CN105586159A - Preparation technology of foam cleaning agent for furniture cleaning - Google Patents
Preparation technology of foam cleaning agent for furniture cleaning Download PDFInfo
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- CN105586159A CN105586159A CN201410561587.3A CN201410561587A CN105586159A CN 105586159 A CN105586159 A CN 105586159A CN 201410561587 A CN201410561587 A CN 201410561587A CN 105586159 A CN105586159 A CN 105586159A
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Abstract
The invention provides a preparation technology of a foam cleaning agent for furniture cleaning. The steps include: fully mixing a solubilizer and D-limonene evenly; putting deionized water, sodium fatty acid methyl ester sulfonate and a corrosion inhibitor into a reaction kettle, and performing stirring till complete dissolution; adding alkyl polyglycoside, triethanolamine and an antifreezing agent into a reaction kettle, and conducting stirring dispersion for 5min-8min; adding the mixed solution of D-limonene and the solubilizer, and conducting high speed dispersion for 10min; adding a bactericide and a defoaming agent, conducting dispersion for 5min to make a cleaning agent matrix; filtering the matrix with a filter net, loading the matrix into an aerosol sealing can, and conducting sealing; filling the aerosol sealing can with a propellant by a filling machine, and mounting a pump head. The foam cleaning agent prepared by the preparation technology provided by the invention has the advantages of good cleaning ability, mild performance, high safety factor, green and environmental protection, and large foaming volume, and is suitable for cleaning home and office furniture hard surfaces, can be used instantly after spraying, has no need for rinsing by clear water, can be wiped directly, and is convenient to use and carry.
Description
Technical field
The present invention relates to furniture cleaning agent field, particularly, relate to a kind of foam cleaning agent preparation technology who cleans for furniture.
Background technology
The crust spot main composition of family and office furniture has: 1. dust and other solid particle sediments. Mainly tiny dust and other solid particles showy in air. the mode by sedimentation and physical absorption is attached on body surface. In the time that body surface exists easy generation static or oily matter, the effect meeting of this absorption is stronger. 2. body metabolism product. Mainly refer to when people aprowl contacts the crusts such as furniture sweat, the grease staying and the hair coming off and epidermal tissue. 3. food. Mainly to pollute because food causes small size, as the coffee stain on desktop etc. 4. the pollutant that utensil itself produces. They are mainly by ironware, especially the aging pollutant that comes off and form of the corrosion on some utensil made of iron surfaces and utensil surface enamelled coating.
Family expenses rinse product is of a great variety, comprises the textile cleansers such as clothes, fruits and vegetables and cleaning agent for dinnerware and individual washing product etc., and its maximum feature needs water to carry out rinsing while use exactly. In the time that spot appears in the crust of family and office furniture, the cleaning method of daily family expenses is just inapplicable. If adopt similar outer surface of automobile foam cleaning technique, the effect of cleaning can change greatly. The advantage that foam cleans has: 1., because the density of foam is low, therefore water consumption is few; 2. the easy Surface Contact with being cleaned, even vertical surface; 3. due to foam dynamically earn the flight of steps leading to a palace hall, the new foam forming is constantly contacted with surperficial dirt, close with the object that reaches cleaning. But at present,, foam cleans the main professional machinery equipment that relies on, and is difficult to use in family and office.
Summary of the invention
Technical problem to be solved by this invention is to provide a kind of foam cleaning agent preparation technology who cleans for furniture, preparation foam cleaning agent gas release large, performance is gentle, spray use, without clear water rinsing, for the direct wiping of furniture item, carry with easy to use.
The present invention addresses the above problem adopted technical scheme:
The foam cleaning agent preparation technology who cleans for furniture, adopts methyl sodiosul foaliphatate, alkyl polyglycoside, triethanolamine, defoamer, corrosion inhibiter, bactericide, D-citrene, solubilizer, antifreezing agent, deionized water, propellant as raw material; Its preparation process comprises the following steps:
S1, solubilizer is fully mixed with D-citrene;
S2, start mixer, deionized water, methyl sodiosul foaliphatate and corrosion inhibiter are dropped in reactor, be stirred to completely and dissolve;
S3, under the rotating speed of 600r/min-900r/min stirs, alkyl polyglycoside, triethanolamine and antifreezing agent are joined in reactor, disperse 5min-8min;
The mixing material of S4, input D-citrene and solubilizer, high speed dispersion 10min;
S5, finally drop into bactericide and defoamer, disperse 5min, make cleaning agent base-material;
S6, cleaning agent base-material is filtered with 400 mesh filter screens after, pack in aerosol hermetically sealed can, valve and aerosol hermetically sealed can are sealed with sealing machine;
S7, in aerosol hermetically sealed can, be filled with propellant with filling machine, load onto pump head, make aerial fog type water base foam cleaning agent.
