CN105623931A - Cleaning agent for chemical industry laboratory experiment instruments and preparation method thereof - Google Patents
Cleaning agent for chemical industry laboratory experiment instruments and preparation method thereof Download PDFInfo
- Publication number
- CN105623931A CN105623931A CN201610108560.8A CN201610108560A CN105623931A CN 105623931 A CN105623931 A CN 105623931A CN 201610108560 A CN201610108560 A CN 201610108560A CN 105623931 A CN105623931 A CN 105623931A
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- China
- Prior art keywords
- parts
- sodium
- preparation
- cleaning agent
- water
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- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
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Classifications
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
- C11D10/00—Compositions of detergents, not provided for by one single preceding group
- C11D10/04—Compositions of detergents, not provided for by one single preceding group based on mixtures of surface-active non-soap compounds and soap
- C11D10/042—Compositions of detergents, not provided for by one single preceding group based on mixtures of surface-active non-soap compounds and soap based on anionic surface-active compounds and soap
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
- C11D10/00—Compositions of detergents, not provided for by one single preceding group
- C11D10/04—Compositions of detergents, not provided for by one single preceding group based on mixtures of surface-active non-soap compounds and soap
- C11D10/045—Compositions of detergents, not provided for by one single preceding group based on mixtures of surface-active non-soap compounds and soap based on non-ionic surface-active compounds and soap
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
- C11D1/00—Detergent compositions based essentially on surface-active compounds; Use of these compounds as a detergent
- C11D1/02—Anionic compounds
- C11D1/12—Sulfonic acids or sulfuric acid esters; Salts thereof
- C11D1/22—Sulfonic acids or sulfuric acid esters; Salts thereof derived from aromatic compounds
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
- C11D1/00—Detergent compositions based essentially on surface-active compounds; Use of these compounds as a detergent
- C11D1/66—Non-ionic compounds
- C11D1/662—Carbohydrates or derivatives
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
- C11D1/00—Detergent compositions based essentially on surface-active compounds; Use of these compounds as a detergent
- C11D1/66—Non-ionic compounds
- C11D1/667—Neutral esters, e.g. sorbitan esters
Landscapes
- Chemical & Material Sciences (AREA)
- Life Sciences & Earth Sciences (AREA)
- Engineering & Computer Science (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Oil, Petroleum & Natural Gas (AREA)
- Wood Science & Technology (AREA)
- Organic Chemistry (AREA)
- Detergent Compositions (AREA)
Abstract
The invention discloses a cleaning agent for chemical industry laboratory experiment instruments and a preparation method thereof. The cleaning agent is prepared from sorbitol monolaurate, sodium dodecyl benzene sulfonate, soap powder, hydroxy propyl cellulose methyl ether, triethanolamine, ethylene oxide, p-hydroxyanisole, sodium hypochlorite, sodium tripolyphosphate, sodium bicarbonate, citric acid and water. The preparation method comprises the steps that the water is heated, and sodium dodecyl benzene sulfonate, sodium hypochlorite, sodium tripolyphosphate and sodium bicarbonate are added to be stirred and mixed to be uniform until the materials are completely dissolved; soap powder and citric acid are added and stirred to be uniform; the remaining raw materials are sequentially added, heating is performed under the microwave condition, full stirring is performed for 4-6 h, and then the finished product is obtained. The cleaning agent can effectively remove residual chemical substances such as acid and alkali and is easy to rinse and high in pertinence, and secondary pollution cannot generated; the preparation method is simple, good in effect and high in speed.
Description
Technical field
The present invention relates to Laboratory Clean reagent field, specifically abluent of a kind of Chemical Engineering Laboratory experimental apparatus and preparation method thereof.
