CN105622044A - Novel fire-proof plate and preparation method thereof - Google Patents
Novel fire-proof plate and preparation method thereof Download PDFInfo
- Publication number
- CN105622044A CN105622044A CN201511017516.8A CN201511017516A CN105622044A CN 105622044 A CN105622044 A CN 105622044A CN 201511017516 A CN201511017516 A CN 201511017516A CN 105622044 A CN105622044 A CN 105622044A
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- CN
- China
- Prior art keywords
- weight
- stearic acid
- plastic laminated
- magnesium oxide
- adlerika
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
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Classifications
-
- C—CHEMISTRY; METALLURGY
- C04—CEMENTS; CONCRETE; ARTIFICIAL STONE; CERAMICS; REFRACTORIES
- C04B—LIME, MAGNESIA; SLAG; CEMENTS; COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDING MATERIALS; ARTIFICIAL STONE; CERAMICS; REFRACTORIES; TREATMENT OF NATURAL STONE
- C04B28/00—Compositions of mortars, concrete or artificial stone, containing inorganic binders or the reaction product of an inorganic and an organic binder, e.g. polycarboxylate cements
- C04B28/30—Compositions of mortars, concrete or artificial stone, containing inorganic binders or the reaction product of an inorganic and an organic binder, e.g. polycarboxylate cements containing magnesium cements or similar cements
-
- C—CHEMISTRY; METALLURGY
- C04—CEMENTS; CONCRETE; ARTIFICIAL STONE; CERAMICS; REFRACTORIES
- C04B—LIME, MAGNESIA; SLAG; CEMENTS; COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDING MATERIALS; ARTIFICIAL STONE; CERAMICS; REFRACTORIES; TREATMENT OF NATURAL STONE
- C04B40/00—Processes, in general, for influencing or modifying the properties of mortars, concrete or artificial stone compositions, e.g. their setting or hardening ability
- C04B40/0028—Aspects relating to the mixing step of the mortar preparation
- C04B40/0039—Premixtures of ingredients
-
- C—CHEMISTRY; METALLURGY
- C04—CEMENTS; CONCRETE; ARTIFICIAL STONE; CERAMICS; REFRACTORIES
- C04B—LIME, MAGNESIA; SLAG; CEMENTS; COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDING MATERIALS; ARTIFICIAL STONE; CERAMICS; REFRACTORIES; TREATMENT OF NATURAL STONE
- C04B2111/00—Mortars, concrete or artificial stone or mixtures to prepare them, characterised by specific function, property or use
- C04B2111/20—Resistance against chemical, physical or biological attack
- C04B2111/28—Fire resistance, i.e. materials resistant to accidental fires or high temperatures
Landscapes
- Chemical & Material Sciences (AREA)
- Engineering & Computer Science (AREA)
- Ceramic Engineering (AREA)
- Materials Engineering (AREA)
- Structural Engineering (AREA)
- Organic Chemistry (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Inorganic Chemistry (AREA)
- Compositions Of Macromolecular Compounds (AREA)
Abstract
The invention discloses a novel fire-proof plate and a preparation method thereof. The fire-proof plate is prepared from the following raw materials in percentage by weight: 0.1 to 8 percent of modifying agents, 55 to 65 percent of magnesium oxide solution, 25 to 35 percent of magnesium sulfate solution and 8 to 12 percent of wood chips. The modifying agent is dissolved into water by adopting paraffin and stearic acid to be prepared into latex. The excellent formula is selected; the finished product is manufactured through stirring, roller flat paving, maintenance template dismounting and cutting polishing. The technical problems of recurrent halogen, frosting and the like are perfectly solved; the high-performance fire-proof and flame retardant requirements can be met; the generation of formaldehyde, methylbenzene and amine is avoided; meanwhile, sawability and nailability are realized.
Description
Technical field
The present invention relates to a kind of decorative sheet, in particular to the novel PLASTIC LAMINATED of one and its preparation method.
