CN105533049A - Preparation method for compound tea of honeysuckle and shiya tea - Google Patents

Preparation method for compound tea of honeysuckle and shiya tea Download PDF

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Publication number
CN105533049A
CN105533049A CN201511023615.7A CN201511023615A CN105533049A CN 105533049 A CN105533049 A CN 105533049A CN 201511023615 A CN201511023615 A CN 201511023615A CN 105533049 A CN105533049 A CN 105533049A
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China
Prior art keywords
tea
honeysuckle
stone precipice
preparation
compound
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CN201511023615.7A
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Chinese (zh)
Inventor
程忠泉
徐宝敏
温宇
吴丽文
孙显屏
杨丹
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Echo Bio Tech Ltd Guilin
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Echo Bio Tech Ltd Guilin
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Priority to CN201511023615.7A priority Critical patent/CN105533049A/en
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    • AHUMAN NECESSITIES
    • A23FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
    • A23FCOFFEE; TEA; THEIR SUBSTITUTES; MANUFACTURE, PREPARATION, OR INFUSION THEREOF
    • A23F3/00Tea; Tea substitutes; Preparations thereof
    • A23F3/34Tea substitutes, e.g. matè; Extracts or infusions thereof

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  • Life Sciences & Earth Sciences (AREA)
  • Chemical & Material Sciences (AREA)
  • Engineering & Computer Science (AREA)
  • Food Science & Technology (AREA)
  • Polymers & Plastics (AREA)
  • Medicines Containing Plant Substances (AREA)
  • Extraction Or Liquid Replacement (AREA)
  • Tea And Coffee (AREA)

Abstract

The invention relates to the technical field of compound tea preparation, and in particular relates to a preparation method for compound tea of honeysuckle and shiya tea. The preparation method comprises the following preparation steps: 1) weighing the honeysuckle and the shiya tea in proportion by weight, and crushing the honeysuckle and the shiya tea; 2) processing the honeysuckle and the shiya tea under high pressure; 3) carrying out microwave extraction on the honeysuckle and the shiya tea; and 4) stirring, concentrating and carrying out spray drying on an extracting solution obtained in the step 3), thereby obtaining the compound tea. The compound of the honeysuckle and the shiya tea, prepared by the preparation method disclosed by the invention, has relatively strong oxidation resistance.