Background technology
In the lab, substantially all using experimental apparatus, including glass apparatus, pottery instrument and rustless steel instrument, the use frequency of these experimental apparatus is significantly high, and cleaning frequency is also significantly high. The chemical substance on surface, bacterium etc., in the process of cleaning, must be cleaned up by current Laboratory Instruments, in order to avoid form secondary pollution when next time uses. But, the abluent kind of current Laboratory Instruments is few, and special kind is less, the scope used is also less, the kind causing abluent total is more, and the cleaning performance of chemicals is poor, cannot thoroughly clean up for being attached to oil stain on instrument surface and other dirts, easily residual, forms secondary pollution. It is thus desirable to existing Laboratory Instruments abluent is improved so that abluent can be suitably used for more instrument.
Summary of the invention
It is an object of the invention to provide abluent of a kind of Chemical Engineering Laboratory experimental apparatus and preparation method thereof, with the problem solving to propose in above-mentioned background technology.
For achieving the above object, the present invention provides following technical scheme:
The abluent of a kind of Chemical Engineering Laboratory experimental apparatus, is prepared from by the raw material of following weight portion: sorbitan monolaurate 11��13 parts, dodecylbenzene sodium sulfonate 12��14 parts, soap powder 17��19 parts, hydroxypropyl cellulose methyl ether 13��15 parts, triethanolamine 16��18 parts, 14��18 parts of oxirane, MEHQ 9��11 parts, sodium hypochlorite 19��21 parts, sodium tripolyphosphate 12��14 parts, sodium bicarbonate 15��17 parts, citric acid 8��12 parts, 80��100 parts of water.
A kind of preparation method of the abluent of described Chemical Engineering Laboratory experimental apparatus, concrete preparation process is as follows: heat water to 40��50 DEG C, it is initially charged dodecylbenzene sodium sulfonate, sodium hypochlorite, sodium tripolyphosphate, sodium bicarbonate is sequentially added in water, it is uniformly mixed, it is completely dissolved to the raw material added, add soap powder and citric acid, stirring 2��3h, finally sequentially add sorbitan monolaurate, hydroxypropyl cellulose methyl ether, triethanolamine, oxirane, MEHQ, microwave heating is carried out under the microwave condition of 1000��1800MHz, heating-up temperature is 60��64 DEG C, and stir 4��6h, get product.
Compared with prior art, the invention has the beneficial effects as follows: abluent of the present invention can remove the chemical substances such as the acid of residual, alkali effectively, and easily rinses, with strong points, can will not form secondary pollution; Preparation method is simple, and effective, speed is fast.
Detailed description of the invention
Below in conjunction with the embodiment of the present invention, the technical scheme in the embodiment of the present invention is clearly and completely described, it is clear that described embodiment is only a part of embodiment of the present invention, rather than whole embodiments. Based on the embodiment in the present invention, the every other embodiment that those of ordinary skill in the art obtain under not making creative work premise, broadly fall into the scope of protection of the invention.
Embodiment 1
The abluent of Chemical Engineering Laboratory experimental apparatus is prepared from by the raw material of following weight portion: sorbitan monolaurate 11 parts, dodecylbenzene sodium sulfonate 14 parts, soap powder 17 parts, hydroxypropyl cellulose methyl ether 15 parts, triethanolamine 16 parts, 18 parts of oxirane, MEHQ 9 parts, sodium hypochlorite 21 parts, sodium tripolyphosphate 12 parts, sodium bicarbonate 17 parts, citric acid 8 parts, 100 parts of water.
In above-described embodiment, the preparation process of abluent is as follows: heat water to 40 DEG C, be initially charged dodecylbenzene sodium sulfonate, sodium hypochlorite, sodium tripolyphosphate, sodium bicarbonate are sequentially added in water, it is uniformly mixed, it is completely dissolved to the raw material added, add soap powder and citric acid, stirring 3h, finally sequentially add sorbitan monolaurate, hydroxypropyl cellulose methyl ether, triethanolamine, oxirane, MEHQ, microwave heating is carried out under the microwave condition of 1800MHz, heating-up temperature is 60 DEG C, and stir 6h, get product.
