CN105542545A - Preparation method for anti-bacterial energy-storage self-adjusting heat-insulating putty - Google Patents

Preparation method for anti-bacterial energy-storage self-adjusting heat-insulating putty Download PDF

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Publication number
CN105542545A
CN105542545A CN201610063161.4A CN201610063161A CN105542545A CN 105542545 A CN105542545 A CN 105542545A CN 201610063161 A CN201610063161 A CN 201610063161A CN 105542545 A CN105542545 A CN 105542545A
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temperature
putty
heat
insulating
preparation
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陈明生
林大伟
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JIANGSU SHIKONG PAINT CO Ltd
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JIANGSU SHIKONG PAINT CO Ltd
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    • C—CHEMISTRY; METALLURGY
    • C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
    • C09D—COATING COMPOSITIONS, e.g. PAINTS, VARNISHES OR LACQUERS; FILLING PASTES; CHEMICAL PAINT OR INK REMOVERS; INKS; CORRECTING FLUIDS; WOODSTAINS; PASTES OR SOLIDS FOR COLOURING OR PRINTING; USE OF MATERIALS THEREFOR
    • C09D5/00—Coating compositions, e.g. paints, varnishes or lacquers, characterised by their physical nature or the effects produced; Filling pastes
    • C09D5/34—Filling pastes

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  • Chemical & Material Sciences (AREA)
  • Life Sciences & Earth Sciences (AREA)
  • Engineering & Computer Science (AREA)
  • Materials Engineering (AREA)
  • Wood Science & Technology (AREA)
  • Organic Chemistry (AREA)
  • Sealing Material Composition (AREA)
  • Paints Or Removers (AREA)

Abstract

The invention relates to a preparation method for anti-bacterial energy-storage self-adjusting heat-insulating putty, and belongs to the field of putty preparation. According to the method, the anti-bacterial energy-storage self-adjusting heat-insulating putty is prepared with the assistance of an anion antibacterial agent by taking an elastic emulsion as a film forming matter, taking shale ceramic powder as heat-insulating filler and taking a phase-change material as energy-storage temperature-adjusting filler; the defects that a conventional heat-insulating layer cracks easily and is poor in stability are overcome; temperature can be adjusted freely by the addition of the phase-change material, so that a stable heat insulating effect is achieved; the anion antibacterial agent can release anions to air for a long time so as to eliminate dust and toxic and harmful gas in the air, inhibit the growth of bacteria and mould, and purify the air; therefore, the anti-bacterial energy-storage self-adjusting heat-insulating putty is an environment-friendly and high-efficiency heat-insulating material.