As a further improvement on the present invention, the mass percent of each raw material is: methyl sodiosul foaliphatate 2%, alkyl polyglycoside 10-14%, triethanolamine 3%, defoamer 0.02%, corrosion inhibiter 0.6%, bactericide 0.48%, D-citrene 4-5%, solubilizer 6-7%, antifreezing agent 0.5%, deionized water 58.4-62.4%, propellant 10%.
Further, described corrosion inhibiter is sodium metasilicate, and described bactericide is triclosan, and described defoamer is polyether modified silicon oil, and described propellant is liquefied petroleum gas.
Further, the mass percent of each raw material is: methyl sodiosul foaliphatate 2%, alkyl polyglycoside 12%, triethanolamine 3%, polyether modified silicon oil 0.02%, sodium metasilicate 0.6%, triclosan 0.48%, D-citrene 5%, solubilizer 6%, antifreezing agent 0.5%, deionized water 60.4%, liquefied petroleum gas 10%.
Further, the mass percent of each raw material is: methyl sodiosul foaliphatate 2%, alkyl polyglycoside 11%, triethanolamine 3%, polyether modified silicon oil 0.02%, sodium metasilicate 0.6%, triclosan 0.48%, D-citrene 4%, solubilizer 7%, antifreezing agent 0.5%, deionized water 61.4%, liquefied petroleum gas 10%.
Further, in step S3, under the rotating speed of 800r/min stirs, disperse 6min.
Further, step S4 high speed is disperseed 10min to refer under the rotating speed of 1500r/min～2000r/min stirs and is disperseed 10min.
Further, in step S4 under the rotating speed of 1000r/min stirs, high speed dispersion 10min.
The invention has the beneficial effects as follows:
To sum up, the foam cleaning agent cleansing power that adopts preparation technology of the present invention to prepare is good, and performance gentleness reaches rust-proof type second standard in JB/T4323.2-1999 " water base metal cleaning agent "; Safety coefficient is high, meets the every regulation in QB2549-2002 " security regulations of general aerosol products "; Select environmental protection raw material, production process and use are environmentally friendly, meet the requirements of HJ458-2009 " environmental labelling product technical requirement house detergent "; Employing foam cleans, and gas release is large, is applicable to the cleaning of family and office furniture crust, is specially adapted to vertical or irregular hard surface cleaning. When use, spray use, can be without clear water rinsing, directly wiping, easy to use and carry.
Detailed description of the invention
Below in conjunction with embodiment, the present invention is done to detailed description further, but embodiments of the present invention are not limited to this.
The foam cleaning agent preparation technology who cleans for furniture, it is characterized in that, adopt methyl sodiosul foaliphatate, alkyl polyglycoside, triethanolamine, defoamer, corrosion inhibiter, bactericide, D-citrene, solubilizer, antifreezing agent, deionized water, propellant as raw material; The mass percent of each raw material is: methyl sodiosul foaliphatate 2%, alkyl polyglycoside 10-14%, triethanolamine 3%, defoamer 0.02%, corrosion inhibiter 0.6%, bactericide 0.48%, D-citrene 4-5%, solubilizer 6-7%, antifreezing agent 0.5%, deionized water 58.4-62.4%, propellant 10%; Described corrosion inhibiter is sodium metasilicate, and described bactericide is triclosan, and described defoamer is polyether modified silicon oil, and described propellant is liquefied petroleum gas.
Its preparation process comprises the following steps:
S1, solubilizer is fully mixed with D-citrene;
S2, start mixer, deionized water, methyl sodiosul foaliphatate and sodium metasilicate are dropped in reactor, be stirred to completely and dissolve;
S3, under the rotating speed of 600r/min-900r/min stirs, alkyl polyglycoside, triethanolamine and antifreezing agent are joined in reactor, disperse 5min-8min;
The mixing material of S4, input D-citrene and solubilizer, high speed dispersion 10min under the rotating speed of 1500r/min～2000r/min stirs;
S5, finally drop into triclosan and polyether modified silicon oil, disperse 5min, make cleaning agent base-material;
S6, cleaning agent base-material is filtered with 400 mesh filter screens after, pack in aerosol hermetically sealed can, valve and aerosol hermetically sealed can are sealed with sealing machine;
S7, in aerosol hermetically sealed can, be filled with liquefied petroleum gas with filling machine, load onto pump head, make aerial fog type water base foam cleaning agent.
