CN105686965A - Hair care product and preparing method and application thereof - Google Patents
Hair care product and preparing method and application thereof Download PDFInfo
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- CN105686965A CN105686965A CN201511022888.XA CN201511022888A CN105686965A CN 105686965 A CN105686965 A CN 105686965A CN 201511022888 A CN201511022888 A CN 201511022888A CN 105686965 A CN105686965 A CN 105686965A
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- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/67—Vitamins
- A61K8/673—Vitamin B group
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/19—Cosmetics or similar toiletry preparations characterised by the composition containing inorganic ingredients
- A61K8/24—Phosphorous; Compounds thereof
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- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
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- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/33—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing oxygen
- A61K8/36—Carboxylic acids; Salts or anhydrides thereof
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- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/33—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing oxygen
- A61K8/36—Carboxylic acids; Salts or anhydrides thereof
- A61K8/362—Polycarboxylic acids
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/33—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing oxygen
- A61K8/36—Carboxylic acids; Salts or anhydrides thereof
- A61K8/365—Hydroxycarboxylic acids; Ketocarboxylic acids
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- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
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- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/33—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing oxygen
- A61K8/37—Esters of carboxylic acids
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- A—HUMAN NECESSITIES
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- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/40—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing nitrogen
- A61K8/41—Amines
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/40—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing nitrogen
- A61K8/44—Aminocarboxylic acids or derivatives thereof, e.g. aminocarboxylic acids containing sulfur; Salts; Esters or N-acylated derivatives thereof
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/72—Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds
- A61K8/81—Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds obtained by reactions involving only carbon-to-carbon unsaturated bonds
- A61K8/8141—Compositions of homopolymers or copolymers of compounds having one or more unsaturated aliphatic radicals, each having only one carbon-to-carbon double bond, and at least one being terminated by only one carboxyl radical, or of salts, anhydrides, esters, amides, imides or nitriles thereof; Compositions of derivatives of such polymers
- A61K8/8147—Homopolymers or copolymers of acids; Metal or ammonium salts thereof, e.g. crotonic acid, (meth)acrylic acid; Compositions of derivatives of such polymers
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/72—Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds
- A61K8/81—Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds obtained by reactions involving only carbon-to-carbon unsaturated bonds
- A61K8/8141—Compositions of homopolymers or copolymers of compounds having one or more unsaturated aliphatic radicals, each having only one carbon-to-carbon double bond, and at least one being terminated by only one carboxyl radical, or of salts, anhydrides, esters, amides, imides or nitriles thereof; Compositions of derivatives of such polymers
- A61K8/8152—Homopolymers or copolymers of esters, e.g. (meth)acrylic acid esters; Compositions of derivatives of such polymers
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/72—Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds
- A61K8/81—Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds obtained by reactions involving only carbon-to-carbon unsaturated bonds
- A61K8/8164—Compositions of homopolymers or copolymers of compounds having one or more unsaturated aliphatic radicals, each having only one carbon-to-carbon double bond, and at least one being terminated by a carboxyl radical, and containing at least one other carboxyl radical in the molecule, or of salts, anhydrides, esters, amides, imides or nitriles thereof; Compositions of derivatives of such polymers, e.g. poly (methyl vinyl ether-co-maleic anhydride)
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/72—Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds
- A61K8/84—Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds obtained by reactions otherwise than those involving only carbon-carbon unsaturated bonds
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- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
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- A61K8/72—Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds
- A61K8/84—Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds obtained by reactions otherwise than those involving only carbon-carbon unsaturated bonds
- A61K8/85—Polyesters
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q5/00—Preparations for care of the hair
- A61Q5/002—Preparations for repairing the hair, e.g. hair cure
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q5/00—Preparations for care of the hair
- A61Q5/12—Preparations containing hair conditioners
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K2800/00—Properties of cosmetic compositions or active ingredients thereof or formulation aids used therein and process related aspects
- A61K2800/40—Chemical, physico-chemical or functional or structural properties of particular ingredients
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Abstract
The invention belongs to the technical field of daily-use chemical industry products, and particularly relates to a hair care product and a preparing method and application thereof.The hair care product comprises raw materials and auxiliary materials.The raw materials include a chelating agent and/or chelate, the molecular structure of the chelating agent comprises negative charges and a polydentate ligand, and the raw materials account for 5-99% of the total weight of the hair care product.The preparing method comprises the steps of weighing the raw materials and auxiliary materials, conducing uniform mixing, increasing temperature to 50-80 DEG C, and conducting uniform stirring to obtain the hair care product.The hair care product is used by being added to alkaline hairdressing products, the problem that hair is damaged due to the use of high-alkaline hairdressing products can be solved, the purpose of making the internal structure of hair firmer is realized finally, and meanwhile, the activity of metal ions is inhibited so as to reduce the damage of high-alkaline hairdressing products to hair.