Description

The preparation method of a kind of honeysuckle stone precipice tea compound tea
Technical field
The present invention relates to compound tea preparing technical field, particularly the preparation method of a kind of honeysuckle stone precipice tea compound tea.
Background technology
Honeysuckle, has another name called honeysuckle (formal name used at school: Lonicerajaponica)." honeysuckle " one comes from Compendium of Material Medica, owing to opening as white at the beginning of FLOSLONICERAE, after transfer yellow to, hence obtain one's name honeysuckle.Medicinal material honeysuckle is Caprifoliaceae woodbine honeysuckle and congener dry flower or is with the flower just opened.Honeysuckle is just extensive and famous with its medical value since ancient times.Its property sweet cold air fragrance, clear heat with drugs of sweet flavour and cold nature and not injuring one's stomach, fragrance thoroughly reaches and can be eliminating evil.Its effect is mainly clearing heat and detoxicating, cures mainly warm disease heating, toxic-heat and blood stasis, ulcer serious case of furuncle etc.Modern study proves, honeysuckle contains the pharmacological component such as chlorogenic acid, cyanidenon glycosides, stronger restraint is had to the various pathogens such as hemolytic streptococcus, Staphylococcus aureus and infection of the upper respiratory tract Causative virus etc., in addition also can develop immunitypty, Robust speaker feature, protect liver, antitumor, anti-inflammatory, antipyretic, hemostasis (blood coagulation), suppress intestinal absorption cholesterol etc., its clinical application widely, can be used for the treatment of respiratory tract infection, bacillary dysentery, acute urinary, hypertension etc. more than 40 with other medicines compatibility and plant illness.
Stone precipice tea, has another name called: Shi Yancha, tor tea.The yellow auspicious wood of the bright leaf of formal name used at school, Yang Tong belongs to, arbor.Because growth is gained the name on steep cliff, its bud-leaf is plump, and made tealeaves soup look beautiful.Pure time of taste is sweet good, endures repeated infusions, and detects through relevant department, because stone precipice tea is not containing caffeine, does not affect sleep after drink, and is rich in Flavonoid substances and has good health-care effect, therefore deeply likes by consumer.Main component is: flavonoids 20%, Tea Polyphenols 23.4%, the multiple element that amino acid 9.73% and wildlife alkali etc. are useful to human body, be find the plant that Flavone content is the highest in natural plants at present, belong to treasure in the tea of domestic rare ecosystem fully natural green plant.
The present invention studies discovery, and with honeysuckle and stone precipice tea for raw material, the compound tea adopting preparation method of the present invention to prepare has stronger antioxidation.
Summary of the invention
Technical problem to be solved by this invention is to provide the preparation method of a kind of honeysuckle stone precipice tea compound tea, and the compound tea that the method prepares has stronger antioxidation.
For achieving the above object, the present invention adopts following technical scheme:
The invention provides the preparation method of a kind of honeysuckle stone precipice tea compound tea, comprise following preparation process:
1) be that 3 ~ 8:5 ~ 14 take honeysuckle and stone precipice tea by weight, pulverize;
2) by honeysuckle and the mixing of stone precipice tea, add their gross weights 3 ~ 6 times of ethanolic solutions, put into pressure pan, be forced into 0.6 ~ 1.8MPa, make its pressure uniform, and keep 3 ~ 8min, recover normal pressure, obtain slurries;
3) to step 2) add honeysuckle and stone precipice tea gross weight 2 ~ 5 times of ethanolic solutions again in the slurries that obtain, under power is 450 ~ 550W, carries out Microwave Extraction, obtains extract;
4) by step 3) extract that obtains stirs at 30 ~ 40 DEG C, and concentrated, spraying dry, obtains compound tea.
Preferably, step 1 of the present invention) in, honeysuckle and stone precipice tea are crushed to 50 ~ 100 orders respectively.
Preferably, the volume fraction of ethanolic solution of the present invention is 80 ~ 95%.
Preferably, step 3 of the present invention) in, microwave heating time is 15 ~ 25s, intermittent action 2 ~ 3 times.
Preferably, step 4 of the present invention) in, stir 5 ~ 10min.
The honeysuckle stone precipice tea compound tea that the present invention also provides described method to prepare, this compound tea has stronger antioxidation.
Honeysuckle of the present invention and stone precipice tea are dry product.
Compared with prior art, the present invention is before Microwave Extraction, with HIGH PRESSURE TREATMENT honeysuckle and stone precipice tea, utilize active ingredient and the different holding capacity of non-active ingredients to high pressure, and active ingredient is separated with non-active ingredients, improve recovery rate, improve effect, use Microwave Extraction raw material again, mild condition, can ensure that active ingredient is not wherein destroyed to large extent, there is higher recovery rate, and comparatively save time, shorten the production cycle, extract is stirred at a certain temperature, honeysuckle and stone precipice tea active ingredient are better neutralized, the honeysuckle stone precipice tea compound tea prepared has stronger antioxidation.
Detailed description of the invention
Below in conjunction with embodiment, the invention will be further described, but the present invention is not limited to these embodiments.
Embodiment 1
1) take honeysuckle and stone precipice tea by weight for 3:14, be crushed to 50 orders;
2) by honeysuckle and the mixing of stone precipice tea, adding their gross weights 6 times of volume fractions is the ethanolic solution of 80%, puts into pressure pan, is forced into 1.8MPa, make its pressure uniform, and keep 3min, recovers normal pressure, obtains slurries;
3) to step 2) add honeysuckle again in the slurries that obtain and tea gross weight 4 times of volume fractions in stone precipice are the ethanolic solution of 80%, under power is 450W, carry out Microwave Extraction, microwave heating time is 25s, and intermittent action 3 times, obtains extract;
4) by step 3) extract that obtains stirs 10min at 30 DEG C, and concentrated, spraying dry, obtains compound tea.
Embodiment 2
1) take honeysuckle and stone precipice tea by weight for 4:11, be crushed to 60 orders;
2) by honeysuckle and the mixing of stone precipice tea, adding their gross weights 5 times of volume fractions is the ethanolic solution of 85%, puts into pressure pan, is forced into 1.5MPa, make its pressure uniform, and keep 4min, recovers normal pressure, obtains slurries;
