A kind of ecological cotton perianth tire and preparation method thereof
Technical field
The present invention relates to textile preparing technical field, relate in particular to a kind of ecological cotton perianth tire and preparation method thereof.
Background technology
Cotton is had long history in China, compatriots also have deep feelings to it. It has good hygroscopicity, warmth retention property strong, to the large characteristic of human body non-stimulated three, the irritated crowd's use of the children that are particularly suitable for sleep environment to have relatively high expectations, pregnant woman and Yi.
Because the shredding of traditional cotton perianth cotton fiber is insufficient, the abundant heaviness of comforter batt, easily harden harden, not fluffy, and easily form broken hole, cause comfortableness, warmth retention property not good. Substituted gradually the market of slowly having faded out by various fiber quilts, eiderdown quilt and silk quilt etc.
Instantly not high to textile comforter batt concern, in the problem that solves anti-compaction, be the way of adopting conventional blending certain proportion polyester fiber, but can bring the side effect that produces static, and inadequate environmental protection, comfortableness is poor, and broken hole problem also happens occasionally. Also there is the method that adopts quilting technique after laying, lack but can bring the consequence that resilience and microcosmic harden, finally fail to overcome the native defect of natural textile comforter batt.
Application number is that 201410298396.2 Chinese patent discloses a kind of super gas permeability without net cotton preparation method and cotton-wadded quilt, and preparation method comprises: one, use cotton machine to carry out mechanical impurity elimination to elementary cotton, the impurity elimination time is 10-15 minute; Two, use bamboo pole that the elementary cotton after impurity elimination is got from cotton machine, and make the secondary cotton of tubbiness; Three,, taking rectangle wooden frame as mould, secondary cotton be laid in mould and form three grades of cottons of rectangle, and being greater than its thickness near four limits by the thickness that manually making of three grades of cottons is become to centre position; Four, adopt wooden flatiron, in unsettled mode, three grades of cottons are carried out to compression process, then three grades of cottons are loaded in gauze. The present invention also provides a kind of cotton-wadded quilt that said method is manufactured of applying. Super gas permeability provided by the invention is without the cotton preparation method of net, and because intermediate portion is thicker, its warming effect is better. Four limits are thinner, can alleviate the load that cotton-wadded quilt causes old man.
Although the cotton-wadded quilt good permeability of above-mentioned patent, still can not solve the shortcoming that cotton is easily hardened, easily forms broken hole.
Summary of the invention
In order to solve the problems of the technologies described above, the invention provides a kind of ecological cotton perianth tire and preparation method thereof. The viviparous state environment protection health of ecological cotton perianth of the present invention, fluffy softness, comfortableness is good, and screen resilience is good, and is difficult for hardening and hardens, and is difficult for forming broken hole.
Concrete technical scheme of the present invention is: a kind of ecological cotton perianth tire, and adopt ecological medium staple cotton, short silk, long silk to be prepared from as raw material, its short-and-medium silk accounts for the 12-13% of comforter batt gross mass, and long silk accounts for the 2-3% of comforter batt gross mass.
For ensureing natural, environmental protection, the health of comforter batt, the operating characteristic of safety, the present invention selects long silk and short silk and ecological medium staple cotton to carry out compound laying from many natural fibers.
A preparation method for ecological cotton perianth tire, step is as follows:
1) adopt meticulous bullet machine respectively ecological medium staple cotton and short silk to be carried out to combing, be made into respectively netted cotton layer and netted mulberry silk layer.
2) described netted cotton layer and netted mulberry silk layer are tiled and are laminated on workbench in interval in proportion, make base tire.
3) employing is rubbed cotton machine described base tire is rubbed to pressure. Base tire is rubbed to pressure, can suitably increase the packing of base tire, so that following process.
4) long silk is punctured to the vertical direction of base tire by puncture machine, make ecological cotton perianth tire after making to form cellular stereoscopic three-dimensional structure in base tire.
Making when comforter batt in comforter batt by the not contour distribution laying of short silk fiber, can effectively solve comforter batt harden problem and broken hole problem. Select suitable density to adopt long silk to carry out loose type puncture perpendicular to comforter batt plane simultaneously, form bat honeycomb fashion stereoscopic three-dimensional structure, cancel original tight type quilting technique. Adopt acupuncture piercing method can improve the soft ability of comforter batt resilience.
