CN105441955A - Metal brightener material composite and preparation method for metal brightener - Google Patents
Metal brightener material composite and preparation method for metal brightener Download PDFInfo
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- CN105441955A CN105441955A CN201510976144.5A CN201510976144A CN105441955A CN 105441955 A CN105441955 A CN 105441955A CN 201510976144 A CN201510976144 A CN 201510976144A CN 105441955 A CN105441955 A CN 105441955A
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- C—CHEMISTRY; METALLURGY
- C23—COATING METALLIC MATERIAL; COATING MATERIAL WITH METALLIC MATERIAL; CHEMICAL SURFACE TREATMENT; DIFFUSION TREATMENT OF METALLIC MATERIAL; COATING BY VACUUM EVAPORATION, BY SPUTTERING, BY ION IMPLANTATION OR BY CHEMICAL VAPOUR DEPOSITION, IN GENERAL; INHIBITING CORROSION OF METALLIC MATERIAL OR INCRUSTATION IN GENERAL
- C23F—NON-MECHANICAL REMOVAL OF METALLIC MATERIAL FROM SURFACE; INHIBITING CORROSION OF METALLIC MATERIAL OR INCRUSTATION IN GENERAL; MULTI-STEP PROCESSES FOR SURFACE TREATMENT OF METALLIC MATERIAL INVOLVING AT LEAST ONE PROCESS PROVIDED FOR IN CLASS C23 AND AT LEAST ONE PROCESS COVERED BY SUBCLASS C21D OR C22F OR CLASS C25
- C23F3/00—Brightening metals by chemical means
- C23F3/02—Light metals
-
- C—CHEMISTRY; METALLURGY
- C23—COATING METALLIC MATERIAL; COATING MATERIAL WITH METALLIC MATERIAL; CHEMICAL SURFACE TREATMENT; DIFFUSION TREATMENT OF METALLIC MATERIAL; COATING BY VACUUM EVAPORATION, BY SPUTTERING, BY ION IMPLANTATION OR BY CHEMICAL VAPOUR DEPOSITION, IN GENERAL; INHIBITING CORROSION OF METALLIC MATERIAL OR INCRUSTATION IN GENERAL
- C23F—NON-MECHANICAL REMOVAL OF METALLIC MATERIAL FROM SURFACE; INHIBITING CORROSION OF METALLIC MATERIAL OR INCRUSTATION IN GENERAL; MULTI-STEP PROCESSES FOR SURFACE TREATMENT OF METALLIC MATERIAL INVOLVING AT LEAST ONE PROCESS PROVIDED FOR IN CLASS C23 AND AT LEAST ONE PROCESS COVERED BY SUBCLASS C21D OR C22F OR CLASS C25
- C23F3/00—Brightening metals by chemical means
- C23F3/04—Heavy metals
- C23F3/06—Heavy metals with acidic solutions
Abstract
The invention discloses a metal brightener material composite and a preparation method for a metal brightener. The composite comprises the following components in parts by weight: 100 parts of water, 10-30 parts of nitric acid, 5-20 parts of lauryl sodium sulfate, 5-15 parts of monopotassium phosphate, 10-20 parts of quartz sand, 1-5 parts of magnesium oxide and 1-5 parts of ammonium nitrate. Through the above design, the effects that the surface of metal can become bright simply and rapidly, and the operation is simple are realized.
Description
Technical field
The present invention relates to metal finishing Material Field, particularly, relate to the preparation method of a kind of metal polish agent material composition and metal polish agent.
Background technology
Metal is as a kind of conventional trolley part material, and use is in the car very extensive, but in the use procedure of metal, often because its storage period is comparatively of a specified duration, its surface brightness is reduced gradually, thus makes the product physicochemical property that obtains poor.
Therefore, provide one that metallic surface can be made quickly and easily to become light, and the preparation method of metal polish agent material composition easy and simple to handle and metal polish agent is the problem that the present invention needs solution badly.
