CN105660843A - Passionflower herb antistaling agent - Google Patents
Passionflower herb antistaling agent Download PDFInfo
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- CN105660843A CN105660843A CN201610095301.6A CN201610095301A CN105660843A CN 105660843 A CN105660843 A CN 105660843A CN 201610095301 A CN201610095301 A CN 201610095301A CN 105660843 A CN105660843 A CN 105660843A
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- CN
- China
- Prior art keywords
- antistaling agent
- herba passiflorae
- passiflorae caeruleae
- parts
- fruit
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- 235000000370 Passiflora edulis Nutrition 0.000 title abstract description 31
- 235000011925 Passiflora alata Nutrition 0.000 title abstract description 30
- 235000011922 Passiflora incarnata Nutrition 0.000 title abstract description 30
- 235000013750 Passiflora mixta Nutrition 0.000 title abstract description 30
- 235000013731 Passiflora van volxemii Nutrition 0.000 title abstract description 30
- 240000008440 Passiflora incarnata Species 0.000 title 1
- 239000003795 chemical substances by application Substances 0.000 claims abstract description 81
- 238000000034 method Methods 0.000 claims abstract description 38
- 239000005820 Prochloraz Substances 0.000 claims abstract description 19
- TVLSRXXIMLFWEO-UHFFFAOYSA-N prochloraz Chemical compound C1=CN=CN1C(=O)N(CCC)CCOC1=C(Cl)C=C(Cl)C=C1Cl TVLSRXXIMLFWEO-UHFFFAOYSA-N 0.000 claims abstract description 19
- ONUFESLQCSAYKA-UHFFFAOYSA-N iprodione Chemical compound O=C1N(C(=O)NC(C)C)CC(=O)N1C1=CC(Cl)=CC(Cl)=C1 ONUFESLQCSAYKA-UHFFFAOYSA-N 0.000 claims abstract description 17
- 238000002360 preparation method Methods 0.000 claims abstract description 14
- HDTRYLNUVZCQOY-UHFFFAOYSA-N α-D-glucopyranosyl-α-D-glucopyranoside Natural products OC1C(O)C(O)C(CO)OC1OC1C(O)C(O)C(O)C(CO)O1 HDTRYLNUVZCQOY-UHFFFAOYSA-N 0.000 claims abstract description 10
- HDTRYLNUVZCQOY-WSWWMNSNSA-N Trehalose Natural products O[C@@H]1[C@@H](O)[C@@H](O)[C@@H](CO)O[C@@H]1O[C@@H]1[C@H](O)[C@@H](O)[C@@H](O)[C@@H](CO)O1 HDTRYLNUVZCQOY-WSWWMNSNSA-N 0.000 claims abstract description 10
- -1 glycosyl trehalose Chemical compound 0.000 claims abstract description 10
- 238000004321 preservation Methods 0.000 claims abstract description 10
- YWIVKILSMZOHHF-QJZPQSOGSA-N sodium;(2s,3s,4s,5r,6r)-6-[(2s,3r,4r,5s,6r)-3-acetamido-2-[(2s,3s,4r,5r,6r)-6-[(2r,3r,4r,5s,6r)-3-acetamido-2,5-dihydroxy-6-(hydroxymethyl)oxan-4-yl]oxy-2-carboxy-4,5-dihydroxyoxan-3-yl]oxy-5-hydroxy-6-(hydroxymethyl)oxan-4-yl]oxy-3,4,5-trihydroxyoxane-2- Chemical compound [Na+].CC(=O)N[C@H]1[C@H](O)O[C@H](CO)[C@@H](O)[C@@H]1O[C@H]1[C@H](O)[C@@H](O)[C@H](O[C@H]2[C@@H]([C@@H](O[C@H]3[C@@H]([C@@H](O)[C@H](O)[C@H](O3)C(O)=O)O)[C@H](O)[C@@H](CO)O2)NC(C)=O)[C@@H](C(O)=O)O1 YWIVKILSMZOHHF-QJZPQSOGSA-N 0.000 claims abstract description 10
- CDQSJQSWAWPGKG-UHFFFAOYSA-N butane-1,1-diol Chemical compound CCCC(O)O CDQSJQSWAWPGKG-UHFFFAOYSA-N 0.000 claims abstract description 9
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims abstract description 9
- 239000004094 surface-active agent Substances 0.000 claims abstract description 5
- 239000002562 thickening agent Substances 0.000 claims abstract description 5
- 238000003801 milling Methods 0.000 claims description 28
- 239000004576 sand Substances 0.000 claims description 28
- 230000008569 process Effects 0.000 claims description 23
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- 239000002002 slurry Substances 0.000 claims description 21
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- 235000021022 fresh fruits Nutrition 0.000 claims description 7
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- 239000003755 preservative agent Substances 0.000 claims description 5
- 230000002335 preservative effect Effects 0.000 claims description 5
- 238000002604 ultrasonography Methods 0.000 claims description 5
- WRIDQFICGBMAFQ-UHFFFAOYSA-N (E)-8-Octadecenoic acid Natural products CCCCCCCCCC=CCCCCCCC(O)=O WRIDQFICGBMAFQ-UHFFFAOYSA-N 0.000 claims description 4
- LQJBNNIYVWPHFW-UHFFFAOYSA-N 20:1omega9c fatty acid Natural products CCCCCCCCCCC=CCCCCCCCC(O)=O LQJBNNIYVWPHFW-UHFFFAOYSA-N 0.000 claims description 4
- CYDQOEWLBCCFJZ-UHFFFAOYSA-N 4-(4-fluorophenyl)oxane-4-carboxylic acid Chemical compound C=1C=C(F)C=CC=1C1(C(=O)O)CCOCC1 CYDQOEWLBCCFJZ-UHFFFAOYSA-N 0.000 claims description 4
- QSBYPNXLFMSGKH-UHFFFAOYSA-N 9-Heptadecensaeure Natural products CCCCCCCC=CCCCCCCCC(O)=O QSBYPNXLFMSGKH-UHFFFAOYSA-N 0.000 claims description 4
- 239000005642 Oleic acid Substances 0.000 claims description 4
- ZQPPMHVWECSIRJ-UHFFFAOYSA-N Oleic acid Natural products CCCCCCCCC=CCCCCCCCC(O)=O ZQPPMHVWECSIRJ-UHFFFAOYSA-N 0.000 claims description 4
- TVXBFESIOXBWNM-UHFFFAOYSA-N Xylitol Natural products OCCC(O)C(O)C(O)CCO TVXBFESIOXBWNM-UHFFFAOYSA-N 0.000 claims description 4
- 125000002252 acyl group Chemical group 0.000 claims description 4