Background technology
" public place fire-retardant product and assembly combustionproperty require and mark " (GB20286-2006) compulsory standard defines the goods entering public place and assembly must possess certain flame retardant properties grade. And household and public place woodwork belong to inflammable material, constitute the hidden danger of building fire. Along with woodwork is popularizing that household and public place are applied, fire safety evaluating problem is more outstanding. For the consideration to human life and property safety, it may also be useful to the wood materials with anti-flaming function is very important, it also it is the problem that industry is paid close attention to the most. Although decorative sheet is of a great variety now, but all there is certain defect. As fire protection flame retarding grade is not up to standard, making processes can produce waste water, waste residue; Owing to the saw property of sheet material, nailability are not good in installation process, and cause internal structure to be destroyed, greatly shorten its work-ing life etc.
Current environmental protection flame retardant dalle, by magnesium oxide, lignocellulose, magnesium chloride solution, and paraffin wax and stearic acid adds water, sodium hydroxide solution is made emulsion, 1-3 layer glasscloth form, and make through stirrer, laminator. But there is following shortcoming: adopt magnesium chloride to mix with magnesium oxide, due to the existence of chlorion in product, the phenomenons such as that can cause the decorative sheet later stage returns halogen, scum occur. Return halogen and namely refer to that plate surface there will be water droplet; Scum refers to that plate surface there will be one layer of bloom. The existence of these two kinds of situations can affect decorative effect greatly, but also can shorten the work-ing life of sheet material. The decorative sheet that magnesia oxychloride cement is made is used for integrated house building, and due to the existence of Lightgage Steel Joist, chlorion can be combined oxidized with ferrous ion again, forms iron rust.
Summary of the invention
The present invention is to overcome defect in above-mentioned prior art, it is proposed to a kind of novel PLASTIC LAMINATED and its preparation method.
A kind of novel PLASTIC LAMINATED, described PLASTIC LAMINATED is made up of the raw material of following weight percent: properties-correcting agent 0.1-8%, magnesium oxide solution 55-65%, Adlerika 25-35%, wood chip 8-12%.
The making method of described properties-correcting agent carries out in accordance with the following steps:
(1) taking paraffin wax and stearic acid, the weight of paraffin wax is the 2-5% of above-mentioned magnesium oxide solution, Adlerika gross weight, and stearic acid weight is the 0.3-1.6% of above-mentioned magnesium oxide solution, Adlerika gross weight;
(2) take paraffin wax and the water of stearic acid gross weight 2.7 times of weight, paraffin wax and stearic acid are added to the water, are heated to boiling point so that it is fully dissolve;
(3) add that weight is paraffin wax and stearic acid sum 2.2%, concentration is the sodium hydroxide solution of 35%, stirs into emulsion, makes properties-correcting agent.
Preferably, the mass concentration of described Adlerika is 22-28%.
Preferably, the mass concentration of described magnesium oxide solution is 22-28%.
Preferably, described fiberglass gridding cloth specification is 140g, 160g or 180g.
The preparation method of above-mentioned novel PLASTIC LAMINATED, carries out in accordance with the following steps:
(1) by properties-correcting agent, magnesium oxide solution, Adlerika, wood chip is put in stirrer by above-mentioned weight percent;
(2) fully stirring, churning time controls at 4-6 minute;
(3) material and the 2-4 layer fiberglass gridding cloth that are stirred make sheet material by the flat forming line of roller;
(4) maintenance form removal: maintenance 18-24 hour, curing temperature 26-30 DEG C, humid control is at 50%-70%, and the sheet material after form removal carries out maintenance 2-3 days again;
(5) sanding process is cut.
