CN105542404A - Novel anti-static textile material and preparation method thereof - Google Patents
Novel anti-static textile material and preparation method thereof Download PDFInfo
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- CN105542404A CN105542404A CN201610030012.8A CN201610030012A CN105542404A CN 105542404 A CN105542404 A CN 105542404A CN 201610030012 A CN201610030012 A CN 201610030012A CN 105542404 A CN105542404 A CN 105542404A
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- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08L—COMPOSITIONS OF MACROMOLECULAR COMPOUNDS
- C08L67/00—Compositions of polyesters obtained by reactions forming a carboxylic ester link in the main chain; Compositions of derivatives of such polymers
- C08L67/02—Polyesters derived from dicarboxylic acids and dihydroxy compounds
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- D—TEXTILES; PAPER
- D01—NATURAL OR MAN-MADE THREADS OR FIBRES; SPINNING
- D01F—CHEMICAL FEATURES IN THE MANUFACTURE OF ARTIFICIAL FILAMENTS, THREADS, FIBRES, BRISTLES OR RIBBONS; APPARATUS SPECIALLY ADAPTED FOR THE MANUFACTURE OF CARBON FILAMENTS
- D01F1/00—General methods for the manufacture of artificial filaments or the like
- D01F1/02—Addition of substances to the spinning solution or to the melt
- D01F1/09—Addition of substances to the spinning solution or to the melt for making electroconductive or anti-static filaments
-
- D—TEXTILES; PAPER
- D01—NATURAL OR MAN-MADE THREADS OR FIBRES; SPINNING
- D01F—CHEMICAL FEATURES IN THE MANUFACTURE OF ARTIFICIAL FILAMENTS, THREADS, FIBRES, BRISTLES OR RIBBONS; APPARATUS SPECIALLY ADAPTED FOR THE MANUFACTURE OF CARBON FILAMENTS
- D01F1/00—General methods for the manufacture of artificial filaments or the like
- D01F1/02—Addition of substances to the spinning solution or to the melt
- D01F1/10—Other agents for modifying properties
-
- D—TEXTILES; PAPER
- D01—NATURAL OR MAN-MADE THREADS OR FIBRES; SPINNING
- D01F—CHEMICAL FEATURES IN THE MANUFACTURE OF ARTIFICIAL FILAMENTS, THREADS, FIBRES, BRISTLES OR RIBBONS; APPARATUS SPECIALLY ADAPTED FOR THE MANUFACTURE OF CARBON FILAMENTS
- D01F8/00—Conjugated, i.e. bi- or multicomponent, artificial filaments or the like; Manufacture thereof
- D01F8/04—Conjugated, i.e. bi- or multicomponent, artificial filaments or the like; Manufacture thereof from synthetic polymers
- D01F8/14—Conjugated, i.e. bi- or multicomponent, artificial filaments or the like; Manufacture thereof from synthetic polymers with at least one polyester as constituent
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- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08K—Use of inorganic or non-macromolecular organic substances as compounding ingredients
- C08K2201/00—Specific properties of additives
- C08K2201/011—Nanostructured additives
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- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08L—COMPOSITIONS OF MACROMOLECULAR COMPOUNDS
- C08L2201/00—Properties
- C08L2201/04—Antistatic
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- Engineering & Computer Science (AREA)
- Chemical Kinetics & Catalysis (AREA)
- General Chemical & Material Sciences (AREA)
- Textile Engineering (AREA)
- Manufacturing & Machinery (AREA)
- Health & Medical Sciences (AREA)
- Medicinal Chemistry (AREA)
- Polymers & Plastics (AREA)
- Organic Chemistry (AREA)
- Artificial Filaments (AREA)
- Compositions Of Macromolecular Compounds (AREA)
Abstract
The invention provides a novel anti-static textile material and a preparation method thereof. The novel anti-static textile material is prepared from the following ingredients: polyethylene terephthalate, polyurethane, nano zinc oxide, sodium hydroxide, ferric trichloride, phosphatidylcholine, phosphatidyl ethanolamine, sodium dodecyl benzene sulfonate, sodium chloride, absolute ethyl alcohol, butylated hydroxytoluene, ascorbyl palmitate, nano titanium dioxide and water. The preparation method comprises the following steps: mixing and bathing polyethylene terephthalate, polyurethane, sodium hydroxide and water; washing the mixture to be neutral; drying the neutral mixture; mixing the dry neutral mixture with phosphatidylcholine, phosphatidyl ethanolamine, sodium dodecyl benzene sulfonate, butylated hydroxytoluene, ascorbyl palmitate and absolute ethyl alcohol to obtain a second mixture; drying the second mixture; mixing the dry second mixture with ferric trichloride, sodium chloride and water to obtain a third mixture; drying the third mixture; finally, mixing the dry third mixture with the rest ingredients to obtain a fourth mixture; performing extrusion molding on the fourth mixture by a double-screw extruder. The novel anti-static textile material has favorable anti-static capability and stretching resistance, excellent air permeability and good comfort degree.