Description
Technical field
The invention belongs to daily chemical product technical field, be specifically related to a kind of conditioner and its production and use。
Background technology
Hair is divided into three layers, and including epidermal area, cortical layer and medullary substance layer, epidermal area is exactly hair scale sheet, and this layer determines gloss and the compliance of hair, so, hair is lackluster, and dry and astringent is all that this pull-up falls to causing。Scale, in hair washing, shines upon, and towel rubbing head is sent out, all can cause coming off in various degree when combing one's hair, here it is long hair sends out the reason that slightly hair quality is bad, be required for when boiling hot dye, hair washing scale layer to open, if misoperation, a large amount of scale can be caused to come off。Opening when meeting alkali components or water when scale layer, so most hair-waving hair dye is all alkaline, generally, alkalescence is more big, and speed of action is more fast, and wound is sent out degree and also strengthened。
Hair dye generally dyes with raw metal, its dyeing major sedimentary on dry surface, color and luster has dimer metal appearance, make hair become fragile hair-waving efficiency step-down。In stain, the content of alkali is also very important, because the higher hair of alkali content easily expands the infiltration being conducive to dyestuff intermediate to hair, but skin has very big stimulation, and alkaline oxidation reaction on the low side carries out not exclusively, because intermediate coupling agent reacts in the basic conditions。And alkaline hair on the low side not easily expands, and hair can not well be permeated by dyestuff intermediate, coupling agent, Color is caused to weaken uneven, not full。The shampoo that consumer commonly uses at present simultaneously mostly also is alkalescence, and oil content can quickly be removed by its alkaline clean, can be very clean after oiliness hair quality。But life-time service can destroy the pH value of hair。
Product is sent out in the pass of existing acidity, owing to price is higher, promotes the use of also without by masses。Current user is after boiling hot hair dyeing, in order to tackle the impaired problem of hair, reduces a high alkalinity pass product and hair extent of injury can be started with from two aspects: the first reinforces hair internal structure, strengthens the hair defensive ability/resistance ability to injury。Its two, reduce Harmful ingredient content, or active degree, reduce its extent of injury to hair。More existing conditioners and hair conditioner series products, it mostly is the product only reinforcing hair internal structure, its product component is many, complicated, the problem that can not solve targetedly to present cationic state inside hair quality hair, such as application number be 201010102688.6 patent of invention disclose a kind of dye after repair hair conditioner and preparation method thereof, it is by deionized water suction agitated kettle, heated and stirred, when temperature rises to 60 DEG C～80 DEG C, it is sequentially added into chelating agen 0.05～0.1 weight portion, the cationic surfactant of fusing and tax fat agent；Stirring and emulsifying cooled down after 10～25 minutes；When temperature is cooled to 45～55 DEG C, it is sequentially added into conditioner 1～3 weight portion, functional additive 1～3 weight portion, odorant 0.2～0.6 weight portion and preservative 0.04～0.08 weight portion, reacts 10～25 minutes；It is cooled to 30～40 DEG C and namely obtains product。Compared with prior art, this invention has and smooths hair top layer scale, promotes the growth of hair, improves hair structure, forms protective layer, to repair the advantages such as impaired hair on hair。But the patented product can not effectively solve the hair quality infringement problem using high alkalinity to cause after closing a product targetedly, as can be seen here, a kind of conditioner can be invented, can solve consumer uses high alkalinity to close the hair quality damage problem sending out product and cause, it is finally reached the purpose making hair internal structure firmer, with the activity of limit metal ion, reduce high alkalinity and close a product injury to hair, become the technical problem that those skilled in the art are urgently to be resolved hurrily。
