CN105624800B - A kind of bio-bleaching method for degummed ramie fiber production - Google Patents

A kind of bio-bleaching method for degummed ramie fiber production Download PDF

Info

Publication number
CN105624800B
CN105624800B CN201410614122.XA CN201410614122A CN105624800B CN 105624800 B CN105624800 B CN 105624800B CN 201410614122 A CN201410614122 A CN 201410614122A CN 105624800 B CN105624800 B CN 105624800B
Authority
CN
China
Prior art keywords
bio
bleaching
ramie
bacterium solution
bar shaped
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Active
Application number
CN201410614122.XA
Other languages
Chinese (zh)
Other versions
CN105624800A (en
Inventor
余龙江
樊培
彭咏絮
金文闻
胡祖德
胡振华
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
HUBEI JINGHUA TEXTILE GROUP CO Ltd
Huazhong University of Science and Technology
Original Assignee
HUBEI JINGHUA TEXTILE GROUP CO Ltd
Huazhong University of Science and Technology
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by HUBEI JINGHUA TEXTILE GROUP CO Ltd, Huazhong University of Science and Technology filed Critical HUBEI JINGHUA TEXTILE GROUP CO Ltd
Priority to CN201410614122.XA priority Critical patent/CN105624800B/en
Publication of CN105624800A publication Critical patent/CN105624800A/en
Application granted granted Critical
Publication of CN105624800B publication Critical patent/CN105624800B/en
Active legal-status Critical Current
Anticipated expiration legal-status Critical

Links

Landscapes

  • Preparation Of Compounds By Using Micro-Organisms (AREA)
  • Micro-Organisms Or Cultivation Processes Thereof (AREA)

Abstract

The present invention relates to a kind of bio-bleaching method for degummed ramie fiber production, it is used for ramie biological bleaching process after being diluted using bacillus sp.HG 116 and Bacillus sp.HG 247 zymocyte liquid, fiber crops are 1: 8~1: 30 with the solid-liquid ratio of bio-bleaching liquid, and bleached ramie is obtained through 5~30min of bio-bleaching at 40~60 DEG C of temperature.The bio-bleaching liquid that the present invention is prepared using microbial inoculum is bleached instead of traditional chemical reagent to ramie, and treatment temperature is gentleer, and caused pollution significantly reduces with energy consumption;Any chemical article need not be added, avoids its injury for ramee;Lignin is effectively removed simultaneously, and degummed ramie whiteness is greatly improved.

