 3 grades, after washing normal temperature dries, can keep the excellent waterproof effect, is specially adapted to various outdoor goods.
Claims (10)
1. washable anti-water-sprinkling fabric; This washable anti-water-sprinkling fabric comprises base cloth and the anti-water-sprinkling coating that is incorporated on the one side of base cloth; It is characterized in that; Said anti-water-sprinkling coating applies agent and obtains through on the one side of base cloth, applying anti-water-sprinkling, and said anti-water-sprinkling applies agent and is made up of the water of thickener, 0.5-3 parts by weight of cross-linking agent and the 74-97 weight portion of the infiltration levelling agent of the silane coupler of the organic fluorine waterproof agent of 1-10 weight portion, 0.4-3 weight portion, 0.1-4 weight portion, 1-6 weight portion.
2. washable anti-water-sprinkling fabric according to claim 1; Wherein, said anti-water-sprinkling applies agent and is made up of the water of thickener, 1-2 parts by weight of cross-linking agent and the 82.7-91.2 weight portion of the infiltration levelling agent of the silane coupler of the organic fluorine waterproof agent of 4-6 weight portion, 0.8-1.3 weight portion, 2-4 weight portion, 1-4 weight portion.
3. washable anti-water-sprinkling fabric according to claim 1 and 2, wherein, said anti-water-sprinkling applies in the agent, and the organic fluorine waterproof agent is perfluoroalkyl acrylate emulsion and/or fluorocarbon.
4. washable anti-water-sprinkling fabric according to claim 1 and 2; Wherein, Said anti-water-sprinkling applies in the agent; Said silane coupler is for being selected from least a in N-cyclohexyl-γ-aminopropyl methyl dimethoxysilane, γ-glycidoxypropyltrietandysilane andysilane, γ-glycidyl ether oxygen propyl trimethoxy silicane and γ-(2,3-epoxy third oxygen) propyl trimethoxy silicane.
5. washable anti-water-sprinkling fabric according to claim 1 and 2; Wherein, Said anti-water-sprinkling applies in the agent, and said infiltration levelling agent is to be selected from contract at least a in oxirane infiltration levelling agent, the two carbon fluorine infiltration of nonionic levelling agent, isopropyl alcohol and the emulsified mineral oil of organosilicon fatty alcohol.
6. washable anti-water-sprinkling fabric according to claim 1 and 2; Wherein, Said anti-water-sprinkling applies in the agent, and said thickener is to be selected from least a in association type acrylic acid ester thickener, polyurethane thickener, modified fibre ether thickener and the mineral oil emulsifing thickener.
7. washable anti-water-sprinkling fabric according to claim 1 and 2, wherein, said anti-water-sprinkling applies in the agent, and said crosslinking agent is to be selected from least a in aziridine crosslinker, isocyanate crosslinking and the organosilicon cross-linking agent.
8. washable anti-water-sprinkling process for making such fabric; This preparation method is included in and applies anti-water-sprinkling on the one side of base cloth and apply agent; And carry out dried; It is characterized in that said anti-water-sprinkling applies agent and is made up of the water of thickener, 0.5-3 parts by weight of cross-linking agent and the 74-97 weight portion of the infiltration levelling agent of the silane coupler of the organic fluorine waterproof agent of 1-10 weight portion, 0.4-3 weight portion, 0.1-4 weight portion, 1-6 weight portion.
9. washable anti-water-sprinkling process for making such fabric according to claim 8 wherein, is not more than in the base cloth grammes per square metre under the situation of 120gsm, and with respect to the area of base cloth, the consumption that anti-water-sprinkling applies agent is 0.063-0.077kg/m
2Under the situation of base cloth grammes per square metre greater than 120gsm, with respect to the area of base cloth, the consumption that anti-water-sprinkling applies agent is 0.077-0.115kg/m
2
10. washable anti-water-sprinkling process for making such fabric according to claim 8, wherein, the condition of said dried comprises: baking temperature is 125-175 ℃, be 30s-120s drying time.
