CN105601111B - A kind of iridescent glaze and its production technology - Google Patents
A kind of iridescent glaze and its production technology Download PDFInfo
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- CN105601111B CN105601111B CN201510996919.5A CN201510996919A CN105601111B CN 105601111 B CN105601111 B CN 105601111B CN 201510996919 A CN201510996919 A CN 201510996919A CN 105601111 B CN105601111 B CN 105601111B
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- C—CHEMISTRY; METALLURGY
- C03—GLASS; MINERAL OR SLAG WOOL
- C03C—CHEMICAL COMPOSITION OF GLASSES, GLAZES OR VITREOUS ENAMELS; SURFACE TREATMENT OF GLASS; SURFACE TREATMENT OF FIBRES OR FILAMENTS MADE FROM GLASS, MINERALS OR SLAGS; JOINING GLASS TO GLASS OR OTHER MATERIALS
- C03C8/00—Enamels; Glazes; Fusion seal compositions being frit compositions having non-frit additions
- C03C8/14—Glass frit mixtures having non-frit additions, e.g. opacifiers, colorants, mill-additions
-
- C—CHEMISTRY; METALLURGY
- C03—GLASS; MINERAL OR SLAG WOOL
- C03C—CHEMICAL COMPOSITION OF GLASSES, GLAZES OR VITREOUS ENAMELS; SURFACE TREATMENT OF GLASS; SURFACE TREATMENT OF FIBRES OR FILAMENTS MADE FROM GLASS, MINERALS OR SLAGS; JOINING GLASS TO GLASS OR OTHER MATERIALS
- C03C8/00—Enamels; Glazes; Fusion seal compositions being frit compositions having non-frit additions
- C03C8/02—Frit compositions, i.e. in a powdered or comminuted form
- C03C8/10—Frit compositions, i.e. in a powdered or comminuted form containing lead
- C03C8/12—Frit compositions, i.e. in a powdered or comminuted form containing lead containing titanium or zirconium
-
- C—CHEMISTRY; METALLURGY
- C04—CEMENTS; CONCRETE; ARTIFICIAL STONE; CERAMICS; REFRACTORIES
- C04B—LIME, MAGNESIA; SLAG; CEMENTS; COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDING MATERIALS; ARTIFICIAL STONE; CERAMICS; REFRACTORIES; TREATMENT OF NATURAL STONE
- C04B41/00—After-treatment of mortars, concrete, artificial stone or ceramics; Treatment of natural stone
- C04B41/45—Coating or impregnating, e.g. injection in masonry, partial coating of green or fired ceramics, organic coating compositions for adhering together two concrete elements
- C04B41/50—Coating or impregnating, e.g. injection in masonry, partial coating of green or fired ceramics, organic coating compositions for adhering together two concrete elements with inorganic materials
- C04B41/5022—Coating or impregnating, e.g. injection in masonry, partial coating of green or fired ceramics, organic coating compositions for adhering together two concrete elements with inorganic materials with vitreous materials
-
- C—CHEMISTRY; METALLURGY
- C04—CEMENTS; CONCRETE; ARTIFICIAL STONE; CERAMICS; REFRACTORIES
- C04B—LIME, MAGNESIA; SLAG; CEMENTS; COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDING MATERIALS; ARTIFICIAL STONE; CERAMICS; REFRACTORIES; TREATMENT OF NATURAL STONE
- C04B41/00—After-treatment of mortars, concrete, artificial stone or ceramics; Treatment of natural stone
- C04B41/80—After-treatment of mortars, concrete, artificial stone or ceramics; Treatment of natural stone of only ceramics
- C04B41/81—Coating or impregnation
- C04B41/85—Coating or impregnation with inorganic materials
- C04B41/86—Glazes; Cold glazes
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- Chemical & Material Sciences (AREA)
- Engineering & Computer Science (AREA)
- Materials Engineering (AREA)
- Organic Chemistry (AREA)
- Ceramic Engineering (AREA)
- Life Sciences & Earth Sciences (AREA)
- Chemical Kinetics & Catalysis (AREA)
- General Chemical & Material Sciences (AREA)
- Geochemistry & Mineralogy (AREA)
- Inorganic Chemistry (AREA)
- Structural Engineering (AREA)
- Glass Compositions (AREA)
Abstract
The present invention provides a kind of iridescent glaze and its production technology, the iridescent glaze is by 95 parts of frits by weight, 46 parts of kaolin, 35 40 parts of water, 0.05 0.2 parts of carboxymethyl celluloses and 0.1 0.2 parts of sodium tripolyphosphate mixing and ball millings, obtain glaze slip, 46 parts of ammonium metavanadates are added into glaze slip to mix, on leaching to base substrate, burn till and obtain；The frit is made up of following components in parts by weight：32 34 parts of red lead, 46 parts of potassium carbonate, 35 parts of mangandolomite, 35 parts of coarse whiting, 36 parts of aluminum oxide, 11 13 parts of zinc oxide, 30 33 parts of quartz and 58 parts of titanium dioxide.Its production technology includes grinding, adjusts proportion, leaching base and burn till.In the present invention, because using ammonium metavanadate in-situ preparation V2O5, more environmentally-friendly health, the molding time that can effectively shorten iridescent glaze；The iridescent glaze is lead zinc-manganese titanium vanadium Quinary system, and its rainbow effect is more bright-coloured bright.