Description

A kind of preparation method of antibacterial energy storage inherent regulation heat preservation putty
Technical field
The present invention relates to a kind of preparation method of antibacterial energy storage inherent regulation heat preservation putty, belong to putty preparation field.
Background technology
Putty is the one decoration gel material of smooth surface of wall, and being a kind of thick slurry coating material, is that coating whitewashes front requisite a kind of product; The object of brushing putty is fill the hole of construction surface and correct the curve deviation of construction surface; lay a solid foundation for obtaining level and smooth, uniform lacquer painting; so; putty should have good cementability and water tolerance; there will not be the phenomenons such as peeling, hollowing and cracking to occur under the long-term corrosion ensureing water vapour in atmosphere, play decoration and provide protection.
Traditional External Thermal Insulation Technology for External is primarily of thermal insulation layer and finish coat two parts composition, and its System structure is: adhesive mortar+styrofoam/polyphenyl particle heat-insulating mortar+plastering mortar coordinates glass fiber reticular cloth+putty layer+veneer coating layer.As everyone knows, when heat-insulation system is by sun direct projection, because polyphenylene heat insulation slab thermal resistance is very large, the heat in protective layer (plastering mortar layer) and facing coating can be made to be difficult to be spread by thermal conduction, and its surface temperature can reach 60 ~ 80 DEG C in summer.In case of suddenly rained cats and dogs, temperature sharply declines, temperature variation can reach more than 30 ~ 50 DEG C, the stress produced by the temperature difference very easily causes protective layer and finish coat to produce crack, and protective layer and finish coat temperature too high, styrofoam can be made to produce irreversible thermal contraction distortion, also can cause the serious cracking of protective layer and finish coat.Once crack of surface layer, will not have waterproof action, rainwater or steam will enter thermal insulation layer and bonded sand pulp layer along crack, cause adhering heat insulating plate strength degradation, time serious, generation systems comes off.
The harmful minimum gas discharged in constructional ornamental material and furniture, the peculiar smell etc. produced as formaldehyde, ammonia, benzene and human body swims in the air, its occurrence status and form are complicated and diversified, what have exists with free gas molecule form, have by a large amount of positive charges absorption floating in air, surround and form positive ion, some minimum gas molecules deposit on already present particle surface, are condensed into aerosol system etc.Just because of above positive ion or aerocolloidal existence, cause the indoor serious air of new finishing without dye, great harm is caused to HUMAN HEALTH.
Summary of the invention
The technical problem that the present invention mainly solves: be made up of thermal insulation layer and finish coat two portions for current conventional outer wall heat preservation technology, it is many to there is seam in this heat insulation system, material internal stress is large, poor dimensional stability, the defects such as the deflection that thermal stresses causes is large, very easily cause thermal insulation dehiscence, then cause protective layer and occur crackle, and cause the deficiency of insulation failure, provide a kind of antibacterial energy storage inherent regulation heat preservation putty, utilize the cohesive strength that putty is suitable, excellent anti-cracking performance, water tolerance, permeability resistance and permeability reduce the generation that temperature becomes crack, and improve indoor thermal environment.The method take elastic emulsion as film forming matter, with shale pottery powder for insulation filler, take phase change material as energy storage temperature adjustment filler, be aided with negative ion antibiotic agent and obtain a kind of antibacterial energy storage inherent regulation heat preservation putty, both solved conventional vacuum layer easily to ftracture, the defect of poor stability, and adding of phase change material freely can carry out temperature adjustment, play stable heat insulation effect, negative ion antibiotic agent can for a long time to anion releasing in air, remove the dust in air and toxic and harmful, the growth of anti-bacteria and mould, purify air, it is a kind of lagging material of environment-friendly high-efficiency.
In order to solve the problems of the technologies described above, the technical solution adopted in the present invention is:
(1) 500 ~ 600mL deionized water, 8 ~ 10g stearoyl lactate, 20 ~ 30g nano grade silica particles are loaded in there-necked flask together with 40 ~ 50g vinylformic acid, stir 10 ~ 15min with glass stick and obtain monomer pre-emulsion;