It is raw material that ecological medium staple cotton adopts Xinjiang high-quality cotton (obtaining Oeko-TexStandard100 certification), in conjunction with advanced cotton carding technology, ecological medium staple cotton is made to individual layer is as thin as cicada's wings, the comforter batt structure of multiple-layer stacked, product uniformity, toughness and fluffy degree are high. Because of " the cicada's wings technology " of its uniqueness, be different from traditional " bow plays gimmick ", increased core pliability, improved core resilience, avoided forming the possibility of broken hole, make it more meet ecology, health, comfortable demand.
By the technological measure of long silk, short silk, the puncture of ecological medium staple cotton planar layer composite stereo, can effectively produce top grade, ecology, environmental protection, safe, comfortable textile comforter batt, and possess the moisture absorption, insulation of textile comforter batt, heat-resisting, health, comfortable basic function. Overcome that the textile comforter batt of cotton fiber hardens simultaneously, broken hole, the poor defect of resilience, meet greatly comfortable, the safety of people to bedding, environmental protection, healthy ecological requirement.
As preferably, the specification of described ecological medium staple cotton is: white cotton 228, more than horse value 4.5(85%), average length 28mm, average fracture strength 28CN/Tex, Length Regularity 83%; The specification of described short silk is: 3A20/22D, fracture strength, 3.0 grams of force per Denier, regain 10%; The specification of described long silk is: F2 × 100/120D, 150S, fracture strength 3.8 grams of force per Denier, regain 11%.
As preferably, the model of described meticulous bullet machine is 6MTB220-III type, wherein divides 620 revs/min of comb diameter 246mm, cylinder rotating speeds.
As preferably, described in rub cotton machine model be WR-I type, wherein spindle speed is 60 revs/min.
As preferably, the model of described puncture machine is LT-CC2 type, and the density that wherein punctures is controlled at 60-160cm2Scope in, puncture speed 50-80 pin/minute.
As preferably, in step 2) while carrying out interval tiling lamination, often, after folded one deck, spray ecological crosslinking agent to netted cotton layer or netted mulberry silk layer surface with vaporific form, to spray and placed the lamination that carries out next layer after 5-15min, wherein sprinkling amount is 5-10ml/m2。
The use of ecological crosslinking agent, can be in the time of tiling lamination, make netted cotton layer and the netted mulberry silk layer of adjacent two layers produce network-like crosslinked, can increase the adhesion between different layers on the one hand, make each layer of difficult point delamination of comforter batt, on the other hand, the netted cotton layer of adjacent two layers and netted mulberry silk layer produce after network-like being cross-linked, can increase the screen resilience of comforter batt, and be difficult for broken hole.
As preferably, the component of described ecological crosslinking agent is: silk-fibroin 1-3wt%, tyrosine 0.5-1.5wt%, the water of ethanol 8-12wt% and surplus.
The ecological crosslinking agent safety and environmental protection that technical solution of the present invention is selected, can not impact health. Silk-fibroin, tyrosine can make to occur between fiber crosslinked, gain in strength, and have homology with silk, can not affect feel, comfort level and outward appearance.
As preferably, the component of described ecological crosslinking agent is: silk-fibroin 1-2wt%, tyrosine 0.5-1wt%, ethylene glycol diglycidylether 0.5-1.5wt%, the water of ethanol 8-12wt% and surplus. Ethylene glycol diglycidylether is that molecular structure two ends have active end group, can with cotton, silk in active group react, thereby produce crosslinked.
As preferably, the preparation method of described silk-fibroin is: silk is immersed in to boiling 1-2h in boiling water, then be silk 0.5-1 potash doubly to adding quality in boiling water, continue at 90 DEG C of insulation 30-40min, after filtration successively, make silk-fibroin after concentrated, dry finally.
The fibroin of preparing through said method, impurity is few, and purity is high, and security is good, and has good activity, is particularly suitable as the active component of the ecological crosslinking agent in comforter batt preparation process of the present invention.
Be compared with the prior art, the invention has the beneficial effects as follows: the viviparous state environment protection health of ecological cotton perianth of the present invention, fluffy softness, comfortableness is good, and screen resilience is good, and is difficult for hardening and hardens, and is difficult for forming broken hole.
Detailed description of the invention
Below in conjunction with embodiment, the invention will be further described.