Description

A kind of bio-bleaching method for degummed ramie fiber production
Technical field
The invention belongs to textile fabric manufacturing field, and in particular to a kind of bio-bleaching side for degummed ramie fiber production Method.
Background technology
In degummed ramie fiber production process, by degumming and the ramie bast fiber handled is flogged, half in bast colloid Cellulose has largely removed with compositions such as pectin, but lignin is generally still largely retained in bastuse surface or fiber Between gap, it is difficult to effectively degraded, so as to form coloured, the indefinite form powder on the keen-witted and capable flaxen fiber of product, extremely influence ramie Performance of the flaxen fiber in subsequently spinning, weave cotton cloth;If clothing is made, it skin is produced prodding and itching feeling, have a strong impact on clothing Performance and class.
It is wooden in ramie phloem by high temperature, high pressure, the Degumming Procedures of alkali white silk in traditional ramie chemical Degumming industry Plain part is combined with alkali, is generated alkali lignin and is dissolved in degumming alkali lye.Do not had an effect with alkali and remain on bastuse Lignin between surface or fiber gap, in following bleaching process, a large amount of bond energys present in lignin molecule are weaker Ehter bond is aoxidized and be broken by strong oxidizer, and coloured groups (such as aromatic radical) come off, or coloured groups are directly by by Strong oxdiative Agent oxidative decoloration, so as to eliminate influence of the lignin to degummed ramie quality.
Ren Chuanrong etc. discloses a kind of ramie fast degumming tech in publication number CN1041012A patent of invention, its Blanching step uses the chemical bleaching liquor that effective chlorine density is 0.5~1g/L;Liu is just elementary publication number CN1130216A's In patent of invention, a kind of biological degumming of ramie technology and equipment are disclosed, its bleaching conditions is 0.8~1.8g/L H2O2, pH value 11 ± 0.5,80~100 DEG C of temperature;Xu Meirong discloses one in publication number CN101037808A patent of invention The extraction and preparation method of kind ramee and application thereof and ramee, it includes blanching step twice, and respectively chlorine floats And oxygen bleaching, chlorine drift concentration is 3~8g/L NaClO, and oxygen bleaching uses 4~6g/L H2O2, 80~100 DEG C of temperature;Zhu Hongzhe exists In publication number CN102644195A patent of invention, disclose it is a kind of for it is fibrilia modified and with bath bleaching function additive and Its preparation method, its blanching step use 50~120g/LNaOH and 15~35g/L H2O2React 3~7h.
The problem of existing technology the is present above mainly chemical levels in bleaching process are larger, treatment temperature High, time length, pollutes big, high energy consumption, present environmental risks, does not meet the fundamental state policy of " environmental protection ", can not fit Answer the requirement of sustainable development.
The content of the invention
The technical problems to be solved by the invention are:A kind of bio-bleaching side for degummed ramie fiber production is provided Method, solves the problems such as chemical levels in existing ramie bleaching process are big, industrial water processing is difficult, environmental hazard is serious.
Technical proposal that the invention solves the above-mentioned problems is:A kind of bio-bleaching side for degummed ramie fiber production is provided Method, comprise the following steps:
S1, bacterium solution culture:Using bacillus sp.HG-116 as strain, by actication of culture step, Expand incubation step and obtain bacterium solution A;Using bacillus sp.HG-247 as strain, respectively by actication of culture Step, expand incubation step acquisition bacterium solution B;Bacillus sp.HG-116 is the bacterium that a plant height produces zytase Strain, the bacterial strain submitted to China typical culture collection center preservation on the 22nd in September in 2014, and address is in Hubei China province Wuhan Wuhan University of city, deposit number are CCTCC No:M 2014438);Bacillus sp.HG-247 produces for a plant height The bacterial strain of mannase, the bacterial strain submitted to China typical culture collection center preservation on 22nd in September in 2014, and address exists Wuhan University of Wuhan City of Hubei China province, deposit number are CCTCC No:M 2014439).Bacterium solution incubation is done in detail below Describe in detail bright:
Ith, bacillus sp.HG-116 fungi preservation, activation and expansion culture
Fungi preservation:Bacillus sp.HG-116 strains are inoculated into by 1% inoculum concentration and fill 80mL In the 250mL shaking flasks of No.1 culture medium, 3h is cultivated under conditions of 36 DEG C, 180r/min rotating speeds, the bacterium solution glycerine after culture Protecting method preserves under the conditions of -20 DEG C, obtains HG-116 strain tubes;
Activation:By HG-116 strain tubes place at room temperature 3min to bacterium solution melt after, be inoculated into by 1.2% inoculum concentration In the 1L shaking flasks for filling 250mL No.1 culture mediums, 4h is cultivated under conditions of 36 DEG C, 160r/min rotating speeds, obtains HG-116 work Change strain.
Expand culture:Bacterial strain HG-116 after activation is inoculated into the specification equipped with No. bis- culture mediums of 30L by 3% inoculum concentration For in 50L first class seed pot, in 36 DEG C, 120r/min rotating speeds and 2m34h is cultivated under conditions of/h throughputs.Then by one-level The bacterium solution of seeding tank is inoculated into by 5% inoculum concentration in the secondary seed tank that the specification equipped with No. bis- culture mediums of 600L is 1t, in 37 DEG C, 70r/min rotating speeds and 7m34h is cultivated under conditions of/h throughputs.
