CN105502948A - Antimicrobial red glaze and preparation and application methods thereof - Google Patents
Antimicrobial red glaze and preparation and application methods thereof Download PDFInfo
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- CN105502948A CN105502948A CN201510973378.4A CN201510973378A CN105502948A CN 105502948 A CN105502948 A CN 105502948A CN 201510973378 A CN201510973378 A CN 201510973378A CN 105502948 A CN105502948 A CN 105502948A
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- glaze
- red
- kojic acid
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Classifications
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- C—CHEMISTRY; METALLURGY
- C03—GLASS; MINERAL OR SLAG WOOL
- C03C—CHEMICAL COMPOSITION OF GLASSES, GLAZES OR VITREOUS ENAMELS; SURFACE TREATMENT OF GLASS; SURFACE TREATMENT OF FIBRES OR FILAMENTS MADE FROM GLASS, MINERALS OR SLAGS; JOINING GLASS TO GLASS OR OTHER MATERIALS
- C03C8/00—Enamels; Glazes; Fusion seal compositions being frit compositions having non-frit additions
- C03C8/14—Glass frit mixtures having non-frit additions, e.g. opacifiers, colorants, mill-additions
-
- C—CHEMISTRY; METALLURGY
- C04—CEMENTS; CONCRETE; ARTIFICIAL STONE; CERAMICS; REFRACTORIES
- C04B—LIME, MAGNESIA; SLAG; CEMENTS; COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDING MATERIALS; ARTIFICIAL STONE; CERAMICS; REFRACTORIES; TREATMENT OF NATURAL STONE
- C04B41/00—After-treatment of mortars, concrete, artificial stone or ceramics; Treatment of natural stone
- C04B41/45—Coating or impregnating, e.g. injection in masonry, partial coating of green or fired ceramics, organic coating compositions for adhering together two concrete elements
- C04B41/50—Coating or impregnating, e.g. injection in masonry, partial coating of green or fired ceramics, organic coating compositions for adhering together two concrete elements with inorganic materials
- C04B41/5025—Coating or impregnating, e.g. injection in masonry, partial coating of green or fired ceramics, organic coating compositions for adhering together two concrete elements with inorganic materials with ceramic materials
- C04B41/5037—Clay, Kaolin
- C04B41/504—Engobes
-
- C—CHEMISTRY; METALLURGY
- C04—CEMENTS; CONCRETE; ARTIFICIAL STONE; CERAMICS; REFRACTORIES
- C04B—LIME, MAGNESIA; SLAG; CEMENTS; COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDING MATERIALS; ARTIFICIAL STONE; CERAMICS; REFRACTORIES; TREATMENT OF NATURAL STONE
- C04B41/00—After-treatment of mortars, concrete, artificial stone or ceramics; Treatment of natural stone
- C04B41/80—After-treatment of mortars, concrete, artificial stone or ceramics; Treatment of natural stone of only ceramics
- C04B41/81—Coating or impregnation
- C04B41/85—Coating or impregnation with inorganic materials
- C04B41/86—Glazes; Cold glazes
-
- C—CHEMISTRY; METALLURGY
- C03—GLASS; MINERAL OR SLAG WOOL
- C03C—CHEMICAL COMPOSITION OF GLASSES, GLAZES OR VITREOUS ENAMELS; SURFACE TREATMENT OF GLASS; SURFACE TREATMENT OF FIBRES OR FILAMENTS MADE FROM GLASS, MINERALS OR SLAGS; JOINING GLASS TO GLASS OR OTHER MATERIALS
- C03C2204/00—Glasses, glazes or enamels with special properties
- C03C2204/02—Antibacterial glass, glaze or enamel
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- Chemical & Material Sciences (AREA)
- Engineering & Computer Science (AREA)
- Ceramic Engineering (AREA)
- Materials Engineering (AREA)
- Organic Chemistry (AREA)
- Inorganic Chemistry (AREA)
- Structural Engineering (AREA)
- Life Sciences & Earth Sciences (AREA)
- Chemical Kinetics & Catalysis (AREA)
- General Chemical & Material Sciences (AREA)
- Geochemistry & Mineralogy (AREA)
- Cosmetics (AREA)
Abstract
The invention relates to antimicrobial red glaze used in a toilet. The antimicrobial red glaze comprises components of raw materials in parts by weight as follows: 25-30 parts of potassium feldspar, 19-24 parts of white mica, 4-7 parts of serpentine, 13-16 parts of talc, 8-11 parts of niter, 6-10 parts of manganese ore, 5-9 parts of kojic dipalmitate, 9-13 parts of kojic acid, 0.3-0.6 parts of sodium sulfite, 2-6 parts of pyroligneous acid, 2-4 parts of ferric chloride, 1-3 parts of lead oxide and 3-5 parts of copper oxide. The invention further relates to preparation and application methods of the glaze. A ceramic product which is prepared from the antimicrobial red glaze and has bright red glazing color is bright and stable in color and has an excellent decorative effect, an antimicrobial function and an inhibition effect on microbial growth and reproduction, the firing temperature is low, the energy-saving effect is good, and the production cost is greatly reduced.