Embodiment 1
A kind of ecological cotton perianth tire, adopts ecological medium staple cotton, short silk, long silk to be prepared from as raw material, and its short-and-medium silk accounts for 12.5% of comforter batt gross mass, and long silk accounts for 2.5% of comforter batt gross mass. The specification of described ecological medium staple cotton is: white cotton 228, more than horse value 4.5(85%), average length 28mm, average fracture strength 28CN/Tex, Length Regularity 83%; The specification of described short silk is: 3A20/22D, fracture strength, 3.0 grams of force per Denier, regain 10%; The specification of described long silk is: F2 × 100/120D, 150S, fracture strength 3.8 grams of force per Denier, regain 11%.
Preparation method's step of this ecological cotton perianth tire is as follows:
1) adopt the meticulous bullet machine of 6MTB220-III type respectively ecological medium staple cotton and short silk to be carried out to combing, be made into respectively netted cotton layer and netted mulberry silk layer. Wherein divide 620 revs/min of comb diameter 246mm, cylinder rotating speeds.
2) described netted cotton layer and netted mulberry silk layer are tiled and are laminated on workbench in interval in proportion, make base tire.
3) adopt WR-I type to rub cotton machine described base tire is rubbed to pressure. Wherein spindle speed is 60 revs/min.
4) long silk is punctured to the vertical direction of base tire by LT-CC2 type puncture machine, make ecological cotton perianth tire after making to form cellular stereoscopic three-dimensional structure in base tire. The density that wherein punctures is controlled at 110cm2Scope in, puncture speed 65 pins/minute.
The product of the present embodiment is carried out to performance test, as follows with standard figures contrast:
Standard compression rate is greater than 30%, and actual measurement compression ratio reaches 50%;
Regain is greater than 60%, actual regain 97%;
The impure rate of standard is less than 1.4%, actual measurement percentage of impurity 0.47%;
Standard short fibre content is less than 25%, actual measurement short fibre content 13%.
Embodiment 2
A kind of ecological cotton perianth tire, adopts ecological medium staple cotton, short silk, long silk to be prepared from as raw material, and its short-and-medium silk accounts for 12% of comforter batt gross mass, and long silk accounts for 2% of comforter batt gross mass. The specification of described ecological medium staple cotton is: white cotton 228, more than horse value 4.5(85%), average length 28mm, average fracture strength 28CN/Tex, Length Regularity 83%; The specification of described short silk is: 3A20/22D, fracture strength, 3.0 grams of force per Denier, regain 10%; The specification of described long silk is: F2 × 100/120D, 150S, fracture strength 3.8 grams of force per Denier, regain 11%.
Preparation method's step of this ecological cotton perianth tire is as follows:
1) adopt the meticulous bullet machine of 6MTB220-III type respectively ecological medium staple cotton and short silk to be carried out to combing, be made into respectively netted cotton layer and netted mulberry silk layer. Wherein divide 620 revs/min of comb diameter 246mm, cylinder rotating speeds.
2) described netted cotton layer and netted mulberry silk layer are tiled and are laminated on workbench in interval in proportion, often folding after one deck, spray ecological crosslinking agent to netted cotton layer or netted mulberry silk layer surface with vaporific form, sprayed and placed the lamination that carries out next layer after 10min, wherein sprinkling amount is 7.5ml/m2. Finally make base tire.
The component of wherein said ecological crosslinking agent is: silk-fibroin 2wt%, tyrosine 1wt%, the water of ethanol 10wt% and surplus.
The preparation method of described silk-fibroin is: silk is immersed in to boiling 1.5h in the boiling water of its 300 times of quality, then in boiling water, add the potash that quality is 0.75 times of silk, continue at 90 DEG C of insulation 35min, after filtration successively, make silk-fibroin after concentrated, dry finally.
3) adopt WR-I type to rub cotton machine described base tire is rubbed to pressure. Wherein spindle speed is 60 revs/min.
4) long silk is punctured to the vertical direction of base tire by LT-CC2 type puncture machine, make ecological cotton perianth tire after making to form cellular stereoscopic three-dimensional structure in base tire. The density that wherein punctures is controlled at 60cm2Scope in, puncture speed 50 pins/minute.