Summary of the invention
The present invention is to solve above-mentioned technical problem, it is provided that a kind of conditioner and its production and use, it is simple that this conditioner has preparation technology, and hair care effect is good, is suitable for batch production and the advantage used。
In order to reach above-mentioned technique effect, the present invention includes techniques below scheme:
A kind of conditioner, including raw material and adjuvant, described raw material includes chelating agen and/or chelate, includes negative charge and multidentate ligand in the molecular structure of described chelating agen, and described raw material accounts for the 5%～99% of conditioner gross weight。
Further, described chelate includes vitamin B12, and described chelating agen includes single compound and/or polymer,
Described single compound include phosphoric acid, oxalic acid, citric acid, tartaric acid, gluconic acid, ethylenediaminetetraacetic acid, aminotriacetic acid, diethylene-triamine pentaacetic acid, ethyl-3-acetic acid ethylenediamine, bicine N-, 1,2,3,4-Pentamethylene. tetrabasic carboxylic acids, 2-fluoroacetic acid propylmalonic acid and 2-fluoroacetic acid base fourth lead one or more in acid and salt thereof；
Described polymer includes polyphosphoric acid, bodied ferric sulfate, aluminium polychlorid, polyacrylic acid, polyacrylamide, polymethylacrylic acid, polymethyl methacrylate, poly, hydrolytic polymaleic anhydride, poly-epoxy succinic acid, poly-aspartate, maleic acid-acrylic acid copolymer, acrylic acid-acrylic acid hydroxypropyl acrylate copolymer, acrylic acid-2-acrylamide-2-methyl propane sulfonic copolymer, acrylic acid-acrylic ester-phosphonic acids-sulfonate quadripolymer, one or more in acrylic acid-acrylic ester-co-polymer of sulfonate and fumaric acid-propene sulfonic acid copolymer。
When overbased products acts on hair, a kind of cationic state can be rendered into inside hair, it is simply that say and inside hair, have a lot of positive charge, such as-NH3+, raw produce in the present invention, because have two simultaneously, or plural negative charge, so it can with two, or plural positive charge forms new chemical bond so that hair internal structure is firmer, more can resist and chemically and physically injure。
High alkalinity is closed a product and is generally all contained many metal ions, and metal ion has very strong catalytic action, it is possible to accelerate the process that in hair, keratin is impaired。Raw produce in the present invention can form coordinate bond, the activity of restriction metal ion with metal ion, thus decreasing high alkalinity to close a product injury to hair。
Further, described adjuvant includes one or more in dispersant, pigment, preservative, spice, thickening agent and solvent。
Further, described adjuvant includes the component of following parts by weight: the thickening agent of 0.5～30 part, the solvent of 0.001～95 part, the dispersant of 0.5～10 part, the pigment of 0.001～1 part, the preservative of 0.001～1 part and 0.001～5 part spice。
Owing to having substantial amounts of component in many hair care compositions, research worker is not only faced with finds suitable component to provide the challenge of desired hair products characteristic, but also is faced with the challenge of the compositions manufacturing these complexity。Such challenge includes Development and Production scheme to manufacture compositions, no matter is for small-scale initial testing or for large-scale commercial market。Greater amount of component is intended to greater amount of manufacture container, and namely this itself be intended to the more time and consume to produce described conditioner。Conditioner is the complex mixture of various ingredients, and due to this complexity, is accomplished by the consideration of carefulness when obtaining hair care composition。