In the present embodiment, the raw material of foam cleaning agent is selected to have the following advantages:
1, adopt alkyl polyglycoside (APG), methyl sodiosul foaliphatate (MES) as surfactant.
The two is green surface-active product, nontoxic, non-stimulated, result of use is good, be easy to process and biological degradability good. APG can reduce the excitant of other anion surfactants composite with it to skin, and can play the effect of stable foam, in the situation that keeping identical foaming power, can save total dosage of surfactant. MES, as important anion surfactant, has remarkable decontamination, foaming and environmental protection performance.
2, select D-citrene as organic solvent
D-citrene is a kind of hydrocarbon solvent extracting from citrus peel. This hydrocarbon solvent has replaced the noxious materials such as dimethylbenzene, and environmental pollution is little, and security performance is good and have a good cleaning performance. D-citrene is water insoluble, need, waiting under the solubilizer effect of composition with alcohol and this dish, be dissolved in the water on a small quantity. For improving the solubility of D-citrene in water, in the present embodiment, in raw material, add appropriate solubilizer.
3, select sodium metasilicate as corrosion inhibiter
At present, domestic modal aerosol products packing jar is can, and water base series products is high to its corrosivity. In order to improve the corrosion resistance of common can, in prior art mainly by applying fine and close butyral resin on can inwall and epoxy resin improves its corrosion resistance. But due to coating processes impact, coating more or less exists sand holes, easily produce at these sand holes places and cause the spot corrosion of perforation fast. Therefore,, although coating can reduce etching extent, improve formula and add effective corrosion inhibiter being still indispensable. Inorganic silicate can effectively prevent the corrosion of the metals such as iron and steel, cast iron, lead, tin, antimony and aluminium with welding and riveting iron construction. Wherein, sodium metasilicate is one of important non-phosphor corrosion inhibitor, and it has the advantages such as effect is better, pollution-free and easy to operate, can form insoluble salt with the heavy metal ion such as calcium, magnesium, and water is played to emollescence, prevent that the soil suspension generating in cleaning process is deposited on substrate old again.
4, triclosan is as bactericide
Water-soluble triclosan, have another name called Triclosan, there is wide spectrum, efficiently, be not infected with product and without outstanding advantages such as any penetrating odors, gram-positive bacteria, Gram-negative bacteria, fungi, yeast and virus etc. are all had extensively, killed efficiently and inhibitory action, and can not react by induced hypersensitivity, without mutagenicity, without teratogenesis, non-carcinogenesis, without photosensitization and without phototoxicity, can in people's intracorporeal organ and tissue, not accumulate, can be used safely in dish washing detergent, for the foam cleaning agent that cleans furniture, human body not damaged.
5, polyether modified silicon oil is as defoamer
Polyether modified silicon oil is in the dimethicone chain of hydrophobic, to introduce hydrophilic polyether chain and a kind of novel silicon oil of obtaining. Polyethers has hydrophily, and the combination of itself and silicone oil has solved silicone oil and has been difficult to water-soluble problem, and hydrophobic dimethicone segment is given its low surface tension, the two advantage of made polyether silicone oil compatibility polyethers and dimethicone. It is low that polyether modified silicon oil has surface tension, high temperature resistant and to ph stability.
6, antifreezing agent
The use of antifreezing agent can improve the adaptability of product, guarantees can normally use under freezing point environment.
7, liquefied petroleum gas (LPG) is as propellant
In the present embodiment, employing is through the liquefied petroleum gas (LPG) of deodorization process processing as propellant, and main component is propane, normal butane and iso-butane. The advantages such as alkanes propellant uses more excellent in foam cleaning agent, and to have constant pressure, ozone depletion be zero, corrosion-free and greenhouse effects potential is low to inhalator jar.
Therefore, the foam cleaning agent cleaning for furniture prepared by the formula providing in employing the present embodiment and preparation technology, dirt-removing power is strong, foaming effect good, and little for the injury of human body, environmental protection, sprays and uses during for the cleaning of family and office furniture crust, can be without clear water rinsing, directly wiping, easy to use and carry, environmentally friendly.
Embodiment 2:
The difference of the present embodiment and embodiment 1 is, the mass percent of each raw material is: methyl sodiosul foaliphatate 2%, alkyl polyglycoside 12%, triethanolamine 3%, polyether modified silicon oil 0.02%, sodium metasilicate 0.6%, triclosan 0.48%, D-citrene 5%, solubilizer 6%, antifreezing agent 0.5%, deionized water 60.4%, liquefied petroleum gas 10%.
In step S3, under the rotating speed of 800r/min stirs, disperse 6min.
