CN105623850A - Equipment for removing aflatoxin from peanut oil by using activated carbon - Google Patents

Equipment for removing aflatoxin from peanut oil by using activated carbon Download PDF

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Publication number
CN105623850A
CN105623850A CN201610178777.6A CN201610178777A CN105623850A CN 105623850 A CN105623850 A CN 105623850A CN 201610178777 A CN201610178777 A CN 201610178777A CN 105623850 A CN105623850 A CN 105623850A
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China
Prior art keywords
valve
standing tank
retort
aflatoxin
peanut oil
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CN201610178777.6A
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CN105623850B (en
Inventor
李秋庭
吴建文
陆建坚
陆顺忠
时胜德
唐宾
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Guangxi University
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Guangxi University
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    • CCHEMISTRY; METALLURGY
    • C11ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
    • C11BPRODUCING, e.g. BY PRESSING RAW MATERIALS OR BY EXTRACTION FROM WASTE MATERIALS, REFINING OR PRESERVING FATS, FATTY SUBSTANCES, e.g. LANOLIN, FATTY OILS OR WAXES; ESSENTIAL OILS; PERFUMES
    • C11B3/00Refining fats or fatty oils
    • C11B3/10Refining fats or fatty oils by adsorption

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  • Life Sciences & Earth Sciences (AREA)
  • Chemical & Material Sciences (AREA)
  • Microbiology (AREA)
  • Engineering & Computer Science (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Oil, Petroleum & Natural Gas (AREA)
  • Wood Science & Technology (AREA)
  • Organic Chemistry (AREA)
  • Water Treatment By Sorption (AREA)
  • Carbon And Carbon Compounds (AREA)
  • Edible Oils And Fats (AREA)
  • Fats And Perfumes (AREA)

Abstract

The invention discloses equipment for removing aflatoxin from peanut oil by using activated carbon. The equipment is characterized by comprising a reaction tank, a standing tank and a supporting frame, wherein the reaction tank and the standing tank are fixed on supporting lugs of supporting columns of the supporting frame respectively; the reaction tank is provided with a feed opening, a stirrer and a blow-off valve A; a hot water outlet and a steam inlet are formed in a jacket of the reaction tank; a driving device and a fixing seat are arranged at the top of the reaction tank; the blow-off valve A is arranged at the bottom of the reaction tank and connected with an upper end cover of the standing tank through a flange; the standing tank is provided with a hand hole, an oil outlet valve and a reject valve; the hand hole is formed in the top of the standing tank; the oil outlet valve is arranged on the lower section of the standing tank; the reject valve is arranged at the bottom of the standing tank; the supporting frame is provided with the 3-4 supporting columns. With the utilization of the equipment for removing aflatoxin from peanut oil, the operation is simple, the original taste and nutriments are reserved in the peanut oil finished product to the greatest extent, the content of aflatoxin is greatly reduced, and various indexes conform to the existing national standards.