The product of the present embodiment is carried out to performance test, as follows with standard figures contrast:
Standard compression rate is greater than 30%, and actual measurement compression ratio reaches 48%;
Regain is greater than 60%, actual regain 96%;
The impure rate of standard is less than 1.4%, actual measurement percentage of impurity 0.49%;
Standard short fibre content is less than 25%, actual measurement short fibre content 12%.
Embodiment 3
A kind of ecological cotton perianth tire, adopts ecological medium staple cotton, short silk, long silk to be prepared from as raw material, and its short-and-medium silk accounts for 13% of comforter batt gross mass, and long silk accounts for 3% of comforter batt gross mass. The specification of described ecological medium staple cotton is: white cotton 228, more than horse value 4.5(85%), average length 28mm, average fracture strength 28CN/Tex, Length Regularity 83%; The specification of described short silk is: 3A20/22D, fracture strength, 3.0 grams of force per Denier, regain 10%; The specification of described long silk is: F2 × 100/120D, 150S, fracture strength 3.8 grams of force per Denier, regain 11%.
Preparation method's step of this ecological cotton perianth tire is as follows:
1) adopt the meticulous bullet machine of 6MTB220-III type respectively ecological medium staple cotton and short silk to be carried out to combing, be made into respectively netted cotton layer and netted mulberry silk layer. Wherein divide 620 revs/min of comb diameter 246mm, cylinder rotating speeds.
2) described netted cotton layer and netted mulberry silk layer are tiled and are laminated on workbench in interval in proportion, often folding after one deck, spray ecological crosslinking agent to netted cotton layer or netted mulberry silk layer surface with vaporific form, sprayed and placed the lamination that carries out next layer after 5min, wherein sprinkling amount is 5ml/m2. Finally make base tire.
The component of wherein said ecological crosslinking agent is: silk-fibroin 1wt%, tyrosine 0.5wt%, the water of ethanol 8wt% and surplus.
The preparation method of described silk-fibroin is: silk is immersed in to boiling 1h in the boiling water of its 250 times of quality, then in boiling water, add the potash that quality is 0.5 times of silk, continue at 90 DEG C of insulation 30min, after filtration successively, make silk-fibroin after concentrated, dry finally.
3) adopt WR-I type to rub cotton machine described base tire is rubbed to pressure. Wherein spindle speed is 60 revs/min.
4) long silk is punctured to the vertical direction of base tire by LT-CC2 type puncture machine, make ecological cotton perianth tire after making to form cellular stereoscopic three-dimensional structure in base tire. The density that wherein punctures is controlled at 160cm2Scope in, puncture speed 80 pins/minute.
The product of the present embodiment is carried out to performance test, as follows with standard figures contrast:
Standard compression rate is greater than 30%, and actual measurement compression ratio reaches 55%;
Regain is greater than 60%, actual regain 98%;
The impure rate of standard is less than 1.4%, actual measurement percentage of impurity 0.50%;
Standard short fibre content is less than 25%, actual measurement short fibre content 11%.
Embodiment 4
A kind of ecological cotton perianth tire, adopts ecological medium staple cotton, short silk, long silk to be prepared from as raw material, and its short-and-medium silk accounts for 12% of comforter batt gross mass, and long silk accounts for 3% of comforter batt gross mass. The specification of described ecological medium staple cotton is: white cotton 228, more than horse value 4.5(85%), average length 28mm, average fracture strength 28CN/Tex, Length Regularity 83%; The specification of described short silk is: 3A20/22D, fracture strength, 3.0 grams of force per Denier, regain 10%; The specification of described long silk is: F2 × 100/120D, 150S, fracture strength 3.8 grams of force per Denier, regain 11%.
Preparation method's step of this ecological cotton perianth tire is as follows:
1) adopt the meticulous bullet machine of 6MTB220-III type respectively ecological medium staple cotton and short silk to be carried out to combing, be made into respectively netted cotton layer and netted mulberry silk layer. Wherein divide 620 revs/min of comb diameter 246mm, cylinder rotating speeds.
2) described netted cotton layer and netted mulberry silk layer are tiled and are laminated on workbench in interval in proportion, often folding after one deck, spray ecological crosslinking agent to netted cotton layer or netted mulberry silk layer surface with vaporific form, sprayed and placed the lamination that carries out next layer after 10min, wherein sprinkling amount is 7.5ml/m2. Finally make base tire.