Description
Technical field
The present invention relates to Material Field, be specifically related to a kind of novel antistatic textile materials and preparation method thereof.
Background technology
The generation of electrostatic mainly because be separated after contacting with each other between two objects, produce superfluous plus or minus electric charge and causes in object.Generally, the non-conductor that specific conductivity is less is more charged in a dry environment.In daily life, generally all there is very high resistance, usually 10 with the closely-related textiles of people
13-10
20between Ω, especially man-made fiber, because ratio resistance is high, water absorbability is poor, very easily produces and accumulate static charge, thus can produce serious electrostatic phenomenon.The existence of electrostatic is to the production of people, and life causes a lot of inconvenience, and therefore, how eliminating this electrostatic phenomenon becomes people's problem demanding prompt solution.The antistatic technique of current textile product mainly contains following 3 kinds: 1. use antistatic agent 2. antistatic material and the blended production fibre of permanent anti-static 3. of macromolecular material to be used the method such as electro-conductive fiber and general fibre blending, mixed fibre and intertexture.
Summary of the invention
the technical problem solved:the object of this invention is to provide a kind of novel antistatic textile materials, there is good antistatic effect, stretch-resistance, have good ventilation property simultaneously, add comfort level.
technical scheme:a kind of novel antistatic textile materials, is prepared from weight part by following composition: polyethylene terephthalate 20-30 part, polyurethane(s) 10-20 part, nano zine oxide 2-5 part, sodium hydroxide 1-2 part, iron trichloride 2-5 part, phosphatidylcholine 1-2 part, phosphatidylethanolamine 1-2 part, Sodium dodecylbenzene sulfonate 1-2 part, sodium-chlor 0.1-0.2 part, dehydrated alcohol 10-20 part, butylated hydroxytoluene 0.1-0.2 part, Quicifal 0.1-0.2 part, nanometer titanium dioxide 1-2 part, water 20-30 part.
Preferred further, described a kind of novel antistatic textile materials, be prepared from weight part by following composition: polyethylene terephthalate 22-28 part, polyurethane(s) 13-17 part, nano zine oxide 3-4 part, sodium hydroxide 1.3-1.7 part, iron trichloride 3-4 part, phosphatidylcholine 1.3-1.7 part, phosphatidylethanolamine 1.2-1.6 part, Sodium dodecylbenzene sulfonate 1.3-1.8 part, sodium-chlor 0.11-0.16 part, dehydrated alcohol 13-18 part, butylated hydroxytoluene 0.12-0.17 part, Quicifal 0.13-0.17 part, nanometer titanium dioxide 1.3-1.8 part, water 23-28 part.
