CN105566998B - A kind of environment-friendlyink ink cleaning agent and preparation method thereof - Google Patents
A kind of environment-friendlyink ink cleaning agent and preparation method thereof Download PDFInfo
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- CN105566998B CN105566998B CN201610100104.9A CN201610100104A CN105566998B CN 105566998 B CN105566998 B CN 105566998B CN 201610100104 A CN201610100104 A CN 201610100104A CN 105566998 B CN105566998 B CN 105566998B
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- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09D—COATING COMPOSITIONS, e.g. PAINTS, VARNISHES OR LACQUERS; FILLING PASTES; CHEMICAL PAINT OR INK REMOVERS; INKS; CORRECTING FLUIDS; WOODSTAINS; PASTES OR SOLIDS FOR COLOURING OR PRINTING; USE OF MATERIALS THEREFOR
- C09D9/00—Chemical paint or ink removers
- C09D9/04—Chemical paint or ink removers with surface-active agents
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- General Chemical & Material Sciences (AREA)
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- Materials Engineering (AREA)
- Wood Science & Technology (AREA)
- Organic Chemistry (AREA)
- Detergent Compositions (AREA)
Abstract
The invention discloses a kind of environment-friendlyink ink cleaning agents and preparation method thereof, it is prepared by sodium bicarbonate, ethyl alcohol, glycine betaine, natural graphite, sodium oxalate, titanium dioxide, oleic acid, polyoxyethylene ether, water, triethanolamine oleate and ricinoleic acid polyester, sodium bicarbonate, natural graphite, sodium oxalate, titanium dioxide are added in container respectively, water is added, is uniformly mixed；Glycine betaine, oleic acid, polyoxyethylene ether, triethanolamine oleate, ricinoleic acid polyester are added separately in container, are sufficiently stirred, is uniformly mixed；Remaining water and ethyl alcohol is added, stirs evenly, is cooled to room temperature, stands.Detergent for ink reasonable composition of the present invention can clean the oil components in dissolution ink very well, and cleaning effect is good, and volatilization is fast, dosage is few, and not easy to blast, pollution-free, safety and environmental protection is at low cost.
Description
Technical field
The present invention relates to cleaning agent field, specifically a kind of environment-friendlyink ink cleaning agent and preparation method thereof.
Background technique
Influence of the ink detergent to printing is increasing, many quality problems occurred in printing, and the origin cause of formation is often straight
It connects or indirectly from ink detergent.Such as rubber roller band water or with performance of ink, lower, glue roller deflection, field density are insufficient, flat
Net floating etc. is, to influence printing quality, to make to print since the improper use of detergent causes rubber roller to go wrong mostly
Downtime increases.The impurity composition on printing rubber roll surface, that is, ink detergent need clean object.Detergent for ink
Ink for cleaning on printing plate, ink roller, metallic roll and blanket, by industrial washing oil, nonionic surfactant, organic acid,
Organic amine and water are mixed by certain technique, are emulsified, have small toxicity, corrosion-free, strong detergency, good fluidity,
The advantages that never degenerating, be highly-safe, cleaning speed is fast.
But existing detergent for ink have the shortcomings that one it is apparent, the content of organic solvent is very high, in machine room
In volatile quantity it is very serious, the health of printing environment and worker are seriously affected, cost is also high.
Summary of the invention
The purpose of the present invention is to provide a kind of environment-friendlyink ink cleaning agents and preparation method thereof, to solve above-mentioned background skill
The problem of being proposed in art.
To achieve the above object, the present invention provides the following technical solutions：
A kind of environment-friendlyink ink cleaning agent, is prepared by the raw material of following parts by weight：8~10 parts of sodium bicarbonate, ethyl alcohol
20~24 parts, 11~13 parts of glycine betaine, 6~8 parts of natural graphite, 20~24 parts of sodium oxalate, 18~22 parts of titanium dioxide, oleic acid 15~
17 parts, 13~15 parts of polyoxyethylene ether, 80~100 parts of water, 11~13 parts of triethanolamine oleate, ricinoleic acid polyester 9~11
Part.
A kind of preparation method of the environment-friendlyink ink cleaning agent, specific preparation process is as follows：
(1) sodium bicarbonate, natural graphite, sodium oxalate, titanium dioxide are added in container respectively, are added 50~70 parts
Water is uniformly mixed；
(2) glycine betaine, oleic acid, polyoxyethylene ether, triethanolamine oleate, ricinoleic acid polyester are added separately to container
In, 6~8h is stirred under the conditions of 55~65 DEG C, is sufficiently mixed uniformly；
(3) at a temperature of 63~67 DEG C, ethyl alcohol and remaining water are added in the mixed liquor in step (2), stirring 30~
40min is cooled to room temperature, and stands 12~16h.