(2) in the there-necked flask that constant pressure funnel, agitator are housed, 300 ~ 400mL deionized water and 10 ~ 12g sodium bicarbonate is added successively, startup agitator is stirred to sodium bicarbonate and dissolves completely, move into water-bath and be warming up to 70 ~ 80 DEG C, in flask, the above-mentioned obtained pre-emulsion of 200 ~ 300mL is dropwise dripped again by dropping funnel, control rate of addition to dropwise in 2 ~ 3h, after insulation 1 ~ 2h, filter, obtain ACRYLIC EMULSION;
(3) 1 ~ 2kg shale raw material are taken, put into after micronizer mill pulverizes 20 ~ 30min and again fragment is loaded ball mill, be that 4:1 adds wolfram varbide ball milling pearl inwards by ratio of grinding media to material, 100 mesh standard sieves are crossed after ball milling 1 ~ 2h, the slate flour obtained is put into retort furnace and calcine 1 ~ 2h at 400 ~ 500 DEG C, obtained shale pottery powder;
(4) by 1 ~ 2L mass concentration be 10% caustic soda soln join in reactor, be heated to 80 ~ 100 DEG C, 100 ~ 200g stearic acid is added until after its thawing, add 200 ~ 400mL distilled water, continue to be warming up to 100 ~ 120 DEG C and make it seethe with excitement under whipped state;
(5) in the reactor of boiling, 200 ~ 300g paraffin is continued to add to after dissolving completely, add the boiling water that 100 ~ 200mL temperature is 98 ~ 100 DEG C again, after stirring, after above-mentioned for 250 ~ 350g obtained shale pottery powder is slowly added, insulated and stirred 1 ~ 2h at the temperature of 75 ~ 85 DEG C, pulverize after Temperature fall, obtained temperature adjustment phase transformation filler, for subsequent use;
(6) 30 ~ 50g Natvosol is joined in 200 ~ 300mL distilled water, be poured in kneader after even with ultrasonic disperse instrument ultrasonic disperse under the power of 100 ~ 200W, the above-mentioned obtained ACRYLIC EMULSION of 300 ~ 400mL, 40 ~ 50g temperature adjustment phase transformation filler, 1 ~ 2g microcrystalline wax and 10 ~ 15g antiseptic-germicide is added under the whipped state of kneader, after stirring kneading 30 ~ 50min, make homogeneous paste, discharging, obtains a kind of antibacterial energy storage inherent regulation heat preservation putty.
Described antiseptic-germicide is the antibacterial system of negative ion powder, is in mass ratio for 20:11:17 mixes obtained by tourmaline powder, cerium oxide and titanium dioxide.
Heat preservation principle of the present invention is: utilize putty layer absorption solar radiant heat and convection of air to conduct heat and temperature rising, when reaching the fusing point of energy storage phase change material, phase change material undergoes phase transition, liquid state is become from solid-state, simultaneously stability heat energy is also stored up, thus control lift velocity and the maximum temperature value of metope temperature, reduce the heat of internally body of wall transmission, when temperature reduces, the temperature of putty layer declines thereupon, when temperature drops to the transformation temperature of phase change material, it produces reverse transformation, be solid-state by liquid state, and by the heat release of storage out, thus slow down the lowering speed of putty layer temperature, and final peak valley temperature slightly improves than control sample, reduce height, Low Temperature Difference, prevent or alleviate thermal insulation layer and become crack because temperature becomes the temperature that too fast or excessive temperature differentials causes, phase change material plays the effect of " peak load shifting " in the temperature change process of bouncing putty.
Embody rule method of the present invention: putty powder the present invention obtained and water are by volume for 2:1 mixes, leave standstill 10 ~ 20min after stirring again to stir, it being draped over one's shoulders uniformly with steel scraper plate or spatula scrapes on wall, repeatedly drape over one's shoulders after scraping 2 ~ 3 times, spend the night and dry, draping over one's shoulders and scraping thickness is 0.8 ~ 1.5cm, and putty consumption is 1 ~ 1.5kg/m 2.
The invention has the beneficial effects as follows: the invention solves that conventional vacuum layer easily ftractures, the defect of poor stability, and adding of phase change material freely can carry out temperature adjustment, play stable heat insulation effect, negative ion antibiotic agent can for a long time to anion releasing in air, remove dust in air and toxic and harmful, anti-bacteria and mould growth, purify air, be a kind of lagging material of environment-friendly high-efficiency.
Embodiment
500 ~ 600mL deionized water, 8 ~ 10g stearoyl lactate, 20 ~ 30g nano grade silica particles are loaded in there-necked flask together with 40 ~ 50g vinylformic acid, stirs 10 ~ 15min with glass stick and obtain monomer pre-emulsion; 300 ~ 400mL deionized water and 10 ~ 12g sodium bicarbonate is added successively in the there-necked flask that constant pressure funnel, agitator are housed, startup agitator is stirred to sodium bicarbonate and dissolves completely, move into water-bath and be warming up to 70 ~ 80 DEG C, in flask, the above-mentioned obtained pre-emulsion of 200 ~ 300mL is dropwise dripped again by dropping funnel, control rate of addition to dropwise in 2 ~ 3h, after insulation 1 ~ 2h, filter, obtain ACRYLIC EMULSION; Take 1 ~ 2kg shale raw material, put into after micronizer mill pulverizes 20 ~ 30min and