Description
Technical field
The present invention relates to technical field ceramic field, and in particular to a kind of iridescent glaze and its production technology.
Background technology
At this stage the china industry in China be all largely ink-jet and silk-screen printing mode come to glazed wall tile carry out
Decoration, color and form using glaze paint after this decorative form are the single of fixation.
Iridescent glaze is that glaze surface shines brilliant, different angle viewing presentation different colours effect, or a variety of face in the sun
The color ring of color, or polychrome rainbow effect, or pearly luster and interference gloss, or a kind of ceramic glaze in silver color pool.
For iridescent glaze into during glaze, its surface separates out crystallization or crystalline film under certain thermodynamic condition, they with
The refractive index of glass phase, reflection are different from absorption characteristic so that the visible ray for inciding the various wavelength of glaze layer produces optical path difference
The interference of light is caused, causes rainbow effect.The composition of parent glaze is controlled, makes the crystal difference of precipitation, difference just occurs in glaze paint
Iridescent colors.
Frit, which is made, in the frit parent glaze of lead-zinc-titanium to reduce firing temperature, but the formation of its iris is slower.
The content of the invention
The defects of to overcome prior art, it is an object of the invention to provide a kind of iridescent glaze of in-situ preparation vanadium.
To achieve the above object, the technical solution adopted in the present invention is as follows：
A kind of iridescent glaze, the iridescent glaze be by 95 parts by weight frits, 4-6 parts by weight kaolin clay, 35-40 parts by weight water,
0.05-0.2 parts by weight carboxymethyl cellulose and the mixing of 0.1-0.2 parts by weight sodium tripolyphosphate, ball milling add into glaze slip into glaze slip
Enter the mixing of 4-6 parts by weight ammonium metavanadate, drench to base substrate, burn till and obtain；
The frit is made up of following components in parts by weight：The red lead of 32-34 parts by weight, the carbonic acid of 4-6 parts by weight
Potassium, the mangandolomite of 3-5 parts by weight, the coarse whiting of 3-5 parts by weight, the aluminum oxide of 3-6 parts by weight, the zinc oxide of 11-13 parts by weight,
The quartz of 30-33 parts by weight and the titanium dioxide of 5-8 parts by weight.
Preferably, the frit is made up of following steps：
1) mix：By the red lead of 32-34 parts by weight, the potassium carbonate of 4-6 parts by weight, the mangandolomite of 3-5 parts by weight, 3-5
The coarse whiting of parts by weight, the aluminum oxide of 3-6 parts by weight, the zinc oxide of 11-13 parts by weight, the quartz and 5-8 weight of 30-33 parts by weight
The titanium dioxide mixing of part, stirs, obtains premix；
2) melt：Premix is put into tank furnace, in 1280-1350 DEG C of fusing, obtains glass metal；
3) water quenching：By above-mentioned glass metal beam into 20-60 DEG C of water, frit is obtained.
Preferably, in step 2), in 1330-1350 DEG C of fusing.
Preferably, in step 2), the water quenching in 20-100 DEG C of water.