Compared with prior art, the beneficial effects of the invention are as follows：Detergent for ink reasonable composition of the present invention, can be clear very well
The oil components in dissolution ink are washed, cleaning effect is good, and volatilization is fast, dosage is few, not easy to blast, pollution-free, safety and environmental protection, cost
It is low.
Specific embodiment
Below in conjunction with the embodiment of the present invention, technical scheme in the embodiment of the invention is clearly and completely described,
Obviously, described embodiments are only a part of the embodiments of the present invention, instead of all the embodiments.Based in the present invention
Embodiment, every other embodiment obtained by those of ordinary skill in the art without making creative efforts, all
Belong to the scope of protection of the invention.
Embodiment 1
Environment-friendlyink ink cleaning agent is prepared by the raw material of following parts by weight：8 parts of sodium bicarbonate, 24 parts of ethyl alcohol, beet
11 parts of alkali, 8 parts of natural graphite, 20 parts of sodium oxalate, 22 parts of titanium dioxide, 15 parts of oleic acid, 15 parts of polyoxyethylene ether, 80 parts of water, oleic acid
13 parts of triethanolamine soap, 9 parts of ricinoleic acid polyester.
In above-described embodiment, the preparation step of environment-friendlyink ink cleaning agent is as follows：
(1) sodium bicarbonate, natural graphite, sodium oxalate, titanium dioxide are added in container respectively, 50 parts of water is added, mixed
It closes uniform；
(2) glycine betaine, oleic acid, polyoxyethylene ether, triethanolamine oleate, ricinoleic acid polyester are added separately to container
In, 8h is stirred under the conditions of 55 DEG C, is sufficiently mixed uniformly；
(3) at a temperature of 63 DEG C, ethyl alcohol and remaining water are added in the mixed liquor in step (2), stir 40min, it is cold
But to room temperature, 16h is stood.
Embodiment 2
Environment-friendlyink ink cleaning agent is prepared by the raw material of following parts by weight：9 parts of sodium bicarbonate, 22 parts of ethyl alcohol, beet
12 parts of alkali, 7 parts of natural graphite, 22 parts of sodium oxalate, 20 parts of titanium dioxide, 16 parts of oleic acid, 14 parts of polyoxyethylene ether, 90 parts of water, oleic acid
12 parts of triethanolamine soap, 10 parts of ricinoleic acid polyester.
In above-described embodiment, the preparation step of environment-friendlyink ink cleaning agent is as follows：
(1) sodium bicarbonate, natural graphite, sodium oxalate, titanium dioxide are added in container respectively, 60 parts of water is added, mixed
It closes uniform；
(2) glycine betaine, oleic acid, polyoxyethylene ether, triethanolamine oleate, ricinoleic acid polyester are added separately to container
In, 7h is stirred under the conditions of 60 DEG C, is sufficiently mixed uniformly；
(3) at a temperature of 65 DEG C, ethyl alcohol and remaining water are added in the mixed liquor in step (2), stir 35min, it is cold
But to room temperature, 14h is stood.
Embodiment 3
Environment-friendlyink ink cleaning agent is prepared by the raw material of following parts by weight：10 parts of sodium bicarbonate, 20 parts of ethyl alcohol, sweet tea
13 parts of dish alkali, 6 parts of natural graphite, 24 parts of sodium oxalate, 18 parts of titanium dioxide, 17 parts of oleic acid, 13 parts of polyoxyethylene ether, 100 parts of water, oil
11 parts of triethylenetetraminehexaacetic acid hydramine soap, 11 parts of ricinoleic acid polyester.
In above-described embodiment, the preparation step of environment-friendlyink ink cleaning agent is as follows：
(1) sodium bicarbonate, natural graphite, sodium oxalate, titanium dioxide are added in container respectively, 70 parts of water is added, mixed
It closes uniform；
(2) glycine betaine, oleic acid, polyoxyethylene ether, triethanolamine oleate, ricinoleic acid polyester are added separately to container
In, 6h is stirred under the conditions of 65 DEG C, is sufficiently mixed uniformly；
(3) at a temperature of 67 DEG C, ethyl alcohol and remaining water are added in the mixed liquor in step (2), stir 30min, it is cold
But to room temperature, 12h is stood.
To the detergent for ink and 10% sodium hydroxide solution (comparative test 1), in the market of above-described embodiment 1-3 preparation
Existing organic base moves back film liquid (comparative test 2) and carries out following test:
1) it is tested using the PCB (PCB surface is covered with solder mask) for being printed with ink, 45 DEG C of test temperature, detection
After surface ink completely cleaned time, cleaning after ink residual condition, cleaning solder mask corrosion condition.