Visible the present inventor is through substantial amounts of creative experiments, filter out inventive formulation product, it is made significantly to be different from existing conditioner and hair conditioner product, though conventional hair conditioner is added with chelating agen, but the content of chelating agen is all relatively low, majority only accounts for the 0.05～0.1% of whole hair conditioner product weight, the present inventor rationally screens inventive formulation component and content, obtaining a kind of consumer that can effectively solve uses high alkalinity to close the hair quality damage problem sending out product and cause, it is finally reached the purpose firmer so that hair internal structure, activity with limit metal ion, reduce high alkalinity and close a product injury to hair。
Further, described solvent includes one or more in water, ethanol, isopropanol, vegetable oil, animal oil and mineral oil；
Described dispersant includes glycerol monostearate and/or sodium lauryl sulfate；
Described pigment includes azopigment and/or food coloring；
Described preservative includes phenoxyethanol and/or the acetic acid that anhydrates；
Described thickening agent includes one or more in hexadecanol, octadecanol and xanthan gum。
The preparation method of a kind of conditioner, described conditioner is above-mentioned conditioner, and described preparation method comprises the following steps: weigh above-mentioned each raw material and adjuvant composition, and Homogeneous phase mixing post-heating, to 50～80 DEG C, stirs prepared。
The purposes of a kind of conditioner, described conditioner is above-mentioned conditioner, for being used in conjunction with basic hair dye, alkalescence agent for permanent hair waving, alkalescence purificant or alkalescence shampoo。
Further, the using method of described conditioner is: described conditioner is added in basic hair dye, alkalescence agent for permanent hair waving, alkalescence purificant or alkalescence shampoo, uses after uniform stirring。
Further, the using method of described conditioner is: after making to be finished basic hair dye, alkalescence agent for permanent hair waving, alkalescence purificant or alkalescence shampoo, takes described conditioner and is applied on hair, and static 10～30min rinses。
Product of the prior art; not yet deposit to close with alkalescence and send out the conditioner that product is used in conjunction with; decrease high alkalinity targetedly and close a product injury to hair; and it is easy to use; consumer can be in after boiling hot dye and use voluntarily, or is directly added into by this product in boiling hot dye product when carrying out scalding dye, while protecting consumer's hair quality; send out product compared to adopting acidity to close, reduce client's consumer cost。
Adopt technique scheme, including following beneficial effect: the present invention provides a kind of conditioner and its production and use, make hair internal structure firmer, more can resist and chemically and physically injure, product of the present invention simultaneously, coordinate bond, the activity of restriction metal ion can be formed, thus decreasing high alkalinity to close a product injury to hair with metal ion。It is relatively big that the present invention is compared to traditional hair conditioner formula for a product cost variance, but its result of use is far superior to traditional hair conditioner, and product specific aim of the present invention is higher, more can meet the user's request after scalding dye, and it is less costly, have broad application prospects, be suitable to widely popularize and use。
Detailed description of the invention
Below by specific embodiment, the present invention is described in further detail。
Embodiment one: a kind of conditioner, including raw material and adjuvant, described raw material includes chelating agen and/or chelate, includes negative charge and multidentate ligand in the molecular structure of described chelating agen, described raw material accounts for the 99% of conditioner gross weight, and described adjuvant accounts for the 1% of conditioner gross weight。。
The preparation method of a kind of conditioner, described conditioner is above-mentioned conditioner, weighs the raw material of 99% and the adjuvant of 1%, and Homogeneous phase mixing post-heating, to 50～80 DEG C, stirs prepared。