- 239000000679 carrageenan Substances 0.000 claims description 4
- 235000010418 carrageenan Nutrition 0.000 claims description 4
- 229920001525 carrageenan Polymers 0.000 claims description 4
- 229940113118 carrageenan Drugs 0.000 claims description 4
- QXJSBBXBKPUZAA-UHFFFAOYSA-N isooleic acid Natural products CCCCCCCC=CCCCCCCCCC(O)=O QXJSBBXBKPUZAA-UHFFFAOYSA-N 0.000 claims description 4
- HEBKCHPVOIAQTA-UHFFFAOYSA-N meso ribitol Natural products OCC(O)C(O)C(O)CO HEBKCHPVOIAQTA-UHFFFAOYSA-N 0.000 claims description 4
- ZQPPMHVWECSIRJ-KTKRTIGZSA-N oleic acid Chemical compound CCCCCCCC\C=C/CCCCCCCC(O)=O ZQPPMHVWECSIRJ-KTKRTIGZSA-N 0.000 claims description 4
- 239000001540 sodium lactate Substances 0.000 claims description 4
- 229940005581 sodium lactate Drugs 0.000 claims description 4
- 235000011088 sodium lactate Nutrition 0.000 claims description 4
- 235000010199 sorbic acid Nutrition 0.000 claims description 4
- 239000004334 sorbic acid Substances 0.000 claims description 4
- 229940075582 sorbic acid Drugs 0.000 claims description 4
- 235000015112 vegetable and seed oil Nutrition 0.000 claims description 4
- 239000008158 vegetable oil Substances 0.000 claims description 4
- 239000000230 xanthan gum Substances 0.000 claims description 4
- 229920001285 xanthan gum Polymers 0.000 claims description 4
- 235000010493 xanthan gum Nutrition 0.000 claims description 4
- 229940082509 xanthan gum Drugs 0.000 claims description 4
- 239000000811 xylitol Substances 0.000 claims description 4
- HEBKCHPVOIAQTA-SCDXWVJYSA-N xylitol Chemical compound OC[C@H](O)[C@@H](O)[C@H](O)CO HEBKCHPVOIAQTA-SCDXWVJYSA-N 0.000 claims description 4
- 229960002675 xylitol Drugs 0.000 claims description 4
- 235000010447 xylitol Nutrition 0.000 claims description 4
- UHVMMEOXYDMDKI-JKYCWFKZSA-L zinc;1-(5-cyanopyridin-2-yl)-3-[(1s,2s)-2-(6-fluoro-2-hydroxy-3-propanoylphenyl)cyclopropyl]urea;diacetate Chemical compound [Zn+2].CC([O-])=O.CC([O-])=O.CCC(=O)C1=CC=C(F)C([C@H]2[C@H](C2)NC(=O)NC=2N=CC(=CC=2)C#N)=C1O UHVMMEOXYDMDKI-JKYCWFKZSA-L 0.000 claims description 4
- NIXOWILDQLNWCW-UHFFFAOYSA-N Acrylic acid Chemical compound OC(=O)C=C NIXOWILDQLNWCW-UHFFFAOYSA-N 0.000 claims description 3
- 239000004354 Hydroxyethyl cellulose Substances 0.000 claims description 3
- 229920000663 Hydroxyethyl cellulose Polymers 0.000 claims description 3
- 229920002125 Sokalan® Polymers 0.000 claims description 3
- 229960001631 carbomer Drugs 0.000 claims description 3
- 235000019447 hydroxyethyl cellulose Nutrition 0.000 claims description 3
- WSWCOQWTEOXDQX-MQQKCMAXSA-M (E,E)-sorbate Chemical compound C\C=C\C=C\C([O-])=O WSWCOQWTEOXDQX-MQQKCMAXSA-M 0.000 claims description 2
- 229940071826 hydroxyethyl cellulose Drugs 0.000 claims description 2
- 229940075554 sorbate Drugs 0.000 claims description 2
- WSWCOQWTEOXDQX-MQQKCMAXSA-N sorbic acid group Chemical group C(\C=C\C=C\C)(=O)O WSWCOQWTEOXDQX-MQQKCMAXSA-N 0.000 claims description 2
- 235000013399 edible fruits Nutrition 0.000 abstract description 58
- 241000218996 Passiflora Species 0.000 abstract description 30
- 238000003860 storage Methods 0.000 abstract description 17
- 210000002615 epidermis Anatomy 0.000 abstract description 5
- 239000000126 substance Substances 0.000 abstract description 5
- 230000008901 benefit Effects 0.000 abstract description 4
- 230000001954 sterilising effect Effects 0.000 abstract description 4
- 150000001875 compounds Chemical class 0.000 abstract description 3
- 238000004659 sterilization and disinfection Methods 0.000 abstract description 3
- 235000012055 fruits and vegetables Nutrition 0.000 abstract description 2
- 230000003020 moisturizing effect Effects 0.000 abstract description 2
- 239000005867 Iprodione Substances 0.000 abstract 1
- 229920002385 Sodium hyaluronate Polymers 0.000 abstract 1
- 230000002035 prolonged effect Effects 0.000 abstract 1
- 238000002791 soaking Methods 0.000 abstract 1
- 229940010747 sodium hyaluronate Drugs 0.000 abstract 1
- 230000001988 toxicity Effects 0.000 abstract 1
- 231100000419 toxicity Toxicity 0.000 abstract 1
- 230000000694 effects Effects 0.000 description 14
- 208000016261 weight loss Diseases 0.000 description 14
- 230000004580 weight loss Effects 0.000 description 14
- 238000010586 diagram Methods 0.000 description 8
- 238000012545 processing Methods 0.000 description 6
- CHHHXKFHOYLYRE-UHFFFAOYSA-M 2,4-Hexadienoic acid, potassium salt (1:1), (2E,4E)- Chemical compound [K+].CC=CC=CC([O-])=O CHHHXKFHOYLYRE-UHFFFAOYSA-M 0.000 description 5
- 235000010241 potassium sorbate Nutrition 0.000 description 5
- 239000004302 potassium sorbate Substances 0.000 description 5
- 229940069338 potassium sorbate Drugs 0.000 description 5
- 230000000844 anti-bacterial effect Effects 0.000 description 4
- 239000007787 solid Substances 0.000 description 4
- 230000032683 aging Effects 0.000 description 3
- 230000018044 dehydration Effects 0.000 description 3