No.1 culture medium includes:Sucrose 25g/L, peptone 6g/L, potassium dihydrogen phosphate 3g/L, bitter salt 1.5g/ L, calcium nitrate 0.7g/L, sodium chloride 1.1g/L;With water constant volume, regulation pH is 7.1.
No. two culture mediums include:Oat xylan 22g/L, ammonium sulfate 8g/L, potassium dihydrogen phosphate 4g/L, bitter salt 2g/L, calcium nitrate 0.7g/L, sodium chloride 3g/L.With water constant volume, regulation pH is 7.1.
IIth, bacillus sp.HG-247 fungi preservation, activation and expansion culture
Fungi preservation:Bacillus sp.HG-247 strains are inoculated into by 1.5% inoculum concentration and filled In the 250mL shaking flasks of No. tri- culture mediums of 80mL, 4h is cultivated under conditions of 36 DEG C, 160r/min rotating speeds, the bacterium solution after culture is used Glycerine protecting method preserves under the conditions of -20 DEG C, obtains HG-247 strain tubes.
Activation:By HG-247 strain tubes place at room temperature 3min to bacterium solution melt after, be inoculated into by 1.5% inoculum concentration In the 1L shaking flasks for filling No. tri- culture mediums of 250mL, 4h is cultivated under conditions of 36 DEG C, 16r/min rotating speeds, obtains HG-247 activation Strain.
Expand culture:HG-247 activated spawns are inoculated into the specification equipped with No. tetra- culture mediums of 30L by 3% inoculum concentration is In 50L first class seed pot, in 36 DEG C, 120r/min rotating speeds and 2.5m35h is cultivated under conditions of/h throughput;Then by one The bacterium solution of level seeding tank is inoculated into by 4% inoculum concentration in the secondary seed tank that the specification equipped with No. tetra- culture mediums of 600L is 1t, In 36 DEG C, 80r/min rotating speeds and 8.5m34h is cultivated under conditions of/h throughputs;
No. three culture mediums include:Glucose 32g/L, peptone 12g/L, yeast extract 7g/L, potassium dihydrogen phosphate 4g/L, nitre Sour calcium 0.7g/L.With water constant volume, regulation pH is 7.0.
No. four culture mediums include:Konjaku flour 35g/L, peptone 14g/L, yeast extract 7g/L, potassium dihydrogen phosphate 7g/L, 0.6g/L.With water constant volume, regulation pH is 7.1.
It is prepared by S2, bio-bleaching liquid:The bacterium solution A and bacterium solution B are mixed according to volume ratio 1: 1~3.75: 1 Bacterium solution, the mixing bacterium solution is diluted with water 3~35 times and obtains dilution mixing bacterium solution, the dilution is mixed into bacterium solution as ramie Bio-bleaching liquid in bio-bleaching process;
S3, bio-bleaching:The bio-bleaching liquid is injected in Bellmer, the ramie after degumming and beating are handled and are drained Fiber crops are immersed in the bio-bleaching liquid, and the ramie and the solid-liquid ratio of the bio-bleaching liquid are 1: 8~1: 30, in temperature 40 5~30min of bio-bleaching obtains bleached ramie at~60 DEG C.
In the bio-bleaching method of the present invention, in the step S3, the bio-bleaching liquid recycles 25~30 times, The mixing bacterium solution that volume fraction is 0.5%~5% is added when recycling every time.
In the bio-bleaching method of the present invention, in the step S2, the Bellmer is bar shaped Bellmer, the bar shaped The both ends of Bellmer be respectively into numb end and going out numb end, be provided with the bar shaped Bellmer from it is described enter numb end to it is described go out First transmission crawler belt of numb end movement.First transmission crawler belt is immersed in bio-bleaching liquid, plays a part of drawing ramie movement, So ramie can be put into bar shaped Bellmer from numb end is entered, pull out from going out numb end, form continuous sample introduction, go out sample process, herein Period completes bleaching process.
In the bio-bleaching method of the present invention, the ramie it is described enter after numb end is placed into the bar shaped Bellmer, Go out numb end described in being moved under the drive of the described first transmission crawler belt.Ramie good dispersion in such a continuous bleaching process, Treating capacity is big, is contacted fully with bio-bleaching liquid, and automaticity is high, greatly reduces the labor intensity of worker.
In the bio-bleaching method of the present invention, the translational speed of the first transmission crawler belt is 0.1~5m/min, described Gradually raise and higher than the wall of the bar shaped Bellmer, carry the drift in the side that first transmission crawler belt goes out numb end described in White ramie leaves the bar shaped Bellmer and enters collection frame.Bleached ramie is held out the water surface by the first transmission crawler belt gradually raised, Most bio-bleaching liquid on bleached ramie, which can leach, flows back to bar shaped Bellmer, reduces the loss of bio-bleaching liquid;Meanwhile The the first transmission crawler belt gradually raised crosses the wall of bar shaped Bellmer, and bleached ramie is taken away into bar shaped Bellmer and taken off automatically Fall, into collection frame, collected manually without worker, simply, conveniently.
The present invention bio-bleaching method in, from it is described enter numb end inject into the bar shaped Bellmer dilution mixing bacterium Liquid, injection rate are 0.5~2m3/min.Constantly there is bleached ramie to be carried over numb end is gone out, bio-bleaching can be carried Liquid, therefore should supplement in time.In order to prevent prolonged continuous processing, the moisture that ramie carries in itself dilutes bio-bleaching Liquid, it can also be properly added and mix bacterium solution to increase the cell concentration in bio-bleaching liquid.