again fragment is loaded ball mill, be that 4:1 adds wolfram varbide ball milling pearl inwards by ratio of grinding media to material, 100 mesh standard sieves are crossed after ball milling 1 ~ 2h, the slate flour obtained is put into retort furnace and calcine 1 ~ 2h at 400 ~ 500 DEG C, obtained shale pottery powder; By 1 ~ 2L mass concentration be 10% caustic soda soln join in reactor, be heated to 80 ~ 100 DEG C, 100 ~ 200g stearic acid is added until after its thawing, add 200 ~ 400mL distilled water, continue to be warming up to 100 ~ 120 DEG C and make it seethe with excitement under whipped state; In the reactor of boiling, continue to add 200 ~ 300g paraffin to after dissolving completely, add the boiling water that 100 ~ 200mL temperature is 98 ~ 100 DEG C again, after stirring, after above-mentioned for 250 ~ 350g obtained shale pottery powder is slowly added, insulated and stirred 1 ~ 2h at the temperature of 75 ~ 85 DEG C, pulverize after Temperature fall, obtained temperature adjustment phase transformation filler, for subsequent use; 30 ~ 50g Natvosol is joined in 200 ~ 300mL distilled water, be poured in kneader after even with ultrasonic disperse instrument ultrasonic disperse under the power of 100 ~ 200W, the above-mentioned obtained ACRYLIC EMULSION of 300 ~ 400mL, 40 ~ 50g temperature adjustment phase transformation filler, 1 ~ 2g microcrystalline wax and 10 ~ 15g antiseptic-germicide is added under the whipped state of kneader, after stirring kneading 30 ~ 50min, make homogeneous paste, discharging, obtains a kind of antibacterial energy storage inherent regulation heat preservation putty.
Described antiseptic-germicide is the antibacterial system of negative ion powder, is in mass ratio for 20:11:17 mixes obtained by tourmaline powder, cerium oxide and titanium dioxide.
Example 1
500mL deionized water, 8g stearoyl lactate, 20g nano grade silica particles are loaded in there-necked flask together with 40g vinylformic acid, stirs 10min with glass stick and obtain monomer pre-emulsion; 300mL deionized water and 10g sodium bicarbonate is added successively in the there-necked flask that constant pressure funnel, agitator are housed, startup agitator is stirred to sodium bicarbonate and dissolves completely, move into water-bath and be warming up to 70 DEG C, in flask, the above-mentioned obtained pre-emulsion of 200mL is dropwise dripped again by dropping funnel, control rate of addition to dropwise in 2h, after insulation 1h, filter, obtain ACRYLIC EMULSION; Take 1kg shale raw material, put into after micronizer mill pulverizes 20min and again fragment is loaded ball mill, be that 4:1 adds wolfram varbide ball milling pearl inwards by ratio of grinding media to material, after ball milling 1h, cross 100 mesh standard sieves, the slate flour obtained is put into retort furnace at 400 DEG C, calcines 1h, obtained shale pottery powder; By 1L mass concentration be 10% caustic soda soln join in reactor, be heated to 80 DEG C, under whipped state, add 100g stearic acid until its melt after, add 200mL distilled water, continue to be warming up to 100 DEG C and make it seethe with excitement; In the reactor of boiling, continue to add 200g paraffin to after dissolving completely, add the boiling water that 100mL temperature is 98 DEG C again, after stirring, after above-mentioned for 250g obtained shale pottery powder is slowly added, insulated and stirred 1h at the temperature of 75 DEG C, pulverize after Temperature fall, obtained temperature adjustment phase transformation filler, for subsequent use; 30g Natvosol is joined in 200mL distilled water, be poured in kneader after even with ultrasonic disperse instrument ultrasonic disperse under the power of 100W, the above-mentioned obtained ACRYLIC EMULSION of 300mL, 40g temperature adjustment phase transformation filler, 1g microcrystalline wax and 10g antiseptic-germicide is added under the whipped state of kneader, stir after mediating 30min, make homogeneous paste, discharging, obtains a kind of antibacterial energy storage inherent regulation heat preservation putty.
Described antiseptic-germicide is the antibacterial system of negative ion powder, is in mass ratio for 20:11:17 mixes obtained by tourmaline powder, cerium oxide and titanium dioxide.
Embody rule method of the present invention: putty powder the present invention obtained and water are by volume for 2:1 mixes, leave standstill 10min after stirring again to stir, it being draped over one's shoulders uniformly with steel scraper plate or spatula scrapes on wall, repeatedly drape over one's shoulders after scraping 2 times, spend the night and dry, draping over one's shoulders and scraping thickness is 0.8cm, and putty consumption is 1kg/m 2.
Example 2