- 238000006297 dehydration reaction Methods 0.000 description 3
- 239000000796 flavoring agent Substances 0.000 description 3
- 235000019634 flavors Nutrition 0.000 description 3
- 235000015203 fruit juice Nutrition 0.000 description 3
- 238000003306 harvesting Methods 0.000 description 3
- 208000015181 infectious disease Diseases 0.000 description 3
- 238000012360 testing method Methods 0.000 description 3
- CIWBSHSKHKDKBQ-JLAZNSOCSA-N Ascorbic acid Chemical compound OC[C@H](O)[C@H]1OC(=O)C(O)=C1O CIWBSHSKHKDKBQ-JLAZNSOCSA-N 0.000 description 2
- 244000115658 Dahlia pinnata Species 0.000 description 2
- 235000012040 Dahlia pinnata Nutrition 0.000 description 2
- VGGSQFUCUMXWEO-UHFFFAOYSA-N Ethene Chemical compound C=C VGGSQFUCUMXWEO-UHFFFAOYSA-N 0.000 description 2
- 239000005977 Ethylene Substances 0.000 description 2
- 239000004283 Sodium sorbate Substances 0.000 description 2
- 230000015572 biosynthetic process Effects 0.000 description 2
- 210000004027 cell Anatomy 0.000 description 2
- 230000008859 change Effects 0.000 description 2
- 239000002131 composite material Substances 0.000 description 2
- 230000003111 delayed effect Effects 0.000 description 2
- 201000010099 disease Diseases 0.000 description 2
- 208000037265 diseases, disorders, signs and symptoms Diseases 0.000 description 2
- BEFDCLMNVWHSGT-UHFFFAOYSA-N ethenylcyclopentane Chemical compound C=CC1CCCC1 BEFDCLMNVWHSGT-UHFFFAOYSA-N 0.000 description 2
- 239000003205 fragrance Substances 0.000 description 2
- 230000005764 inhibitory process Effects 0.000 description 2
- 238000002372 labelling Methods 0.000 description 2
- 230000000813 microbial effect Effects 0.000 description 2
- 235000015097 nutrients Nutrition 0.000 description 2
- 235000016709 nutrition Nutrition 0.000 description 2
- 230000004224 protection Effects 0.000 description 2
- LROWVYNUWKVTCU-STWYSWDKSA-M sodium sorbate Chemical compound [Na+].C\C=C\C=C\C([O-])=O LROWVYNUWKVTCU-STWYSWDKSA-M 0.000 description 2
- 235000019250 sodium sorbate Nutrition 0.000 description 2
- 208000019901 Anxiety disease Diseases 0.000 description 1
- 241000196324 Embryophyta Species 0.000 description 1
- 241000238631 Hexapoda Species 0.000 description 1
- 244000288157 Passiflora edulis Species 0.000 description 1
- 241000218995 Passifloraceae Species 0.000 description 1
- 229930182558 Sterol Natural products 0.000 description 1
- 235000009392 Vitis Nutrition 0.000 description 1
- 241000219095 Vitis Species 0.000 description 1
- 241000607479 Yersinia pestis Species 0.000 description 1
- 240000008042 Zea mays Species 0.000 description 1
- 235000005824 Zea mays ssp. parviglumis Nutrition 0.000 description 1
- 235000002017 Zea mays subsp mays Nutrition 0.000 description 1
- 230000003213 activating effect Effects 0.000 description 1
- 230000000845 anti-microbial effect Effects 0.000 description 1
- 230000036506 anxiety Effects 0.000 description 1
- 235000010323 ascorbic acid Nutrition 0.000 description 1
- 229960005070 ascorbic acid Drugs 0.000 description 1
- 239000011668 ascorbic acid Substances 0.000 description 1
- QVGXLLKOCUKJST-UHFFFAOYSA-N atomic oxygen Chemical compound [O] QVGXLLKOCUKJST-UHFFFAOYSA-N 0.000 description 1
- 244000052616 bacterial pathogen Species 0.000 description 1
- 230000009286 beneficial effect Effects 0.000 description 1
- 238000009395 breeding Methods 0.000 description 1
- 230000001488 breeding effect Effects 0.000 description 1
- 150000001720 carbohydrates Chemical class 0.000 description 1
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- 229920002678 cellulose Polymers 0.000 description 1
- 238000006243 chemical reaction Methods 0.000 description 1
- 235000005822 corn Nutrition 0.000 description 1
- 230000006866 deterioration Effects 0.000 description 1
- 238000011161 development Methods 0.000 description 1
- 230000018109 developmental process Effects 0.000 description 1
- 229940117389 dichlorobenzene Drugs 0.000 description 1
- 125000001495 ethyl group Chemical group [H]C([H])([H])C([H])([H])* 0.000 description 1
- 230000004345 fruit ripening Effects 0.000 description 1
- 230000000855 fungicidal effect Effects 0.000 description 1
- 239000000417 fungicide Substances 0.000 description 1
- 229940091173 hydantoin Drugs 0.000 description 1
- 150000002460 imidazoles Chemical class 0.000 description 1
- 239000010410 layer Substances 0.000 description 1
- 231100000053 low toxicity Toxicity 0.000 description 1
- 238000012423 maintenance Methods 0.000 description 1
- 238000004519 manufacturing process Methods 0.000 description 1
- 244000005700 microbiome Species 0.000 description 1
- 239000002541 mycostatic Substances 0.000 description 1
- 230000001557 mycostatic effect Effects 0.000 description 1
- 231100000252 nontoxic Toxicity 0.000 description 1
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- 238000007254 oxidation reaction Methods 0.000 description 1