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| CN2011103860608A CN102517896A (en) | 2011-11-28 | 2011-11-28 | Washing-resistant and spill-resistant fabric and preparation method thereof |
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| CN2011103860608A CN102517896A (en) | 2011-11-28 | 2011-11-28 | Washing-resistant and spill-resistant fabric and preparation method thereof |
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Cited By (10)
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| CN103469597A (en) * | 2012-06-06 | 2013-12-25 | 上海日多高分子材料有限公司 | Preparation method of perfluoroalkyl alcohol water-splashing agent for shoe leather |
| CN103726325A (en) * | 2013-12-05 | 2014-04-16 | 常熟虞贵人家居用品有限公司 | Fabric waterproof processing liquid |
| CN104499290A (en) * | 2014-01-20 | 2015-04-08 | 丹东优耐特纺织品有限公司 | Fabric coating agent, ultrathin windproof and moisture permeable ultraviolet resistant fabric and preparation method thereof |
| CN105040442A (en) * | 2015-07-17 | 2015-11-11 | 湖州天鑫皮革涂饰剂厂 | Waterproof coating |
| TWI548707B (en) * | 2015-07-22 | 2016-09-11 | 聚紡股份有限公司 | A high resistant rain waterproof breathable water-repellent processing method |
| CN106543810A (en) * | 2016-10-31 | 2017-03-29 | 安徽博泰氟材料科技有限公司 | Organic fluorine waterproof agent is used in a kind of PU leatherware processing |
| CN106637950A (en) * | 2016-12-15 | 2017-05-10 | 吴江市北厍盛源纺织品助剂厂 | Finishing agent having function of reinforcing air permeability of textiles and preparation method of finishing agent |
| CN106758233A (en) * | 2016-12-13 | 2017-05-31 | 宁波芸生纺织品科技有限公司 | A kind of textile water-repellent finishing method |
| CN113073471A (en) * | 2021-04-09 | 2021-07-06 | 南通帝人有限公司 | Water-repellent fabric and preparation method thereof |
| CN114836983A (en) * | 2022-05-10 | 2022-08-02 | 常州旭荣针织印染有限公司 | Efficient water-splashing-preventing T/S brushing cloth and preparation process thereof |
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Cited By (13)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN103469597A (en) * | 2012-06-06 | 2013-12-25 | 上海日多高分子材料有限公司 | Preparation method of perfluoroalkyl alcohol water-splashing agent for shoe leather |
| CN103726325A (en) * | 2013-12-05 | 2014-04-16 | 常熟虞贵人家居用品有限公司 | Fabric waterproof processing liquid |
| CN104499290A (en) * | 2014-01-20 | 2015-04-08 | 丹东优耐特纺织品有限公司 | Fabric coating agent, ultrathin windproof and moisture permeable ultraviolet resistant fabric and preparation method thereof |
| CN104499290B (en) * | 2014-01-20 | 2016-08-17 | 丹东优耐特纺织品有限公司 | A kind of textile coating agent, ultra-thin Wind-proof, moisture-permeability uvioresistant fabrics and preparation method thereof |
| CN105040442A (en) * | 2015-07-17 | 2015-11-11 | 湖州天鑫皮革涂饰剂厂 | Waterproof coating |
| CN106638014A (en) * | 2015-07-22 | 2017-05-10 | 聚纺股份有限公司 | Method for processing fabric with rain-proof, high air permeability, water-repellent and waterproof characteristics |
| TWI548707B (en) * | 2015-07-22 | 2016-09-11 | 聚紡股份有限公司 | A high resistant rain waterproof breathable water-repellent processing method |
| CN106543810A (en) * | 2016-10-31 | 2017-03-29 | 安徽博泰氟材料科技有限公司 | Organic fluorine waterproof agent is used in a kind of PU leatherware processing |
| CN106758233A (en) * | 2016-12-13 | 2017-05-31 | 宁波芸生纺织品科技有限公司 | A kind of textile water-repellent finishing method |
| CN106637950A (en) * | 2016-12-15 | 2017-05-10 | 吴江市北厍盛源纺织品助剂厂 | Finishing agent having function of reinforcing air permeability of textiles and preparation method of finishing agent |
| CN113073471A (en) * | 2021-04-09 | 2021-07-06 | 南通帝人有限公司 | Water-repellent fabric and preparation method thereof |
| CN114836983A (en) * | 2022-05-10 | 2022-08-02 | 常州旭荣针织印染有限公司 | Efficient water-splashing-preventing T/S brushing cloth and preparation process thereof |
| CN114836983B (en) * | 2022-05-10 | 2024-03-08 | 常州旭荣针织印染有限公司 | Efficient water-splashing-preventing T/S bristle cloth and preparation process thereof |
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Application publication date: 20120627 |