CN105523537A - Method for vacuum calcination of bamboo charcoal in tunneling kiln - Google Patents

Method for vacuum calcination of bamboo charcoal in tunneling kiln Download PDF

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Publication number
CN105523537A
CN105523537A CN201610001295.3A CN201610001295A CN105523537A CN 105523537 A CN105523537 A CN 105523537A CN 201610001295 A CN201610001295 A CN 201610001295A CN 105523537 A CN105523537 A CN 105523537A
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bamboo charcoal
kiln
vacuum
bamboo
charcoal
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CN201610001295.3A
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Chinese (zh)
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马俊吉
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Individual
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Priority to CN201610001295.3A priority Critical patent/CN105523537A/en
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    • YGENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
    • Y02TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
    • Y02PCLIMATE CHANGE MITIGATION TECHNOLOGIES IN THE PRODUCTION OR PROCESSING OF GOODS
    • Y02P20/00Technologies relating to chemical industry
    • Y02P20/10Process efficiency
    • Y02P20/129Energy recovery, e.g. by cogeneration, H2recovery or pressure recovery turbines

Abstract

The present invention discloses a method for vacuum calcination of bamboo charcoal in a tunneling kiln, steps are as follows: 3-5 years old mao bamboos are cut into segments according to specifications, then the segments are packed into a bowl, and dried in a drying hole at 0 DEG C-350 DEG C, a bamboo vinegar liquid is extracted in the drying process, after the drying, the segments are buried and filled into rice husks or refractory materials for vacuum treatment, then fired at 1000 DEG C to 1300 DEG C for 36 hours to 60 hours, and cooled to obtain the bamboo charcoal, and the bamboo charcoal is calcined in the tunneling kiln in vacuum way, the bamboo charcoal can be extensively developed in south places rich in mao bamboos, and the bamboo charcoal can play a unique role in all fields, and can play inestimable value especially in environmental protection. The charcoal yield can reach 30%-45%, compared with the traditional process, the charcoal yield is improved by 10%-15%, the method is simple and easy in temperature control, product quality is stable, the failure rate is reduced, the method is environmentally-friendly and energy-saving, can effectively use lands, has a cycle of 3-5 years, and continuous development can be achieved.