In the bio-bleaching method of the present invention, also include after the step S3:
S4, cleaning:The bleached ramie is woven into service sink with water by solid-liquid ratio 1: 20~1: 120, and immersion 3~ Take out, drain after 20min.Microbial cells and its secretion (such as protein) in bio-bleaching liquid can be adsorbed in bleaching ramie The surface of fiber crops, cleaning step are removed to it, avoid its quality to degummed ramie from having an impact.
In the bio-bleaching method of the present invention, the service sink is bar shaped service sink, is set in the bar shaped service sink There is the second transmission crawler belt, the bleached ramie is moved into one end of the bar shaped service sink and is fully submerged into water, second Transmit and picked up under the transmission of crawler belt after 3~20min is moved to the other end of the bar shaped Bellmer.Bar shaped service sink with it is foregoing Bar shaped Bellmer has similar structure, itself has certain water capacity, and bleached ramie receives the band of the second transmission crawler belt Action is used, and is moved into from one end of bar shaped service sink, other end removal, is haveed the function that cleaning.
In the bio-bleaching method of the present invention, the bar shaped service sink includes water inlet and delivery port, from water inlet The water of injection flows through the bar shaped service sink and flowed out from the delivery port, the water (flow) direction and the shifting of the described second transmission crawler belt It is dynamic in opposite direction.Because bleached ramie is continuously added into the delivery port side of bar shaped service sink, the bleached ramie direction of motion and water Stream is in opposite direction, constitutes a kind of counter-current relationship, therefore delivery port cell concentration or protein concentration are higher, then directly flows Go out, water inlet cell concentration or protein concentration are relatively low, and lasting have clear water to be supplemented in bar shaped service sink.Such a design can be with Reduce water consumption and make cleaning more thorough.
In the bio-bleaching method of the present invention, the water-carrying capacity of the water inlet is 0.5~5m3/min。
Implement the present invention, have the advantages that:The bio-bleaching liquid prepared using microbial inoculum replaces traditional Work reagent is bleached to ramie, and treatment temperature is gentleer, and caused pollution is significantly reduced with energy consumption, while lignin is had Effect removes, and degummed ramie whiteness is greatly improved.Degummed ramie its delignification rate of the present invention, degummed ramie residual gum content, whiteness, Bleaching process water consumption and COD and conventional method and standard GB/T/T 20793-2006 degummed ramie fiber primes indexs Contrast is as shown in table 1:
The bleaching results of table 1
1Refer to and often produce water consumption and COD caused by 1t degummed ramie fibers.
Embodiment
In order to make the purpose , technical scheme and advantage of the present invention be clearer, with reference to embodiments, to the present invention It is further elaborated.It should be appreciated that specific implementation described herein is not used to limit only to explain the present invention The present invention.
Embodiment 1
Bacterium solution A and bacterium solution B is mixed according to volume ratio 1: 1 and obtains mixing bacterium solution, mixing bacterium solution is diluted with water into 3 times obtains Dilution mixes bacterium solution, and dilution is mixed into bacterium solution as the bio-bleaching liquid in ramie biological bleaching process;Bio-bleaching liquid is noted Enter in Bellmer, the ramie after degumming and beating are handled and are drained is immersed in bio-bleaching liquid, ramie and bio-bleaching liquid Solid-liquid ratio be 1: 8, bio-bleaching 30min obtains bleached ramie at 40 DEG C of temperature, and bio-bleaching liquid recycles 30 times, often The mixing bacterium solution that volume fraction is 5% is added during secondary recycling.Bleached ramie is woven into service sink with water by solid-liquid ratio 1: 120 In, take out, drain after immersion 20min.
After testing, by the obtained degummed ramie of the present invention, delignification rate 77.5%, degummed ramie residual gum content 1.85%, Whiteness 51.5, bleaching process often produce water consumption 6.2t, COD88mg/L caused by 1t degummed ramie fibers.
Embodiment 2
Bacterium solution A and bacterium solution B is mixed according to volume ratio 3.75: 1 and obtains mixing bacterium solution, bacterium solution will be mixed and be diluted with water 35 times Obtain dilution and mix bacterium solution, dilution is mixed into bacterium solution as the bio-bleaching liquid in ramie biological bleaching process;By bio-bleaching In liquid injection Bellmer, the ramie after degumming and beating are handled and are drained is immersed in bio-bleaching liquid, and ramie floats with biology The solid-liquid ratio of white liquor is 1: 30, and bio-bleaching 5min obtains bleached ramie under temperature 60 C, and bio-bleaching liquid recycles 25 It is secondary, the mixing bacterium solution that volume fraction is 0.5% is added when recycling every time.Bleached ramie is woven into water by solid-liquid ratio 1: 20 In service sink, take out, drain after immersion 3min.
After testing, by the obtained degummed ramie of the present invention, delignification rate 79.1%, degummed ramie residual gum content 1.82%, Whiteness 51.7, bleaching process often produce water consumption 1.8t, COD265mg/L caused by 1t degummed ramie fibers.