Compared with prior art, the present invention has following useful effect: the present invention's blender used adopts magnesium sulfate to substitute the magnesium chloride of prior art, perfect can solve and return the technical barrier such as halogen, scum, it has environmental-protecting performance, is mainly reflected in generation formaldehydeless, any toxic and harmful such as toluene, amine; It has flame retardant properties, is mainly reflected in flame retardant rating and reaches A level. It has saw property, nailability, is mainly reflected in construction and installation process, can saw and can follow closely, and internal structure can not be destroyed.
Embodiment
Below the specific embodiment of the present invention is described in detail, it should be understood that protection scope of the present invention is not by the restriction of embodiment.
Embodiment 1
A kind of novel PLASTIC LAMINATED, is made up of the raw material of following weight percent: Adlerika 30% that magnesium oxide solution 58% that properties-correcting agent 2%, mass concentration are 22%, mass concentration are 25%, wood chip 10%.
The making method of described properties-correcting agent carries out in accordance with the following steps:
(1) take paraffin wax and stearic acid, the weight of paraffin wax be magnesium oxide solution, Adlerika gross weight 3%, stearic acid weight be magnesium oxide solution, Adlerika gross weight 0.7%;
(2) take paraffin wax and stearic acid gross weight 2.7 times of weight water, paraffin wax and stearic acid are added to the water, are heated to boiling point so that it is fully dissolve;
(3) add weight be paraffin wax and stearic acid sum 2.2%, concentration be the sodium hydroxide solution of 35%, stir into emulsion, make properties-correcting agent.
The preparation method of above-mentioned novel PLASTIC LAMINATED, carries out in accordance with the following steps:
(1) by properties-correcting agent, magnesium oxide solution, Adlerika, wood chip is put in stirrer by above-mentioned part by weight;
(2) fully stirring, churning time is 5 minutes;
(3) material being stirred and 3 layers of fiberglass gridding cloth make sheet material by the flat forming line of roller, and the first layer and the second layer select 140g fiberglass gridding cloth, and third layer selects 160g fiberglass gridding cloth;
(4) maintenance form removal: maintenance 24 hours, curing temperature 28 DEG C, humid control is 65%, and the sheet material after form removal carries out maintenance 2 days again;
(5) sanding process is cut.
The PLASTIC LAMINATED of the present embodiment solves returns the technical barrier such as halogen, scum, can meet high-performance fire-resistant flame-retardancy requirements, and formaldehydeless, toluene, amine produce again, have saw property, nailability simultaneously.
Embodiment 2
A kind of novel PLASTIC LAMINATED, is made up of the raw material of following weight percent: Adlerika 35% that magnesium oxide solution 55% that properties-correcting agent 0.1%, mass concentration are 25%, mass concentration are 28%, wood chip 9.9%.
The making method of described properties-correcting agent carries out in accordance with the following steps:
(1) take paraffin wax and stearic acid, the weight of paraffin wax be magnesium oxide solution, Adlerika gross weight 2%, stearic acid weight be magnesium oxide solution, Adlerika gross weight 0.3%;
(2) take paraffin wax and stearic acid gross weight 2.7 times of weight water, paraffin wax and stearic acid are added to the water, are heated to boiling point so that it is fully dissolve;
(3) add weight be paraffin wax and stearic acid sum 2.2%, concentration be the sodium hydroxide solution of 35%, stir into emulsion, make properties-correcting agent.
The preparation method of above-mentioned novel PLASTIC LAMINATED, carries out in accordance with the following steps:
(1) by properties-correcting agent, magnesium oxide solution, Adlerika, wood chip is put in stirrer by above-mentioned part by weight;
(2) fully stirring, churning time is 4 minutes;
(3) material being stirred and 3 layers of fiberglass gridding cloth make sheet material by the flat forming line of roller, and the first layer and the second layer select 140g fiberglass gridding cloth, and third layer selects 160g fiberglass gridding cloth;
(4) maintenance form removal: maintenance 18 hours, curing temperature 26 DEG C, humid control is 50%, and the sheet material after form removal carries out maintenance 2 days again;
(5) sanding process is cut.