The clearance of acid is 99.8% by the abluent that the present embodiment provides, and the clearance to alkali is 99.9%, and the clearance to various bacterium is 100%, and vessel remain without abluent.
Embodiment 2
The abluent of Chemical Engineering Laboratory experimental apparatus is prepared from by the raw material of following weight portion: sorbitan monolaurate 12 parts, dodecylbenzene sodium sulfonate 13 parts, soap powder 18 parts, hydroxypropyl cellulose methyl ether 14 parts, triethanolamine 17 parts, 16 parts of oxirane, MEHQ 10 parts, sodium hypochlorite 20 parts, sodium tripolyphosphate 13 parts, sodium bicarbonate 16 parts, citric acid 10 parts, 90 parts of water.
In above-described embodiment, the preparation process of abluent is as follows: heat water to 45 DEG C, be initially charged dodecylbenzene sodium sulfonate, sodium hypochlorite, sodium tripolyphosphate, sodium bicarbonate are sequentially added in water, it is uniformly mixed, it is completely dissolved to the raw material added, add soap powder and citric acid, stirring 2.5h, finally sequentially add sorbitan monolaurate, hydroxypropyl cellulose methyl ether, triethanolamine, oxirane, MEHQ, microwave heating is carried out under the microwave condition of 1800MHz, heating-up temperature is 62 DEG C, and stir 5h, get product.
The clearance of acid is 99.9% by the abluent that the present embodiment provides, and the clearance to alkali is 99.9%, and the clearance to various bacterium is 100%, and vessel remain without abluent.
Embodiment 3
The abluent of Chemical Engineering Laboratory experimental apparatus is prepared from by the raw material of following weight portion: sorbitan monolaurate 13 parts, dodecylbenzene sodium sulfonate 12 parts, soap powder 19 parts, hydroxypropyl cellulose methyl ether 13 parts, triethanolamine 18 parts, 14 parts of oxirane, MEHQ 11 parts, sodium hypochlorite 19 parts, sodium tripolyphosphate 14 parts, sodium bicarbonate 15 parts, citric acid 12 parts, 80 parts of water.
In above-described embodiment, the preparation process of abluent is as follows: heat water to 50 DEG C, be initially charged dodecylbenzene sodium sulfonate, sodium hypochlorite, sodium tripolyphosphate, sodium bicarbonate are sequentially added in water, it is uniformly mixed, it is completely dissolved to the raw material added, add soap powder and citric acid, stirring 2h, finally sequentially add sorbitan monolaurate, hydroxypropyl cellulose methyl ether, triethanolamine, oxirane, MEHQ, microwave heating is carried out under the microwave condition of 1800MHz, heating-up temperature is 64 DEG C, and stir 4h, get product.
The clearance of acid is 99.8% by the abluent that the present embodiment provides, and the clearance to alkali is 99.9%, and the clearance to various bacterium is 99.9%, and vessel remain without abluent.
It is obvious to a person skilled in the art that the invention is not restricted to the details of above-mentioned one exemplary embodiment, and when without departing substantially from the spirit of the present invention or basic feature, it is possible to realize the present invention in other specific forms. Therefore, no matter from which point, embodiment all should be regarded as exemplary, and be nonrestrictive, the scope of the invention rather than described above limits, it is intended that all changes in the implication of the equivalency dropping on claim and scope included in the present invention.
Claims (2)
1. the abluent of a Chemical Engineering Laboratory experimental apparatus, it is characterised in that be prepared from by the raw material of following weight portion: sorbitan monolaurate 11��13 parts, dodecylbenzene sodium sulfonate 12��14 parts, soap powder 17��19 parts, hydroxypropyl cellulose methyl ether 13��15 parts, triethanolamine 16��18 parts, 14��18 parts of oxirane, MEHQ 9��11 parts, sodium hypochlorite 19��21 parts, sodium tripolyphosphate 12��14 parts, sodium bicarbonate 15��17 parts, citric acid 8��12 parts, 80��100 parts of water.