Embodiment 3
Bacterium solution A and bacterium solution B is mixed according to volume ratio 2: 1 and obtains mixing bacterium solution, mixing bacterium solution is diluted with water into 10 times obtains Bacterium solution is mixed to dilution, dilution is mixed into bacterium solution as the bio-bleaching liquid in ramie biological bleaching process;By bio-bleaching liquid Inject in Bellmer, the ramie after degumming and beating are handled and are drained is immersed in bio-bleaching liquid, ramie and bio-bleaching The solid-liquid ratio of liquid is 1: 15, and bio-bleaching 20min obtains bleached ramie under temperature 45 C, and bio-bleaching liquid recycles 26 It is secondary, the mixing bacterium solution that volume fraction is 2% is added when recycling every time.Bleached ramie is woven into clearly with water by solid-liquid ratio 1: 40 In wash pool, take out, drain after immersion 10min.
After testing, by the obtained degummed ramie of the present invention, delignification rate 80.4%, degummed ramie residual gum content 1.78%, Whiteness 52.6, bleaching process often produce water consumption 3.7t, COD120mg/L caused by 1t degummed ramie fibers.
Embodiment 4
Bacterium solution A and bacterium solution B is mixed according to volume ratio 2: 1 and obtains mixing bacterium solution, mixing bacterium solution is diluted with water into 15 times obtains Bacterium solution is mixed to dilution, dilution is mixed into bacterium solution as the bio-bleaching liquid in ramie biological bleaching process;By bio-bleaching liquid Inject in bar shaped Bellmer, the ramie after degumming and beating are handled and are drained is immersed in bio-bleaching liquid, ramie and biology The solid-liquid ratio of bleaching liquid is 1: 20, and the translational speed of the first transmission crawler belt is 0.1m/min, from entering numb end into bar shaped Bellmer The speed that injection dilution mixes bacterium solution is 0.5m3/ min, bio-bleaching 30min, obtains bleached ramie under temperature 50 C.Bleaching Ramie is woven into bar shaped service sink with water by solid-liquid ratio 1: 60, and the water-carrying capacity of water inlet is 5m3/ min, water (flow) direction and second The moving direction of crawler belt is transmitted on the contrary, bleached ramie reaches under the transmission of the second transmission crawler belt through 20min from delivery port one end The water inlet other end.
After testing, by the obtained degummed ramie of the present invention, delignification rate 81.4%, degummed ramie residual gum content 1.75%, Whiteness 52.7, bleaching process often produce water consumption 6.9t, COD82mg/L caused by 1t degummed ramie fibers.
Embodiment 5
Bacterium solution A and bacterium solution B is mixed according to volume ratio 3: 1 and obtains mixing bacterium solution, mixing bacterium solution is diluted with water into 20 times obtains Bacterium solution is mixed to dilution, dilution is mixed into bacterium solution as the bio-bleaching liquid in ramie biological bleaching process;By bio-bleaching liquid Inject in bar shaped Bellmer, the ramie after degumming and beating are handled and are drained is immersed in bio-bleaching liquid, ramie and biology The solid-liquid ratio of bleaching liquid is 1: 15, and the translational speed of the first transmission crawler belt is 5m/min, is noted from numb end is entered into bar shaped Bellmer The speed for entering dilution mixing bacterium solution is 2m3/ min, the bio-bleaching 5min at 55 DEG C of temperature, obtains bleached ramie.Bleached ramie It is woven into water by solid-liquid ratio 1: 80 in bar shaped service sink, the water-carrying capacity of water inlet is 0.5m3/ min, water (flow) direction pass with second The moving direction of crawler belt is sent on the contrary, bleached ramie is reached into water under the transmission of the second transmission crawler belt through 3min from delivery port one end The mouth other end.
After testing, by the obtained degummed ramie of the present invention, delignification rate 84.4%, degummed ramie residual gum content 1.74%, Whiteness 53.5, bleaching process often produce water consumption 2.2t, COD140mg/L caused by 1t degummed ramie fibers.
Embodiment 6
Bacterium solution A and bacterium solution B is mixed according to volume ratio 2.5: 1 and obtains mixing bacterium solution, bacterium solution will be mixed and be diluted with water 18 times Obtain dilution and mix bacterium solution, dilution is mixed into bacterium solution as the bio-bleaching liquid in ramie biological bleaching process;By bio-bleaching In liquid injection bar shaped Bellmer, the ramie after degumming and beating are handled and are drained is immersed in bio-bleaching liquid, ramie and life The solid-liquid ratio of thing bleaching liquid is 1: 18, and the translational speed of the first transmission crawler belt is 2m/min, from entering numb end into bar shaped Bellmer The speed that injection dilution mixes bacterium solution is 1m3/ min, bio-bleaching 12min, obtains bleached ramie under temperature 45 C.Bleach ramie Fiber crops are woven into bar shaped service sink with water by solid-liquid ratio 1: 50, and the water-carrying capacity of water inlet is 2m3/ min, water (flow) direction pass with second The moving direction of crawler belt is sent on the contrary, bleached ramie is reached into water under the transmission of the second transmission crawler belt through 7min from delivery port one end The mouth other end.
After testing, by the obtained degummed ramie of the present invention, delignification rate 86.2%, degummed ramie residual gum content 1.73%, Whiteness 53.8, bleaching process often produce water consumption 3.4t, COD102mg/L caused by 1t degummed ramie fibers.