The purposes of a kind of conditioner, described conditioner is above-mentioned conditioner, for being used in conjunction with basic hair dye, alkalescence agent for permanent hair waving, alkalescence purificant or alkalescence shampoo。
Outward appearance: the liquid of opaque, thickness；Abnormal smells from the patient: coupling standard。
Embodiment two: a kind of conditioner, including raw material and adjuvant, described raw material includes component 2% phosphoric acid of following percetage by weight, 3% poly-aspartate and 1% ethyl-3-acetic acid ethylenediamine, described adjuvant accounts for the 95% of conditioner gross weight, and described adjuvant includes the component of following parts by weight: the water of 0.001 part, the glycerol monostearate of 10 parts, the food coloring of 0.001 part, the phenoxyethanol of 1 part and 0.001 part spice。
The preparation method of a kind of conditioner, weighs raw material and the adjuvant of above-mentioned percetage by weight, and Homogeneous phase mixing post-heating, to 50～80 DEG C, stirs prepared。
The purposes of a kind of conditioner, is added into the conditioner of above-mentioned preparation in basic hair dye, alkalescence agent for permanent hair waving, alkalescence purificant or alkalescence shampoo, uses after uniform stirring。
Outward appearance: the liquid of opaque, thickness；Abnormal smells from the patient: coupling standard。
Embodiment three: a kind of conditioner, including raw material and adjuvant, described raw material includes the component of following percetage by weight: 10% tartaric acid, 5% citric acid, 8% acrylic acid-2-acrylamide-2-methyl propane sulfonic copolymer, 10% ethylenediamine tetraacetic acid (EDTA), 15% vitamin B12,12% gluconic acid, 8% aminotriacetic acid and 2% ethyl-3-acetic acid ethylenediamine；Described adjuvant accounts for the 30% of conditioner gross weight, and described adjuvant includes the component of following parts by weight: the isopropanol of 25 parts, the mineral oil of 20 parts, the glycerol monostearate of 1 part, the sodium lauryl sulfate of 2 parts, the pigment of 0.05 part, the water acetic acid of 0.08 part and 2 parts spice。
The preparation method of a kind of conditioner, weighs raw material and the adjuvant of above-mentioned percetage by weight, and Homogeneous phase mixing post-heating, to 50～80 DEG C, stirs prepared。
The purposes of a kind of conditioner, the using method of described conditioner is: after making to be finished basic hair dye, alkalescence agent for permanent hair waving, alkalescence purificant or alkalescence shampoo, takes described conditioner and is applied on hair, and static 10～30min rinses。
Outward appearance: the liquid of opaque, thickness；Abnormal smells from the patient: coupling standard。
Embodiment four: a kind of conditioner, including raw material and adjuvant, described raw material includes component 20% citric acid of following percetage by weight, 30% vitamin B12 and 30% maleic acid-acrylic acid copolymer, described adjuvant accounts for the 20% of conditioner gross weight, and described adjuvant includes the component of following parts by weight: the ethanol of 95 parts, the sodium lauryl sulfate of 0.5 part, the pigment of 1 part, the spice of anhydrate acetic acid and 5 parts of 0.001 part。
The preparation method of a kind of conditioner, weighs raw material and the adjuvant of above-mentioned percetage by weight, and Homogeneous phase mixing post-heating, to 50～80 DEG C, stirs prepared。
The using method of described conditioner is, the conditioner of above-mentioned preparation is added in basic hair dye, alkalescence agent for permanent hair waving, alkalescence purificant or alkalescence shampoo, uses after uniform stirring。
Outward appearance: the liquid of opaque, thickness；Abnormal smells from the patient: coupling standard。