Description

A kind of method of tunnel furnace vacuum calcining bamboo charcoal
Technical field
The present invention relates to a kind of method of tunnel furnace vacuum calcining bamboo charcoal.
Background technology
At present, China's bamboo carbon mode of production perplexs this product and breaks through, although aboundresources, production technique still adopts old-fashioned technique, application earth kiln production method, and production quantity, produces carbon rate, and quality product is subject to affecting in various degree can not continuous seepage.The effect of production in enormous quantities scale can not be reached, waste energy again.Environmental protection is had a strong impact on, and novel appts also cannot improve output, the developing of puzzlement bamboo charcoal product and development.Carbonization method and the direct firing process of earth kiln two kinds of bamboo charcoal preparation methods are mainly contained in prior art.
Carbonization method can use predry to water ratio to be the bamboo wood of 20% ~ 25%, also can use the bamboo wood without predry, but to use the bamboo wood through predry to be good.Owing to substantially there is not bamboo charcoal problem of oxidation in sintering procedure, therefore bamboo charcoal yield is higher, is generally about 25%, Gao Zheke and reaches 35%.But refining temperature is carried not high, affect bamboo charcoal density; Retort volume is little, and bamboo charcoal yields poorly.
Earth kiln firing process has predrying, dry, the pre-charing of sootiness, charing, the calcining stage such as (refining), naturally cooling usually.There is different temperature in each stage, and sootiness pre-drying phase is 60 ~ 100 DEG C, and drying stage is 100 ~ 150 DEG C, and pre-carbonization stage is 150 ~ 270 DEG C, and carbonization stage is 270 ~ 450 DEG C, and calcination stage is 450 DEG C to about 1000 DEG C.From the process that earth kiln is made charcoal, the temperature in each stage and charing rate " observe nasil " by operator, and one is the change observing chimney and wicket smoke outlet cigarette; Two is determine by hearing smoke.The fresh mao bamboon of earth kiln, generally outdoor placement about a week, putting into kiln, to carry out sootiness predrying, and approximately want 1 week, and also need one week when naturally cooling to kilneye temperature 50 ~ 60 DEG C, kiln discharge generally also takes 2 days.So generally take 25 ~ 30 days from loading of kiln to going out charcoal, bamboo charcoal yield is generally about 20%.But the amount of later stage oxidizing fire can lower than 20%, even lower (bleed because of air or air capacity enters excessive).Earth kiln low cost, refining temperature is high, and bamboo charcoal density is large, but quality stability is poor, and yield is not high.
Therefore, prior art needs further improvement and develops.
Summary of the invention
In view of above-mentioned the deficiencies in the prior art, the object of the present invention is to provide a kind of method of tunnel furnace vacuum calcining bamboo charcoal, under the prerequisite ensureing bamboo charcoal burning quality, carry high carbon output rate.
For solving the problems of the technologies described above, technical solution of the present invention comprises:
A method for tunnel furnace vacuum calcining bamboo charcoal, it comprises the following steps:
A, by the setation bamboo of 3-5 fell after be cut into multiple mao bamboon section according to alms bowl (kiln) the tool specification in kiln car, mao bamboon section is put into the alms bowl tool of kiln car, utilize residual heat of tunnel kiln 0 DEG C of-350 DEG C of condition in tunnel furnace drying hole under, carries out drying;
B, dried kiln car is carried out vacuum-treat, with rice husk or refractory materials mao bamboon in alms bowl tool buried and enter the stage of burning till, carry out the process of vacuum kiln;
C, under 1000 DEG C of-1300 DEG C of conditions, fire 36 hours-60 hours, obtain bamboo charcoal by after the kiln car cooling in tunnel furnace.
Described method, wherein, concrete also the comprising of above-mentioned steps A: be all furnished with recycling pipeline in each kiln car, recycling pipeline is for extracting the bamboo vinegar liquid produced in mao bamboon drying process.
Described method, wherein, above-mentioned steps C also comprises: by bamboo charcoal vacuum packaging, and carries out mark according to the kind of simple carbon, sheet carbon, broken carbon and powder carbon.
The method of a kind of tunnel furnace vacuum calcining bamboo charcoal provided by the invention, tunnel furnace vacuum mode is utilized to calcine bamboo charcoal, the ground extensive exploitation of mao bamboon can be abounded with in south, bamboo charcoal can play its unique effect in every field, especially in environmental protection, immeasurable value is played, its method is simple, is convenient to temperature and controls, and producing carbon rate can reach.Tunnel furnace vacuum forging bamboo charcoal, is convenient to temperature and controls, and produces carbon rate and can arrive 30%-40%, and produce carbon rate compared to traditional technology and can improve about 10%, constant product quality, disqualification rate reduces, and utilizes soil within 3-5 years, to be the cycle, can growth and development continuously.
Embodiment
The invention provides a kind of method of tunnel furnace vacuum calcining bamboo charcoal, for making object of the present invention, technical scheme and effect clearly, clearly, the present invention is described in more detail below.Should be appreciated that specific embodiment described herein only in order to explain the present invention, be not intended to limit the present invention.
The invention provides a kind of method of tunnel furnace vacuum calcining bamboo charcoal, it comprises the following steps:
Step one, is cut into multiple mao bamboon section according to alms bowl (kiln) the tool specification in kiln car after being felled by the setation bamboo of 3-5, mao bamboon section is put into the alms bowl tool of kiln car, carry out drying under utilizing residual heat of tunnel kiln 0 DEG C of-350 DEG C of condition in tunnel furnace drying hole;
Step 2, carries out vacuum-treat by dried kiln car, to be buried by mao bamboon in alms bowl tool and enters the stage of burning till, carry out the process of vacuum kiln with rice husk or refractory materials;
Step 3, moves into the kiln car of vacuum kiln process in tunnel furnace, fires 48 hours-72 hours under 1000 DEG C of-1500 DEG C of conditions, obtains bamboo charcoal by after the kiln car cooling in tunnel furnace.
In another preferred embodiment of the present invention, concrete also the comprising of above-mentioned steps one: be all furnished with recycling pipeline in each kiln car, recycling pipeline is for extracting the bamboo vinegar liquid produced in mao bamboon drying process.
And above-mentioned steps three also comprises: by bamboo charcoal vacuum packaging, and carry out mark according to the kind of simple carbon, sheet carbon, broken carbon and powder carbon.
Certainly; more than illustrate and be only preferred embodiment of the present invention; the present invention is not limited to enumerate above-described embodiment; should be noted that; any those of ordinary skill in the art are under the instruction of this specification sheets; made all equivalently to substitute, obvious variant, within the essential scope all dropping on this specification sheets, protection of the present invention ought to be subject to.