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- 229910052760 oxygen Inorganic materials 0.000 description 1
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Classifications
-
- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23B—PRESERVING, e.g. BY CANNING, MEAT, FISH, EGGS, FRUIT, VEGETABLES, EDIBLE SEEDS; CHEMICAL RIPENING OF FRUIT OR VEGETABLES; THE PRESERVED, RIPENED, OR CANNED PRODUCTS
- A23B7/00—Preservation or chemical ripening of fruit or vegetables
- A23B7/14—Preserving or ripening with chemicals not covered by groups A23B7/08 or A23B7/10
- A23B7/153—Preserving or ripening with chemicals not covered by groups A23B7/08 or A23B7/10 in the form of liquids or solids
- A23B7/154—Organic compounds; Microorganisms; Enzymes
-
- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23V—INDEXING SCHEME RELATING TO FOODS, FOODSTUFFS OR NON-ALCOHOLIC BEVERAGES AND LACTIC OR PROPIONIC ACID BACTERIA USED IN FOODSTUFFS OR FOOD PREPARATION
- A23V2002/00—Food compositions, function of food ingredients or processes for food or foodstuffs
Abstract
The invention relates to the technical field of fruit and vegetable preservation, and discloses a passionflower herb antistaling agent. The passionflower herb antistaling agent is prepared from, by weight, 20-100 parts of prochloraz and/or iprodione, 10-30 parts of butanediol, 1-5 parts of glycosyl trehalose, 0.1-1 part of sodium hyaluronate, 0.1-1 part of thickener, 5-10 parts of surfactant and 100-500 parts of water. The invention further provides a preparation method of the passionflower herb antistaling agent and a method for conducting preservation treatment on passionflower herb through the antistaling agent. The antistaling agent can significantly control epidermis shrinking and fruit rotting of the passionflower herb through a technology of combining sterilizing and moisturizing, the storage period and shelf life of the passionflower herb are effectively prolonged, and the commodity value and economic benefit are improved; meanwhile, by means of the antistaling agent and negative pressure or ultrasonic wave compound soaking treatment, chemical preservation and physical sterilization are compounded, safety is achieved, and toxicity does not exist. The preparation method of the passionflower herb antistaling agent is simple, efficient, safe and wide in application prospect.
Description
Technical field
The present invention relates to fruits and vegetable stock and preserving freshness field, particularly relate to a kind of Herba Passiflorae Caeruleae antistaling agent.
Background technology
Herba Passiflorae Caeruleae, belongs to maximum and most important Passiflora in Passifloraceae, for tropical perennial herbaceous stem to half bejuco, is mainly distributed on the Guangxi of China, Taiwan, Fujian, Yunnan, Guangdong etc. and economizes (district). Herba Passiflorae Caeruleae is with rich flavor, and fragrance is pleasant. The particularity of its fragrance, rich in nutritional labeling and the medical value such as potential anxiety, the deep accreditation by the numerous common people. But owing to its fruit maturation is in high temperature season, peel easily tarnishes, dehydration shrinkage and be subject to infection process and rot, thus losing commercial value. Therefore, the research strengthening Herba Passiflorae Caeruleae post-harvest fresh-keeping technology is particularly significant. Its fruit shape is spherical shape, and centre is cavity, and mainly there are pulp with rich flavor and pseudosperm in the inside. The ascorbic acid content that passion flower fruit contains is that every 100 grams of fruits are heavy containing 20-30mg, and in particular, its edible seed fraction is extraordinary edible cellulose source. And, Herba Passiflorae Caeruleae also contains very abundant natural phenolic compound, and it has the activity of inhibited oxidation damage. In general, passion flower fruit Post-harvest quality is mainly determined by harvest time and holding conditions. Postharvest decay mainly, microbial infection dimmed by moisture loss, fruit colour and what nutrient substance loss caused. These factors can cause forfeiture appearance value in fruit production process, thus losing commodity value. These external appearance characteristics include that shrinkage, peel be dimmed, the shortage etc. of postharvest decay and nutritional labeling. From physiology's aspect, Herba Passiflorae Caeruleae breathes peculiar property due to it, and ethylene produces, climacteric, and the responsing reaction of some responses is classified in climacteric type fruit. Degenerating, it is dehydration immediately after gathering passion flower fruit quality and appearance stablity.The peak of this breathing rate having the substantial amounts of biosynthesis of ethylene to cause in After-ripening of gathering mainly due to Herba Passiflorae Caeruleae.
