CN105466819A - Spectrum film manufacturing method and spectrum film - Google Patents
Spectrum film manufacturing method and spectrum film Download PDFInfo
- Publication number
- CN105466819A CN105466819A CN201610042117.5A CN201610042117A CN105466819A CN 105466819 A CN105466819 A CN 105466819A CN 201610042117 A CN201610042117 A CN 201610042117A CN 105466819 A CN105466819 A CN 105466819A
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- China
- Prior art keywords
- spectral slice
- making
- substrate
- lines
- slice method
- Prior art date
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- 238000004519 manufacturing process Methods 0.000 title abstract description 17
- 238000001228 spectrum Methods 0.000 title abstract description 9
- 238000000034 method Methods 0.000 claims abstract description 35
- 239000000084 colloidal system Substances 0.000 claims abstract description 32
- 239000000758 substrate Substances 0.000 claims abstract description 31
- 239000002562 thickening agent Substances 0.000 claims abstract description 26
- 239000003960 organic solvent Substances 0.000 claims abstract description 23
- 238000002360 preparation method Methods 0.000 claims abstract description 4
- 230000003595 spectral effect Effects 0.000 claims description 45
- 239000003513 alkali Substances 0.000 claims description 5
- 125000000129 anionic group Chemical group 0.000 claims description 5
- 230000008961 swelling Effects 0.000 claims description 5
- 238000001035 drying Methods 0.000 abstract description 4
- 238000004458 analytical method Methods 0.000 abstract description 2
- XEEYBQQBJWHFJM-UHFFFAOYSA-N Iron Chemical compound [Fe] XEEYBQQBJWHFJM-UHFFFAOYSA-N 0.000 description 6
- 239000011521 glass Substances 0.000 description 3
- 229910052742 iron Inorganic materials 0.000 description 3
- 231100000252 nontoxic Toxicity 0.000 description 2
- 230000003000 nontoxic effect Effects 0.000 description 2
- 239000004809 Teflon Substances 0.000 description 1
- 229920006362 Teflon® Polymers 0.000 description 1
- 239000012752 auxiliary agent Substances 0.000 description 1
- 230000009286 beneficial effect Effects 0.000 description 1
- 238000005260 corrosion Methods 0.000 description 1
- 230000007797 corrosion Effects 0.000 description 1
- 238000001514 detection method Methods 0.000 description 1
- 238000007865 diluting Methods 0.000 description 1
- 239000000428 dust Substances 0.000 description 1
- 230000000694 effects Effects 0.000 description 1
- 238000005516 engineering process Methods 0.000 description 1
- 230000007613 environmental effect Effects 0.000 description 1
- 230000007774 longterm Effects 0.000 description 1
- 230000001105 regulatory effect Effects 0.000 description 1
- 238000000518 rheometry Methods 0.000 description 1
- 239000000126 substance Substances 0.000 description 1
- 230000008719 thickening Effects 0.000 description 1
- 239000002699 waste material Substances 0.000 description 1
Classifications
-
- G—PHYSICS
- G01—MEASURING; TESTING
- G01N—INVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
- G01N15/00—Investigating characteristics of particles; Investigating permeability, pore-volume or surface-area of porous materials
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B05—SPRAYING OR ATOMISING IN GENERAL; APPLYING FLUENT MATERIALS TO SURFACES, IN GENERAL
- B05D—PROCESSES FOR APPLYING FLUENT MATERIALS TO SURFACES, IN GENERAL
- B05D3/00—Pretreatment of surfaces to which liquids or other fluent materials are to be applied; After-treatment of applied coatings, e.g. intermediate treating of an applied coating preparatory to subsequent applications of liquids or other fluent materials
- B05D3/02—Pretreatment of surfaces to which liquids or other fluent materials are to be applied; After-treatment of applied coatings, e.g. intermediate treating of an applied coating preparatory to subsequent applications of liquids or other fluent materials by baking
- B05D3/0254—After-treatment
Landscapes
- Chemical & Material Sciences (AREA)
- Dispersion Chemistry (AREA)
- Physics & Mathematics (AREA)
- Health & Medical Sciences (AREA)
- Life Sciences & Earth Sciences (AREA)
- Analytical Chemistry (AREA)
- Biochemistry (AREA)
- General Health & Medical Sciences (AREA)
- General Physics & Mathematics (AREA)
- Immunology (AREA)
- Pathology (AREA)
- Investigating Or Analysing Materials By Optical Means (AREA)
Abstract
The invention relates to the field of ferrographic analysis systems and particularly discloses a spectrum film manufacturing method and a spectrum film. The spectrum film manufacturing method comprises the steps that organic solvent and a thickening agent are mixed into organic colloid; a dispenser is adopted for dotting lines on a substrate with the organic colloid; the substrate is baked. According to the spectrum film manufacturing method, the organic colloid is used for manufacturing the lines, and compared with traditional organic solvent, drying is easier; the dispenser is used for dotting the lines, the manufacturing speed is higher than that of a traditional method of dotting the lines manually, uniformity is good, and the requirement for batch preparation can be met; baking is only carried out once, compared with the traditional mode of carrying out baking twice, spectrum film manufacturing time is shortened, product yield is greatly increased, and product quality is greatly improved.