3) to step 2) add honeysuckle again in the slurries that obtain and tea gross weight 5 times of volume fractions in stone precipice are the ethanolic solution of 85%, under power is 480W, carry out Microwave Extraction, microwave heating time is 22s, and intermittent action 2 times, obtains extract;
4) by step 3) extract that obtains stirs 9min at 33 DEG C, and concentrated, spraying dry, obtains compound tea.
Embodiment 3
1) take honeysuckle and stone precipice tea by weight for 5:9, be crushed to 70 orders;
2) by honeysuckle and the mixing of stone precipice tea, adding their gross weights 5 times of volume fractions is the ethanolic solution of 90%, puts into pressure pan, is forced into 1.2MPa, make its pressure uniform, and keep 5min, recovers normal pressure, obtains slurries;
3) to step 2) add honeysuckle again in the slurries that obtain and tea gross weight 4 times of volume fractions in stone precipice are the ethanolic solution of 90%, under power is 500W, carry out Microwave Extraction, microwave heating time is 20s, and intermittent action 3 times, obtains extract;
4) by step 3) extract that obtains stirs 8min at 35 DEG C, and concentrated, spraying dry, obtains compound tea.
Embodiment 4
1) take honeysuckle and stone precipice tea by weight for 6:7, be crushed to 90 orders;
2) by honeysuckle and the mixing of stone precipice tea, adding their gross weights 4 times of volume fractions is the ethanolic solution of 95%, puts into pressure pan, is forced into 0.9MPa, make its pressure uniform, and keep 7min, recovers normal pressure, obtains slurries;
3) to step 2) add honeysuckle again in the slurries that obtain and tea gross weight 3 times of volume fractions in stone precipice are the ethanolic solution of 95%, under power is 520W, carry out Microwave Extraction, microwave heating time is 18s, and intermittent action 3 times, obtains extract;
4) by step 3) extract that obtains stirs 6min at 38 DEG C, and concentrated, spraying dry, obtains compound tea.
Embodiment 5
1) take honeysuckle and stone precipice tea by weight for 8:5, be crushed to 100 orders;
2) by honeysuckle and the mixing of stone precipice tea, adding their gross weights 3 times of volume fractions is the ethanolic solution of 85%, puts into pressure pan, is forced into 0.6MPa, make its pressure uniform, and keep 8min, recovers normal pressure, obtains slurries;
3) to step 2) add honeysuckle again in the slurries that obtain and tea gross weight 2 times of volume fractions in stone precipice are the ethanolic solution of 85%, under power is 550W, carry out Microwave Extraction, microwave heating time is 15s, and intermittent action 2 times, obtains extract;
4) by step 3) extract that obtains stirs 5min at 40 DEG C, and concentrated, spraying dry, obtains compound tea.
Test example: the honeysuckle stone precipice tea compound tea antioxidation that the method for the invention prepares
1, the honeysuckle stone precipice tea compound tea that material: A (general commercially available honeysuckle), B (general commercially available stone precipice tea), embodiment 3 prepare.
2, test method:
(1) A and B crude extract prepares extracting method: get each 10g of A and B, pulverize respectively, by solid-liquid ratio 1:25 extracting in water, extract three times, merge extract, be concentrated into certain volume, add the ethanolic solution precipitation of 3 times 95%, get supernatant concentration, drying, obtain A and B crude extract for subsequent use.
The honeysuckle stone precipice tea compound tea processing method that embodiment 3 prepares: add its ethanolic solution of 3 times 95% precipitation, get supernatant concentration, drying, obtain C.
(2) mensuration of reducing power: sample is by the potassium ferricyanide (K 3fe (CN) 6) be reduced into potassium ferrocyanide (K 4fe (CN) 6), potassium ferrocyanide again with Fe 3+effect, generate ferric ferrocyanide (Prussian blue), to detect the size that Prussian blue absorbance represents reducing power at 700nm wavelength place, absorbance is higher, and the reducing power of sample is stronger, and non-oxidizability is stronger.At 700nm wavelength place, measuring concentration is respectively A and the B crude extract of 5mg/ml and the light absorption value of C.
(3) superoxide anion experiment is removed: at generation ultra-oxygen anion free radical (O 2-) reaction system in, add A and B crude extract and C that concentration is 5mg/ml respectively, measure their clearance rates.
(4) experiment of hydroxyl radical free radical is removed: FeSO 4with H 2o 2reaction produces OH, and in system, add salicylic acid, can catch hydroxyl radical free radical and produce coloring matter, this material has absorption maximum at 510nm place, and when there is OH free radical scavenger in reaction system, this oxidizing process is suppressed, and absorbance then reduces.At FeSO 4with H 2o 2in reaction system, add A and B crude extract and C that concentration is 30mg/ml respectively, measure clearance rate.
(5) NO under SGF pH condition 2-cleaning reaction effect: cleaning nitrite is one of approach effectively preventing N-nitroso compound carcinogenic.Add in simulated system and add A and the B crude extract and C that concentration is 14mg/ml respectively, measure clearance rate.
(6) DPPH method measures antioxidation activity: DPPH is a kind of stable free radical in organic solvent, is widely used in anti-oxidant appraisement system.In system, add A and B crude extract and C that concentration is 30mg/ml respectively, measure clearance rate.
3, result of the test:
The reducing power of table 1 different material extract
A B C
Light absorption value 0.425 0.987 1.246
Table 1 result shows, A and B crude extract and C have reducing power, and C reducing power is better than A and B.
Table 2 different material extract removes the ability of superoxide anion
A B C
Clearance rate 15% 31% 49%
Table 2 shows, A and B crude extract and C have the ability removing superoxide anion, and C Scavenging activity is better than A and B.
Table 3 different material extract removes the ability of hydroxyl radical free radical
A B C
Clearance rate 32% 45% 66%
Table 3 shows, A and B crude extract and C have the ability removing hydroxyl radical free radical, and C Scavenging activity is better than A and B.
Table 4 different material extract is to NO 2-scavenging action
A B C
Clearance rate 27% 40% 64%
Table 4 shows, A and B crude extract and C are to NO 2-have scavenging action, C Scavenging activity is better than A and B.
Table 5 different material extract is to DPPH elimination effect
A B C
Clearance rate 28% 39% 57%
Table 5 shows, A and B crude extract and C have elimination effect to DPPH, and C elimination effect is better than A and B.
Comprehensive above-mentioned oxidation reaction system result of the test, illustrates that the honeysuckle stone precipice tea compound tea that the inventive method prepares has stronger antioxidation.