Embodiment five: a kind of conditioner, including raw material and adjuvant, described raw material includes component 14% poly of following percetage by weight, 20% polyphosphoric acid, 7% poly-aspartate, 3%1, 2, 3, 4-Pentamethylene. tetrabasic carboxylic acid and 6% polymethyl methacrylate, described adjuvant accounts for the 50% of conditioner gross weight, described adjuvant includes the component of following parts by weight: the hexadecanol of 0.2 part, the xanthan gum of 0.3 part, the vegetable oil of 0.001 part, the glycerol monostearate of 10 parts, the color element of 0.001 part, the phenoxyethanol of 0.5 part, the spice of the water acetic acid of 0.5 part and 0.001 part。
The preparation method of a kind of conditioner, weighs raw material and the adjuvant of above-mentioned percetage by weight, and Homogeneous phase mixing post-heating, to 50～80 DEG C, stirs prepared。
The purposes of a kind of conditioner, the using method of described conditioner is: after making to be finished basic hair dye, alkalescence agent for permanent hair waving, alkalescence purificant or alkalescence shampoo, takes described conditioner and is applied on hair, and static 10～30min rinses。
Outward appearance: the liquid of opaque, thickness；Abnormal smells from the patient: coupling standard。
Embodiment six: a kind of conditioner, including raw material and adjuvant, described raw material includes component 4% bodied ferric sulfate of following percetage by weight, 3% acrylic acid-acrylic ester-phosphonic acids-sulfonate quadripolymer and 3%2-fluoroacetic acid propylmalonic acid, described adjuvant accounts for the 90% of conditioner gross weight, and described adjuvant includes the component of following parts by weight: the octadecanol of 10 parts, the hexadecanol of 5 parts, the water of 20 parts, the sodium lauryl sulfate of 1 part, the pigment of 0.01 part, the phenoxyethanol of 0.005 part and 1 part spice。
The preparation method of a kind of conditioner, weighs raw material and the adjuvant of above-mentioned percetage by weight, and Homogeneous phase mixing post-heating, to 50～80 DEG C, stirs prepared。
The using method of described conditioner is, the conditioner of above-mentioned preparation is added in basic hair dye, alkalescence agent for permanent hair waving, alkalescence purificant or alkalescence shampoo, uses after uniform stirring。
Outward appearance: the liquid of opaque, thickness；Abnormal smells from the patient: coupling standard。
Embodiment seven: a kind of conditioner, including raw material and adjuvant, described raw material includes the component 16% acrylic acid-acrylic ester-co-polymer of sulfonate of following percetage by weight, 2% aluminium polychlorid and 2% diethylene-triamine pentaacetic acid, described adjuvant accounts for the 80% of conditioner gross weight, and described adjuvant includes the component of following parts by weight: the xanthan gum of 15 parts, the hexadecanol of 15 parts, the isopropanol of 0.001 part, the glycerol monostearate of 10 parts, the food coloring of 0.001 part, the phenoxyethanol of 1 part and 0.001 part spice。
The preparation method of a kind of conditioner, weighs raw material and the adjuvant of above-mentioned percetage by weight, and Homogeneous phase mixing post-heating, to 50～80 DEG C, stirs prepared。
The purposes of a kind of conditioner, the using method of described conditioner is: after making to be finished basic hair dye, alkalescence agent for permanent hair waving, alkalescence purificant or alkalescence shampoo, takes described conditioner and is applied on hair, and static 10～30min rinses。
Outward appearance: the liquid of opaque, thickness；Abnormal smells from the patient: coupling standard。
Embodiment eight: a kind of conditioner, including raw material and adjuvant, described raw material includes the component 16% acrylic acid-acrylic ester-co-polymer of sulfonate of following percetage by weight, 6% aluminium polychlorid and 8% diethylene-triamine pentaacetic acid, described adjuvant accounts for the 70% of conditioner gross weight, and described adjuvant includes the component of following parts by weight: the water of 35 parts, the sodium lauryl sulfate of 0.5 part, the azopigment of 0.04 part, the food coloring of 0.04 part, the acetic acid that anhydrates of 0.001 part, the spice of 5 parts and 16 parts octadecanol。
The preparation method of a kind of conditioner, weighs raw material and the adjuvant of above-mentioned percetage by weight, and Homogeneous phase mixing post-heating, to 50～80 DEG C, stirs prepared。