Description
[technical field]
The present invention relates to analyzing iron spectrum system regions, particularly relate to the making of spectral slice.
[background technology]
At present, the production method of iron spectral slice is by oil sample to be measured after organic solvent diluting, with pen by positioning fixture dot-dash U-shaped lines on the glass sheet, adopts the roasting mode of high temperature after first low temperature, toast at a constant temperature at twice after drying.This method speed of production by the manual U-shaped lines of dot-dash is on the glass sheet slow and outward appearance consistance is poor, and have higher requirement to the operation skill of producers, baking time is longer, and product yield is lower.
[summary of the invention]
The speed of production that the present invention is intended to solve traditional spectral slice method for making is slow, and outward appearance consistance is poor, and the shortcoming such as yield poorly, and provide a kind of spectral slice method for making and spectral slice of improvement, technical scheme is as follows:
On the one hand, the invention provides a kind of spectral slice method for making, comprising:
Organic solvent and thickening agent are deployed into organic colloid;
Adopt point gum machine by described organic colloid dot-dash lines on substrate;
Toast described substrate.
In certain embodiments, described organic solvent is polytetrafluoroethylsolution solution.
In certain embodiments, described thickening agent is anionic hydrophobically-modified alkali swelling type thickening agent.
In certain embodiments, the ratio range of described organic solvent and described thickening agent is 100:(0.5-1.5).
In certain embodiments, described point gum machine is automatic dispensing machine.
In certain embodiments, adopt point gum machine by before the step of described organic colloid dot-dash lines on substrate, described spectral slice method for making also comprises: the dimensional requirement of point gum machine according to described lines programmed.
In certain embodiments, before toasting the step of described substrate, described spectral slice method for making also comprises: dry and/or dry described substrate.
In certain embodiments, toast in the step of described substrate, the temperature range of baking is 360-430 DEG C.
In certain embodiments, toast in the step of described substrate, the time range of baking is 8-15 minute.
On the other hand, the invention provides a kind of spectral slice, described spectral slice is made based on above-described spectral slice method for making.
The beneficial effect of the specific embodiment of the invention is, spectral slice method for making provided by the invention, uses organic colloid to make lines, compared to traditional organic solvent, more easily dry; By point gum machine dot-dash lines, manufacturing speed is faster than the method for traditional-handwork dot-dash lines, and consistance is good, can meet the demand of batch preparation; Only once toast, compared to twice traditional baking, shorten spectral slice Production Time, drastically increase product yield and quality.
[accompanying drawing explanation]
The schematic flow sheet of a kind of spectral slice method for making that Fig. 1 provides for one embodiment of the invention.
The schematic flow sheet of the another kind of spectral slice method for making that Fig. 2 provides for one embodiment of the invention.
The schematic flow sheet of another spectral slice method for making that Fig. 3 provides for one embodiment of the invention.
[embodiment]
In order to make object of the present invention, technical scheme and advantage clearly understand, below in conjunction with drawings and Examples, the present invention is further elaborated.Should be appreciated that specific embodiment described herein only in order to explain the present invention, be not intended to limit the present invention.
As shown in Figure 1, the invention provides a kind of spectral slice method for making, comprising:
S101: organic solvent and thickening agent are deployed into organic colloid.
Preferably, organic solvent can be polytetrafluoroethylsolution solution.Teflon has excellent chemical stability and corrosion resistance, and to human non-toxic, can long-term work at the temperature of-180 DEG C to+250 DEG C.
Preferably, thickening agent can be anionic hydrophobically-modified alkali swelling type thickening agent.Such as, the model of domestic production is the anionic hydrophobically-modified alkali swelling type thickening agent of TRM203, the thickening agent of this model is not containing organic solvent, be a kind of nontoxic, low smell and the rheology modified auxiliary agent of environmental protection, there is efficient thickening efficiency, under relatively low consumption, just effectively can improve the shear viscosity in solution.The anionic hydrophobically-modified alkali swelling type thickening agent of thickening agent can also to be external model of producing be TT935.
Preferably, the ratio range of organic solvent and thickening agent is 100:(0.5-1.5).The viscosity of amount of thickener and organic colloid is proportional, can be determined the viscosity of organic colloid by proportioning.
