CN105621894B - A kind of composite foam glass insulation spill guide and preparation method thereof - Google Patents
A kind of composite foam glass insulation spill guide and preparation method thereof Download PDFInfo
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- CN105621894B CN105621894B CN201510959924.9A CN201510959924A CN105621894B CN 105621894 B CN105621894 B CN 105621894B CN 201510959924 A CN201510959924 A CN 201510959924A CN 105621894 B CN105621894 B CN 105621894B
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- foam glass
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- spill guide
- modified pitch
- insulation spill
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Classifications
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- C—CHEMISTRY; METALLURGY
- C03—GLASS; MINERAL OR SLAG WOOL
- C03C—CHEMICAL COMPOSITION OF GLASSES, GLAZES OR VITREOUS ENAMELS; SURFACE TREATMENT OF GLASS; SURFACE TREATMENT OF FIBRES OR FILAMENTS MADE FROM GLASS, MINERALS OR SLAGS; JOINING GLASS TO GLASS OR OTHER MATERIALS
- C03C17/00—Surface treatment of glass, not in the form of fibres or filaments, by coating
- C03C17/006—Surface treatment of glass, not in the form of fibres or filaments, by coating with materials of composite character
- C03C17/007—Surface treatment of glass, not in the form of fibres or filaments, by coating with materials of composite character containing a dispersed phase, e.g. particles, fibres or flakes, in a continuous phase
-
- C—CHEMISTRY; METALLURGY
- C03—GLASS; MINERAL OR SLAG WOOL
- C03C—CHEMICAL COMPOSITION OF GLASSES, GLAZES OR VITREOUS ENAMELS; SURFACE TREATMENT OF GLASS; SURFACE TREATMENT OF FIBRES OR FILAMENTS MADE FROM GLASS, MINERALS OR SLAGS; JOINING GLASS TO GLASS OR OTHER MATERIALS
- C03C17/00—Surface treatment of glass, not in the form of fibres or filaments, by coating
- C03C17/006—Surface treatment of glass, not in the form of fibres or filaments, by coating with materials of composite character
- C03C17/008—Surface treatment of glass, not in the form of fibres or filaments, by coating with materials of composite character comprising a mixture of materials covered by two or more of the groups C03C17/02, C03C17/06, C03C17/22 and C03C17/28
- C03C17/009—Mixtures of organic and inorganic materials, e.g. ormosils and ormocers
-
- C—CHEMISTRY; METALLURGY
- C03—GLASS; MINERAL OR SLAG WOOL
- C03C—CHEMICAL COMPOSITION OF GLASSES, GLAZES OR VITREOUS ENAMELS; SURFACE TREATMENT OF GLASS; SURFACE TREATMENT OF FIBRES OR FILAMENTS MADE FROM GLASS, MINERALS OR SLAGS; JOINING GLASS TO GLASS OR OTHER MATERIALS
- C03C2217/00—Coatings on glass
- C03C2217/40—Coatings comprising at least one inhomogeneous layer
- C03C2217/43—Coatings comprising at least one inhomogeneous layer consisting of a dispersed phase in a continuous phase
- C03C2217/44—Coatings comprising at least one inhomogeneous layer consisting of a dispersed phase in a continuous phase characterized by the composition of the continuous phase
- C03C2217/445—Organic continuous phases
-
- C—CHEMISTRY; METALLURGY
- C03—GLASS; MINERAL OR SLAG WOOL
- C03C—CHEMICAL COMPOSITION OF GLASSES, GLAZES OR VITREOUS ENAMELS; SURFACE TREATMENT OF GLASS; SURFACE TREATMENT OF FIBRES OR FILAMENTS MADE FROM GLASS, MINERALS OR SLAGS; JOINING GLASS TO GLASS OR OTHER MATERIALS
- C03C2217/00—Coatings on glass
- C03C2217/40—Coatings comprising at least one inhomogeneous layer
- C03C2217/43—Coatings comprising at least one inhomogeneous layer consisting of a dispersed phase in a continuous phase
- C03C2217/46—Coatings comprising at least one inhomogeneous layer consisting of a dispersed phase in a continuous phase characterized by the dispersed phase
- C03C2217/47—Coatings comprising at least one inhomogeneous layer consisting of a dispersed phase in a continuous phase characterized by the dispersed phase consisting of a specific material
- C03C2217/475—Inorganic materials
-
- C—CHEMISTRY; METALLURGY
- C03—GLASS; MINERAL OR SLAG WOOL
- C03C—CHEMICAL COMPOSITION OF GLASSES, GLAZES OR VITREOUS ENAMELS; SURFACE TREATMENT OF GLASS; SURFACE TREATMENT OF FIBRES OR FILAMENTS MADE FROM GLASS, MINERALS OR SLAGS; JOINING GLASS TO GLASS OR OTHER MATERIALS
- C03C2217/00—Coatings on glass
- C03C2217/70—Properties of coatings
- C03C2217/76—Hydrophobic and oleophobic coatings
Landscapes
- Chemical & Material Sciences (AREA)
- General Chemical & Material Sciences (AREA)
- Composite Materials (AREA)
- Life Sciences & Earth Sciences (AREA)
- Engineering & Computer Science (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Geochemistry & Mineralogy (AREA)
- Materials Engineering (AREA)