Ink residual condition is observed with Lycra DM2700M microscope after cleaning；The corrosion feelings of solder mask after cleaning
Condition uses visual observations.
2) using the erosion copper rate covered in copper PCB test cleaning process, testing time 2min.
Test result is as shown in table 1
Table 1
It is obvious to a person skilled in the art that invention is not limited to the details of the above exemplary embodiments, Er Qie
In the case where without departing substantially from spirit or essential attributes of the invention, the present invention can be realized in other specific forms.Therefore, no matter
From the point of view of which point, the present embodiments are to be considered as illustrative and not restrictive, and the scope of the present invention is by appended power
Benefit requires rather than above description limits, it is intended that all by what is fallen within the meaning and scope of the equivalent elements of the claims
Variation is included within the present invention.
Claims (2)
1. a kind of environment-friendlyink ink cleaning agent, which is characterized in that be prepared by the raw material of following parts by weight：Sodium bicarbonate 8~
10 parts, 20~24 parts of ethyl alcohol, 11~13 parts of glycine betaine, 6~8 parts of natural graphite, 20~24 parts of sodium oxalate, titanium dioxide 18~22
Part, 15~17 parts of oleic acid, 13~15 parts of polyoxyethylene ether, 80~100 parts of water, 11~13 parts of triethanolamine oleate, castor oil
9~11 parts of acid polyester.
2. a kind of preparation method of environment-friendlyink ink cleaning agent as described in claim 1, which is characterized in that specific preparation step
It is as follows：
（1）Sodium bicarbonate, natural graphite, sodium oxalate, titanium dioxide are added in container respectively, 50~70 parts of water is added, is mixed
It closes uniform；
（2）Glycine betaine, oleic acid, polyoxyethylene ether, triethanolamine oleate, ricinoleic acid polyester are added separately in container,
6~8h is stirred under the conditions of 55~65 DEG C, is sufficiently mixed uniformly；
（3）At a temperature of 63~67 DEG C, step is added in ethyl alcohol and remaining water（2）In mixed liquor in, stirring 30~
40min is cooled to room temperature, and stands 12~16h.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201610100104.9A CN105566998B (en) | 2016-02-24 | 2016-02-24 | A kind of environment-friendlyink ink cleaning agent and preparation method thereof |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201610100104.9A CN105566998B (en) | 2016-02-24 | 2016-02-24 | A kind of environment-friendlyink ink cleaning agent and preparation method thereof |
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| Publication Number | Publication Date |
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| CN105566998A CN105566998A (en) | 2016-05-11 |
| CN105566998B true CN105566998B (en) | 2018-11-27 |
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| CN110813098B (en) * | 2019-11-18 | 2022-03-08 | 上海安赐环保科技股份有限公司 | Sulfuric acid method titanium dioxide production method and cleaning method of membrane equipment |
Citations (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN102775840A (en) * | 2012-08-11 | 2012-11-14 | 福建鸿博印刷股份有限公司 | Printing ink cleaning agent and preparation process thereof |
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Patent Citations (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN102775840A (en) * | 2012-08-11 | 2012-11-14 | 福建鸿博印刷股份有限公司 | Printing ink cleaning agent and preparation process thereof |
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| Date | Code | Title | Description |
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| C06 | Publication | ||
| PB01 | Publication | ||
| C10 | Entry into substantive examination | ||
| SE01 | Entry into force of request for substantive examination | ||
| TA01 | Transfer of patent application right |
Effective date of registration: 20181008 Address after: 322000 Dongyuan characteristic industrial park, Jiangdong Street, Yiwu, Jinhua, Zhejiang Applicant after: ZHEJIANG ZHENGDA SHUMEIJIA INDUSTRY AND TRADE CO., LTD. Address before: 322000 10 groups of Liu Er Cun, Beiyuan street, Yiwu, Jinhua, Zhejiang Applicant before: Yang Xiaoting |
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| TA01 | Transfer of patent application right | ||
| GR01 | Patent grant | ||
| GR01 | Patent grant | ||
| CP03 | Change of name, title or address |
Address after: 322000 No. 35 Dongshan Road, Jiangdong Street, Yiwu City, Zhejiang Province Patentee after: Zhejiang Yiwu Shumeijia Science and Technology Co., Ltd. Address before: 322000 Dongyuan characteristic industrial park, Jiangdong Street, Yiwu, Jinhua, Zhejiang Patentee before: ZHEJIANG ZHENGDA SHUMEIJIA INDUSTRY AND TRADE CO., LTD. |
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| CP03 | Change of name, title or address |