Description
Technical field
The present invention relates to ceramic glaze technical field, more specifically, relate to a kind of antimicrobial red glaze and preparation and application thereof.
Background technology
For the pottery of kitchen guarding aspect, as ceramic tile, sitting wc pan etc., due to many-sided factors such as environments for use, frequent contact dirt sewage, the very easily microorganism such as breed bacteria, and it is closely bound up with people's daily life, as kitchen tile is related to the diet of people, sitting wc pan especially with direct body contact, the bacterium grown then directly can endanger the health of people.By frequently using antibiosis and sterilization agent to come wiping cleaning ceramic surface, one bothers, and two carry out life-time service can damage ceramic surface and cause its service life reduction, and three can only eliminate microbial bacterial instantly, cannot provide long-term and suppress and protection.
Ceramic glaze is the requisite finishing material of ceramic, along with growth in the living standard, people are except having certain requirement to the functional of pottery, also more and more higher to the pursuit of the decorative effects such as color, although the research technically for color glaze is ripe gradually, but possess the ceramic colour glaze of antimicrobial function, be still in space state at present.
Summary of the invention
The object of the invention is to overcome the deficiencies in the prior art, provide a kind of color glaze, its glaze colours is large red, and evenly, elegant, has sight to jade-like stone profit, and has antimicrobial property.
The preparation and application of this antimicrobial red glaze is provided simultaneously.
The object of the invention is achieved by the following technical programs:
There is provided a kind of antimicrobial red glaze, raw material comprises following component according to weight part: potassium felspar sand 25 ~ 30 parts, white mica 19 ~ 24 parts, 4 ~ 7 parts, serpentine, 13 ~ 16 parts, talcum, 8 ~ 11 parts, nitre, 6 ~ 10 parts, manganese stone, Kojic Acid Dipalmitate 5 ~ 9 parts, kojic acid 9 ~ 13 parts, S-WAT 0.3 ~ 0.6 part, 2 ~ 6 parts, wood vinegar, 2 ~ 4 parts, iron(ic) chloride, 1 ~ 3 part, plumbous oxide, cupric oxide 3 ~ 5 parts.
Preferably, raw material comprises following component according to weight part: potassium felspar sand 27 parts, white mica 21 parts, 5 parts, serpentine, 14 parts, talcum, 10 parts, nitre, 9 parts, manganese stone, Kojic Acid Dipalmitate 7 parts, kojic acid 11 parts, S-WAT 0.4 part, 5 parts, wood vinegar, 3 parts, iron(ic) chloride, 2 parts, plumbous oxide, cupric oxide 4 parts.
Present invention also offers the preparation method of above-mentioned antimicrobial red glaze, by potassium felspar sand, white mica, serpentine, talcum, nitre, manganese stone by weight mixing, successively through coarse crushing, in small, broken bits, grinding, cross 200 mesh sieves; Add Kojic Acid Dipalmitate more by weight, kojic acid, S-WAT, iron(ic) chloride, plumbous oxide, cupric oxide mix, obtain dry powder; Dry powder and water are mixed according to weight ratio 100:65 ~ 75, crosses 300 mesh sieves, then add wood vinegar and mix, obtain antimicrobial red glaze.
Present invention also offers the using method of above-mentioned antimicrobial red glaze, adopt glaze spraying or leaching glaze mode glaze to be imposed on the billet surface of forming, enter 600 ~ 780 DEG C, kiln and fire 7 ~ 9 hours, naturally cool to room temperature.