- Organic Chemistry (AREA)
- Inorganic Chemistry (AREA)
- Dispersion Chemistry (AREA)
- Compositions Of Macromolecular Compounds (AREA)
- Paints Or Removers (AREA)
Abstract
The present invention provides a kind of composite foam glass insulation spill guide, it is characterised in that：The insulation spill guide includes modified pitch, foam glass.Modified pitch is coated on foam glass.The modified pitch, including following parts by weight of component：50~55 parts of heavy traffic paving asphalt, 15~20 parts of second line of distillation oil, 5~12 parts of SBS1401.Modified pitch coating thickness is 2.5mm.Insulation spill guide of the present invention has good waterproof effect and heat insulation effect, it can be achieved that the pressure of 0.5MPa is waterproof simultaneously；The thermal coefficient of insulation spill guide of the present invention is 0.05W/M.K.
Description
Technical field
The present invention relates to architectural waterproof material more particularly to a kind of composite foam glass insulation spill guide and its preparation sides
Method belongs to field of waterproof materials.
Background technology
Splash guard is can both to prevent liquid from oozing using high molecular polymer as a kind of impervious material made of base stock
Leakage, can also prevent gaseous volatilization.The extensive utilization in building, traffic, subway, tunnel, engineering construction.
Foam glass is also known as cellular glass, internal to be full of countless openings or silent spilehole, and the area of stomata accounts for
The 80%~90% of total volume, pore size are 0.5~5mm, small to several microns also had.The primary raw material of foam glass is typically
Cullet, workable acidity slag substance, such as volcanic ash, float stone, perlite, obsidian, blast-furnace cinder.
Now, foam glass is applied seldom at home, is a kind of novel material, can be used as energy saving glass pane or be built
Build the heat preserving and insulating material of building enclosure.
With economic development, global economy increases energy demand, and in ever-increasing energy consumption, building energy conservation is
How a general orientation of building materials from now on provides a kind of not only kept the temperature but also the environment-friendly type composite heat-insulating splash guard of waterproof is one and needs to solve
Certainly the problem of.
The prior art has following defect：（1）Existing splash guard waterproof effect is only that the pressure of 0.2~0.3MPa is impermeable
Water cannot realize the effect of preferable heat preservation and waterproof simultaneously；（2）Existing thermal insulation board and splash guard can volatilize certain
Volatile organic compounds pollutes environment, is also harmful to human body；（3）Existing thermal insulation board, splash guard production cost are higher, raw
It is low to produce efficiency, construction is inconvenient, and efficiency is low.
Invention content
To solve the shortcomings of the prior art, a kind of composite foam glass insulation spill guide of present invention offer and its preparation
Method, to realize following goal of the invention：
1, keep the temperature composite foam glass insulation spill guide prepared by the present invention, good water-proof effect；
2, make composite foam glass insulation spill guide reactive organometal compound volatilization prepared by the present invention, it is environmentally safe,
Realize green, environmental protection；
3, cost is reduced, production efficiency and construction efficiency are improved.
In order to solve the above technical problems, using following technical scheme：
A kind of composite foam glass insulation spill guide, the insulation spill guide include modified pitch, foam glass.
It is to be further improved to above-mentioned technical proposal below：
The modified pitch is coated on foam glass.
The modified pitch, including following parts by weight of component：50~55 parts of heavy traffic paving asphalt, second line of distillation oil 15~20
Part, 5~12 parts of SBS1401,22~24 parts of light weight calcium.
The modified pitch, including following parts by weight of component：50~55 parts of heavy traffic paving asphalt, second line of distillation oil 15~20
Part, 5~12 parts of SBS1401,4~6 parts of anti-aging agent, 2~5 parts of rubber powder, 14~16 parts of talcum powder.
The modified pitch, including following parts by weight of component：50 parts of heavy traffic paving asphalt, second line of distillation oil 20 parts, SBS1401
5 parts, 5 parts of anti-aging agent, 5 parts of rubber powder, 15 parts of talcum powder.