In the present embodiment, first take organic solvent and thickening agent respectively according to actual production use amount, avoid unnecessary waste.
S102: adopt point gum machine by described organic colloid dot-dash lines on substrate.
Preferably, described point gum machine is automatic dispensing machine.
Further, as shown in Figure 2, when using automatic dispensing machine, before step S102, described spectral slice method for making can also comprise:
S1021: the dimensional requirement of point gum machine according to described lines is programmed.
Adopt automatic dispensing machine, in advance the dimensional requirement of the lines of dot-dash is programmed, the parameter such as shape, width, height of lines is accurately controlled, then adopts automatic dispensing machine to carry out dot-dash, more desirable lines can be obtained.When producing in batches, the consistance of lines can be made far above the result of manual dot-dash, and speed is faster.In the present embodiment, substrate can be glass sheet, and the spectral slice of making can be used as analyzing iron spectrum, and lines can be the U-shaped lines of ferrograph analysis.
In the present embodiment, first deployed organic colloid is loaded in the syringe of automatic dispensing machine, again syringe to be arranged on automatic dispensing machine and to mix up the atmospheric pressure of syringe, the scope of the atmospheric pressure of syringe can be 0.2-0.5MPa, the setting of this scope and the viscosity of organic colloid proportional, that is to say with the proportioning of organic solvent and thickening agent proportional, the atmospheric pressure of syringe can be set by the proportioning value of organic solvent and thickening agent.
Preferably, as described in Figure 3, after step s 102, described spectral slice method for making also comprises:
S104: dry and/or dry described substrate.
In the present embodiment, the substrate completing lines dot-dash is carried out drying and/or drying, object is the moisture in order to volatilize in organic colloid, separating out organic dust makes substrate in bake process, keep the complete, attractive in appearance of the shape of lines, therefore, dry without the need to too high temperature, temperature generally adopts higher than normal temperature, lower than 100 DEG C, the temperature of the moisture in organic colloid that can volatilize.
S103: toast described substrate.
Preferably, in step s 103, the temperature range of baking can be 360-430 DEG C, and the time range of baking is 8-15 minute.In the present embodiment, substrate is put into baking box at the temperature of 360-430 DEG C and toast 8-15 minute, its effect is shaped completely by the lines of dot-dash, facilitates the subsequent detection of spectral slice to operate.In the present embodiment, the temperature and time of baking and the width of lines and thickness proportional, namely line thickness is less, the thinner then baking temperature of thickness is lower, the time of baking is shorter.The viscosity of the width of lines and thickness and organic colloid, the pressure of syringe are proportional, therefore, can by regulating the proportioning of organic solvent and thickening agent, the pressure of syringe, meets the width of client to lines and the requirement of thickness.
Spectral slice method for making provided by the invention uses organic colloid to make lines, compared to traditional organic solvent, more easily dry; By the automatic dot-dash lines of point gum machine, manufacturing speed is faster than the method for traditional-handwork dot-dash lines, and consistance is good, can meet the demand of batch preparation; Only once toast, compared to twice traditional baking, shorten spectral slice Production Time, drastically increase product yield and quality.
Embodiment 1
Organic solvent and thickening agent are deployed into organic colloid by the proportioning of 100:0.5; Then this organic colloid is loaded in the syringe of point gum machine, syringe is arranged on point gum machine and by the atmospheric pressure of syringe and is set to 0.2MPa; Adopt this point gum machine by organic colloid dot-dash lines on substrate, then substrate is put into baking box and toast 8 minutes at the temperature of 360 DEG C.
Embodiment 2
Organic solvent and thickening agent are deployed into organic colloid by the proportioning of 100:1; Then this organic colloid is loaded in the syringe of point gum machine, syringe is arranged on point gum machine and by the atmospheric pressure of syringe and is set to 0.35MPa; Adopt this point gum machine by organic colloid dot-dash lines on substrate, then substrate is put into baking box and toast 11 minutes at the temperature of 400 DEG C.
Embodiment 3
Organic solvent and thickening agent are deployed into organic colloid by the proportioning of 100:1; Then this organic colloid is loaded in the syringe of point gum machine, syringe is arranged on point gum machine and by the atmospheric pressure of syringe and is set to 0.5MPa; Adopt this point gum machine by organic colloid dot-dash lines on substrate, then substrate is put into baking box and toast 11 minutes at the temperature of 430 DEG C.
Embodiment 4
Organic solvent and thickening agent are deployed into organic colloid by the proportioning of 100:1.5; Then this organic colloid is loaded in the syringe of point gum machine, syringe is arranged on point gum machine and by the atmospheric pressure of syringe and is set to 0.5MPa; Adopt this point gum machine by organic colloid dot-dash lines on substrate, then substrate is put into baking box and toast 15 minutes at the temperature of 430 DEG C.