The preparation method of above-mentioned novel antistatic textile materials comprises the following steps:
Step 1: polyethylene terephthalate, polyurethane(s), sodium hydroxide and half water are mixed, extremely neutral with clear water punching after water-bath 3-4 hour at temperature 60-70 DEG C;
Step 2: put into baking oven and dry at 40-60 DEG C;
Step 3: mixed with phosphatidylcholine, phosphatidylethanolamine, Sodium dodecylbenzene sulfonate, butylated hydroxytoluene, Quicifal, dehydrated alcohol by step 2 gains, to stir after 1-2 hour and dries at 30-40 DEG C in an oven under magnetic stirrer rotating speed is 200-300r/min;
Step 4: by step 3 gains and iron trichloride, sodium-chlor, the mixing of remaining water, to stir after 1-2 hour and dries at 30-40 DEG C in an oven under magnetic stirrer rotating speed is 200-300r/min;
Step 5: by step 4 gains and remaining ingredient mixing, add in twin screw extruder and carry out extrusion moulding, screw speed 200-230r/min, a district is 160-180 DEG C to five district's temperature, and six district's temperature are 170-190 DEG C.
Preferred further, in step 1, bath temperature is 62-67 DEG C, and water bath time is 3.2-3.6 hour.
Preferred further, in step 2, oven temperature is 45-55 DEG C.
Preferred further, step 3 medium speed is 220-270r/min, and churning time is 1.2-1.7 hour, and drying temperature is 34-38 DEG C.
Preferred further, step 4 medium speed is 230-280r/min, and churning time is 1.1-1.6 hour, and drying temperature is 33-38 DEG C.
Preferred further, screw speed 210-220r/min in step 5, a district is 165-175 DEG C to five district's temperature, and six district's temperature are 175-185 DEG C.
beneficial effect:novel antistatic textile materials of the present invention has very strong antistatic effect, can the harm that destatics of solution effectively, tensile resistance is also better, and maximum elongation at break can reach 35.6%, there is good ventilation property simultaneously, effectively can improve the comfort level to human body.
Embodiment
Embodiment 1
A kind of novel antistatic textile materials, is prepared from weight part by following composition: polyethylene terephthalate 28 parts, polyurethane(s) 17 parts, nano zine oxide 4 parts, 1.7 parts, sodium hydroxide, iron trichloride 4 parts, phosphatidylcholine 1.7 parts, phosphatidylethanolamine 1.6 parts, Sodium dodecylbenzene sulfonate 1.8 parts, 0.16 part, sodium-chlor, dehydrated alcohol 18 parts, butylated hydroxytoluene 0.17 part, Quicifal 0.17 part, nanometer titanium dioxide 1.8 parts, 28 parts, water.
The preparation method of above-mentioned novel antistatic textile materials is: first by polyethylene terephthalate, polyurethane(s), sodium hydroxide and the mixing of half water, at temperature 67 DEG C, water-bath is extremely neutral with clear water punching after 3.6 hours, then put into baking oven to dry at 55 DEG C, again with phosphatidylcholine, phosphatidylethanolamine, Sodium dodecylbenzene sulfonate, butylated hydroxytoluene, Quicifal, dehydrated alcohol mixes, to stir under magnetic stirrer rotating speed is 270r/min after 1.7 hours and dry at 38 DEG C in an oven, again and iron trichloride, sodium-chlor, remaining water mixing, to stir under magnetic stirrer rotating speed is 280r/min after 1.6 hours and dry at 38 DEG C in an oven, last and remaining ingredient mixes, add in twin screw extruder and carry out extrusion moulding, screw speed 220r/min, one district is 175 DEG C to five district's temperature, six district's temperature are 185 DEG C.
Embodiment 2
A kind of novel antistatic textile materials, is prepared from weight part by following composition: polyethylene terephthalate 25 parts, polyurethane(s) 15 parts, nano zine oxide 3.5 parts, 1.5 parts, sodium hydroxide, iron trichloride 3.5 parts, phosphatidylcholine 1.5 parts, phosphatidylethanolamine 1.5 parts, Sodium dodecylbenzene sulfonate 1.5 parts, 0.15 part, sodium-chlor, dehydrated alcohol 15 parts, butylated hydroxytoluene 0.15 part, Quicifal 0.15 part, nanometer titanium dioxide 1.5 parts, 25 parts, water.