The modified pitch coating thickness is 2.5mm.
The foam glass：Long 200~2000mm, wide 200~2000mm, 20~500mm of thickness.
The heavy traffic paving asphalt is No. 70 heavy traffic paving asphalts；
The anti-aging agent is p phenylenediamine type antioxidant；
The rubber powder is the tire glue powder of 60 mesh.
A kind of preparation method of composite foam glass insulation spill guide, including drying foam glass, mix asphalt and machine oil,
Modified pitch, coating, cooling step is made in heating.
The drying foam glass：Drying temperature is 160 DEG C, drying time 20s；
The mix asphalt and machine oil：It is stirred after mixing, mixing speed 60rpm, mixing time 10min；
The heating：The mixture of pitch and machine oil is warming up to 160 DEG C~180 DEG C；
The obtained modified pitch：To remaining ingredient, stirring in the mixture of pitch and machine oil, is added, temperature controls
At 180 DEG C~200 DEG C, after stirring 2~2.5 hours, control material temperature is at 180 DEG C~190 DEG C；
The coating：The upstream face that position is foam glass, coating thickness 2.5mm are coated, application temperature is 180 DEG C
~190 DEG C；
The cooling：Air-cooled cooling, until below temperature 50 C.
Compared with prior art, the beneficial effects of the invention are as follows：
（1）The good water-proof effect of insulation spill guide of the present invention is, it can be achieved that the pressure of 0.5MPa is waterproof；The present invention is kept the temperature
Splash guard has good heat insulation effect, thermal coefficient 0.05W/M.K；
（2）The compression strength of insulation spill guide of the present invention is 0.82~0.9Mpa, and flexural strength is 0.8~0.87Mpa；
（3）Insulation spill guide reactive organometal compound volatilization of the present invention, it is environmentally friendly, pollution-free；
（4）Realize waterproof and insulation integrated, easy for installation, construction efficiency raising 35~40%；
Production cost is low, and production efficiency is high, per second to produce 8 pieces~10 pieces.
Specific implementation mode
A kind of 1 composite foam glass insulation spill guide of embodiment
The insulation spill guide includes modified pitch, foam glass；Modified pitch is coated on foam glass, coating is thick
Degree is 2.5mm；
（1）The modified pitch, including following parts by weight of component：50 parts of 70# heavy traffic paving asphalts, second line of distillation oil 15 parts,
12 parts of SBS1401,23 parts of light weight calcium；
The light weight calcium：Fineness is 400 mesh；
（2）The foam glass：Long 300mm, wide 200mm, thick 40mm；
Compression strength 0.8Mpa, flexural strength 0.7Mpa, thermal coefficient 0.05W/M.K.
After tested, this composite foam glass insulation spill guide compression strength 0.9Mpa, flexural strength 0.85Mpa, heat conduction system
Number 0.05W/M.K.
A kind of 2 composite foam glass insulation spill guide of embodiment
The insulation spill guide is plain edition composite foam glass insulation spill guide；
The insulation spill guide includes modified pitch, foam glass；Modified pitch is coated on foam glass, coating is thick
Degree is 2.5mm；
（1）The modified pitch, including following parts by weight of component：55 parts of 70# heavy traffic paving asphalts, 15 parts of second line of distillation oil,
8 parts of SBS1401,5 parts of anti-aging agent, 2 parts of rubber powder, 15 parts of talcum powder；
The anti-aging agent is antioxidant 4010；
The rubber powder is 60 mesh tire glue powders；
（2）The foam glass：Long 300mm, wide 200mm, thick 40mm,
Compression strength 0.8Mpa, flexural strength 0.7Mpa thermal coefficients 0.05W/M.K.
After tested, this composite foam glass insulation spill guide compression strength 0.85Mpa, flexural strength 0.8Mpa, heat conduction system
Number 0.05W/M.K.
A kind of 3 composite foam glass insulation spill guide of embodiment
The insulation spill guide is self-adhering-type composite foam glass insulation spill guide；
The insulation spill guide includes modified pitch, foam glass；Modified pitch is coated on foam glass, coating is thick
Degree is 2.5mm；
（1）The modified pitch, including following parts by weight of component：50 parts of 70# heavy traffic paving asphalts, 20 parts of second line of distillation oil,
5 parts of SBS1401,5 parts of anti-aging agent, 5 parts of rubber powder, 15 parts of talcum powder；
The anti-aging agent is antioxidant 4010；
The rubber powder is 60 mesh tire glue powders；
（2）The foam glass：Long 300mm, wide 200mm, thick 40mm,
Compression strength 0.8Mpa, flexural strength 0.7Mpa thermal coefficients 0.05W/M.K.