Compared with prior art, the present invention has following beneficial effect: have employed distinctive composition and engineering, and kojic acid is combined with iron(ic) chloride has color development effect, Kojic Acid Dipalmitate has color-protecting function, obtained glaze colours is the ceramic bowl of large red, and bright in colour stable, decorative effect is fabulous; Possess antimicrobial function, restraining effect is played to microbial growth and breeding; Firing temperature is low, good energy-conserving effect, greatly reduces production cost.
Embodiment
Below in conjunction with specific embodiment, the present invention is further illustrated.Toilet base substrate in ceramic tile blank in embodiment 1 ~ 3 and embodiment 4 ~ 6 is the biscuit that commercially available ceramic batch is fired.Unless stated otherwise, the technique that the embodiment of the present invention adopts is the technique that this area routine uses.
Embodiment 1
By weight by potassium felspar sand 30 parts, white mica 24 parts, 7 parts, serpentine, 16 parts, talcum, 11 parts, nitre, the mixing of 10 parts, manganese stone, successively through coarse crushing, in small, broken bits, grinding, crosses 200 mesh sieves; Add Kojic Acid Dipalmitate 5 parts more by weight, kojic acid 9 parts, S-WAT 0.3 part, 2 parts, iron(ic) chloride, 1 part, plumbous oxide, cupric oxide 3 parts mixes, and obtains dry powder; Dry powder and water are mixed according to weight ratio 100:75, crosses 300 mesh sieves, then add 2 parts, wood vinegar, mix, obtain antimicrobial red glaze.
Leaching glaze mode is adopted glaze to be imposed on the ceramic tile blank surface of forming, enter 600 DEG C, kiln and fire 7 hours, obtain the red tile with anti-microbial effect, ceramic tile surface is bright-coloured large red, color and luster jade-like stone profit evenly, color development is stablized, and decorative effect is extremely strong, and inhibited with breeding to microbial growth.
Embodiment 2
By weight by potassium felspar sand 29 parts, white mica 20 parts, 5 parts, serpentine, 14 parts, talcum, 10 parts, nitre, the mixing of 8 parts, manganese stone, successively through coarse crushing, in small, broken bits, grinding, crosses 200 mesh sieves; Add Kojic Acid Dipalmitate 7 parts more by weight, kojic acid 12 parts, S-WAT 0.4 part, 4 parts, iron(ic) chloride, 1 part, plumbous oxide, cupric oxide 5 parts mixes, and obtains dry powder; Dry powder and water are mixed according to weight ratio 100:68, crosses 300 mesh sieves, then add 5 parts, wood vinegar, mix, obtain antimicrobial red glaze.
Leaching glaze mode is adopted glaze to be imposed on the ceramic tile blank surface of forming, enter 650 DEG C, kiln and fire 8 hours, obtain the red tile with anti-microbial effect, ceramic tile surface is bright-coloured large red, color and luster jade-like stone profit evenly, color development is stablized, and decorative effect is extremely strong, and inhibited with breeding to microbial growth.
Embodiment 3
By weight by potassium felspar sand 26 parts, white mica 21 parts, 6 parts, serpentine, 13 parts, talcum, 11 parts, nitre, the mixing of 7 parts, manganese stone, successively through coarse crushing, in small, broken bits, grinding, crosses 200 mesh sieves; Add Kojic Acid Dipalmitate 8 parts more by weight, kojic acid 11 parts, S-WAT 0.6 part, 3.5 parts, iron(ic) chloride, 1.5 parts, plumbous oxide, cupric oxide 4.5 parts mixes, and obtains dry powder; Dry powder and water are mixed according to weight ratio 100:68, crosses 300 mesh sieves, then add 6 parts, wood vinegar, mix, obtain antimicrobial red glaze.
Leaching glaze mode is adopted glaze to be imposed on the ceramic tile blank surface of forming, enter 680 DEG C, kiln and fire 7.5 hours, obtain the red tile with anti-microbial effect, ceramic tile surface is bright-coloured large red, color and luster jade-like stone profit evenly, color development is stablized, and decorative effect is extremely strong, and inhibited with breeding to microbial growth.