These deterioration cause that fruit loses market value and unsalable, and appropriate postharvest handling and reserve temperature can keep the various quality characteristics of garden crop, and extend its shelf life. Storage period Herba Passiflorae Caeruleae is processed by the biochemical antistaling agent of application, is improve storage fresh-keeping effect, the effective ways of Shelf-life at present. Thus, antistaling agent exploitation safely and efficiently is also a current very important content, and the development of Herba Passiflorae Caeruleae industry is significant.
Summary of the invention
The goal of the invention of the present invention is in that: for above-mentioned Problems existing, it is provided that a kind of Herba Passiflorae Caeruleae antistaling agent, and it can effectively extend Herba Passiflorae Caeruleae storage period and shelf life, improves commodity value and economic benefit, has good exploitation application potential. Meanwhile, the preparation method that the present invention also provides for a kind of above-mentioned antistaling agent, and use the method that Herba Passiflorae Caeruleae carries out Preservation Treatment by above-mentioned antistaling agent.
In order to realize foregoing invention purpose, the technical solution used in the present invention is as follows:
A kind of Herba Passiflorae Caeruleae antistaling agent, in parts by weight, described antistaling agent component is: Prochloraz and/or RP-26019 20 ~ 100 parts, butanediol 10 ~ 30 parts, glycosyl trehalose 1 ~ 5 part, hyaluronate sodium 0.1 ~ 1 part, thickening agent 0.1 ~ 1 part, 5 ~ 10 parts of surfactant, 100 ~ 500 parts of water.
Further, described thickening agent is one or more in xanthan gum, carrageenan, carbomer or hydroxyethyl cellulose.
Further, described surfactant is vegetable oil acyl group sodium lactate or xylitol oleic acid monoester.
Further, described antistaling agent also includes preservative 0.5 ~ 1 part.
Further, described preservative is sorbic acid or sorbate.
The preparation method that present invention also offers above-mentioned antistaling agent, described preparation method is:
(1) weigh each composition according to described proportion relation, join mix homogeneously in high-speed shearing machine, obtain mixed material;
(2) mixed material being carried out sand milling, obtain sand milling disposed slurry, the particle diameter D50 controlling sand milling disposed slurry is 0.5 μm ~ 10 μm;
(3) again sand milling disposed slurry is carried out homogenizing, obtain described antistaling agent.
Present invention also offers the using method of above-mentioned antistaling agent, described using method is: the Herba Passiflorae Caeruleae fresh fruit gathered is immersed described Herba Passiflorae Caeruleae antistaling agent, immersion treatment 3 ~ 8 minutes, dries.
Further, described immersion treatment is negative pressure immersion treatment, and condition of negative pressure is-0.05MPa, and the process time is 5 ~ 8 minutes.
Further, described immersion treatment is ultrasound wave immersion treatment, and supersonic frequency is 20 ~ 30KHz, and the process time is 3 ~ 5 minutes.
Prochloraz in the present composition; chemical name is N-propyl group-N-[2-(2; 4; 6-Trichlorophenoxy) ethyl]-imidazoles-1-Methanamide; it is a kind of wide spectrum, low-toxicity imidazoles antibacterial; work by suppressing the biosynthesis of pathogenic bacteria cell membrane sterol, there is the effects such as Uptake and translocation, prevention, protection and treatment in plant.
RP-26019 in the present composition; chemical name is 3-(3; 5-Dichlorobenzene base)-1-isopropyl-carbamoyl hydantoin; it is protective fungicide; it is widely used in the storage of Fructus Vitis viniferae, fruit tree, flowers, vegetable, corn, Rhizoma Solani tuber osi and fruit etc., prevents and treats the multiple diseases such as gray mold, crown rot.
Prochloraz in the present composition and RP-26019 composition mixture preparation, can be used for fruit freshness preserving sterilization and anticorrosion and controlling disease etc., expand use crop and controlling object.
Glycosyl trehalose in the present composition, is a kind of natural saccharide, and it can protect epidermis cell membrane structure, activating cell effectively, and it can form protecting film one layer special at cell surface layer, is effective against fruit surface aging.
Hyaluronate sodium in the present composition, is the glutinous sugar of a kind of bionical thing, and molecular weight is more than 1,000,000, and not only moistening effect is good for it, moreover it is possible to eliminates the own base of oxygen, repairs the epidermis that fruit is aging.
Adopting potassium sorbate, sodium sorbate or sorbic acid in the present composition is preservative, and it has higher anti-microbial property, can effectively press down mycostatic growth and breeding.
Herba Passiflorae Caeruleae is adopted the contracting of consequence rhicnosis and fruit rot mainly, microbial infection dimmed by moisture loss, fruit colour and nutrient substance loss and is caused. Prochloraz in instant component and RP-26019 are antibacterial, are killed the microorganisms such as the antibacterial infected by antibacterial, delay passion flower-fruit peel shrinkage and sarcocarp to rot; Butanediol, glycosyl trehalose and hyaluronate sodium are wetting agent, it is prevented that also have the effect of protection epidermal tissue, hydrophilic and water suction while moisture loss, effectively prevent fruit surface aging.