Claims (10)

  1. A kind of 1. bio-bleaching method for degummed ramie fiber production, it is characterised in that comprise the following steps:
    S1, bacterium solution culture:Using bacillus sp.HG-116 as strain, by actication of culture step, expand Incubation step obtains bacterium solution A;Using bacillus sp.HG-247 as strain, walked respectively by actication of culture Suddenly, expand incubation step and obtain bacterium solution B;
    It is prepared by S2, bio-bleaching liquid:The bacterium solution A and bacterium solution B is mixed according to volume ratio 1: 1~3.75: 1 and obtains mixing bacterium Liquid, the mixing bacterium solution is diluted with water 3~35 times and obtains dilution mixing bacterium solution, the dilution is mixed into bacterium solution gives birth to as ramie Bio-bleaching liquid in thing bleaching process;
    S3, bio-bleaching:The bio-bleaching liquid is injected in Bellmer, the ramie leaching after degumming and beating are handled and are drained Not in the bio-bleaching liquid, the ramie and the solid-liquid ratio of the bio-bleaching liquid are 1: 8~1: 30, in temperature 40~60 5~30min of bio-bleaching obtains bleached ramie at DEG C.
  2. 2. bio-bleaching method according to claim 1, it is characterised in that in the step S3, the bio-bleaching liquid Recycle 25~30 times, the mixing bacterium solution that volume fraction is 0.5%~5% is added when recycling every time.
  3. 3. bio-bleaching method according to claim 1, it is characterised in that in the step S2, the Bellmer is bar Shape Bellmer, the both ends of the bar shaped Bellmer are respectively into numb end and go out numb end, be provided with the bar shaped Bellmer from It is described enter numb end to it is described go out the movement of numb end the first transmission crawler belt.
  4. 4. bio-bleaching method according to claim 3, it is characterised in that the ramie it is described enter numb end be placed into institute After stating bar shaped Bellmer, be moved under the drive of the described first transmission crawler belt it is described go out numb end.
  5. 5. bio-bleaching method according to claim 4, it is characterised in that it is described first transmission crawler belt translational speed be 0.1~5m/min, the side that the first transmission crawler belt goes out numb end described in are gradually raised and are higher than the bar shaped Bellmer Wall, carry the bleached ramie and leave the bar shaped Bellmer and enter collection frame.
  6. 6. the bio-bleaching method according to any one in claim 3~5, it is characterised in that from it is described enter numb end to Injection dilution mixes bacterium solution in the bar shaped Bellmer, and injection rate is 0.5~2m3/min。
  7. 7. bio-bleaching method according to claim 1, it is characterised in that also include after the step S3:
    S4, cleaning:The bleached ramie is woven into service sink with water by solid-liquid ratio 1: 20~1: 120, after soaking 3~20min Take out, drain.
  8. 8. bio-bleaching method according to claim 3, it is characterised in that the service sink is bar shaped service sink, described The second transmission crawler belt is provided with bar shaped service sink, the bleached ramie is moved into one end of the bar shaped service sink and fully soaked Submerge in water, picked up under the transmission of the second transmission crawler belt after 3~20min is moved to the other end of the bar shaped Bellmer.
  9. 9. bio-bleaching method according to claim 8, it is characterised in that the bar shaped service sink include water inlet and Delivery port, flow through the bar shaped service sink from the water of water inlet injection and flowed out from the delivery port, the water (flow) direction with it is described The moving direction of second transmission crawler belt is opposite.
  10. 10. bio-bleaching method according to claim 9, it is characterised in that the water-carrying capacity of the water inlet be 0.5~ 5m3/min。
CN201410614122.XA 2014-11-04 2014-11-04 A kind of bio-bleaching method for degummed ramie fiber production Active CN105624800B (en)