Embodiment 5
The invention provides a kind of spectral slice, described spectral slice adopts spectral slice method for making provided by the invention to be prepared from, and the particular content of this spectral slice method for making refers to embodiment of the method for the present invention, repeats no more herein.
Adopt spectral slice prepared by spectral slice method for making provided by the invention, Production Time is short, and the consistance of lines is good, and quality is higher.
The foregoing is only preferred embodiment of the present invention, not in order to limit the present invention, all any amendments done within the spirit and principles in the present invention, equivalent replacement and improvement etc., all should be included within protection scope of the present invention.
Claims (10)
1. a spectral slice method for making, is characterized in that, comprising:
Organic solvent and thickening agent are deployed into organic colloid;
Adopt point gum machine by described organic colloid dot-dash lines on substrate;
Toast described substrate.
2. spectral slice method for making as claimed in claim 1, it is characterized in that, described organic solvent is polytetrafluoroethylsolution solution.
3. spectral slice preparation method as claimed in claim 1, it is characterized in that, described thickening agent is anionic hydrophobically-modified alkali swelling type thickening agent.
4. spectral slice method for making as claimed in claim 1, it is characterized in that, the ratio range of described organic solvent and described thickening agent is 100:(0.5-1.5).
5. spectral slice method for making as claimed in claim 1, it is characterized in that, described point gum machine is automatic dispensing machine.
6. spectral slice method for making as claimed in claim 5, is characterized in that, adopt point gum machine by before the step of described organic colloid dot-dash lines on substrate, described spectral slice method for making also comprises: the dimensional requirement of point gum machine according to described lines programmed.
7. spectral slice method for making as claimed in claim 1, it is characterized in that, before toasting the step of described substrate, described spectral slice method for making also comprises: dry and/or dry described substrate.
8. spectral slice method for making as claimed in claim 1, it is characterized in that, toast in the step of described substrate, the temperature range of baking is 360-430 DEG C.
9. spectral slice method for making as claimed in claim 1, it is characterized in that, toast in the step of described substrate, the time range of baking is 8-15 minute.
10. a spectral slice, is characterized in that, described spectral slice is made based on the spectral slice method for making described in any one of claim 1-9.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201610042117.5A CN105466819A (en) | 2016-01-21 | 2016-01-21 | Spectrum film manufacturing method and spectrum film |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201610042117.5A CN105466819A (en) | 2016-01-21 | 2016-01-21 | Spectrum film manufacturing method and spectrum film |
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| Publication Number | Publication Date |
|---|---|
| CN105466819A true CN105466819A (en) | 2016-04-06 |
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| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN201610042117.5A Pending CN105466819A (en) | 2016-01-21 | 2016-01-21 | Spectrum film manufacturing method and spectrum film |
Country Status (1)
| Country | Link |
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| CN (1) | CN105466819A (en) |
Citations (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN103575573A (en) * | 2012-07-18 | 2014-02-12 | 上海宝钢工业技术服务有限公司 | Treatment method for analytical ferrograph ferrogram-making oil sample |
| CN103935083A (en) * | 2014-04-15 | 2014-07-23 | 江苏维凯科技股份有限公司 | PTFE (Poly Tetra Fluoro Ethylene) glass fiber single-surface composite material |
| CN104912272A (en) * | 2015-05-20 | 2015-09-16 | 赵国平 | Teflon fireproof self-cleaning wall cloth membrane material |
-
2016
- 2016-01-21 CN CN201610042117.5A patent/CN105466819A/en active Pending
Patent Citations (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN103575573A (en) * | 2012-07-18 | 2014-02-12 | 上海宝钢工业技术服务有限公司 | Treatment method for analytical ferrograph ferrogram-making oil sample |
| CN103935083A (en) * | 2014-04-15 | 2014-07-23 | 江苏维凯科技股份有限公司 | PTFE (Poly Tetra Fluoro Ethylene) glass fiber single-surface composite material |
| CN104912272A (en) * | 2015-05-20 | 2015-09-16 | 赵国平 | Teflon fireproof self-cleaning wall cloth membrane material |
Non-Patent Citations (4)
| Title |
|---|
| 余国兴等: "《现代电子装联工艺基础》", 31 May 2007 * |
| 张鄂: "《铁谱技术及其工业应用》", 31 October 2001 * |
| 朱桂兵: "《电子制造设备原理与维护》", 31 December 2011 * |
| 董忠良: "《化工产品手册 树脂与塑料》", 31 August 2008 * |
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Application publication date: 20160406 |