After tested, this composite foam glass insulation spill guide compression strength 0.82Mpa, flexural strength 0.87Mpa, heat conduction system
Number 0.05W/M.K.
A kind of preparation method of 4 composite foam glass insulation spill guide of embodiment
The preparation method comprises the following steps：
1, foam glass is dried
Foam glass is dried through dry-heat air, sets drying temperature as 160 DEG C, drying time 20s.
2, each component of modified pitch is weighed by formula rate；
3, mix asphalt and machine oil
70# heavy traffic paving asphalts, second line of distillation oil, stirring are mixed, mixing speed control stirs 10min, obtain pitch in 60rpm
With the mixture of machine oil；
4, it heats up
The mixture of pitch and machine oil is warming up to 160 DEG C~180 DEG C；
5, modified pitch is made
To remaining ingredient, stirring in the mixture of pitch and machine oil, is added, temperature is controlled at 180 DEG C~200 DEG C, stirring
After 2 hours~2.5 hours, control material temperature obtains modified pitch at 180 DEG C~190 DEG C；
6, it coats
Modified pitch is coated in foam glass surface, coating position is the upstream face of foam glass, and coating thickness is
2.5mm；Application temperature is 180 DEG C~190 DEG C.
7, cooling
Air-cooled cooling, until then temperature 50 C is hereinafter, packed, acquisition composite foam glass insulation spill guide；Production
Speed control is in 8 pieces~10 pieces/s.
A kind of 5 composite foam glass insulation spill guide of embodiment
The insulation spill guide is self-adhering-type composite foam glass insulation spill guide；
The insulation spill guide includes modified pitch, foam glass；Modified pitch is coated on foam glass, coating is thick
Degree is 2.1mm；
（1）The modified pitch, including following parts by weight of component：52 parts of 70# heavy traffic paving asphalts, second line of distillation oil 17 parts,
9 parts of SBS1401, N- phenyl-α -4.5 parts of aniline, 3.4 parts of haze tallow, 2.5 parts of ferrous sulfate, 1.9 parts of guar gum, wood vinegar
0.7 part, 8 parts of magnesia-chrome sand, 770 3.5 parts of light stabilizer, 0.8 part of laurene.
The second line of distillation oil：Density is 943.1g/cm3, condensation point is 5 DEG C, and flash-point is 210 DEG C；
The SBS：Fugitive constituent≤0.7%, melt flow rate (MFR) are 1~5g/10min；
The haze tallow：Fusing point is 48 DEG C -52 DEG C；Oil content is 2%；
The magnesia-chrome sand：Density is 4.429g/cm3, 2180 DEG C of fusing point, Mohs' hardness 5.5.
（2）The foam glass：Long 300mm, wide 200mm, thick 40mm,
Compression strength is 0.8Mpa, flexural strength 0.7Mpa, thermal coefficient 0.05W/M.K.
Preparation method：
It is prepared as described in Example 4.
The composite foam glass insulation spill guide of the present embodiment is tested；
After tested, this composite foam glass insulation spill guide compression strength 0.82Mpa, flexural strength 0.87Mpa, heat conduction system
Number 0.05W/M.K；
After tested：For waterproof test pressure in 0.5MPa, insulation spill guide is not permeable.
Composite foam glass insulation spill guide provided by the present invention and preparation method thereof, realizes the combination of thermal insulation material
Diversified, waterproof and insulation integrated, production cost is low, and production efficiency and construction efficiency are efficient.
Composite foam glass insulation spill guide provided by the present invention and preparation method thereof, composite foam glass thermal-insulating waterproof
Plate good integrity, scene is convenient for segmentation.It meets the requirement of waterproof and good heat preservation is provided, the load of external decoration can be born.
Raw material environmental protection, heat insulation effect is good, splices position sealing compound and sticks fiberglass reinforced layer.It is easy for installation, it further increases anti-
Water and heat insulation effect.
The several embodiments that these are only the embodiment of the present invention are not intended to limit the invention embodiment, all at this
Within the spirit and principle of inventive embodiments, any modification, same replacement, improvement for being made etc. should be included in of the invention real
Apply the protection domain etc of example.