550mL deionized water, 9g stearoyl lactate, 25g nano grade silica particles are loaded in there-necked flask together with 45g vinylformic acid, stirs 13min with glass stick and obtain monomer pre-emulsion; 350mL deionized water and 11g sodium bicarbonate is added successively in the there-necked flask that constant pressure funnel, agitator are housed, startup agitator is stirred to sodium bicarbonate and dissolves completely, move into water-bath and be warming up to 75 DEG C, in flask, the above-mentioned obtained pre-emulsion of 250mL is dropwise dripped again by dropping funnel, control rate of addition to dropwise in 2h, after insulation 1h, filter, obtain ACRYLIC EMULSION; Take 1kg shale raw material, put into after micronizer mill pulverizes 25min and again fragment is loaded ball mill, be that 4:1 adds wolfram varbide ball milling pearl inwards by ratio of grinding media to material, after ball milling 2h, cross 100 mesh standard sieves, the slate flour obtained is put into retort furnace at 450 DEG C, calcines 2h, obtained shale pottery powder; By 2L mass concentration be 10% caustic soda soln join in reactor, be heated to 90 DEG C, under whipped state, add 150g stearic acid until its melt after, add 300mL distilled water, continue to be warming up to 110 DEG C and make it seethe with excitement; In the reactor of boiling, continue to add 250g paraffin to after dissolving completely, add the boiling water that 150mL temperature is 99 DEG C again, after stirring, after above-mentioned for 300g obtained shale pottery powder is slowly added, insulated and stirred 2h at the temperature of 80 DEG C, pulverize after Temperature fall, obtained temperature adjustment phase transformation filler, for subsequent use; 40g Natvosol is joined in 250mL distilled water, be poured in kneader after even with ultrasonic disperse instrument ultrasonic disperse under the power of 150W, the above-mentioned obtained ACRYLIC EMULSION of 350mL, 45g temperature adjustment phase transformation filler, 1g microcrystalline wax and 13g antiseptic-germicide is added under the whipped state of kneader, stir after mediating 40min, make homogeneous paste, discharging, obtains a kind of antibacterial energy storage inherent regulation heat preservation putty.
Described antiseptic-germicide is the antibacterial system of negative ion powder, is in mass ratio for 20:11:17 mixes obtained by tourmaline powder, cerium oxide and titanium dioxide.
Embody rule method of the present invention: putty powder the present invention obtained and water are by volume for 2:1 mixes, leave standstill 15min after stirring again to stir, it being draped over one's shoulders uniformly with steel scraper plate or spatula scrapes on wall, repeatedly drape over one's shoulders after scraping 2 times, spend the night and dry, draping over one's shoulders and scraping thickness is 1.2cm, and putty consumption is 1.3kg/m 2.
Example 3
600mL deionized water, 10g stearoyl lactate, 30g nano grade silica particles are loaded in there-necked flask together with 50g vinylformic acid, stirs 15min with glass stick and obtain monomer pre-emulsion; 400mL deionized water and 12g sodium bicarbonate is added successively in the there-necked flask that constant pressure funnel, agitator are housed, startup agitator is stirred to sodium bicarbonate and dissolves completely, move into water-bath and be warming up to 80 DEG C, in flask, the above-mentioned obtained pre-emulsion of 300mL is dropwise dripped again by dropping funnel, control rate of addition to dropwise in 3h, after insulation 2h, filter, obtain ACRYLIC EMULSION; Take 2kg shale raw material, put into after micronizer mill pulverizes 30min and again fragment is loaded ball mill, be that 4:1 adds wolfram varbide ball milling pearl inwards by ratio of grinding media to material, after ball milling 2h, cross 100 mesh standard sieves, the slate flour obtained is put into retort furnace at 500 DEG C, calcines 2h, obtained shale pottery powder; By 2L mass concentration be 10% caustic soda soln join in reactor, be heated to 100 DEG C, under whipped state, add 200g stearic acid until its melt after, add 400mL distilled water, continue to be warming up to 120 DEG C and make it seethe with excitement; In the reactor of boiling, continue to add 300g paraffin to after dissolving completely, add the boiling water that 200mL temperature is 100 DEG C again, after stirring, after above-mentioned for 350g obtained shale pottery powder is slowly added, insulated and stirred 2h at the temperature of 85 DEG C, pulverize after Temperature fall, obtained temperature adjustment phase transformation filler, for subsequent use; 50g Natvosol is joined in 300mL distilled water, be poured in kneader after even with ultrasonic disperse instrument ultrasonic disperse under the power of 200W, the above-mentioned obtained ACRYLIC EMULSION of 400mL, 50g temperature adjustment phase transformation filler, 2g microcrystalline wax and 15g antiseptic-germicide is added under the whipped state of kneader, stir after mediating 50min, make homogeneous paste, discharging, obtains a kind of antibacterial energy storage inherent regulation heat preservation putty.
Described antiseptic-germicide is the antibacterial system of negative ion powder, is in mass ratio for 20:11:17 mixes obtained by tourmaline powder, cerium oxide and titanium dioxide.
Embody rule method of the present invention: putty powder the present invention obtained and water are by volume for 2:1 mixes, leave standstill 20min after stirring again to stir, it being draped over one's shoulders uniformly with steel scraper plate or spatula scrapes on wall, repeatedly drape over one's shoulders after scraping 3 times, spend the night and dry, draping over one's shoulders and scraping thickness is 1.5cm, and putty consumption is 1.5kg/m 2.