Another object of the present invention is to provide the production technology of above-mentioned iridescent glaze, comprise the following steps：
1) slurrying：By 95 parts by weight frits, 4-6 parts by weight kaolin clay, 35-40 parts by weight water, 0.05-0.2 parts by weight carboxylics
Methylcellulose and the mixing of 0.1-0.2 parts by weight sodium tripolyphosphate, wear into glaze slip；
2) proportion is adjusted：4-6 parts by weight ammonium metavanadates are added into glaze slip；
3) base is drenched：The glaze slip that step 2) is obtained is uniformly on leaching to base substrate；
4) burn till：Burnt till in 1110-1130 DEG C, obtain iridescent glaze.
Preferably, comprise the following steps：
1) slurrying：By 95 parts by weight frits, 5 parts by weight kaolin clay, 36 parts by weight water, 0.1 parts by weight carboxymethyl cellulose
Mixed with 0.15 parts by weight sodium tripolyphosphate, glaze slip can be obtained by 325 sieves by being milled to；
2) proportion is adjusted：5 parts by weight ammonium metavanadates are added into glaze slip；
3) base is drenched：The glaze slip that step 2) is obtained is uniformly on leaching to base substrate；
4) burn till：Burnt till in 1120 DEG C, obtain iridescent glaze.
Relative to prior art, the present invention has advantages below：
1st, in the present invention, because ammonium metavanadate is being made after glaze slip in addition system, so V2O5Be it is generated in-situ,
Traditional iridescent glaze containing vanadium is greatly reduced in production technology, because containing V2O5Glass metal or glaze liquid are being shifted to production environment
And the pollution of water body etc., more environmentally-friendly health；
2nd, the present invention adds ammonium metavanadate after glaze slurry system is worn into, and can effectively shorten the molding time of iridescent glaze；
3rd, iridescent glaze provided by the invention is lead-zinc-manganese-titanium-vanadium Quinary system, and its rainbow effect is more bright-coloured bright.
The present invention is described in further detail with reference to specific embodiment.
Embodiment
The present invention provides a kind of iridescent glaze, and the iridescent glaze is by 95 parts by weight frits, 4-6 parts by weight kaolin clay, 35-40 weights
Measure part water, 0.05-0.2 parts by weight carboxymethyl cellulose and the mixing of 0.1-0.2 parts by weight sodium tripolyphosphate, ball milling is into glaze slip, outside
The ammonium metavanadates of 4-6 parts by weight is added to drench to base substrate, burn till and obtain the ratio recanalization of glaze slip to 1.75-1.85；
The frit is made up of following components in parts by weight：The red lead of 32-34 parts by weight, the carbonic acid of 4-6 parts by weight
Potassium, the mangandolomite of 3-5 parts by weight, the coarse whiting of 3-5 parts by weight, the aluminum oxide of 3-6 parts by weight, the zinc oxide of 11-13 parts by weight,
The quartz of 30-33 parts by weight and the titanium dioxide of 5-8 parts by weight.
Embodiment 1
A kind of iridescent glaze, its frit are made up of following components：32kg red leads, 4kg potassium carbonate, 5kg mangandolomites, 5kg weights
Calcium, 3kg aluminum oxide, 13kg zinc oxide, 33kg quartz and 8kg titanium dioxides；
The frit is made up of following steps：
1) mix：Above-mentioned material stirring is uniform, obtain premix；
2) melt：Premix is put into tank furnace, in 1280-1310 DEG C of fusing, obtains glass metal；
3) water quenching：By above-mentioned glass metal beam into 50-60 DEG C of water, frit is obtained；
Ammonium metavanadate is added by the ratio recanalization of glaze slip to 1.75-1.85, leaching after the iridescent glaze is worn into glaze slip by frit
To base substrate, burn till and obtain；
The production technology of the iridescent glaze comprises the following steps：
1) slurrying：By 95kg frits, 5kg kaolin, 36kg water, 0.1kg carboxymethyl celluloses and 0.15kg tripolyphosphates
Sodium is mixed, and glaze slip can be obtained by 325 sieves by being milled to；
2) proportion is adjusted：5kg ammonium metavanadates are added into glaze slip, the proportion of glaze slip is 1.8 after stirring；
3) base is drenched：The glaze slip that step 2) is obtained is uniformly on leaching to base substrate；
4) burn till：Burnt till in 1120 DEG C, obtain iridescent glaze.