Description

A kind of gac removes the equipment of aflatoxin in peanut oil
Technical field
The invention belongs to grain and oil processing technique field, it is specifically related to the equipment that a kind of gac removes aflatoxin in peanut oil.
Background technology
Edible peanut oil contains abundant nutritive ingredient, very popular. But, peanut oil especially easily suffers the pollution of aflatoxin in production, transportation; And, along with the change of region weather type, the contaminated degree difference of peanut oil is very big, and particularly in the southern area of warming shed method, pollution condition is even more serious. Aflatoxin is the material that a kind of toxicity is extremely strong. The hazardness of aflatoxin is that people and animal livers tissue are had destruction, and liver cancer can be caused time serious even dead. In the food of natural contamination, the most common with aflatoxin B1, its toxicity and carinogenicity are also the strongest. At present, peanut and goods thereof have all been worked out the limitation value of harsh aflatoxin by developed country, and trend generally will be more and more stricter.
At present, the method removing aflatoxin in peanut oil mainly contains: biologic enzymolysis method, organic solvent extraction, ultraviolet irradiation and sorbent material method etc. But, there are some shortcomings in these prior aries: the processing efficiency of biologic enzymolysis method is low, and needs bigger cost; The first ether extraction that organic solvent extraction is developed such as Japan, though the low easy removal of the boiling point of organic solvent first ether, peanut oil has the residual of organic solvent; Ultraviolet irradiation effect is not remarkable.
Summary of the invention
For above-mentioned problems of the prior art, the present invention provides a kind of gac to remove the equipment of aflatoxin in peanut oil, peanut oil finished product after removing aflatoxin with this equipment maximum degree can not only retain its original flavour and nutrition, and can greatly reduce aflatoxin content, meet existing national standard.
The technical scheme of the present invention is as follows:
A kind of gac removes the equipment of aflatoxin in peanut oil, it is characterised in that: arrange and comprise retort, standing tank and resting support; Described retort, standing tank are separately fixed on the supporting ear of supporting post of resting support, and the bottom of retort and the upper end cover of standing tank pass through Flange joint;
Described retort arranges charging opening, agitator, blow-off valve A, and the chuck of retort arranges hot water outlet and steam inlet; The top of described retort arranges drive unit and permanent seat;
Described retort arranges charging opening, agitator, blow-off valve A, and the chuck of retort arranges hot water outlet and steam inlet; The top of described retort arranges drive unit and permanent seat, and the bottom of retort arranges blow-off valve A and upper end cover with standing tank passes through Flange joint;
Described standing tank arranges hand hole mouth, fuel-displaced valve, residual cake valve; Described hand hole mouth is located at the top of standing tank, and fuel-displaced valve is located at the hypomere of standing tank, and residual cake valve is located at the bottom of standing tank;
Described resting support arranges 3��4 supporting posts, and cross bar welding reinforced by the adjacent supporting post arranging the resting support of 4 supporting posts.
As preferably, the export of finished oil place on described fuel-displaced valve arranges filtering net; Described filtering net is stainless steel filter membrane, is fixed in the fuel-displaced mouth of pipe by screw thread or the mode of being inserted in.
As preferably, also arranging bypass discharging pipe between described retort and standing tank; Described bypass discharging pipe upper section be provided with blow-off valve B and be connected with the hypomere of retort, the lower end of bypass discharging pipe is connected with the upper end of standing tank.
As preferably, described standing tank (1) arranges more than 1, when arranging more than 2 standing tank (1), employing is connected in parallel, and arranges valve respectively.
As preferably, described blow-off valve A adopts overhead valve and bottom valve.
Principle of work: peanut oil activated carbon granule and aflatoxin exceeded standard joins retort from charging opening, open drive unit, open steam inlet to lead to and heat into steam, and open hot water outlet, fully stir with agitator, blow-off valve B is opened after leaving standstill, peanut oil is discharged in standing tank, close blow-off valve B, activated carbon granule in retort can second stage employ, again add activated carbon granule and peanut oil that aflatoxin exceeds standard, activated carbon granule add-on reduced than first time, repeat above-mentioned steps, after activated carbon granule absorption completely, open blow-off valve A, mixture is discharged in standing tank, after leaving standstill, open fuel-displaced valve, filter, collect processed oil, finally open residual cake valve, activity breeze is discharged and leaves standstill tank recovery and reusing and recycling.