Summary of the invention
For above-mentioned prior art, to the object of the invention is to overcome in prior art in the use procedure of metal, often because its storage period is more of a specified duration, its surface brightness is reduced gradually, thus the problem making the product physicochemical property that obtains poor, thus provide one that metallic surface can be made quickly and easily to become light, and the preparation method of metal polish agent material composition easy and simple to handle and metal polish agent.
To achieve these goals, the invention provides a kind of metal polish agent material composition, wherein, described composition comprises water, nitric acid, sodium lauryl sulphate, potassium primary phosphate, quartz sand, magnesium oxide and ammonium nitrate; Wherein,
Relative to the described water of 100 weight parts, the content of described nitric acid is 10-30 weight part, the content of described sodium lauryl sulphate is 5-20 weight part, the content of described potassium primary phosphate is 5-15 weight part, the content of described quartz sand is 10-20 weight part, described magnesian content is 1-5 weight part, and the content of described ammonium nitrate is 1-5 weight part.
Present invention also offers a kind of preparation method of metal polish agent, wherein, described preparation method comprises: by metal polish agent obtained after the mixing of water, nitric acid, sodium lauryl sulphate, potassium primary phosphate, quartz sand, magnesium oxide and ammonium nitrate; Wherein,
Relative to the described water of 100 weight parts, the consumption of described nitric acid is 10-30 weight part, the consumption of described sodium lauryl sulphate is 5-20 weight part, the consumption of described potassium primary phosphate is 5-15 weight part, the consumption of described quartz sand is 10-20 weight part, described magnesian consumption is 1-5 weight part, and the consumption of described ammonium nitrate is 1-5 weight part.
Pass through technique scheme, water, nitric acid, sodium lauryl sulphate, potassium primary phosphate, quartz sand, magnesium oxide and ammonium nitrate are mixed rear obtained metal polish agent by the present invention according to a certain percentage, thus make it possible to the metal simply immersing of mattness in the effect that wherein can realize improving metallic surface glossiness, greatly save running cost, improve production efficiency.
Other features and advantages of the present invention are described in detail in embodiment part subsequently.
Embodiment
Below the specific embodiment of the present invention is described in detail.Should be understood that, embodiment described herein, only for instruction and explanation of the present invention, is not limited to the present invention.
The invention provides a kind of metal polish agent material composition, wherein, described composition comprises water, nitric acid, sodium lauryl sulphate, potassium primary phosphate, quartz sand, magnesium oxide and ammonium nitrate; Wherein,
Relative to the described water of 100 weight parts, the content of described nitric acid is 10-30 weight part, the content of described sodium lauryl sulphate is 5-20 weight part, the content of described potassium primary phosphate is 5-15 weight part, the content of described quartz sand is 10-20 weight part, described magnesian content is 1-5 weight part, and the content of described ammonium nitrate is 1-5 weight part.
Above-mentioned design is by mixing rear obtained metal polish agent according to a certain percentage by water, nitric acid, sodium lauryl sulphate, potassium primary phosphate, quartz sand, magnesium oxide and ammonium nitrate, thus make it possible to the metal simply immersing of mattness in the effect that wherein can realize improving metallic surface glossiness, greatly save running cost, improve production efficiency.
One of the present invention preferred embodiment in, in order to make the brightness effect of the metal polish agent obtained better, relative to the described water of 100 weight parts, the content of described nitric acid is 15-25 weight part, the content of described sodium lauryl sulphate is 10-15 weight part, and the content of described potassium primary phosphate is 8-12 weight part, and the content of described quartz sand is 13-17 weight part, described magnesian content is 2-4 weight part, and the content of described ammonium nitrate is 2-4 weight part.
Of the present invention another preferred embodiment in, described composition can also comprise sulfuric acid and oxalic acid.
The amount that the content of described sulfuric acid and described oxalic acid can use according to this area routine is selected, such as, one of the present invention preferred embodiment in, relative to the described water of 100 weight parts, the content of described sulfuric acid is 1-10 weight part, and the content of described oxalic acid is 1-10 weight part.