Embodiment 4
By weight by potassium felspar sand 27 parts, white mica 21 parts, 5 parts, serpentine, 14 parts, talcum, 10 parts, nitre, the mixing of 9 parts, manganese stone, successively through coarse crushing, in small, broken bits, grinding, crosses 200 mesh sieves; Add Kojic Acid Dipalmitate 7 parts more by weight, kojic acid 11 parts, S-WAT 0.4 part, 3 parts, iron(ic) chloride, 2 parts, plumbous oxide, cupric oxide 4 parts mixes, and obtains dry powder; Dry powder and water are mixed according to weight ratio 100:70, crosses 300 mesh sieves, then add 5 parts, wood vinegar, mix, obtain antimicrobial red glaze.
Glaze spraying mode is adopted glaze to be imposed on the toilet billet surface of forming, enter 700 DEG C, kiln and fire 8 hours, obtain the red toilet with anti-microbial effect, toilet surface is bright-coloured large red, color and luster jade-like stone profit evenly, color development is stablized, and decorative effect is extremely strong, and inhibited with breeding to microbial growth.
Embodiment 5
By weight by potassium felspar sand 25 parts, white mica 19 parts, 4 parts, serpentine, 13 parts, talcum, 8 parts, nitre, the mixing of 6 parts, manganese stone, successively through coarse crushing, in small, broken bits, grinding, crosses 200 mesh sieves; Add Kojic Acid Dipalmitate 9 parts more by weight, kojic acid 13 parts, S-WAT 0.6 part, 4 parts, iron(ic) chloride, 3 parts, plumbous oxide, cupric oxide 5 parts mixes, and obtains dry powder; Dry powder and water are mixed according to weight ratio 100:65, crosses 300 mesh sieves, then add 6 parts, wood vinegar, mix, obtain antimicrobial red glaze.
Glaze spraying mode is adopted glaze to be imposed on the toilet billet surface of forming, enter 780 DEG C, kiln and fire 9 hours, obtain the red toilet with anti-microbial effect, toilet surface is bright-coloured large red, color and luster jade-like stone profit evenly, color development is stablized, and decorative effect is extremely strong, and inhibited with breeding to microbial growth.
Embodiment 6
By weight by potassium felspar sand 28 parts, white mica 23 parts, 5 parts, serpentine, 14 parts, talcum, 9 parts, nitre, the mixing of 7 parts, manganese stone, successively through coarse crushing, in small, broken bits, grinding, crosses 200 mesh sieves; Add Kojic Acid Dipalmitate 6 parts more by weight, kojic acid 11 parts, S-WAT 0.4 part, 3.5 parts, iron(ic) chloride, 1.5 parts, plumbous oxide, cupric oxide 3.5 parts mixes, and obtains dry powder; Dry powder and water are mixed according to weight ratio 100:72, crosses 300 mesh sieves, then add 3 parts, wood vinegar, mix, obtain the antimicrobial red glaze for toilet.
Glaze spraying mode is adopted glaze to be imposed on the toilet billet surface of forming, enter 720 DEG C, kiln and fire 7.5 hours, obtain the red toilet with anti-microbial effect, toilet surface is bright-coloured large red, color and luster jade-like stone profit evenly, color development is stablized, and decorative effect is extremely strong, and inhibited with breeding to microbial growth.
Tested by ceramic tile obtained by embodiment 1 ~ 3, the microbial suspension 0.5ml got containing streptococcus aureus is coated in product surface respectively, and the streptococcus aureus of suspension is about 10
6~ 10
7individual/ml, at room temperature places the different time, then tests, and determines that the residue microbe population of still surviving accounts for the ratio of initial microbial population, the percentages namely shown in form.Test result is as shown in the table:
Tested by toilet obtained by embodiment 4 ~ 6, get and be coated in product surface respectively containing colibacillary microbial suspension 0.5ml, the intestinal bacteria of suspension are about 10
6~ 10
7individual/ml, at room temperature places the different time, then tests, and determines that the residue microbe population of still surviving accounts for the ratio of initial microbial population, the percentages namely shown in form.Test result is as shown in the table:
From test result, the toilet obtained by embodiment 1 ~ 6 possesses antimicrobial property, can avoid breed bacteria, plays good protection effect to HUMAN HEALTH.