Claims (6)

1. a preparation method for honeysuckle stone precipice tea compound tea, is characterized in that, comprises following preparation process:
1) be that 3 ~ 8:5 ~ 14 take honeysuckle and stone precipice tea by weight, pulverize;
2) by honeysuckle and the mixing of stone precipice tea, add their gross weights 3 ~ 6 times of ethanolic solutions, put into pressure pan, be forced into 0.6 ~ 1.8MPa, make its pressure uniform, and keep 3 ~ 8min, recover normal pressure, obtain slurries;
3) to step 2) add honeysuckle and stone precipice tea gross weight 2 ~ 5 times of ethanolic solutions again in the slurries that obtain, under power is 450 ~ 550W, carries out Microwave Extraction, obtains extract;
4) by step 3) extract that obtains stirs at 30 ~ 40 DEG C, and concentrated, spraying dry, obtains compound tea.
2. the preparation method of honeysuckle stone precipice according to claim 1 tea compound tea, is characterized in that: described step 1) in, honeysuckle and stone precipice tea are crushed to 50 ~ 100 orders respectively.
3. the preparation method of honeysuckle stone precipice according to claim 1 tea compound tea, is characterized in that: the volume fraction of described ethanolic solution is 80 ~ 95%.
4. the preparation method of honeysuckle stone precipice according to claim 3 tea compound tea, is characterized in that: described step 3) in, microwave heating time is 15 ~ 25s, intermittent action 2 ~ 3 times.
5. the preparation method of honeysuckle stone precipice according to claim 1 tea compound tea, is characterized in that: described step 4) in, stir 5 ~ 10min.
6. the honeysuckle stone precipice tea compound tea that the method according to Claims 1 to 5 any one prepares.
CN201511023615.7A 2015-12-31 2015-12-31 Preparation method for compound tea of honeysuckle and shiya tea Pending CN105533049A (en)

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Cited By (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN108813041A (en) * 2018-06-26 2018-11-16 广西昭平县凝香翠茶厂 A kind of stone precipice compounded health tea and preparation method thereof

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* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN104432381A (en) * 2014-12-12 2015-03-25 广州中国科学院先进技术研究所 Honeysuckle health beverage and preparation method thereof
CN104585447A (en) * 2015-02-06 2015-05-06 桂林双象生物科技有限公司 Preparation method of Shi-ya tea compound tea and drink of Shi-ya tea compound tea
CN104585446A (en) * 2015-02-06 2015-05-06 桂林双象生物科技有限公司 Momordica grosvenori rock tea and preparation method for drink of momordica grosvenori rock tea

Patent Citations (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN104432381A (en) * 2014-12-12 2015-03-25 广州中国科学院先进技术研究所 Honeysuckle health beverage and preparation method thereof
CN104585447A (en) * 2015-02-06 2015-05-06 桂林双象生物科技有限公司 Preparation method of Shi-ya tea compound tea and drink of Shi-ya tea compound tea
CN104585446A (en) * 2015-02-06 2015-05-06 桂林双象生物科技有限公司 Momordica grosvenori rock tea and preparation method for drink of momordica grosvenori rock tea

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何伟平等: "罗汉果功能特性及产品开发研究现状", 《中国新技术新产品》 *
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Cited By (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN108813041A (en) * 2018-06-26 2018-11-16 广西昭平县凝香翠茶厂 A kind of stone precipice compounded health tea and preparation method thereof

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Application publication date: 20160504