Present invention also offers a kind of preparation method of metal polish agent, wherein, described preparation method comprises: by metal polish agent obtained after the mixing of water, nitric acid, sodium lauryl sulphate, potassium primary phosphate, quartz sand, magnesium oxide and ammonium nitrate; Wherein,
Relative to the described water of 100 weight parts, the consumption of described nitric acid is 10-30 weight part, the consumption of described sodium lauryl sulphate is 5-20 weight part, the consumption of described potassium primary phosphate is 5-15 weight part, the consumption of described quartz sand is 10-20 weight part, described magnesian consumption is 1-5 weight part, and the consumption of described ammonium nitrate is 1-5 weight part.
One of the present invention preferred embodiment in, relative to the described water of 100 weight parts, the consumption of described nitric acid is 15-25 weight part, the consumption of described sodium lauryl sulphate is 10-15 weight part, the consumption of described potassium primary phosphate is 8-12 weight part, the consumption of described quartz sand is 13-17 weight part, and described magnesian consumption is 2-4 weight part, and the consumption of described ammonium nitrate is 2-4 weight part.
Of the present invention another preferred embodiment in, described preparation method can also comprise and add sulfuric acid and oxalic acid mixes.
Similarly, one of the present invention preferred embodiment in, relative to the described water of 100 weight parts, the consumption of described sulfuric acid is 1-10 weight part, and the consumption of described oxalic acid is 1-10 weight part.
The mode that described mixing process can adopt according to this area routine operate, such as, one of the present invention preferred embodiment in, described mixing process can for being uniformly mixed, and stir speed (S.S.) is 100-200r/min.
Below will be described the present invention by embodiment.In following examples, described nitric acid, described sodium lauryl sulphate, described potassium primary phosphate, described quartz sand, described magnesium oxide and described ammonium nitrate are conventional commercial product.
Embodiment 1
The mixing of 100g water, 15g nitric acid, 10g sodium lauryl sulphate, 8g potassium primary phosphate, 13g quartz sand, 2g magnesium oxide, 2g ammonium nitrate, 1g sulfuric acid and 1g oxalic acid being placed in stir speed (S.S.) is obtained metal polish agent A1 after stirring under the condition of 100r/min.
Embodiment 2
The mixing of 100g water, 25g nitric acid, 15g sodium lauryl sulphate, 12g potassium primary phosphate, 17g quartz sand, 4g magnesium oxide, 4g ammonium nitrate, 10g sulfuric acid and 10g oxalic acid being placed in stir speed (S.S.) is obtained metal polish agent A2 after stirring under the condition of 200r/min.
Embodiment 3
The mixing of 100g water, 20g nitric acid, 12g sodium lauryl sulphate, 10g potassium primary phosphate, 15g quartz sand, 3g magnesium oxide, 3g ammonium nitrate, 5g sulfuric acid and 5g oxalic acid being placed in stir speed (S.S.) is obtained metal polish agent A3 after stirring under the condition of 150r/min.
Embodiment 4
Be prepared according to the preparation method of embodiment 1, unlike, the consumption of described nitric acid is 10g, the consumption of described sodium lauryl sulphate is 5g, and the consumption of described potassium primary phosphate is 5g, and the consumption of described quartz sand is 10g, described magnesian consumption is 1g, the consumption of described ammonium nitrate is 1g, does not add sulfuric acid and oxalic acid, obtained metal polish agent A4.
Embodiment 5
Be prepared according to the preparation method of embodiment 2, unlike, the consumption of described nitric acid is 30g, the consumption of described sodium lauryl sulphate is 20g, and the consumption of described potassium primary phosphate is 15g, and the consumption of described quartz sand is 20g, described magnesian consumption is 5g, the consumption of described ammonium nitrate is 5g, does not add sulfuric acid and oxalic acid, obtained metal polish agent A5.
Comparative example 1
Be prepared according to the preparation method of embodiment 3, unlike, the consumption of described nitric acid is 5g, the consumption of described sodium lauryl sulphate is 2g, the consumption of described potassium primary phosphate is 2g, and the consumption of described quartz sand is 5g, and described magnesian consumption is 0.5g, the consumption of described ammonium nitrate is 0.5g, obtained metal polish agent D1.