In step S4 under the rotating speed of 1000r/min stirs, high speed dispersion 10min.
Embodiment 3:
The difference of the present embodiment and embodiment 1 is, the mass percent of each raw material is: methyl sodiosul foaliphatate 2%, alkyl polyglycoside 11%, triethanolamine 3%, polyether modified silicon oil 0.02%, sodium metasilicate 0.6%, triclosan 0.48%, D-citrene 4%, solubilizer 7%, antifreezing agent 0.5%, deionized water 61.4%, liquefied petroleum gas 10%.
The foam cleaning agent that the present invention is also prepared the composition and engineering adopting in above-described embodiment is tested, and test result shows: its security has reached the index request in QB2549-2002 " security regulations of general aerosol products "; The washing oil rate of its cleaning capacity reaches more than 95%; The sterilizing rate of Escherichia coli, staphylococcus aureus, Candida albicans and salmonella was reached more than 87% in 2 minutes, within 3 minutes, reach above more than 94%, within 6 minutes, reach above 100%; Can not cause corrosion to cleaning products;
To sum up, the foam cleaning agent that adopts preparation technology of the present invention to prepare, cleansing power is good, and performance gentleness reaches rust-proof type second standard in JB/T4323.2-1999 " water base metal cleaning agent "; Safety coefficient is high, meets the every regulation in QB2549-2002 " security regulations of general aerosol products "; Select environmental protection raw material, production process and use are environmentally friendly, meet the requirements of HJ458-2009 " environmental labelling product technical requirement house detergent "; Employing foam cleans, and gas release is large, is applicable to the cleaning of family and office furniture crust, is specially adapted to vertical or irregular hard surface cleaning.
Below be only the preferred embodiment of the present invention, protection scope of the present invention is also not only confined to above-described embodiment, and all technical schemes belonging under thinking of the present invention all belong to protection scope of the present invention. It should be pointed out that for those skilled in the art, some improvements and modifications without departing from the principles of the present invention, should be considered as protection scope of the present invention.
Claims (8)
1. the foam cleaning agent preparation technology who cleans for furniture, it is characterized in that, adopt methyl sodiosul foaliphatate, alkyl polyglycoside, triethanolamine, defoamer, corrosion inhibiter, bactericide, D-citrene, solubilizer, antifreezing agent, deionized water, propellant as raw material; Its preparation process comprises the following steps:
S1, solubilizer is fully mixed with D-citrene;
S2, start mixer, deionized water, methyl sodiosul foaliphatate and corrosion inhibiter are dropped in reactor, be stirred to completely and dissolve;
S3, under the rotating speed of 600r/min-900r/min stirs, alkyl polyglycoside, triethanolamine and antifreezing agent are joined in reactor, disperse 5min-8min;
The mixing material of S4, input D-citrene and solubilizer, high speed dispersion 10min;
S5, finally drop into bactericide and defoamer, disperse 5min, make cleaning agent base-material;
S6, cleaning agent base-material is filtered with 400 mesh filter screens after, pack in aerosol hermetically sealed can, valve and aerosol hermetically sealed can are sealed with sealing machine;
S7, in aerosol hermetically sealed can, be filled with propellant with filling machine, load onto pump head, make aerial fog type water base foam cleaning agent.
2. the foam cleaning agent preparation technology who cleans for furniture according to claim 1, it is characterized in that, the mass percent of each raw material is: methyl sodiosul foaliphatate 2%, alkyl polyglycoside 10-14%, triethanolamine 3%, defoamer 0.02%, corrosion inhibiter 0.6%, bactericide 0.48%, D-citrene 4-5%, solubilizer 6-7%, antifreezing agent 0.5%, deionized water 58.4-62.4%, propellant 10%.
3. the foam cleaning agent preparation technology who cleans for furniture according to claim 2, is characterized in that, described corrosion inhibiter is sodium metasilicate, and described bactericide is triclosan, and described defoamer is polyether modified silicon oil, and described propellant is liquefied petroleum gas.
4. the foam cleaning agent preparation technology who cleans for furniture according to claim 3, it is characterized in that, the mass percent of each raw material is: methyl sodiosul foaliphatate 2%, alkyl polyglycoside 12%, triethanolamine 3%, polyether modified silicon oil 0.02%, sodium metasilicate 0.6%, triclosan 0.48%, D-citrene 5%, solubilizer 6%, antifreezing agent 0.5%, deionized water 60.4%, liquefied petroleum gas 10%.