Embodiment 2
A kind of iridescent glaze, its frit are made up of following components in parts by weight：34kg red leads, 6kg potassium carbonate, 3kg manganese
Dolomite, 3kg coarse whitings, 6kg aluminum oxide, 11kg zinc oxide, 30kg quartz and 5kg titanium dioxides；
The frit is made up of following steps：
1) mix：Above-mentioned material stirring is uniform, obtain premix；
2) melt：Premix is put into tank furnace, in 1330-1350 DEG C of fusing, obtains glass metal；
3) water quenching：By above-mentioned glass metal beam into 20-30 DEG C of water, frit is obtained；
The iridescent glaze is worn into by frit ammonium metavanadate is added after glaze slip by the ratio recanalization of glaze slip to 1.8, drenched to base substrate
On, burn till and obtain；
The production technology of the iridescent glaze comprises the following steps：
1) slurrying：By 95kg frits, 4kg kaolin, 36kg water, 0.2kg carboxymethyl celluloses and 0.1kg sodium tripolyphosphates
Mixing, glaze slip can be obtained by 325 sieves by being milled to；
2) proportion is adjusted：6kg ammonium metavanadates are added into glaze slip, glaze slip proportion is 1.8 after mixing；
3) base is drenched：The glaze slip that step 2) is obtained is uniformly on leaching to base substrate；
4) burn till：Burnt till in 1130 DEG C, obtain iridescent glaze.
Embodiment 3
A kind of iridescent glaze, its frit are made up of following components in parts by weight：34kg red leads, 6kg potassium carbonate, 3kg manganese
Dolomite, 3kg coarse whitings, 6kg aluminum oxide, 11kg zinc oxide, 30kg quartz and 5kg titanium dioxides；
The frit is made up of following steps：
1) mix：Above-mentioned material stirring is uniform, obtain premix；
2) melt：Premix is put into tank furnace, in 1310-1330 DEG C of fusing, obtains glass metal；
3) water quenching：By above-mentioned glass metal beam into 40-50 DEG C of water, frit is obtained；
The iridescent glaze is worn into by frit ammonium metavanadate is added after glaze slip by the ratio recanalization of glaze slip to 1.8, drenched to base substrate
On, burn till and obtain；
The production technology of the iridescent glaze comprises the following steps：
1) slurrying：By 95 parts by weight frits, 6 parts by weight kaolin clay, 30 parts by weight water, 0.1 parts by weight carboxymethyl cellulose
Mixed with 0.2 parts by weight sodium tripolyphosphate, glaze slip can be obtained by 325 sieves by being milled to；
2) proportion is adjusted：5kg ammonium metavanadates are added into glaze slip, glaze slip proportion is 1.82 after mixing；
3) base is drenched：The glaze slip that step 2) is obtained is uniformly on leaching to base substrate；
4) burn till：Burnt till in 1110 DEG C, obtain iridescent glaze.
Comparative example 1
As different from Example 1, in frit manufacturing process, step 2) fusion temperature is 1330-1350 DEG C to comparative example 1；
Comparative example 2
As different from Example 1, in frit manufacturing process, step 2) reclaimed water extraction temperature is 20-30 DEG C to comparative example 2；
Performance detection
The iridescent glaze that embodiment 1-3 is obtained, after kiln discharge, its outward appearance is observed, its result is as shown in table 2.
From the comparison of embodiment 1 and comparative example 1, the gloss color that raising fusion temperature can help to iridescent glaze is more beautiful
Beautiful, the comparison of embodiment 1 and embodiment 2 can confirm this result, and the heat endurance of iridescent glaze does not reduce；By embodiment
1 understands with the comparison of comparative example 2, reduces water extraction temperature, iridescent glaze surface pearly luster effect is more prominent, and other performance is not
Reduce.
Above-mentioned embodiment is only the preferred embodiment of the present invention, it is impossible to the scope of protection of the invention is limited with this,
The change and replacement for any unsubstantiality that those skilled in the art is done on the basis of the present invention belong to institute of the present invention
Claimed scope.