In sum, owing to have employed technique scheme, the invention has the beneficial effects as follows:
(1) antistaling agent of the present invention significantly controls the generation of Herba Passiflorae Caeruleae epidermis shrinkage and fruit rot by the technology sterilized and moisturizing combines, and effectively extends Herba Passiflorae Caeruleae storage period and shelf life, improves commodity value and economic benefit;
(2) present invention adopts antistaling agent and negative pressure or ultrasound wave compound immersion treatment technology, fresh chemically and physical sterilization technology compound, safety non-toxic, and treatment effect is better than individual processing;
(3) antistaling agent preparation method of the present invention is simple, highly effective and safe, has good exploitation application potential in the links such as Herba Passiflorae Caeruleae storage, transport and sale.
Accompanying drawing explanation
Examples of the present invention will be described by way of reference to the accompanying drawings, wherein:
The antistaling agent that Fig. 1 is embodiment 1 ~ 5 processes the variation diagram to Herba Passiflorae Caeruleae shrinkage index;
The antistaling agent that Fig. 2 is embodiment 1 ~ 5 processes the variation diagram to Herba Passiflorae Caeruleae shrinkage weight-loss ratio;
The antistaling agent that Fig. 3 is embodiment 1 ~ 5 processes the variation diagram to Herba Passiflorae Caeruleae soluble solid content;
The antistaling agent that Fig. 4 is embodiment 1 ~ 5 processes the variation diagram to dahlia fruit juice pH value.
Detailed description of the invention
All features disclosed in this specification, or the step in disclosed all methods or process, except mutually exclusive feature and/or step, all can combine by any way.
This specification (include any accessory claim, summary) disclosed in any feature, unless specifically stated otherwise, all can by other equivalences or there is the alternative features of similar purpose replaced. That is, unless specifically stated otherwise, each feature is an example in a series of equivalence or similar characteristics.
Embodiment 1
A kind of Herba Passiflorae Caeruleae antistaling agent, described antistaling agent component is: Prochloraz 800g, butanediol 200g, glycosyl trehalose 30g, hyaluronate sodium 3g, xanthan gum 5g, potassium sorbate 7g, water 3000g.
The preparation method of the above-mentioned antistaling agent of the present invention is:
(1) weigh each composition according to described proportion relation, join mix homogeneously in high-speed shearing machine, obtain mixed material;
(2) mixed material being carried out sand milling, obtain sand milling disposed slurry, the particle diameter D50 controlling sand milling disposed slurry is 0.5 μm ~ 10 μm;
(3) again sand milling disposed slurry is carried out homogenizing, obtain described antistaling agent.
The using method of the above-mentioned antistaling agent of the present invention is:
The Herba Passiflorae Caeruleae fresh fruit gathered is immersed above-mentioned Herba Passiflorae Caeruleae antistaling agent, and negative pressure immersion treatment 5 minutes, condition of negative pressure is-0.05MPa, then pulls out and dries, subpackage.
Embodiment 2
A kind of Herba Passiflorae Caeruleae antistaling agent, described antistaling agent component is: RP-26019 800g, butanediol 200g, glycosyl trehalose 30g, hyaluronate sodium 10g, carrageenan 5g, potassium sorbate 7g, vegetable oil acyl group sodium lactate 80g, water 3000g.
The preparation method of the above-mentioned antistaling agent of the present invention is:
(1) weigh each composition according to described proportion relation, join mix homogeneously in high-speed shearing machine, obtain mixed material;
(2) mixed material being carried out sand milling, obtain sand milling disposed slurry, the particle diameter D50 controlling sand milling disposed slurry is 0.5 μm ~ 10 μm;
(3) again sand milling disposed slurry is carried out homogenizing, obtain described antistaling agent.
The using method of the above-mentioned antistaling agent of the present invention is:
The Herba Passiflorae Caeruleae fresh fruit gathered is immersed above-mentioned Herba Passiflorae Caeruleae antistaling agent, and negative pressure immersion treatment 8 minutes, condition of negative pressure is-0.05MPa, then pulls out and dries, subpackage.
Embodiment 3
A kind of Herba Passiflorae Caeruleae antistaling agent, described antistaling agent component is: Prochloraz 550g and RP-26019 250g, butanediol 200g, glycosyl trehalose 30g, hyaluronate sodium 5g, carbomer 10g, potassium sorbate 7g, vegetable oil acyl group sodium lactate 80g, water 3000g.
The preparation method of the above-mentioned antistaling agent of the present invention is:
(1) weigh each composition according to described proportion relation, join mix homogeneously in high-speed shearing machine, obtain mixed material;
(2) mixed material being carried out sand milling, obtain sand milling disposed slurry, the particle diameter D50 controlling sand milling disposed slurry is 0.5 μm ~ 10 μm;
(3) again sand milling disposed slurry is carried out homogenizing, obtain described antistaling agent.
The using method of the above-mentioned antistaling agent of the present invention is:
The Herba Passiflorae Caeruleae fresh fruit gathered is immersed above-mentioned Herba Passiflorae Caeruleae antistaling agent, and negative pressure immersion treatment 5 minutes, condition of negative pressure is-0.05MPa, then pulls out and dries, subpackage.
Embodiment 4
A kind of Herba Passiflorae Caeruleae antistaling agent, described antistaling agent component is: Prochloraz 200g, butanediol 100g, glycosyl trehalose 50g, hyaluronate sodium 5g, hydroxyethyl cellulose 1g, potassium sorbate and sodium sorbate 10g, xylitol oleic acid monoester 50g, water 1000g.