Claims (2)

1. a preparation method for antibacterial energy storage inherent regulation heat preservation putty, is characterized in that concrete preparation process is:
(1) 500 ~ 600mL deionized water, 8 ~ 10g stearoyl lactate, 20 ~ 30g nano grade silica particles are loaded in there-necked flask together with 40 ~ 50g vinylformic acid, stir 10 ~ 15min with glass stick and obtain monomer pre-emulsion;
(2) in the there-necked flask that constant pressure funnel, agitator are housed, 300 ~ 400mL deionized water and 10 ~ 12g sodium bicarbonate is added successively, startup agitator is stirred to sodium bicarbonate and dissolves completely, move into water-bath and be warming up to 70 ~ 80 DEG C, in flask, the above-mentioned obtained pre-emulsion of 200 ~ 300mL is dropwise dripped again by dropping funnel, control rate of addition to dropwise in 2 ~ 3h, after insulation 1 ~ 2h, filter, obtain ACRYLIC EMULSION;
(3) 1 ~ 2kg shale raw material are taken, put into after micronizer mill pulverizes 20 ~ 30min and again fragment is loaded ball mill, be that 4:1 adds wolfram varbide ball milling pearl inwards by ratio of grinding media to material, 100 mesh standard sieves are crossed after ball milling 1 ~ 2h, the slate flour obtained is put into retort furnace and calcine 1 ~ 2h at 400 ~ 500 DEG C, obtained shale pottery powder;
(4) by 1 ~ 2L mass concentration be 10% caustic soda soln join in reactor, be heated to 80 ~ 100 DEG C, 100 ~ 200g stearic acid is added until after its thawing, add 200 ~ 400mL distilled water, continue to be warming up to 100 ~ 120 DEG C and make it seethe with excitement under whipped state;
(5) in the reactor of boiling, 200 ~ 300g paraffin is continued to add to after dissolving completely, add the boiling water that 100 ~ 200mL temperature is 98 ~ 100 DEG C again, after stirring, after above-mentioned for 250 ~ 350g obtained shale pottery powder is slowly added, insulated and stirred 1 ~ 2h at the temperature of 75 ~ 85 DEG C, pulverize after Temperature fall, obtained temperature adjustment phase transformation filler, for subsequent use;
(6) 30 ~ 50g Natvosol is joined in 200 ~ 300mL distilled water, be poured in kneader after even with ultrasonic disperse instrument ultrasonic disperse under the power of 100 ~ 200W, the above-mentioned obtained ACRYLIC EMULSION of 300 ~ 400mL, 40 ~ 50g temperature adjustment phase transformation filler, 1 ~ 2g microcrystalline wax and 10 ~ 15g antiseptic-germicide is added under the whipped state of kneader, after stirring kneading 30 ~ 50min, make homogeneous paste, discharging, obtains a kind of antibacterial energy storage inherent regulation heat preservation putty.
2. the preparation method of a kind of antibacterial energy storage inherent regulation heat preservation putty according to claim 1, is characterized in that: described antiseptic-germicide is the antibacterial system of negative ion powder, is in mass ratio for 20:11:17 mixes obtained by tourmaline powder, cerium oxide and titanium dioxide.
CN201610063161.4A 2016-01-30 2016-01-30 Preparation method for anti-bacterial energy-storage self-adjusting heat-insulating putty Pending CN105542545A (en)

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Publication number Priority date Publication date Assignee Title
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CN102504636A (en) * 2011-11-23 2012-06-20 唐国军 Flexible environment-friendly interior wall putty
CN102518220A (en) * 2011-12-31 2012-06-27 北京国泰瑞华精藻硅特种材料有限公司 Construction method for heat-insulating wall body of building
CN102702826A (en) * 2012-06-12 2012-10-03 天长市巨龙车船涂料有限公司 Antibacterial negative ion putty powder

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Application publication date: 20160504