Claims (4)
1. an antimicrobial red glaze, is characterized in that, raw material comprises following component according to weight percent: potassium felspar sand 25 ~ 30 parts, white mica 19 ~ 24 parts, 4 ~ 7 parts, serpentine, 13 ~ 16 parts, talcum, 8 ~ 11 parts, nitre, 6 ~ 10 parts, manganese stone, Kojic Acid Dipalmitate 5 ~ 9 parts, kojic acid 9 ~ 13 parts, S-WAT 0.3 ~ 0.6 part, 2 ~ 6 parts, wood vinegar, 2 ~ 4 parts, iron(ic) chloride, 1 ~ 3 part, plumbous oxide, cupric oxide 3 ~ 5 parts.
2. antimicrobial red glaze according to claim 1, is characterized in that, raw material comprises following component according to weight percent: potassium felspar sand 27 parts, white mica 21 parts, 5 parts, serpentine, 14 parts, talcum, 10 parts, nitre, 9 parts, manganese stone, Kojic Acid Dipalmitate 7 parts, kojic acid 11 parts, S-WAT 0.4 part, 5 parts, wood vinegar, 3 parts, iron(ic) chloride, 2 parts, plumbous oxide, cupric oxide 4 parts.
3. the preparation method of the antimicrobial red glaze described in claim 1 ~ 2, is characterized in that, by potassium felspar sand, white mica, serpentine, talcum, nitre, manganese stone by weight mixing, successively through coarse crushing, in small, broken bits, grinding, crosses 200 mesh sieves; Add Kojic Acid Dipalmitate more by weight, kojic acid, S-WAT, iron(ic) chloride, plumbous oxide, cupric oxide mix, obtain dry powder; Dry powder and water are mixed according to weight ratio 100:65 ~ 75, crosses 300 mesh sieves, then add wood vinegar and mix, obtain antimicrobial red glaze.
4. the using method of antimicrobial red glaze according to claim 1, is characterized in that, glaze spraying or leaching glaze mode can be adopted glaze to be imposed on the billet surface of forming, enter 600 ~ 780 DEG C, kiln and fire 7 ~ 9 hours, naturally cool to room temperature.
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Cited By (4)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN107226620A (en) * | 2017-05-18 | 2017-10-03 | 东北大学 | A kind of orange red have glazing type material of tangerine peel texture and preparation method thereof |
CN109896745A (en) * | 2019-04-04 | 2019-06-18 | 福建省德化县哈维陶瓷有限公司 | A kind of Sub-shine glaze and its manufacture craft |
CN110217990A (en) * | 2019-07-17 | 2019-09-10 | 福建省德化县鹏欣陶瓷有限公司 | A kind of red glaze and preparation method thereof |
CN112429968A (en) * | 2020-12-28 | 2021-03-02 | 湖州南浔百迪电子商务有限公司 | Antibacterial glaze for bathroom products and preparation method thereof |
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CN104355678A (en) * | 2014-10-28 | 2015-02-18 | 山东中大药业有限公司 | Anion far-infrared ecological antibacterial healthcare ceramic glaze and preparation method thereof |
CN105036804A (en) * | 2015-06-16 | 2015-11-11 | 德化均能手造陶瓷有限公司 | Health-preserving antimicrobial ceramic glaze |
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CN1337379A (en) * | 2001-09-04 | 2002-02-27 | 武汉理工大学 | Infrared radiation ceramic glaze layer with bacteriostasis function and its prepn process |
US20050196430A1 (en) * | 2004-01-21 | 2005-09-08 | Microban Products Company | Antimicrobial enamel glaze |
KR20060022797A (en) * | 2004-09-08 | 2006-03-13 | 동서산업주식회사 | Composition for glaze having anion emitting function, far infrared ray radiating function, germicidal function and manufacturing method thereof |
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Cited By (4)
Publication number | Priority date | Publication date | Assignee | Title |
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CN107226620A (en) * | 2017-05-18 | 2017-10-03 | 东北大学 | A kind of orange red have glazing type material of tangerine peel texture and preparation method thereof |
CN109896745A (en) * | 2019-04-04 | 2019-06-18 | 福建省德化县哈维陶瓷有限公司 | A kind of Sub-shine glaze and its manufacture craft |
CN110217990A (en) * | 2019-07-17 | 2019-09-10 | 福建省德化县鹏欣陶瓷有限公司 | A kind of red glaze and preparation method thereof |
CN112429968A (en) * | 2020-12-28 | 2021-03-02 | 湖州南浔百迪电子商务有限公司 | Antibacterial glaze for bathroom products and preparation method thereof |
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