5. the foam cleaning agent preparation technology who cleans for furniture according to claim 3, it is characterized in that, the mass percent of each raw material is: methyl sodiosul foaliphatate 2%, alkyl polyglycoside 11%, triethanolamine 3%, polyether modified silicon oil 0.02%, sodium metasilicate 0.6%, triclosan 0.48%, D-citrene 4%, solubilizer 7%, antifreezing agent 0.5%, deionized water 61.4%, liquefied petroleum gas 10%.
6. according to the arbitrary described foam cleaning agent preparation technology who cleans for furniture of claim 1 to 5, it is characterized in that, in step S3, under the rotating speed of 800r/min stirs, disperse 6min.
7. according to the arbitrary described foam cleaning agent preparation technology who cleans for furniture of claim 1 to 5, it is characterized in that, step S4 high speed is disperseed 10min to refer under the rotating speed of 1500r/min～2000r/min stirs and is disperseed 10min.
8. the foam cleaning agent preparation technology who cleans for furniture according to claim 7, is characterized in that, in step S4 under the rotating speed of 1000r/min stirs, high speed dispersion 10min.
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| CN201410561587.3A CN105586159A (en) | 2014-10-21 | 2014-10-21 | Preparation technology of foam cleaning agent for furniture cleaning |
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| CN201410561587.3A CN105586159A (en) | 2014-10-21 | 2014-10-21 | Preparation technology of foam cleaning agent for furniture cleaning |
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Cited By (7)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN106011864A (en) * | 2016-06-16 | 2016-10-12 | 深圳市彩虹精细化工股份有限公司 | Aerosol type metal decontaminating polishing agent and preparation method thereof |
| CN106497696A (en) * | 2016-10-07 | 2017-03-15 | 常州创索新材料科技有限公司 | The preparation method of shield agent washed by a kind of safety furniture |
| CN109705995A (en) * | 2018-12-25 | 2019-05-03 | 常州中天气雾制品有限公司 | A kind of cleaning agent of low toxic and environment-friendly |
| CN109821047A (en) * | 2019-01-24 | 2019-05-31 | 四川旅发环保科技有限公司 | A kind of antifreeze foam solution |
| CN111592940A (en) * | 2020-05-21 | 2020-08-28 | 上海毅诺生物科技有限公司 | Multi-surface cleaning agent containing sodium cumene sulfonate compounded hydrotrope and preparation method thereof |
| CN112375632A (en) * | 2020-11-17 | 2021-02-19 | 浙江绿岛科技有限公司 | Environment-friendly bio-based cleaning aerosol and preparation method thereof |
| US11773293B2 (en) | 2017-11-15 | 2023-10-03 | S. C. Johnson & Son, Inc. | Freeze-thaw stable water-in-oil emulsion cleaner and/or polish compositions |
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2014
- 2014-10-21 CN CN201410561587.3A patent/CN105586159A/en active Pending
Cited By (10)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN106011864A (en) * | 2016-06-16 | 2016-10-12 | 深圳市彩虹精细化工股份有限公司 | Aerosol type metal decontaminating polishing agent and preparation method thereof |
| CN106011864B (en) * | 2016-06-16 | 2019-10-08 | 深圳市兆新能源股份有限公司 | Aerial fog type metal decontamination polisher and preparation method thereof |
| CN106497696A (en) * | 2016-10-07 | 2017-03-15 | 常州创索新材料科技有限公司 | The preparation method of shield agent washed by a kind of safety furniture |
| US11773293B2 (en) | 2017-11-15 | 2023-10-03 | S. C. Johnson & Son, Inc. | Freeze-thaw stable water-in-oil emulsion cleaner and/or polish compositions |
| CN109705995A (en) * | 2018-12-25 | 2019-05-03 | 常州中天气雾制品有限公司 | A kind of cleaning agent of low toxic and environment-friendly |
| CN109705995B (en) * | 2018-12-25 | 2021-03-23 | 常州中天气雾制品有限公司 | Low-toxicity cleaning agent |
| CN109821047A (en) * | 2019-01-24 | 2019-05-31 | 四川旅发环保科技有限公司 | A kind of antifreeze foam solution |
| CN111592940A (en) * | 2020-05-21 | 2020-08-28 | 上海毅诺生物科技有限公司 | Multi-surface cleaning agent containing sodium cumene sulfonate compounded hydrotrope and preparation method thereof |
| CN111592940B (en) * | 2020-05-21 | 2021-08-13 | 上海毅诺生物科技有限公司 | Multi-surface cleaning agent containing sodium cumene sulfonate compounded hydrotrope and preparation method thereof |
| CN112375632A (en) * | 2020-11-17 | 2021-02-19 | 浙江绿岛科技有限公司 | Environment-friendly bio-based cleaning aerosol and preparation method thereof |
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