2. the preparation method of the abluent of a Chemical Engineering Laboratory experimental apparatus as claimed in claim 1, it is characterized in that, concrete preparation process is as follows: heat water to 40��50 DEG C, it is initially charged dodecylbenzene sodium sulfonate, sodium hypochlorite, sodium tripolyphosphate, sodium bicarbonate is sequentially added in water, it is uniformly mixed, it is completely dissolved to the raw material added, add soap powder and citric acid, stirring 2��3h, finally sequentially add sorbitan monolaurate, hydroxypropyl cellulose methyl ether, triethanolamine, oxirane, MEHQ, microwave heating is carried out under the microwave condition of 1000��1800MHz, heating-up temperature is 60��64 DEG C, and stir 4��6h, get product.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201610108560.8A CN105623931A (en) | 2016-02-27 | 2016-02-27 | Cleaning agent for chemical industry laboratory experiment instruments and preparation method thereof |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201610108560.8A CN105623931A (en) | 2016-02-27 | 2016-02-27 | Cleaning agent for chemical industry laboratory experiment instruments and preparation method thereof |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| CN105623931A true CN105623931A (en) | 2016-06-01 |
Family
ID=56039286
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN201610108560.8A Pending CN105623931A (en) | 2016-02-27 | 2016-02-27 | Cleaning agent for chemical industry laboratory experiment instruments and preparation method thereof |
Country Status (1)
| Country | Link |
|---|---|
| CN (1) | CN105623931A (en) |
Citations (6)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN1814722A (en) * | 2006-01-16 | 2006-08-09 | 张宏格 | Liquid detergent viscosity-increasing agent |
| CN101368139A (en) * | 2007-08-15 | 2009-02-18 | 江苏海迅实业集团股份有限公司 | Laboratory glassware detergent |
| CN102329699A (en) * | 2011-09-02 | 2012-01-25 | 山东新华医疗器械股份有限公司 | Alkaline cleaning agent and preparation method thereof |
| CN104087925A (en) * | 2014-07-24 | 2014-10-08 | 司徒建辉 | Metal surface high-efficiency deoiling/derusting agent |
| CN104194953A (en) * | 2014-08-18 | 2014-12-10 | 北京三药科技开发公司 | Detergent for cleaning laboratory glassware |
| CN104403854A (en) * | 2014-11-19 | 2015-03-11 | 苏州佑君环境科技有限公司 | Glassware cleaning agent for laboratory detection and preparation method of glassware cleaning agent |
-
2016
- 2016-02-27 CN CN201610108560.8A patent/CN105623931A/en active Pending
Patent Citations (6)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN1814722A (en) * | 2006-01-16 | 2006-08-09 | 张宏格 | Liquid detergent viscosity-increasing agent |
| CN101368139A (en) * | 2007-08-15 | 2009-02-18 | 江苏海迅实业集团股份有限公司 | Laboratory glassware detergent |
| CN102329699A (en) * | 2011-09-02 | 2012-01-25 | 山东新华医疗器械股份有限公司 | Alkaline cleaning agent and preparation method thereof |
| CN104087925A (en) * | 2014-07-24 | 2014-10-08 | 司徒建辉 | Metal surface high-efficiency deoiling/derusting agent |
| CN104194953A (en) * | 2014-08-18 | 2014-12-10 | 北京三药科技开发公司 | Detergent for cleaning laboratory glassware |
| CN104403854A (en) * | 2014-11-19 | 2015-03-11 | 苏州佑君环境科技有限公司 | Glassware cleaning agent for laboratory detection and preparation method of glassware cleaning agent |
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| Date | Code | Title | Description |
|---|---|---|---|
| C06 | Publication | ||
| PB01 | Publication | ||
| C10 | Entry into substantive examination | ||
| SE01 | Entry into force of request for substantive examination | ||
| RJ01 | Rejection of invention patent application after publication |
Application publication date: 20160601 |
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| RJ01 | Rejection of invention patent application after publication |