The preparation method of the above-mentioned antistaling agent of the present invention is:
(1) weigh each composition according to described proportion relation, join mix homogeneously in high-speed shearing machine, obtain mixed material;
(2) mixed material being carried out sand milling, obtain sand milling disposed slurry, the particle diameter D50 controlling sand milling disposed slurry is 0.5 μm ~ 10 μm;
(3) again sand milling disposed slurry is carried out homogenizing, obtain described antistaling agent.
The using method of the above-mentioned antistaling agent of the present invention is:
The Herba Passiflorae Caeruleae fresh fruit gathered is immersed above-mentioned Herba Passiflorae Caeruleae antistaling agent, and ultrasound wave immersion treatment 5 minutes, supersonic frequency is 20KHz, then pulls out and dries, subpackage.
Embodiment 5
A kind of Herba Passiflorae Caeruleae antistaling agent, described antistaling agent component is: RP-26019 1000g, butanediol 300g, glycosyl trehalose 50g, hyaluronate sodium 10g, xanthan gum and carrageenan 10g, sorbic acid 10g, xylitol oleic acid monoester 100g, water 5000g.
The preparation method of the above-mentioned antistaling agent of the present invention is:
(1) weigh each composition according to described proportion relation, join mix homogeneously in high-speed shearing machine, obtain mixed material;
(2) mixed material being carried out sand milling, obtain sand milling disposed slurry, the particle diameter D50 controlling sand milling disposed slurry is 0.5 μm ~ 10 μm;
(3) again sand milling disposed slurry is carried out homogenizing, obtain described antistaling agent.
The using method of the above-mentioned antistaling agent of the present invention is:
The Herba Passiflorae Caeruleae fresh fruit gathered is immersed above-mentioned Herba Passiflorae Caeruleae antistaling agent, and ultrasound wave immersion treatment 3 minutes, supersonic frequency is 30KHz, then pulls out and dries, subpackage.
Select eight to ninety percent Maturity respectively, size, shape, color even, have no mechanical damage and the passionfruit of insect pest is practically applicable to carry out the test of the present embodiment 1-5, then respectively the main quality index of fruit that is untreated and that process through the present embodiment 1-5 test is measured.
The main quality index measured is following 4:
(1) shr and shrinkage index
Observe 5 Herba Passiflorae Caeruleae shrinkage areas, it is determined that (0 represents pucker-free to its shr every time; 1 represents 0-25% shrinkage; 2 represent 25%-50% shrinkage; 3 represent 50%-75% shrinkage; 4 represent 75%-100% shrinkage), three repetitions are set. This degree Herba Passiflorae Caeruleae number of shrinkage index=∑ shr */Herba Passiflorae Caeruleae sum;
(2) weight-loss ratio computing formula: weight-loss ratio/%=[before (before storage fruit weight-storage consequence weight)/storage fruit weight]/100;
(3) soluble solid content measures and adopts hand-hold refractometer to measure
(4) pH pH meter directly measures fruit juice pH
Test result is respectively referring to accompanying drawing 1 ~ 4.
(1) fruit shr is one of important indicator evaluating fruit storage quality, and fruit surface dehydration shrinkage can have a strong impact on the exterior quality of fruit, thus affecting its commodity value. The variation diagram to Herba Passiflorae Caeruleae shrinkage index is processed referring to the antistaling agent that accompanying drawing 1 is embodiment 1 ~ 5. Result shows, untreated passion flower fruit (i.e. matched group) is extremely shrinkage after three days, and substantially all shrinkage after a week loses commodity value, and part fruit surface starts to decay; Under room temperature in 0-3 days, all there is not shrinkage phenomenon in treated Herba Passiflorae Caeruleae epidermis, and after the 3rd day, Herba Passiflorae Caeruleae all starts to occur shrinkage, and right shrinkage index is far below matched group; Wherein, the Herba Passiflorae Caeruleae shrinkage degree that Prochloraz processes is the lightest, and slowly, most fruit surface shrinkage area, less than 20%, preserves the shr of 24 days all less than 1 to variation tendency, and fruit commercialization effect is fine; The Herba Passiflorae Caeruleae shrinkage area change that RP-26019 processes is very fast, but still has inhibition, preserves the shr of 12 days less than 1; Prochloraz and RP-26019 mixed processing shrinkage area change are relatively large. From accompanying drawing 1 it can be seen that antistaling agent of the present invention has significantly delayed the shr of passion flower fruit storage room temperature, maintain exterior quality during it is preserved, be conducive to preservation and freshness.
(2) variation diagram to Herba Passiflorae Caeruleae shrinkage weight-loss ratio is processed referring to the antistaling agent that accompanying drawing 2 is embodiment 1 ~ 5. Result shows, three days later weight-loss ratios of untreated passion flower fruit (i.e. matched group) substantially increase, until preserving the 36th day, the trend all linearly increased, and fruit is shrivelled, loses commodity value; Under room temperature in 0-3 days, treated passion flower fruit weight-loss ratio is less, and after the 3rd day, passion flower fruit weight-loss ratio starts to increase, but weight-loss ratio is far below matched group; Wherein, the Herba Passiflorae Caeruleae weight-loss ratio that Prochloraz processes is minimum, and variation tendency is slow, preserves 36 days most fruit weight-loss ratios less than 1%, and storage fruit commercialization effect is fine; Prochloraz and RP-26019 mixed processing weight-loss ratio increase relatively large. From accompanying drawing 2 it can be seen that antistaling agent of the present invention has significantly delayed the weight-loss ratio of passion flower fruit storage room temperature, maintain exterior quality during it is preserved, be conducive to preservation and freshness.