The purposes of a kind of conditioner, the using method of described conditioner is: after making to be finished basic hair dye, alkalescence agent for permanent hair waving, alkalescence purificant or alkalescence shampoo, takes described conditioner and is applied on hair, and static 10～30min rinses。
Outward appearance: the liquid of opaque, thickness；Abnormal smells from the patient: coupling standard。
Embodiment nine:
Formula for a product component of the present invention and content screening experiment
Data are provided by table 1, prepare each sequence number conditioner, the quality summation of its Raw and adjuvant is 100%, take 8 number of hairs topknots identical with hair quality situation, number consecutively is 1～8, the number of hairs of each topknot is identical and be A, and gather original photo under the microscope, statistics topknot occurs significantly shrink the number of hairs A1 with phenomenon of rupture, A2, then topknot is sequentially carried out same amount and brand hair bleaching product treatment, after process completes, the conditioner taking sequence number 1～8 is applied in the topknot of sequence number 1～8 respectively, after static 10～30min, rinse, cleaning dries up, until being completely dried, after tidy, gather final photo under the microscope, there is the number of hairs A3 of significantly contraction and phenomenon of rupture in statistics again, A4, finally calculate hair shrinkage factor and fracture rate。Enumerating of following raw material type, it is not limited to the kind listed in list, the raw material components to be screened that this table provides is only lists exemplary, and described table Raw can carry out the equal replacement of identical type raw material。
Calculate:
Shrinkage factor %=100* (A3-A1)/(A-A1)
Fracture rate %=100* (A4-A2)/(A-A2)
Final data result is shown in Table 1。
Table 1 formula for a product component of the present invention and content screening experiment result
Experiment conclusion: in table 1 data, the weight of raw material and adjuvant is comprehensively the 100% of conditioner quality。From table 1 data, when raw material of the present invention accounts for the 5%～99% of conditioner gross weight, and described adjuvant includes the spice of the thickening agent that parts by weight are 0.5～30 part, the solvent of 0.001～95 part, the dispersant of 0.5～10 part, the pigment of 0.001～1 part, the preservative of 0.001～1 part and 0.001～5 part, its shrinkage factor and fracture rate are less, and all less than 3%。
Embodiment ten:
Embodiment one to embodiment eight hair care effect experiment statistics result
Take 9 phase number of hairs topknots identical with hair quality situation, number consecutively is 1～8, the number of hairs of each topknot is identical and be A, and gather original photo under the microscope, statistics topknot occurs significantly shrink the number of hairs A1 with phenomenon of rupture, A2, then topknot is sequentially carried out same amount and brand hair bleaching product treatment, the wherein topknot of numbering 1～7, after addition hair bleaching agent completes bleaching step, the conditioner of the embodiment of the present invention of 25% is added in hair bleaching agent, the topknot correspondence of each sequence number adds the conditioner of corresponding sequence number embodiment, wherein it is numbered 8 topknots, after having rinsed, use commercially available routine to execute magnificent cool conditioner and carry out hair care repair process。After continuously repeating above-mentioned steps three times, cleaning dries up, until being completely dried, after tidy, gathers final photo under the microscope, and significantly shrinking and the number of hairs A3 of phenomenon of rupture, A4 occurs in statistics again, finally calculates hair shrinkage factor and fracture rate。
Calculate:
Shrinkage factor %=100* (A3-A1)/(A-A1)
Fracture rate %=100* (A4-A2)/(A-A2)
Experimental result is in Table 2
Table 2 embodiment hair care effect experiment statistics result
| Topknot is numbered | Conditioner | Shrinkage factor % | Fracture rate % |
| 1 | Embodiment one | 4% | 3% |
| 2 | Embodiment three | 0% | 0% |
| 3 | Embodiment four | 0% | 0% |