Comparative example 2
Be prepared according to the preparation method of embodiment 3, unlike, the consumption of described nitric acid is 50g, the consumption of described sodium lauryl sulphate is 40g, the consumption of described potassium primary phosphate is 30g, and the consumption of described quartz sand is 40g, and described magnesian consumption is 10g, the consumption of described ammonium nitrate is 10g, obtained metal polish agent D2.
Test case
Above-mentioned obtained A1-A5, D1 and D2 are soaked respectively the metal of mattness, the result obtained is as shown in table 1.
Table 1
Numbering | Outward appearance |
A1 | Glossiness is high |
A2 | Glossiness is high |
A3 | Glossiness is high |
A4 | Comparatively gloss |
A5 | Comparatively gloss |
D1 | Matt |
D2 | Matt |
More than describe the preferred embodiment of the present invention in detail; but the present invention is not limited to the detail in above-mentioned embodiment, within the scope of technical conceive of the present invention; can carry out multiple simple variant to technical scheme of the present invention, these simple variant all belong to protection scope of the present invention.
It should be noted that in addition, each concrete technical characteristic described in above-mentioned embodiment, in reconcilable situation, can be combined by any suitable mode, in order to avoid unnecessary repetition, the present invention illustrates no longer separately to various possible array mode.
In addition, also can carry out arbitrary combination between various different embodiment of the present invention, as long as it is without prejudice to thought of the present invention, it should be considered as content disclosed in this invention equally.
Claims (9)
1. a metal polish agent material composition, is characterized in that, described composition comprises water, nitric acid, sodium lauryl sulphate, potassium primary phosphate, quartz sand, magnesium oxide and ammonium nitrate; Wherein,
Relative to the described water of 100 weight parts, the content of described nitric acid is 10-30 weight part, the content of described sodium lauryl sulphate is 5-20 weight part, the content of described potassium primary phosphate is 5-15 weight part, the content of described quartz sand is 10-20 weight part, described magnesian content is 1-5 weight part, and the content of described ammonium nitrate is 1-5 weight part.
2. composition according to claim 1, wherein, relative to the described water of 100 weight parts, the content of described nitric acid is 15-25 weight part, the content of described sodium lauryl sulphate is 10-15 weight part, and the content of described potassium primary phosphate is 8-12 weight part, and the content of described quartz sand is 13-17 weight part, described magnesian content is 2-4 weight part, and the content of described ammonium nitrate is 2-4 weight part.
3. composition according to claim 1 and 2, wherein, described composition also comprises sulfuric acid and oxalic acid.
4. composition according to claim 3, wherein, relative to the described water of 100 weight parts, the content of described sulfuric acid is 1-10 weight part, and the content of described oxalic acid is 1-10 weight part.
5. a preparation method for metal polish agent, is characterized in that, described preparation method comprises: by metal polish agent obtained after the mixing of water, nitric acid, sodium lauryl sulphate, potassium primary phosphate, quartz sand, magnesium oxide and ammonium nitrate; Wherein,
Relative to the described water of 100 weight parts, the consumption of described nitric acid is 10-30 weight part, the consumption of described sodium lauryl sulphate is 5-20 weight part, the consumption of described potassium primary phosphate is 5-15 weight part, the consumption of described quartz sand is 10-20 weight part, described magnesian consumption is 1-5 weight part, and the consumption of described ammonium nitrate is 1-5 weight part.
6. preparation method according to claim 5, wherein, relative to the described water of 100 weight parts, the consumption of described nitric acid is 15-25 weight part, the consumption of described sodium lauryl sulphate is 10-15 weight part, and the consumption of described potassium primary phosphate is 8-12 weight part, and the consumption of described quartz sand is 13-17 weight part, described magnesian consumption is 2-4 weight part, and the consumption of described ammonium nitrate is 2-4 weight part.
7. the preparation method according to claim 5 or 6, wherein, described preparation method also comprises and adds sulfuric acid and oxalic acid mixes.
8. preparation method according to claim 7, wherein, relative to the described water of 100 weight parts, the consumption of described sulfuric acid is 1-10 weight part, and the consumption of described oxalic acid is 1-10 weight part.