The PLASTIC LAMINATED of the present embodiment solves returns the technical barrier such as halogen, scum, can meet high-performance fire-resistant flame-retardancy requirements, and formaldehydeless, toluene, amine produce again, have saw property, nailability simultaneously.
Embodiment 3
A kind of novel PLASTIC LAMINATED, is made up of the raw material of following weight percent: Adlerika 25% that magnesium oxide solution 55% that properties-correcting agent 8%, mass concentration are 26%, mass concentration are 26%, wood chip 12%.
The making method of described properties-correcting agent carries out in accordance with the following steps:
(1) take paraffin wax and stearic acid, the weight of paraffin wax be magnesium oxide solution, Adlerika gross weight 5%, stearic acid weight be magnesium oxide solution, Adlerika gross weight 1.6%;
(2) take paraffin wax and stearic acid gross weight 2.7 times of weight water, paraffin wax and stearic acid are added to the water, are heated to boiling point so that it is fully dissolve;
(3) add weight be paraffin wax and stearic acid sum 2.2%, concentration be the sodium hydroxide solution of 35%, stir into emulsion, make properties-correcting agent.
The preparation method of above-mentioned novel PLASTIC LAMINATED, carries out in accordance with the following steps:
(1) by properties-correcting agent, magnesium oxide solution, Adlerika, wood chip is put in stirrer by above-mentioned part by weight;
(2) fully stirring, churning time is 6 minutes;
(3) material being stirred and 3 layers of fiberglass gridding cloth make sheet material by the flat forming line of roller, and the first layer and the second layer select 140g fiberglass gridding cloth, and third layer selects 160g fiberglass gridding cloth;
(4) maintenance form removal: maintenance 20 hours, curing temperature 30 DEG C, humid control is 70%, and the sheet material after form removal carries out maintenance 2 days again;
(5) sanding process is cut.
The PLASTIC LAMINATED of the present embodiment solves returns the technical barrier such as halogen, scum, can meet high-performance fire-resistant flame-retardancy requirements, and formaldehydeless, toluene, amine produce again, have saw property, nailability simultaneously.
Embodiment 4
A kind of novel PLASTIC LAMINATED, is made up of the raw material of following weight percent: Adlerika 30% that magnesium oxide solution 56% that properties-correcting agent 2%, mass concentration are 22%, mass concentration are 25%, wood chip 10%, phlomis umbrosa extract 2%.
The extracting method of described phlomis umbrosa extract is as follows: is dried by phlomis umbrosa, clays into power, and adds the 70% aqueous ethanolic solution refluxing extraction 3 times of 3-5 times of weight part number, and merging filtrate, steams drying one-tenth.
The making method of described properties-correcting agent carries out in accordance with the following steps:
(1) take paraffin wax and stearic acid, the weight of paraffin wax be magnesium oxide solution, Adlerika gross weight 3%, stearic acid weight be magnesium oxide solution, Adlerika gross weight 0.7%;
(2) take paraffin wax and stearic acid gross weight 2.7 times of weight water, paraffin wax and stearic acid are added to the water, are heated to boiling point so that it is fully dissolve;
(3) add weight be paraffin wax and stearic acid sum 2.2%, concentration be the sodium hydroxide solution of 35%, stir into emulsion, make properties-correcting agent;
The preparation method of above-mentioned novel PLASTIC LAMINATED, carries out in accordance with the following steps:
(1) by properties-correcting agent, magnesium oxide solution, Adlerika, wood chip is put in stirrer by above-mentioned part by weight;
(2) fully stirring, churning time is 5 minutes;
(3) material being stirred and 3 layers of fiberglass gridding cloth make sheet material by the flat forming line of roller, and the first layer and the second layer select 140g fiberglass gridding cloth, and third layer selects 160g fiberglass gridding cloth;
(4) maintenance form removal: maintenance 24 hours, curing temperature 28 DEG C, humid control is 65%, and the sheet material after form removal carries out maintenance 2 days again;
(5) sanding process is cut.