Priority Applications (1)

Application Number Priority Date Filing Date Title
CN201410614122.XA CN105624800B (en) 2014-11-04 2014-11-04 A kind of bio-bleaching method for degummed ramie fiber production

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
CN201410614122.XA CN105624800B (en) 2014-11-04 2014-11-04 A kind of bio-bleaching method for degummed ramie fiber production

Publications (2)

Publication Number Publication Date
CN105624800A CN105624800A (en) 2016-06-01
CN105624800B true CN105624800B (en) 2018-01-23

Family

ID=56040129

Family Applications (1)

Application Number Title Priority Date Filing Date
CN201410614122.XA Active CN105624800B (en) 2014-11-04 2014-11-04 A kind of bio-bleaching method for degummed ramie fiber production

Country Status (1)

Country Link
CN (1) CN105624800B (en)

Families Citing this family (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN107142712B (en) * 2017-06-23 2019-03-08 山东理工大学 The technique decolourized using aerobic fermentation method to wool fiber
CN107156975B (en) * 2017-06-23 2018-11-02 山东理工大学 The method that biological fermentation process removes melanin in human hair fiber
CN107173896B (en) * 2017-06-23 2018-11-02 山东理工大学 The biological decolouring technique of Yangization Fa treatment oil dyeing human hair fibers