(3) variation diagram to Herba Passiflorae Caeruleae soluble solid (TSS) content is processed referring to the antistaling agent that accompanying drawing 3 is embodiment 1 ~ 5.Its TSS content of the passion flower fruit of these several process is all totally on a declining curve, especially untreated passion flower fruit, its TSS content is sharply downward trend, and through antistaling agent of the present invention process after Herba Passiflorae Caeruleae TSS changes of contents trend slower, wherein, its TSS content downward trend of passion flower fruit that Prochloraz processes slowly, is preserved 36 days most fruit TSS content and is remained at more than 16%, fruit commercialization effect is fine, is conducive to preservation and freshness; Preserve the 36 days fruit TSS content through Prochloraz and RP-26019 mixed processing and be also maintained at about 16%; The passion flower fruit TSS changes of contents that RP-26019 processes is relatively fast, but still has inhibition, and the fruit TSS content preserved 24 days is also maintained at about 16%. Illustrate that antistaling agent of the present invention processes passion flower fruit and is conducive to the maintenance of soluble solid content.
(4) pH value is the important indicator of passion flower fruit, is the important indicator determining fruit-like flavour. Processing the variation diagram to dahlia fruit juice pH value referring to the antistaling agent that accompanying drawing 4 is embodiment 1 ~ 5, pH value amplitude of variation is more big, and fresh-keeping effect is more poor. Result shows, untreated passion flower fruit (i.e. matched group) pH value is in the trend risen again that declines afterwards that first rises, and amplitude of variation is big; Treated passion flower fruit pH value is in downward trend after first rising, and amplitude of variation is little; Wherein, the passion flower fruit pH value amplitude of variation that Prochloraz processes is minimum, and storage fruit commercialization effect is fine; Prochloraz and RP-26019 mixed processing pH value amplitude of variation are relatively large. From accompanying drawing 4 it can be seen that antistaling agent of the present invention significantly reduces the pH value amplitude of variation of passion flower fruit, its fresh-keeping effect presented also is much better than untreated matched group.
In sum, the passion flower fruit processed through antistaling agent of the present invention can effectively delay shr and the weight-loss ratio that under room temperature, passion flower fruit is preserved, and be conducive to keeping the TSS content of fruit, significantly extend Herba Passiflorae Caeruleae storage period and shelf life, improve commodity value and economic benefit; Wherein under delaying room temperature in the shr of passion flower fruit storage, weight-loss ratio and pH value amplitude of variation, the effect that Prochloraz processes is better than RP-26019, and to be better than both composite, and on the TSS content keeping fruit, the effect that Prochloraz processes is better than that both are composite is better than RP-26019.
The invention is not limited in aforesaid detailed description of the invention. The present invention expands to any new feature disclosed in this manual or any new combination, and the step of the arbitrary new method disclosed or process or any new combination.
Claims (9)
1. a Herba Passiflorae Caeruleae antistaling agent, it is characterised in that in parts by weight, described antistaling agent component is: Prochloraz and/or RP-26019 20 ~ 100 parts, butanediol 10 ~ 30 parts, glycosyl trehalose 1 ~ 5 part, hyaluronate sodium 0.1 ~ 1 part, thickening agent 0.1 ~ 1 part, 5 ~ 10 parts of surfactant, 100 ~ 500 parts of water.
2. Herba Passiflorae Caeruleae antistaling agent according to claim 1, it is characterised in that described thickening agent is one or more in xanthan gum, carrageenan, carbomer or hydroxyethyl cellulose.
3. Herba Passiflorae Caeruleae antistaling agent according to claim 1, it is characterised in that described surfactant is vegetable oil acyl group sodium lactate or xylitol oleic acid monoester.
4. Herba Passiflorae Caeruleae antistaling agent according to claim 1, it is characterised in that described antistaling agent also includes preservative 0.5 ~ 1 part.
5. Herba Passiflorae Caeruleae antistaling agent according to claim 4, it is characterised in that described preservative is sorbic acid or sorbate.
6. the preparation method of the Herba Passiflorae Caeruleae antistaling agent according to claim 1 to 5 any claim, it is characterised in that described preparation method is:
(1) weigh each composition according to described proportion relation, join mix homogeneously in high-speed shearing machine, obtain mixed material;
(2) mixed material being carried out sand milling, obtain sand milling disposed slurry, the particle diameter D50 controlling sand milling disposed slurry is 0.5 μm ~ 10 μm;
(3) again sand milling disposed slurry is carried out homogenizing, obtain described antistaling agent.
7. the preservation method of the Herba Passiflorae Caeruleae antistaling agent according to claim 1 to 5 any claim, it is characterised in that the Herba Passiflorae Caeruleae fresh fruit gathered is immersed described Herba Passiflorae Caeruleae antistaling agent, immersion treatment 3 ~ 8 minutes, dries.
8. the preservation method of Herba Passiflorae Caeruleae antistaling agent according to claim 7, it is characterised in that described immersion treatment is negative pressure immersion treatment, and condition of negative pressure is-0.05MPa, the process time is 5 ~ 8 minutes.
9. the preservation method of Herba Passiflorae Caeruleae antistaling agent according to claim 7, it is characterised in that described immersion treatment is ultrasound wave immersion treatment, supersonic frequency is 20 ~ 30KHz, and the process time is 3 ~ 5 minutes.
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CN113995012A (en) * | 2021-09-30 | 2022-02-01 | 广西南亚热带农业科学研究所 | Method for preserving and storing macadimia nuts |
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