The preparation method of above-mentioned novel antistatic textile materials is: first by polyethylene terephthalate, polyurethane(s), sodium hydroxide and the mixing of half water, at temperature 65 DEG C, water-bath is extremely neutral with clear water punching after 3.5 hours, then put into baking oven to dry at 50 DEG C, again with phosphatidylcholine, phosphatidylethanolamine, Sodium dodecylbenzene sulfonate, butylated hydroxytoluene, Quicifal, dehydrated alcohol mixes, to stir under magnetic stirrer rotating speed is 250r/min after 1.5 hours and dry at 35 DEG C in an oven, again and iron trichloride, sodium-chlor, remaining water mixing, to stir under magnetic stirrer rotating speed is 250r/min after 1.5 hours and dry at 35 DEG C in an oven, last and remaining ingredient mixes, add in twin screw extruder and carry out extrusion moulding, screw speed 215r/min, one district is 170 DEG C to five district's temperature, six district's temperature are 180 DEG C.
Embodiment 3
A kind of novel antistatic textile materials, is prepared from weight part by following composition: polyethylene terephthalate 22 parts, polyurethane(s) 13 parts, nano zine oxide 3 parts, 1.3 parts, sodium hydroxide, iron trichloride 3 parts, phosphatidylcholine 1.3 parts, phosphatidylethanolamine 1.2 parts, Sodium dodecylbenzene sulfonate 1.3 parts, 0.11 part, sodium-chlor, dehydrated alcohol 13 parts, butylated hydroxytoluene 0.12 part, Quicifal 0.13 part, nanometer titanium dioxide 1.3 parts, 23 parts, water.
The preparation method of above-mentioned novel antistatic textile materials is: first by polyethylene terephthalate, polyurethane(s), sodium hydroxide and the mixing of half water, at temperature 62 DEG C, water-bath is extremely neutral with clear water punching after 3.2 hours, then put into baking oven to dry at 45 DEG C, again with phosphatidylcholine, phosphatidylethanolamine, Sodium dodecylbenzene sulfonate, butylated hydroxytoluene, Quicifal, dehydrated alcohol mixes, to stir under magnetic stirrer rotating speed is 220r/min after 1.2 hours and dry at 34 DEG C in an oven, again and iron trichloride, sodium-chlor, remaining water mixing, to stir under magnetic stirrer rotating speed is 230r/min after 1.1 hours and dry at 33 DEG C in an oven, last and remaining ingredient mixes, add in twin screw extruder and carry out extrusion moulding, screw speed 210r/min, one district is 165 DEG C to five district's temperature, six district's temperature are 175 DEG C.
Embodiment 4
A kind of novel antistatic textile materials, is prepared from weight part by following composition: polyethylene terephthalate 30 parts, polyurethane(s) 20 parts, nano zine oxide 5 parts, 2 parts, sodium hydroxide, iron trichloride 5 parts, phosphatidylcholine 2 parts, phosphatidylethanolamine 2 parts, Sodium dodecylbenzene sulfonate 2 parts, 0.2 part, sodium-chlor, dehydrated alcohol 20 parts, butylated hydroxytoluene 0.2 part, Quicifal 0.2 part, nanometer titanium dioxide 2 parts, 30 parts, water.