Citations (8)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN1232092A (en) * 1998-04-10 1999-10-20 中国科学院成都生物研究所 Process for enzyme-chemically degumming ramie
CN101173264A (en) * 2007-10-31 2008-05-07 天津大学 Beta-mannase composite preparations and method for producing the same
CN101235547A (en) * 2008-03-06 2008-08-06 北京林业大学 Method for producing bamboo dissolving pulp
CN101581034A (en) * 2008-05-14 2009-11-18 哈尔滨理工大学 Biologically-aided totally-chlorine-free bleaching technology of flax cloth or fiber
CN102102229A (en) * 2009-12-21 2011-06-22 沅江市明星麻业有限公司 Process and device for water-bath continuous fermentation of biologic degumming fibrilia
CN102146589A (en) * 2011-01-13 2011-08-10 祝洪哲 Short-flow environment-friendly degumming and bleaching method for hemp fibers
CN102888366A (en) * 2012-09-17 2013-01-23 贾平 Compound bacteria and method for preparing textile fiber using same
CN103937771A (en) * 2014-03-05 2014-07-23 天津科技大学 Alkaline pectinase preparation for cannabissalival degumming, and cannabissalival degumming method

Patent Citations (8)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN1232092A (en) * 1998-04-10 1999-10-20 中国科学院成都生物研究所 Process for enzyme-chemically degumming ramie
CN101173264A (en) * 2007-10-31 2008-05-07 天津大学 Beta-mannase composite preparations and method for producing the same
CN101235547A (en) * 2008-03-06 2008-08-06 北京林业大学 Method for producing bamboo dissolving pulp
CN101581034A (en) * 2008-05-14 2009-11-18 哈尔滨理工大学 Biologically-aided totally-chlorine-free bleaching technology of flax cloth or fiber
CN102102229A (en) * 2009-12-21 2011-06-22 沅江市明星麻业有限公司 Process and device for water-bath continuous fermentation of biologic degumming fibrilia
CN102146589A (en) * 2011-01-13 2011-08-10 祝洪哲 Short-flow environment-friendly degumming and bleaching method for hemp fibers
CN102888366A (en) * 2012-09-17 2013-01-23 贾平 Compound bacteria and method for preparing textile fiber using same
CN103937771A (en) * 2014-03-05 2014-07-23 天津科技大学 Alkaline pectinase preparation for cannabissalival degumming, and cannabissalival degumming method

Also Published As

Publication number Publication date
CN105624800A (en) 2016-06-01

Similar Documents

Publication Publication Date Title
CN105624800B (en) A kind of bio-bleaching method for degummed ramie fiber production
CN102031568B (en) Short-flow environmentally-friendly production method for jute fibers
CN103436969B (en) A kind of cal rolling-dodge quick-fried-combing removal of impurities combination hemp degumming method
CN103952918B (en) Cotton fabrics biology enzyme cold pad--batch short route open width continual scouring and bleaching dye production technology
CN106087075A (en) A kind of production method of the bamboo fiber of good spinnability
CN104278335A (en) Hemp pretreatment technology
CN101581034A (en) Biologically-aided totally-chlorine-free bleaching technology of flax cloth or fiber
CN103898616B (en) A kind of sisal hemp degumming technique
CN109295735A (en) A kind of production technology of pure flax cheese
CN101838856B (en) Online ramie biological degumming method
CN101713150A (en) Compound enzyme preparation for textile fabrics and applications thereof
CN102703994A (en) Process for combining flax enzyme and chemical degumming with bleaching
CN107142747B (en) Yarn dyeing and finishing process for 3D fly-knitted vamp
CN107268091A (en) A kind of bluish dogbane bast Degumming method
CN100439573C (en) Stabilizer for use in sodium chlorite degumming and bleaching of flax and its preparation method and application
CN106368020A (en) Dyeing technology for silk cotton products
CN109989114A (en) A kind of method of flax degumming
CN105734684A (en) Degumming agent special for ramie and preparation method and application of degumming agent
CN108166240A (en) A kind of concise finishing agent of denim garment desizing and its preparation process
CN105671833A (en) Cold-pad batch dyeing process of loose fibers
CN108823792A (en) A kind of preparation method of medical non-woven fabrics
CN109137564A (en) A kind of acetic acid Light of Mulberry Silk Fabrics manufacture craft
CN105442296A (en) Method for biologically bleaching linen fibers
CN101775665B (en) Low-alkali degumming process for hemp plants at room temperature
CN101338526B (en) Annealing and dyeing integration process for producing flax

Legal Events

Date Code Title Description
C06 Publication
PB01 Publication
C10 Entry into substantive examination
SE01 Entry into force of request for substantive examination
GR01 Patent grant
GR01 Patent grant