The PLASTIC LAMINATED of the present embodiment solves returns the technical barrier such as halogen, scum, can meet high-performance fire-resistant flame-retardancy requirements, and formaldehydeless, toluene, amine produce again, have saw property, nailability and good soundproof effect simultaneously.
Comparative example 1
A kind of novel PLASTIC LAMINATED, is made up of the raw material of following weight percent: Adlerika 30% that magnesium oxide solution 60% that mass concentration is 22%, mass concentration are 25%, wood chip 10%.
The preparation method of above-mentioned novel PLASTIC LAMINATED, carries out in accordance with the following steps:
(1) by magnesium oxide solution, Adlerika, wood chip is put in stirrer by above-mentioned part by weight;
(2) fully stirring, churning time is 5 minutes;
(3) material being stirred and 3 layers of fiberglass gridding cloth make sheet material by the flat forming line of roller, and the first layer and the second layer select 140g fiberglass gridding cloth, and third layer selects 160g fiberglass gridding cloth;
(4) maintenance form removal: maintenance 24 hours, curing temperature 28 DEG C, humid control is 65%, and the sheet material after form removal carries out maintenance 2 days again;
(5) sanding process is cut.
The PLASTIC LAMINATED of the present embodiment easily produces to return the phenomenon such as halogen, scum, can not meet high-performance fire-resistant flame-retardancy requirements.
Specific embodiments of the invention it are only disclosed in above, but, the present invention is not limited thereto, and the changes that any person skilled in the art can think of all should fall into protection scope of the present invention.
Claims (6)
1. a novel PLASTIC LAMINATED, it is characterised in that, described PLASTIC LAMINATED is made up of the raw material of following weight percent: properties-correcting agent 0.1-8%, magnesium oxide solution 55-65%, Adlerika 25-35%, wood chip 8-12%.
2. the novel PLASTIC LAMINATED of one according to claim 1, it is characterised in that, the making method of described properties-correcting agent carries out in accordance with the following steps:
(1) taking paraffin wax and stearic acid, the weight of paraffin wax is the 2-5% of magnesium oxide solution described in claim 1, Adlerika gross weight, and stearic acid weight is the 0.3-1.6% of magnesium oxide solution described in claim 1, Adlerika gross weight;
(2) take paraffin wax and the water of stearic acid gross weight 2.7 times of weight, paraffin wax and stearic acid are added to the water, are heated to boiling point so that it is fully dissolve;
(3) add that weight is paraffin wax and stearic acid sum 2.2%, concentration is the sodium hydroxide solution of 35%, stirs into emulsion, makes properties-correcting agent.
3. the novel PLASTIC LAMINATED of one according to claim 1, it is characterised in that, the mass concentration of described Adlerika is 22-28%.
4. the novel PLASTIC LAMINATED of one according to claim 1, it is characterised in that, the mass concentration of described magnesium oxide solution is 22-28%.
5. the novel PLASTIC LAMINATED of one according to claim 1, it is characterised in that, described fiberglass gridding cloth specification is 140g, 160g or 180g.