9. the preparation method according to claim 5 or 6, wherein, described mixing process is for being uniformly mixed, and stir speed (S.S.) is 100-200r/min.
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CN201510976144.5A CN105441955A (en) | 2015-12-22 | 2015-12-22 | Metal brightener material composite and preparation method for metal brightener |
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Cited By (2)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
WO2019115395A1 (en) * | 2017-12-12 | 2019-06-20 | Chemetall Gmbh | Boric acid-free composition for removing deposits containing cryolite |
RU2784962C2 (en) * | 2017-12-12 | 2022-12-01 | Хеметалл Гмбх | Composition not containing boron for removal of cryolite-containing deposits |
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JP2004123921A (en) * | 2002-10-02 | 2004-04-22 | Fujimi Inc | Polishing composition |
US20050112894A1 (en) * | 2003-10-09 | 2005-05-26 | Jeong-Heon Park | CMP slurry for forming aluminum film, CMP method using the slurry, and method for forming aluminum wiring using the CMP method |
CN101457362A (en) * | 2009-01-07 | 2009-06-17 | 湖南鑫美格新型装饰材料有限公司 | Aluminum section bar three acid polishing and leveling fog inhibitor for furniture and finishing method thereof |
CN102329572A (en) * | 2011-09-20 | 2012-01-25 | 深圳市力合材料有限公司 | Copper chemical and mechanical polishing combination |
CN103725256A (en) * | 2013-12-31 | 2014-04-16 | 上海集成电路研发中心有限公司 | Grinding particle system and polishing liquid for CMP (Chemical Mechanical Polishing) |
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2015
- 2015-12-22 CN CN201510976144.5A patent/CN105441955A/en active Pending
Patent Citations (5)
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JP2004123921A (en) * | 2002-10-02 | 2004-04-22 | Fujimi Inc | Polishing composition |
US20050112894A1 (en) * | 2003-10-09 | 2005-05-26 | Jeong-Heon Park | CMP slurry for forming aluminum film, CMP method using the slurry, and method for forming aluminum wiring using the CMP method |
CN101457362A (en) * | 2009-01-07 | 2009-06-17 | 湖南鑫美格新型装饰材料有限公司 | Aluminum section bar three acid polishing and leveling fog inhibitor for furniture and finishing method thereof |
CN102329572A (en) * | 2011-09-20 | 2012-01-25 | 深圳市力合材料有限公司 | Copper chemical and mechanical polishing combination |
CN103725256A (en) * | 2013-12-31 | 2014-04-16 | 上海集成电路研发中心有限公司 | Grinding particle system and polishing liquid for CMP (Chemical Mechanical Polishing) |
Cited By (7)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
WO2019115395A1 (en) * | 2017-12-12 | 2019-06-20 | Chemetall Gmbh | Boric acid-free composition for removing deposits containing cryolite |
CN111417744A (en) * | 2017-12-12 | 2020-07-14 | 凯密特尔有限责任公司 | Boric acid-free composition for removing cryolite-containing deposits |
JP2021505774A (en) * | 2017-12-12 | 2021-02-18 | ケメタル ゲゼルシャフト ミット ベシュレンクテル ハフツング | Boric acid-free composition for removing precipitates containing cliolite |
US11434573B2 (en) | 2017-12-12 | 2022-09-06 | Chemetall Gmbh | Boric acid-free composition for removing deposits containing cryolite |
RU2784962C2 (en) * | 2017-12-12 | 2022-12-01 | Хеметалл Гмбх | Composition not containing boron for removal of cryolite-containing deposits |
JP7394761B2 (en) | 2017-12-12 | 2023-12-08 | ケメタル ゲゼルシャフト ミット ベシュレンクテル ハフツング | Boric acid-free composition for removing deposits containing cryolite |
KR102655537B1 (en) * | 2017-12-12 | 2024-04-09 | 케메탈 게엠베하 | Boric acid-free composition for removing deposits containing cryolite |
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Application publication date: 20160330 |