Wherein, the component of described ecological crosslinking agent is: silk-fibroin 1.5wt%, tyrosine 0.75wt%, ethylene glycol diglycidylether 1wt%, the water of ethanol 10wt% and surplus.
The preparation method of described silk-fibroin is: silk is immersed in to boiling 1.5h in the boiling water of its 200 times of quality, then in boiling water, add the potash that quality is 0.75 times of silk, continue at 90 DEG C of insulation 35min, after filtration successively, make silk-fibroin after concentrated, dry finally.
3) adopt WR-I type to rub cotton machine described base tire is rubbed to pressure. Wherein spindle speed is 60 revs/min.
4) long silk is punctured to the vertical direction of base tire by LT-CC2 type puncture machine, make ecological cotton perianth tire after making to form cellular stereoscopic three-dimensional structure in base tire. The density that wherein punctures is controlled at 100cm2Scope in, puncture speed 60 pins/minute.
The product of the present embodiment is carried out to performance test, as follows with standard figures contrast:
Standard compression rate is greater than 30%, and actual measurement compression ratio reaches 52%;
Regain is greater than 60%, actual regain 95%;
The impure rate of standard is less than 1.4%, actual measurement percentage of impurity 0.45%;
Standard short fibre content is less than 25%, actual measurement short fibre content 14%.
Embodiment 5
A kind of ecological cotton perianth tire, adopts ecological medium staple cotton, short silk, long silk to be prepared from as raw material, and its short-and-medium silk accounts for 13% of comforter batt gross mass, and long silk accounts for 2% of comforter batt gross mass. The specification of described ecological medium staple cotton is: white cotton 228, more than horse value 4.5(85%), average length 28mm, average fracture strength 28CN/Tex, Length Regularity 83%; The specification of described short silk is: 3A20/22D, fracture strength, 3.0 grams of force per Denier, regain 10%; The specification of described long silk is: F2 × 100/120D, 150S, fracture strength 3.8 grams of force per Denier, regain 11%.
Preparation method's step of this ecological cotton perianth tire is as follows:
1) adopt the meticulous bullet machine of 6MTB220-III type respectively ecological medium staple cotton and short silk to be carried out to combing, be made into respectively netted cotton layer and netted mulberry silk layer. Wherein divide 620 revs/min of comb diameter 246mm, cylinder rotating speeds.
2) described netted cotton layer and netted mulberry silk layer are tiled and are laminated on workbench in interval in proportion, often folding after one deck, spray ecological crosslinking agent to netted cotton layer or netted mulberry silk layer surface with vaporific form, sprayed and placed the lamination that carries out next layer after 15min, wherein sprinkling amount is 10ml/m2. Finally make base tire.
Wherein, the component of described ecological crosslinking agent is: silk-fibroin 2wt%, tyrosine 1wt%, ethylene glycol diglycidylether 1.5wt%, the water of ethanol 12wt% and surplus.
The preparation method of described silk-fibroin is: silk is immersed in to boiling 2h in the boiling water of its 300 times of quality, then in boiling water, add the potash that quality is 1 times of silk, continue at 90 DEG C of insulation 40min, after filtration successively, make silk-fibroin after concentrated, dry finally.
3) adopt WR-I type to rub cotton machine described base tire is rubbed to pressure. Wherein spindle speed is 60 revs/min.
4) long silk is punctured to the vertical direction of base tire by LT-CC2 type puncture machine, make ecological cotton perianth tire after making to form cellular stereoscopic three-dimensional structure in base tire. The density that wherein punctures is controlled in the scope of 90cm2, puncture speed 70 pins/minute.
The product of the present embodiment is carried out to performance test, as follows with standard figures contrast:
Standard compression rate is greater than 30%, and actual measurement compression ratio reaches 49%;
Regain is greater than 60%, actual regain 95%;
The impure rate of standard is less than 1.4%, actual measurement percentage of impurity 0.48%;
Standard short fibre content is less than 25%, actual measurement short fibre content 15%.
Raw materials used in the present invention, equipment, unless otherwise noted, be conventional raw material, the equipment of this area; Method therefor in the present invention, unless otherwise noted, is the conventional method of this area.
The above; it is only preferred embodiment of the present invention; not the present invention is imposed any restrictions, every any simple modification, change and equivalent transformation of above embodiment being done according to the technology of the present invention essence, all still belongs to the protection domain of technical solution of the present invention.