6. the preparation method of novel PLASTIC LAMINATED according to claim 1, it is characterised in that, carry out in accordance with the following steps:
(1) by properties-correcting agent, magnesium oxide solution, Adlerika, wood chip is put in stirrer by weight percent described in claim 1;
(2) fully stirring, churning time controls at 4-6 minute;
(3) material and the 2-4 layer fiberglass gridding cloth that are stirred make sheet material by the flat forming line of roller;
(4) maintenance form removal: maintenance 18-24 hour, curing temperature 26-30 DEG C, humid control is at 50%-70%, and the sheet material after form removal carries out maintenance 2-3 days again;
(5) sanding process is cut.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201511017516.8A CN105622044A (en) | 2015-12-29 | 2015-12-29 | Novel fire-proof plate and preparation method thereof |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201511017516.8A CN105622044A (en) | 2015-12-29 | 2015-12-29 | Novel fire-proof plate and preparation method thereof |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| CN105622044A true CN105622044A (en) | 2016-06-01 |
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Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
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| CN201511017516.8A Pending CN105622044A (en) | 2015-12-29 | 2015-12-29 | Novel fire-proof plate and preparation method thereof |
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Cited By (5)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN106187054A (en) * | 2016-07-27 | 2016-12-07 | 张家港市盛港绿色防火建材有限公司 | A kind of integrated house and special magnesium sulfate floor, integrated movable room |
| CN106431171A (en) * | 2016-07-04 | 2017-02-22 | 卓达新材料科技集团威海股份有限公司 | Board for high fireproof logistics packing box and preparation method |
| CN107253838A (en) * | 2016-11-11 | 2017-10-17 | 成都杰雷遮阳工程有限公司 | A kind of preparation method of environment-friendly fire-proof plate for passageway for fire apparatus |
| US11020940B2 (en) * | 2017-01-12 | 2021-06-01 | Euro Trade Flooring, S.L. | Plate for covering horizontal and vertical surfaces |
| CN113372089A (en) * | 2021-07-16 | 2021-09-10 | 万华生态板业集成设备有限公司 | Glass magnesium board floor base material and production method thereof |
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| CN101250062A (en) * | 2008-03-12 | 2008-08-27 | 李锦富 | Magnesium cement fireproof board having excellent water-resistance and preparation thereof |
| CN102359239A (en) * | 2011-09-06 | 2012-02-22 | 孙振芳 | Environment-friendly and flame-retardant decorative plate and production method thereof |
| KR20130043473A (en) * | 2011-10-20 | 2013-04-30 | 이영철 | Reinforced composition for corrugated board sheet and corrugated board using the same |
| CN105130350A (en) * | 2015-08-13 | 2015-12-09 | 惠州美森板业有限公司 | Novel inorganic decoration base material plate and preparation method thereof |
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2015
- 2015-12-29 CN CN201511017516.8A patent/CN105622044A/en active Pending
Patent Citations (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN101250062A (en) * | 2008-03-12 | 2008-08-27 | 李锦富 | Magnesium cement fireproof board having excellent water-resistance and preparation thereof |
| CN102359239A (en) * | 2011-09-06 | 2012-02-22 | 孙振芳 | Environment-friendly and flame-retardant decorative plate and production method thereof |
| KR20130043473A (en) * | 2011-10-20 | 2013-04-30 | 이영철 | Reinforced composition for corrugated board sheet and corrugated board using the same |
| CN105130350A (en) * | 2015-08-13 | 2015-12-09 | 惠州美森板业有限公司 | Novel inorganic decoration base material plate and preparation method thereof |
Cited By (5)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN106431171A (en) * | 2016-07-04 | 2017-02-22 | 卓达新材料科技集团威海股份有限公司 | Board for high fireproof logistics packing box and preparation method |
| CN106187054A (en) * | 2016-07-27 | 2016-12-07 | 张家港市盛港绿色防火建材有限公司 | A kind of integrated house and special magnesium sulfate floor, integrated movable room |
| CN107253838A (en) * | 2016-11-11 | 2017-10-17 | 成都杰雷遮阳工程有限公司 | A kind of preparation method of environment-friendly fire-proof plate for passageway for fire apparatus |
| US11020940B2 (en) * | 2017-01-12 | 2021-06-01 | Euro Trade Flooring, S.L. | Plate for covering horizontal and vertical surfaces |
| CN113372089A (en) * | 2021-07-16 | 2021-09-10 | 万华生态板业集成设备有限公司 | Glass magnesium board floor base material and production method thereof |
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Application publication date: 20160601 |
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