The useful effect of the present invention is:
1. the equipment removing aflatoxin in peanut oil with gac of the present invention, bypass discharging pipe is set, activated carbon granule in retort can repeatedly utilize, adsorb completely, the activated carbon dosage of later batch process can be reduced, reduce the active breeze discharged, easy cleaning processes, recovery and reusing and recycling, reduces production cost;
2. blow-off valve bottom the retort of the equipment of the present invention is set to overhead valve and bottom valve, effectively avoids activated carbon granule to be deposited in the mouth of pipe, and gac can effectively utilize, and adsorption effect is better;
3. the equipment removing aflatoxin in peanut oil with gac of the present invention, rational in infrastructure, makes simple, and easy to operate, cost is low, effective, has good economic benefit;
4. adopt gac to remove aflatoxin in peanut oil with the equipment of the present invention, belong to physical method and remove aflatoxin, maximum degree can retain the original flavour of peanut oil and nutrition, there is good social benefit.
Accompanying drawing explanation
Fig. 1 be the present invention removal peanut oil in the apparatus structure schematic diagram of aflatoxin.
Fig. 2 be the present invention removal peanut oil in aflatoxin more than 2, device leave standstill jar structure schematic diagram.
Figure identifies: 1-leaves standstill tank, 2-resting support, 3-retort, 4-bypass discharging pipe, 5-blow-off valve B, 6-chuck, 7-agitator, 8-charging opening, 9-drive unit, 10-permanent seat, fixing ear A, 12-hot water outlet of 11-, 13-steam inlet, 14-blow-off valve A, 15-hand hole mouth, the 16-fixing fuel-displaced valve of ear B, 17-, 18-filtering net, 19-residual cake valve.
Embodiment
Below in conjunction with specific embodiment, the invention will be further described, but does not limit the scope of the invention and range of application.
Embodiment 1:
A kind of gac removes the equipment of aflatoxin in peanut oil, it is characterised in that: arrange and comprise retort 3, standing tank 1 and resting support 2; Described retort 3, standing tank 1 are separately fixed on the supporting ear of supporting post of resting support 2, and the bottom of retort 3 and the upper end cover of standing tank 1 pass through Flange joint;
Described retort 3 arranges charging opening 8, agitator 7, blow-off valve A14, and the chuck 6 of retort 3 arranges hot water outlet 12 and steam inlet 13; The top of described retort 3 arranges drive unit 9 and permanent seat 10;
Described standing tank 1 arranges hand hole mouth 15, fuel-displaced valve 17, residual cake valve 19; Described hand hole mouth 15 is located at the top of standing tank 1, and fuel-displaced valve 17 is located at the hypomere of standing tank 1, and residual cake valve 19 is located at the bottom of standing tank 1;
Described resting support 2 arranges 4 supporting posts, and the middle hypomere of adjacent 2 supporting posts reinforces cross bar welding.
Described blow-off valve A14 adopts overhead valve and bottom valve.
During equipment work, shut blow-off valve A14, first adopt KOH as activator, the charcoal that longan branch is made is activated, then to pulverize into specific surface area be 2000m2The activated carbon granule of/g, then it is the mass ratio of peanut oil according to 0.1:100 of 55.74 �� g/kg by activated carbon granule and aflatoxin content, join retort 3 from charging opening 8, open drive unit 9, open steam inlet 13 to lead to and heat into steam, and open hot water outlet 12, 1h is fully stirred with agitator 7, stirring velocity is 20r/min, whipping temp maintains 40 DEG C, after having reacted, shut fuel-displaced valve 17 and the residual cake valve 19 of standing tank 1, then blow-off valve A14 is opened, mixture is discharged in standing tank 1, after leaving standstill 3h, open fuel-displaced valve 17, filtered by filtering net 18, collect processed oil, finally open residual cake valve 19, activity breeze is discharged and leaves standstill tank 1.
Embodiment 2:
A kind of gac removes the equipment of aflatoxin in peanut oil, it is characterised in that: arrange and comprise retort 3, standing tank 1 and resting support 2; Described retort 3, standing tank 1 are separately fixed on the supporting ear of supporting post of resting support 2;
Described retort 3 arranges charging opening 8, agitator 7, blow-off valve A14, and the chuck 6 of retort 3 arranges hot water outlet 12 and steam inlet 13; The top of described retort 3 arranges drive unit 9 and permanent seat 10, and the bottom of retort 3 arranges blow-off valve A14 and upper end cover with standing tank 1 passes through Flange joint;
Described standing tank 1 arranges hand hole mouth 15, fuel-displaced valve 17, residual cake valve 19; Described hand hole mouth 15 is located at the top of standing tank 1, and fuel-displaced valve 17 is located at the hypomere of standing tank 1, and residual cake valve 19 is located at the bottom of standing tank 1;