| 4 | Embodiment five | 0% | 0% |
| 5 | Embodiment six | 3% | 2% |
| 6 | Embodiment seven | 4% | 2% |
| 7 | Embodiment eight | 3% | 3% |
| 8 | Shi Hua is cool | 35% | 30% |
From the data in table 2, it can be seen that the product of the present invention is compared with commercially available prod, it is possible to greatly reduce high alkalinity and close a product injury to hair, be finally reached the purpose making hair internal structure firmer。And embodiment three to embodiment five is optimum embodiment of the present invention。
The foregoing is only the preferred embodiments of the present invention, be not limited to the present invention, for a person skilled in the art, the present invention can have various modifications and variations。All within the spirit and principles in the present invention, any amendment of making, equivalent replacement, improvement etc., should be included within protection scope of the present invention。
Claims (7)
1. a conditioner, including raw material and adjuvant, it is characterised in that described raw material includes chelating agen and/or chelate, includes negative charge and multidentate ligand in the molecular structure of described chelating agen, and described raw material accounts for the 5%～99% of conditioner gross weight。
2. a kind of conditioner according to claim 1, it is characterised in that described chelate includes vitamin B12, and described chelating agen includes single compound and/or polymer,
Described single compound include phosphoric acid, oxalic acid, citric acid, tartaric acid, gluconic acid, ethylenediaminetetraacetic acid, aminotriacetic acid, diethylene-triamine pentaacetic acid, ethyl-3-acetic acid ethylenediamine, bicine N-, 1,2,3,4-Pentamethylene. tetrabasic carboxylic acids, 2-fluoroacetic acid propylmalonic acid and 2-fluoroacetic acid base fourth lead one or more in acid and salt thereof；
Described polymer includes polyphosphoric acid, bodied ferric sulfate, aluminium polychlorid, polyacrylic acid, polyacrylamide, polymethylacrylic acid, polymethyl methacrylate, poly, hydrolytic polymaleic anhydride, poly-epoxy succinic acid, poly-aspartate, maleic acid-acrylic acid copolymer, acrylic acid-acrylic acid hydroxypropyl acrylate copolymer, acrylic acid-2-acrylamide-2-methyl propane sulfonic copolymer, acrylic acid-acrylic ester-phosphonic acids-sulfonate quadripolymer, one or more in acrylic acid-acrylic ester-co-polymer of sulfonate and fumaric acid-propene sulfonic acid copolymer。
3. a kind of conditioner according to any one of claim 1～2, it is characterised in that described adjuvant includes one or more in dispersant, pigment, preservative, spice, thickening agent and solvent。
4. a kind of conditioner according to claim 3, it is characterized in that, described adjuvant includes the component of following parts by weight: the thickening agent of 0.5～30 part, the solvent of 0.001～95 part, the dispersant of 0.5～10 part, the pigment of 0.001～1 part, the preservative of 0.001～1 part and 0.001～5 part spice。
5. a kind of conditioner according to claim 3, it is characterised in that described solvent includes one or more in water, ethanol, isopropanol, vegetable oil, animal oil and mineral oil；
Described dispersant includes glycerol monostearate and/or sodium lauryl sulfate；
Described pigment includes azopigment and/or food coloring；
Described preservative includes phenoxyethanol and/or the acetic acid that anhydrates；
Described thickening agent includes one or more in hexadecanol, octadecanol and xanthan gum。
6. the preparation method of a conditioner, it is characterized in that, described conditioner is the conditioner described in any one of Claims 1 to 5, and described preparation method comprises the following steps: weigh each raw material and adjuvant composition, Homogeneous phase mixing post-heating, to 50～80 DEG C, stirs prepared。
7. the purposes of the conditioner described in an any one of Claims 1 to 5, it is characterised in that described conditioner be for basic hair dye, alkalescence agent for permanent hair waving, alkalescence purificant or the alkalescence conditioner that is used in conjunction with of shampoo。
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