The preparation method of above-mentioned novel antistatic textile materials is: first by polyethylene terephthalate, polyurethane(s), sodium hydroxide and the mixing of half water, under temperature 70 C, water-bath is extremely neutral with clear water punching after 4 hours, then put into baking oven to dry at 60 DEG C, again with phosphatidylcholine, phosphatidylethanolamine, Sodium dodecylbenzene sulfonate, butylated hydroxytoluene, Quicifal, dehydrated alcohol mixes, to stir under magnetic stirrer rotating speed is 300r/min after 2 hours and dry at 40 DEG C in an oven, again and iron trichloride, sodium-chlor, remaining water mixing, to stir under magnetic stirrer rotating speed is 300r/min after 2 hours and dry at 40 DEG C in an oven, last and remaining ingredient mixes, add in twin screw extruder and carry out extrusion moulding, screw speed 230r/min, one district is 180 DEG C to five district's temperature, six district's temperature are 190 DEG C.
Embodiment 5
A kind of novel antistatic textile materials, is prepared from weight part by following composition: polyethylene terephthalate 20 parts, polyurethane(s) 10 parts, nano zine oxide 2 parts, 1 part, sodium hydroxide, iron trichloride 2 parts, phosphatidylcholine 1 part, phosphatidylethanolamine 1 part, Sodium dodecylbenzene sulfonate 1 part, 0.1 part, sodium-chlor, dehydrated alcohol 10 parts, butylated hydroxytoluene 0.1 part, Quicifal 0.1 part, nanometer titanium dioxide 1 part, 20 parts, water.
The preparation method of above-mentioned novel antistatic textile materials is: first by polyethylene terephthalate, polyurethane(s), sodium hydroxide and the mixing of half water, under temperature 60 C, water-bath is extremely neutral with clear water punching after 3 hours, then put into baking oven to dry at 40 DEG C, again with phosphatidylcholine, phosphatidylethanolamine, Sodium dodecylbenzene sulfonate, butylated hydroxytoluene, Quicifal, dehydrated alcohol mixes, to stir under magnetic stirrer rotating speed is 200r/min after 1 hour and dry at 30 DEG C in an oven, again and iron trichloride, sodium-chlor, remaining water mixing, to stir under magnetic stirrer rotating speed is 200r/min after 1 hour and dry at 30 DEG C in an oven, last and remaining ingredient mixes, add in twin screw extruder and carry out extrusion moulding, screw speed 200r/min, one district is 160 DEG C to five district's temperature, six district's temperature are 170 DEG C.
Comparative example 1
The difference of the present embodiment and embodiment 5 is not containing phosphatidylcholine and phosphatidylethanolamine.Specifically:
A kind of novel antistatic textile materials, is prepared from weight part by following composition: polyethylene terephthalate 20 parts, polyurethane(s) 10 parts, nano zine oxide 2 parts, 1 part, sodium hydroxide, iron trichloride 2 parts, Sodium dodecylbenzene sulfonate 1 part, 0.1 part, sodium-chlor, dehydrated alcohol 10 parts, butylated hydroxytoluene 0.1 part, Quicifal 0.1 part, nanometer titanium dioxide 1 part, 20 parts, water.
The preparation method of above-mentioned novel antistatic textile materials is: first by polyethylene terephthalate, polyurethane(s), sodium hydroxide and the mixing of half water, under temperature 60 C, water-bath is extremely neutral with clear water punching after 3 hours, then put into baking oven to dry at 40 DEG C, again with Sodium dodecylbenzene sulfonate, butylated hydroxytoluene, Quicifal, dehydrated alcohol mixes, to stir under magnetic stirrer rotating speed is 200r/min after 1 hour and dry at 30 DEG C in an oven, again and iron trichloride, sodium-chlor, remaining water mixing, to stir under magnetic stirrer rotating speed is 200r/min after 1 hour and dry at 30 DEG C in an oven, last and remaining ingredient mixes, add in twin screw extruder and carry out extrusion moulding, screw speed 200r/min, one district is 160 DEG C to five district's temperature, six district's temperature are 170 DEG C.