Described resting support 2 arranges 4 supporting posts, and cross bar welding reinforced by adjacent supporting post.
Export of finished oil place on described fuel-displaced valve 17 arranges filtering net 18; Described filtering net 18 is stainless steel filter membrane, is fixed in the fuel-displaced mouth of pipe by engagement thread.
Described blow-off valve A14 adopts overhead valve and bottom valve.
During equipment work, shut blow-off valve A14, first adopt KOH as activator, the charcoal that lichee branch is made is activated, then to pulverize into specific surface area be 4000m2The activated carbon granule of/g, then it is the mass ratio of peanut oil according to 10:100 of 55.74 �� g/kg by activated carbon granule and aflatoxin content, join retort 3 from charging opening 8, open drive unit 9, open steam inlet 13 to lead to and heat into steam, and open hot water outlet 12, 4h is fully stirred with agitator 7, stirring velocity is 80r/min, whipping temp maintains 70 DEG C, shut fuel-displaced valve 17 and residual cake valve 19, then blow-off valve A14 is opened, mixture is discharged in standing tank 1, after leaving standstill 4h, open fuel-displaced valve 17, filtered by filtering net 18, collect processed oil, finally open residual cake valve 19, activity breeze is discharged and leaves standstill tank 1.
Embodiment 3:
A kind of gac removes the equipment of aflatoxin in peanut oil, it is characterised in that: arrange and comprise retort 3, standing tank 1 and resting support 2; Described retort 3, standing tank 1 are separately fixed on the supporting ear of supporting post of resting support 2;
Described retort 3 arranges charging opening 8, agitator 7, blow-off valve A14, and the chuck 6 of retort 3 arranges hot water outlet 12 and steam inlet 13; The top of described retort 3 arranges drive unit 9 and permanent seat 10, and the bottom of retort 3 arranges blow-off valve A14 and upper end cover with standing tank 1 passes through Flange joint;
Described standing tank 1 arranges hand hole mouth 15, fuel-displaced valve 17, residual cake valve 19; Described hand hole mouth 15 is located at the top of standing tank 1, and fuel-displaced valve 17 is located at the hypomere of standing tank 1, and residual cake valve 19 is located at the bottom of standing tank 1;
Described resting support 2 arranges 3 supporting posts.
Export of finished oil place on described fuel-displaced valve 17 arranges filtering net 18; Described filtering net 18 is stainless steel filter membrane, is fixed in the fuel-displaced mouth of pipe by the mode of being inserted in.
Bypass discharging pipe 4 is also set between described retort 3 and standing tank 1; Described bypass discharging pipe 4 upper section be provided with blow-off valve B5 and hypomere with retort 3 is connected, the lower end of bypass discharging pipe 4 is connected with the upper end of standing tank 1.
Described standing tank 1 arranges 2, and employing is connected in parallel, and arranges valve respectively.
Described blow-off valve A14 adopts overhead valve and bottom valve.
During equipment work, shutting blow-off valve A14 and blow-off valve B5, first adopt NaOH as activator, the charcoal being mixed with 1:6 by the branch of longan and lichee activates, then to pulverize into specific surface area be 2200m2The activated carbon granule of/g, then it is the mass ratio of peanut oil according to 1.5:100 of 55.74 �� g/kg by activated carbon granule and aflatoxin content, join retort 3 from charging opening 8, open drive unit 9, open steam inlet 13 to lead to and heat into steam, and open hot water outlet 12, 3.5h is fully stirred with agitator 7, stirring velocity is 60r/min, whipping temp maintains 20 DEG C, leave standstill 1h, shut fuel-displaced valve 17 and the residual cake valve 19 of the 1st standing tank 1, then blow-off valve B5 is opened, peanut oil is discharged in the 1st standing tank 1, close blow-off valve B5, activated carbon granule in retort 3 stays does the 2nd batch of de-etiolation aspertoxin process. again add activated carbon granule and during peanut oil that aflatoxin exceeds standard, activated carbon granule add-on reduces 1/2 than first time, repeat above-mentioned steps, after activated carbon granule absorption completely, shut fuel-displaced valve 17 and the residual cake valve 19 of the 1st standing tank 1, open blow-off valve A14, mixture is discharged in the 2nd standing tank 1, after leaving standstill 3h, open the fuel-displaced valve 17 of two standing tanks 1, filtered by filtering net 18, collect processed oil, finally open the residual cake valve 19 of two standing tanks 1, activity breeze is discharged.
In the processed oil of embodiment of the present invention 1-3, aflatoxin content significantly reduces, main nutrient matter: the content of fat, energy does not change, and micronutrient levels reduces a little, and every index all meets existing national standard.
Concrete detection data are as follows:

Claims (6)

1. remove the equipment of aflatoxin in peanut oil with gac for one kind, it is characterised in that: arrange and comprise retort (3), standing tank (1) and resting support (2); Described retort (3), standing tank (1) are separately fixed on the supporting ear of supporting post of resting support (2), and the bottom of retort (3) and the upper end cover of standing tank (1) pass through Flange joint;
Described retort (3) arranges charging opening (8), agitator (7), blow-off valve A(14), the chuck (6) of retort (3) arranges hot water outlet (12) and steam inlet (13); The top of described retort (3) arranges drive unit (9) and permanent seat (10);
Described standing tank (1) arranges hand hole mouth (15), fuel-displaced valve (17), residual cake valve (19); Described hand hole mouth (15) is located at the top of standing tank (1), and fuel-displaced valve (17) is located at the hypomere of standing tank (1), and residual cake valve (19) is located at the bottom of standing tank (1);
Described resting support (2) arranges 3��4 supporting posts, and cross bar welding reinforced by the adjacent supporting post arranging the resting support (2) of 4 supporting posts.
2. gac according to claim 1 removes the equipment of aflatoxin in peanut oil, it is characterised in that: the export of finished oil place on described fuel-displaced valve (17) arranges filtering net (18).
3. gac according to claim 2 removes the equipment of aflatoxin in peanut oil, it is characterised in that: described filtering net (18) is stainless steel filter membrane, is fixed in the fuel-displaced mouth of pipe by screw thread or the mode of being inserted in.
4. gac according to claim 1 removes the equipment of aflatoxin in peanut oil, it is characterised in that: bypass discharging pipe (4) is also set between described retort (3) and standing tank (1); Described bypass discharging pipe (4) upper section be provided with blow-off valve B(5) and hypomere with retort (3) be connected, the lower end of bypass discharging pipe (4) is connected with the upper end of standing tank (1).
5. gac according to claim 1 removes the equipment of aflatoxin in peanut oil, it is characterised in that: described standing tank (1) arranges more than 1, and when arranging more than 2 standing tank (1), employing is connected in parallel, and arranges valve respectively.
6. gac according to claim 1 removes the equipment of aflatoxin in peanut oil, it is characterised in that: described blow-off valve A(14) adopt overhead valve and bottom valve.
CN201610178777.6A 2016-03-28 2016-03-28 Equipment for removing aflatoxin in peanut oil by using activated carbon Active CN105623850B (en)

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Cited By (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN107469790A (en) * 2017-09-07 2017-12-15 广州尊卓环保科技有限公司 Remove filter medium, filter core and the preparation method of aflatoxin in edible oil
CN109370776A (en) * 2018-10-29 2019-02-22 山东省农业科学院农业质量标准与检测技术研究所 The eliminating equipment and method of aflatoxin in a kind of peanut oil

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CN104164299A (en) * 2013-05-15 2014-11-26 无锡市新耀生物工程技术有限公司 Equipment for removing toxins from edible oil raw materials and oil byproduct (raw material meal)
CN103589510A (en) * 2013-11-19 2014-02-19 福建华仁油脂有限公司 Nigre removal process and equipment for vegetable oil and vegetable oil production process
CN204918535U (en) * 2015-08-19 2015-12-30 佘季秋 Utilize oil tank of sea foam characteristic purification vegetable oil

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Cited By (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN107469790A (en) * 2017-09-07 2017-12-15 广州尊卓环保科技有限公司 Remove filter medium, filter core and the preparation method of aflatoxin in edible oil
CN109370776A (en) * 2018-10-29 2019-02-22 山东省农业科学院农业质量标准与检测技术研究所 The eliminating equipment and method of aflatoxin in a kind of peanut oil

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