Claims (3)

1. a method for tunnel furnace vacuum calcining bamboo charcoal, it comprises the following steps:
A, by the setation bamboo of 3-5 fell after be cut into multiple mao bamboon section according to the alms bowl tool specification in kiln car, mao bamboon section is put into the alms bowl tool of kiln car, utilize residual heat of tunnel kiln 0 DEG C of-350 DEG C of condition in tunnel furnace drying hole under, carries out drying;
B, dried kiln car is carried out vacuum-treat, with rice husk or refractory materials mao bamboon in alms bowl tool buried and enter the stage of burning till, carry out the process of vacuum kiln;
C, under 1000 DEG C of-1300 DEG C of conditions, fire 36 hours-60 hours, obtain bamboo charcoal by after the kiln car cooling in tunnel furnace.
2. method according to claim 1, is characterized in that, concrete also the comprising of above-mentioned steps A: be all furnished with recycling pipeline in each kiln car, and recycling pipeline is for extracting the bamboo vinegar liquid produced in mao bamboon drying process.
3. method according to claim 1, is characterized in that, above-mentioned steps C also comprises: by bamboo charcoal vacuum packaging, and carries out mark according to the kind of simple carbon, sheet carbon, broken carbon and powder carbon.
CN201610001295.3A 2016-01-05 2016-01-05 Method for vacuum calcination of bamboo charcoal in tunneling kiln Pending CN105523537A (en)

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Application Number Priority Date Filing Date Title
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Cited By (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN110655058A (en) * 2019-10-24 2020-01-07 深圳市松博宇科技股份有限公司 Preparation method of electrostatic dissipation biological material and electrostatic removal plate prepared by same

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CN1075495A (en) * 1992-02-17 1993-08-25 四川省林业科学研究院 The charing method of fuel stick
CN101683980A (en) * 2008-09-24 2010-03-31 上海市长宁区少年科技指导站 Method for preparing bamboo charcoal capable of removing smell by utilizing waste bamboo chopsticks
CN101921604A (en) * 2010-08-30 2010-12-22 浙江建中竹业科技有限公司 Dry distillation charring method for bamboos
CN102442663A (en) * 2010-10-08 2012-05-09 宁夏宝塔石化集团有限公司 Mechanized production process for activated carbon
CN105174257A (en) * 2015-05-31 2015-12-23 浙江富来森能源科技有限公司 Roller-type multi-temperature section continuous production tunnel kiln

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* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN1075495A (en) * 1992-02-17 1993-08-25 四川省林业科学研究院 The charing method of fuel stick
CN101683980A (en) * 2008-09-24 2010-03-31 上海市长宁区少年科技指导站 Method for preparing bamboo charcoal capable of removing smell by utilizing waste bamboo chopsticks
CN101921604A (en) * 2010-08-30 2010-12-22 浙江建中竹业科技有限公司 Dry distillation charring method for bamboos
CN102442663A (en) * 2010-10-08 2012-05-09 宁夏宝塔石化集团有限公司 Mechanized production process for activated carbon
CN105174257A (en) * 2015-05-31 2015-12-23 浙江富来森能源科技有限公司 Roller-type multi-temperature section continuous production tunnel kiln

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张文标等: "《竹炭.竹醋液的生产与应用》", 30 April 2006 *
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Cited By (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN110655058A (en) * 2019-10-24 2020-01-07 深圳市松博宇科技股份有限公司 Preparation method of electrostatic dissipation biological material and electrostatic removal plate prepared by same
CN110655058B (en) * 2019-10-24 2023-10-03 深圳市松博宇科技股份有限公司 Preparation method of static dissipation biological material and static removal plate prepared by preparation method

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