Comparative example 2
The difference of the present embodiment and embodiment 5 is, not containing nanometer titanium dioxide, to replace with nano zine oxide.Specifically:
A kind of novel antistatic textile materials, is prepared from weight part by following composition: polyethylene terephthalate 20 parts, polyurethane(s) 10 parts, nano zine oxide 2 parts, 1 part, sodium hydroxide, iron trichloride 2 parts, phosphatidylcholine 1 part, phosphatidylethanolamine 1 part, Sodium dodecylbenzene sulfonate 1 part, 0.1 part, sodium-chlor, dehydrated alcohol 10 parts, butylated hydroxytoluene 0.1 part, Quicifal 0.1 part, 20 parts, water.
The preparation method of above-mentioned novel antistatic textile materials is: first by polyethylene terephthalate, polyurethane(s), sodium hydroxide and the mixing of half water, under temperature 60 C, water-bath is extremely neutral with clear water punching after 3 hours, then put into baking oven to dry at 40 DEG C, again with phosphatidylcholine, phosphatidylethanolamine, Sodium dodecylbenzene sulfonate, butylated hydroxytoluene, Quicifal, dehydrated alcohol mixes, to stir under magnetic stirrer rotating speed is 200r/min after 1 hour and dry at 30 DEG C in an oven, again and iron trichloride, sodium-chlor, remaining water mixing, to stir under magnetic stirrer rotating speed is 200r/min after 1 hour and dry at 30 DEG C in an oven, last and remaining ingredient mixes, add in twin screw extruder and carry out extrusion moulding, screw speed 200r/min, one district is 160 DEG C to five district's temperature, six district's temperature are 170 DEG C.
Each embodiment and comparative example are compared, comparing result is as following table 1:
The performance index of table 1 novel antistatic textile materials
Name of product | Resistivity (Ω cm) | Elongation at break (%) | Ventilation property (L/ (m 2·s)) |
Embodiment 1 | 206 | 35.6 | 352 |
Embodiment 2 | 213 | 35.1 | 345 |
Embodiment 3 | 215 | 35.0 | 340 |
Embodiment 4 | 219 | 35.3 | 347 |
Embodiment 5 | 209 | 34.7 | 333 |
Comparative example 1 | 236 | 31.6 | 326 |
Comparative example 2 | 279 | 34.5 | 312 |
As known from Table 1, embodiment 1-5 has very strong antistatic effect, and tensile resistance is also better, and maximum elongation at break can reach 35.6%, and have good ventilation property, comfort level is good simultaneously.Compare with comparative example, the indices of discovery comparative example 1 declines all to some extent but is too obvious, and in comparative example 2, resistivity has obvious rising, and antistatic effect declines, and illustrates that nanometer titanium dioxide has for raising antistatic effect the effect shown.
Claims (8)
1. a novel antistatic textile materials, is characterized in that: be prepared from weight part by following composition: polyethylene terephthalate 20-30 part, polyurethane(s) 10-20 part, nano zine oxide 2-5 part, sodium hydroxide 1-2 part, iron trichloride 2-5 part, phosphatidylcholine 1-2 part, phosphatidylethanolamine 1-2 part, Sodium dodecylbenzene sulfonate 1-2 part, sodium-chlor 0.1-0.2 part, dehydrated alcohol 10-20 part, butylated hydroxytoluene 0.1-0.2 part, Quicifal 0.1-0.2 part, nanometer titanium dioxide 1-2 part, water 20-30 part.
2. a kind of novel antistatic textile materials according to claim 1, it is characterized in that: be prepared from weight part by following composition: polyethylene terephthalate 22-28 part, polyurethane(s) 13-17 part, nano zine oxide 3-4 part, sodium hydroxide 1.3-1.7 part, iron trichloride 3-4 part, phosphatidylcholine 1.3-1.7 part, phosphatidylethanolamine 1.2-1.6 part, Sodium dodecylbenzene sulfonate 1.3-1.8 part, sodium-chlor 0.11-0.16 part, dehydrated alcohol 13-18 part, butylated hydroxytoluene 0.12-0.17 part, Quicifal 0.13-0.17 part, nanometer titanium dioxide 1.3-1.8 part, water 23-28 part.