Claims (1)
1. a kind of composite foam glass insulation spill guide, it is characterised in that：The insulation spill guide includes modified pitch, foam
Glass；
The compression strength 0.8Mpa of the foam glass, flexural strength 0.7Mpa, thermal coefficient 0.05W/M.K；
The modified pitch, including following parts by weight of component：50 parts of heavy traffic paving asphalt, second line of distillation oil 20 parts, 5 parts of SBS1401,
5 parts of anti-aging agent, 5 parts of rubber powder, 15 parts of talcum powder；
The heavy traffic paving asphalt is No. 70 heavy traffic paving asphalts；
The anti-aging agent is antioxidant 4010；
The rubber powder is 60 mesh tire glue powders；
The described composite foam glass insulation spill guide compression strength 0.82Mpa, flexural strength 0.87Mpa, thermal coefficient
0.05W/M.K；
The modified pitch is coated on foam glass；
The modified pitch coating thickness is 2.5mm；
The foam glass：Long 200~2000mm, wide 200~2000mm, 20~500mm of thickness；
A kind of preparation method of composite foam glass insulation spill guide, including drying foam glass, mix asphalt and machine
Heating, modified pitch, coating, cooling step is made in oil；
The drying foam glass：Drying temperature is 160 DEG C, drying time 20s；
The mix asphalt and machine oil：It is stirred after mixing, mixing speed 60rpm, mixing time 10min；
The heating：The mixture of pitch and machine oil is warming up to 160 DEG C~180 DEG C；
The obtained modified pitch：To remaining ingredient, stirring in the mixture of pitch and machine oil, is added, temperature is controlled 180
DEG C~200 DEG C, after stirring 2~2.5 hours, control material temperature is at 180 DEG C~190 DEG C；
The coating：Coat position be foam glass upstream face, coating thickness 2.5mm, application temperature be 180 DEG C~
190℃；
The cooling：Air-cooled cooling, until below temperature 50 C.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201510959924.9A CN105621894B (en) | 2015-12-21 | 2015-12-21 | A kind of composite foam glass insulation spill guide and preparation method thereof |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201510959924.9A CN105621894B (en) | 2015-12-21 | 2015-12-21 | A kind of composite foam glass insulation spill guide and preparation method thereof |
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| Publication Number | Publication Date |
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| CN105621894A CN105621894A (en) | 2016-06-01 |
| CN105621894B true CN105621894B (en) | 2018-08-21 |
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Families Citing this family (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN107060121A (en) * | 2017-06-15 | 2017-08-18 | 毅可新材料科技（上海）有限公司 | Overlay film foam glass board and preparation method thereof |
Citations (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| GB1558176A (en) * | 1976-07-07 | 1979-12-19 | Evode Waterproofing Systems Lt | Thermal insulating material |
| US4469731A (en) * | 1981-07-02 | 1984-09-04 | Nord Bitumi Di Marco Danese & C. S.A.S. | Composite insulating article for making prefabricated coverings |
| CN2174516Y (en) * | 1992-09-09 | 1994-08-17 | 施韦西建筑师有限公司 | Building element |
| CN103911117A (en) * | 2013-01-05 | 2014-07-09 | 上海东方雨虹防水技术有限责任公司 | Modified bitumen waterproof coiled material, coating material and preparation method thereof |
-
2015
- 2015-12-21 CN CN201510959924.9A patent/CN105621894B/en active Active
Patent Citations (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| GB1558176A (en) * | 1976-07-07 | 1979-12-19 | Evode Waterproofing Systems Lt | Thermal insulating material |
| US4469731A (en) * | 1981-07-02 | 1984-09-04 | Nord Bitumi Di Marco Danese & C. S.A.S. | Composite insulating article for making prefabricated coverings |
| CN2174516Y (en) * | 1992-09-09 | 1994-08-17 | 施韦西建筑师有限公司 | Building element |
| CN103911117A (en) * | 2013-01-05 | 2014-07-09 | 上海东方雨虹防水技术有限责任公司 | Modified bitumen waterproof coiled material, coating material and preparation method thereof |
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Address after: 262735 Taitou Town, Shouguang City, Weifang City, Shandong Province, 2000 meters west of the government Patentee after: Hongyuan Waterproof Technology Group Co., Ltd. Address before: 262735 Taitou Town, Shouguang City, Weifang City, Shandong Province, 2000 meters west of the government Patentee before: Weifang Hongyuan Waterproof Material Co., Ltd. |
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Denomination of invention: Composite foam glass thermal insulation waterproof board and preparation method thereof Effective date of registration: 20220329 Granted publication date: 20180821 Pledgee: Zhejiang Commercial Bank Co.,Ltd. Weifang branch Pledgor: HONGYUAN WATERPROOF TECHNOLOGY GROUP Co.,Ltd. Registration number: Y2022980003440 |