Claims (5)
1. a kind of iridescent glaze, it is characterised in that the iridescent glaze is by 95 parts by weight frits, 4-6 parts by weight kaolin clay, 35-40 weights
Measure part water, 0.05-0.2 parts by weight carboxymethyl cellulose and the mixing of 0.1-0.2 parts by weight sodium tripolyphosphate, ball milling into glaze slip, to
4-6 parts by weight ammonium metavanadate is added in glaze slip to mix, and is drenched to base substrate, is burnt till and obtain；
The frit is made up of following components in parts by weight：The red lead of 32-34 parts by weight, the potassium carbonate of 4-6 parts by weight, 3-
The mangandolomite of 5 parts by weight, the coarse whiting of 3-5 parts by weight, the aluminum oxide of 3-6 parts by weight, the zinc oxide of 11-13 parts by weight, 30-33
The quartz of parts by weight and the titanium dioxide of 5-8 parts by weight.
2. iridescent glaze as claimed in claim 1, it is characterised in that the frit is made up of following steps：
1) mix：By the red lead of 32-34 parts by weight, the potassium carbonate of 4-6 parts by weight, the mangandolomite of 3-5 parts by weight, 3-5 weight
The coarse whiting of part, the aluminum oxide of 3-6 parts by weight, the zinc oxide of 11-13 parts by weight, quartz and the 5-8 parts by weight of 30-33 parts by weight
Titanium dioxide mixes, and stirs, obtains premix；
2) melt：Premix is put into tank furnace, in 1280-1350 DEG C of fusing, obtains glass metal；
3) water quenching：By above-mentioned glass metal beam into 20-60 DEG C of water, frit is obtained.
3. iridescent glaze as claimed in claim 2, it is characterised in that in step 2), in 1330-1350 DEG C of fusing.
4. the production technology of iridescent glaze as claimed in claim 1, comprises the following steps：
1) slurrying：By 95 parts by weight frits, 4-6 parts by weight kaolin clay, 35-40 parts by weight water, 0.05-0.2 parts by weight carboxymethyls
Cellulose and the mixing of 0.1-0.2 parts by weight sodium tripolyphosphate, wear into glaze slip；
2) proportion is adjusted：4-6 parts by weight ammonium metavanadates are added into glaze slip；
3) base is drenched：The glaze slip that step 2) is obtained is uniformly on leaching to base substrate；
4) burn till：Burnt till in 1110-1130 DEG C, obtain iridescent glaze.
5. production technology as claimed in claim 4, comprises the following steps：
1) slurrying：By 95 parts by weight frits, 5 parts by weight kaolin clay, 36 parts by weight water, 0.1 parts by weight carboxymethyl cellulose and
0.15 parts by weight sodium tripolyphosphate is mixed, and glaze slip can be obtained by 325 sieves by being milled to；
2) proportion is adjusted：5 parts by weight ammonium metavanadates are added into glaze slip；
3) base is drenched：The glaze slip that step 2) is obtained is uniformly on leaching to base substrate；
4) burn till：Burnt till in 1120 DEG C, obtain iridescent glaze.
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| CN201510996919.5A CN105601111B (en) | 2015-12-24 | 2015-12-24 | A kind of iridescent glaze and its production technology |
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| CN201510996919.5A CN105601111B (en) | 2015-12-24 | 2015-12-24 | A kind of iridescent glaze and its production technology |
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| CN110498668A (en) * | 2019-07-06 | 2019-11-26 | 福建省乐普陶板制造有限公司 | A kind of colorful glaze ceramic plate and preparation method thereof |
| CN113735445B (en) * | 2021-08-27 | 2023-04-25 | 湖南泉湘陶瓷有限公司 | Iridescent pearl glaze and preparation method thereof |
Citations (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN101948335A (en) * | 2010-08-24 | 2011-01-19 | 霍镰泉 | Novel low temperature frit, crystal floor tile and method for producing crystal floor tile |
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| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN101948335A (en) * | 2010-08-24 | 2011-01-19 | 霍镰泉 | Novel low temperature frit, crystal floor tile and method for producing crystal floor tile |
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