3. the preparation method of a kind of novel antistatic textile materials described in any one of claim 1 to 2, is characterized in that: comprise the following steps:
Step 1: polyethylene terephthalate, polyurethane(s), sodium hydroxide and half water are mixed, extremely neutral with clear water punching after water-bath 3-4 hour at temperature 60-70 DEG C;
Step 2: put into baking oven and dry at 40-60 DEG C;
Step 3: mixed with phosphatidylcholine, phosphatidylethanolamine, Sodium dodecylbenzene sulfonate, butylated hydroxytoluene, Quicifal, dehydrated alcohol by step 2 gains, to stir after 1-2 hour and dries at 30-40 DEG C in an oven under magnetic stirrer rotating speed is 200-300r/min;
Step 4: by step 3 gains and iron trichloride, sodium-chlor, the mixing of remaining water, to stir after 1-2 hour and dries at 30-40 DEG C in an oven under magnetic stirrer rotating speed is 200-300r/min;
Step 5: by step 4 gains and remaining ingredient mixing, add in twin screw extruder and carry out extrusion moulding, screw speed 200-230r/min, a district is 160-180 DEG C to five district's temperature, and six district's temperature are 170-190 DEG C.
4. the preparation method of a kind of novel antistatic textile materials according to claim 3, it is characterized in that: in described step 1, bath temperature is 62-67 DEG C, water bath time is 3.2-3.6 hour.
5. the preparation method of a kind of novel antistatic textile materials according to claim 3, is characterized in that: in described step 2, oven temperature is 45-55 DEG C.
6. the preparation method of a kind of novel antistatic textile materials according to claim 3, it is characterized in that: described step 3 medium speed is 220-270r/min, churning time is 1.2-1.7 hour, and drying temperature is 34-38 DEG C.
7. the preparation method of a kind of novel antistatic textile materials according to claim 3, it is characterized in that: described step 4 medium speed is 230-280r/min, churning time is 1.1-1.6 hour, and drying temperature is 33-38 DEG C.
8. the preparation method of a kind of novel antistatic textile materials according to claim 3, it is characterized in that: screw speed 210-220r/min in described step 5, a district is 165-175 DEG C to five district's temperature, and six district's temperature are 175-185 DEG C.
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CN107699976A (en) * | 2017-11-01 | 2018-02-16 | 安徽创荣服装辅料有限公司 | A kind of antistatic PET filament and preparation method thereof |
CN109704106A (en) * | 2019-02-22 | 2019-05-03 | 信阳颐和非织布有限责任公司 | A kind of preparation process of anti-static nonwoven fabric |
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CN104530656A (en) * | 2014-11-26 | 2015-04-22 | 苏州新区佳合塑胶有限公司 | Antistatic PBT material and preparation method thereof |
CN104945865A (en) * | 2015-06-29 | 2015-09-30 | 青岛精石通精密机械制造有限公司 | High-performance anti-static PET composite material |
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CN103351585A (en) * | 2013-07-08 | 2013-10-16 | 常熟市沪联印染有限公司 | Antibacterial and antistatic polyester resin slice |
CN104530656A (en) * | 2014-11-26 | 2015-04-22 | 苏州新区佳合塑胶有限公司 | Antistatic PBT material and preparation method thereof |
CN104945865A (en) * | 2015-06-29 | 2015-09-30 | 青岛精石通精密机械制造有限公司 | High-performance anti-static PET composite material |
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CN107699976A (en) * | 2017-11-01 | 2018-02-16 | 安徽创荣服装辅料有限公司 | A kind of antistatic PET filament and preparation method thereof |
CN109704106A (en) * | 2019-02-22 | 2019-05-03 | 信阳颐和非织布有限责任公司 | A kind of preparation process of anti-static nonwoven fabric |
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